Asphalts, Tars, Pitches And Resins Patents (Class 208/22)
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Publication number: 20110280275Abstract: A reduced puffing needle coke is formed, which includes a reduced nitrogen content within the coke so that the coke particles do not experience as much puffing during the formation of graphitized carbon articles produced from such coke upon heating to graphitization temperatures.Type: ApplicationFiled: July 21, 2011Publication date: November 17, 2011Applicant: GrafTech International Holdings, Inc.Inventors: Douglas J. Miller, Ching-Feng Chang, Irwin C. Lewis, Richard T. Lewis, Aaron Tomasek, Richard L. Shao
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Publication number: 20110280274Abstract: A reduced puffing needle coke is formed from decant oil, which includes a lesser amount of nitrogen within the coke so that carbon articles produced from such coke experience minimal expansion upon heating to graphitization temperatures.Type: ApplicationFiled: July 21, 2011Publication date: November 17, 2011Applicant: GrafTech International Holdings, Inc.Inventors: Douglas J. Miller, Ching-Feng Chang, Irwin C. Lewis, Aaron Tomasek, Richard L. Shao
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Publication number: 20110274136Abstract: A reduced puffing needle coke is formed, which includes a lesser amount of nitrogen within the coke so that carbon articles produced from such coke experience minimal expansion upon heating to graphitization temperatures.Type: ApplicationFiled: July 21, 2011Publication date: November 10, 2011Applicant: GrafTech International Holdings, IncInventors: Douglas J. Miller, Ching-Feng Chang, Irwin C. Lewis, Aaron Tomasek, Richard L. Shao
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Publication number: 20110253593Abstract: The present invention provides a raw coke having such a structure that the graphitized product resulting from graphitization of the raw coke at a temperature of 2800° C. under an inactive gas atmosphere will have ratios of the crystallite size to the lattice constant of 360 or less in the (002) plane and 1500 or less in the (110) plane, as a raw coke providing active carbon produced by alkali-activating the raw coke, which is reduced in remaining alkali content and can simplify washing operation because washing liquid can easily pass through the activated carbon, or as a raw coke for the production of needle coke.Type: ApplicationFiled: June 10, 2011Publication date: October 20, 2011Applicants: NIPPON PETROLEUM REFINING COMPANY, LIMITED, NIPPON OIL CORPORATIONInventors: Takashi OYAMA, Kazuhisa NAKANISHI, Tamotsu TANO, Keiji HIGASHI, Ippei FUJINAGA, Hiromitsu HASHISAKA, Toshitaka FUJII, Takashi NORO, Akio SAKAMOTO, Kiwamu TAKESHITA, Keizou IKAI, Masaki FUJII, Hideki ONO
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Patent number: 8022118Abstract: A system for reducing pressure drop associated with the turbulent flow of asphaltenic crude oil through a conduit. The crude oil has a high asphaltene content and/or a low API gravity. Such reduction in pressure drop is achieved by treating the asphaltenic crude oil with a high molecular weight drag reducing polymer that can have a solubility parameter within about 20 percent of the solubility parameter of the heavy crude oil. The drag reducing polymer can also comprise the residues of monomers having at least one heteroatom.Type: GrantFiled: December 22, 2006Date of Patent: September 20, 2011Assignee: ConocoPhillips CompanyInventors: Stuart N. Milligan, Ray L. Johnston, Timothy L. Burden, Wayne R. Dreher, Jr., Kenneth W. Smith, William F. Harris
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Patent number: 8007657Abstract: Described is the use, for preparing or treating bituminous compositions, of at least one compound selected among: esters of glycolic, lactic and gluconic acids, methylic, ethylic and isobutylic esters of glutaric, succinic and adipic acids, and ethers or esters of a product resulting from internal dehydration of a sugar, preferably a hydrogenated sugar. Also described is a method for preparing or treating such compositions and the resulting compositions.Type: GrantFiled: December 20, 2005Date of Patent: August 30, 2011Assignee: Roquette FreresInventors: Léon Mentink, Joël Bernaerts, Michel Maze, Frédéric Delfosse
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Publication number: 20110206455Abstract: A method of applying building a pavement structure using a polymer modified hot-applied tack coat is disclosed. This polymer modified tack coat is non-adhesive at ambient temperatures, and, thus, also non tracking. The tack is applied while hot, but cools quickly. The subsequent application of hot mix asphalt results in a superior bond between the asphalt layer and the tack layer. It is particularly well suited to bonded friction course applications since it removes the necessity of specialized spray paving machinery and allows the use of conventional asphalt distributors and pavers.Type: ApplicationFiled: February 24, 2011Publication date: August 25, 2011Applicant: BLACKLIDGE EMULSIONS, INC.Inventor: Roy Brittany Blacklidge
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Patent number: 7988846Abstract: A method for modifying asphalt comprises blowing an oxygen-containing gas through a base asphalt at a high gas flow rate while simultaneously agitating the base asphalt at a high shear rate and at an elevated temperature for a period of time that is effective to substantially improve at least two paving properties of the base asphalt. In preferred embodiments, modified asphalts are produced having both substantially improved rutting resistance and substantially improved fatigue resistance as compared to the base asphalt.Type: GrantFiled: January 14, 2010Date of Patent: August 2, 2011Assignee: Asphalt Technology LLCInventors: Michael V Burris, Bryan B Burris, Hossein Ajideh
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Patent number: 7968020Abstract: Systems and methods for pelletizing hot asphaltenes are provided. Asphaltenic hydrocarbons can be dispersed to provide two or more asphaltenic particles. The asphaltenic hydrocarbons can be at a temperature of from about 175° C. to about 430° C. The asphaltenic particles can be contacted with a film of cooling medium. The film can have a thickness of from about 1 mm to about 500 mm. At least a portion of the asphaltenic particles can be solidified by transferring heat from the asphaltenic particles to the cooling medium to provide solid asphaltenic particles. The solid asphaltenic particles can be separated from at least a portion of the cooling medium.Type: GrantFiled: April 30, 2008Date of Patent: June 28, 2011Assignee: Kellogg Brown & Root LLCInventors: Gary L. Behelfer, Maury Schlossman
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Patent number: 7906011Abstract: Methods and systems for efficiently manufacturing modified asphalt materials include agitating a base asphalt at a high shear rate using an in-line mixer equipped with a rotor-stator mixing tool while simultaneously exposing the asphalt to oxygen by blowing an oxygen-containing gas at a high gas flow rate through openings in the rotor-stator mixing tool and heating the asphalt at an elevated temperature.Type: GrantFiled: June 12, 2009Date of Patent: March 15, 2011Assignee: Asphalt Technology LLCInventors: Michael V. Burris, Bryan B. Burris, Hossein Ajideh, Andrew Clayton
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Patent number: 7906010Abstract: The invention relates to the use of steam cracked tar with the bottoms product of a flash drum integrated with a pyrolysis furnace. In embodiments, the steam cracked tar is added to fuel oil.Type: GrantFiled: January 13, 2006Date of Patent: March 15, 2011Assignee: ExxonMobil Chemical Patents Inc.Inventors: Paul F. Keusenkothen, Alok Srivastava
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Patent number: 7901563Abstract: The present invention relates to a method for preparing an industrial asphalt comprising (1) heating an asphalt flux to a temperature which is within the range of about 400° F. (204° C.) to 550° F. (288° C.) to produce a hot asphalt flux, (2) sparging an oxygen containing gas through the hot asphalt flux for a period of time which is sufficient to increase the softening point of the asphalt flux to a value of at least 100° F. (38° C.), to produce an underblown asphalt composition; and (3) mixing a sufficient amount of a polyphosphoric acid throughout the underblown asphalt composition while the underblown asphalt composition is maintained at a temperature which is within the range of 200° F. (93° C.) to 550° F. (288° C.) to attain a softening point which is within the range of 185° F. (85° C.) to 250° F. (121° C.) and a penetration value of at least 15 dmm at 77° F. (25° C.) to produce the industrial asphalt.Type: GrantFiled: February 1, 2006Date of Patent: March 8, 2011Assignee: Building Materials Investment CorporationInventors: Yonghong Ruan, William K. Longcor, IV, Peter Lars Johnson
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Publication number: 20100326882Abstract: A process and apparatus is disclosed for converting heavy hydrocarbon feed into lighter hydrocarbon products. The heavy hydrocarbon feed is slurried with a particulate solid material to form a heavy hydrocarbon slurry and hydrocracked in a slurry hydrocracking unit to produce vacuum gas oil (VGO) and pitch. A first vacuum column separates VGO from pitch, and a second vacuum column further separates VGO from pitch. As much as 15 wt-% of VGO can be recovered by the second vacuum column and recycled to the slurry hydrocracking unit. A pitch composition is obtained which can be made into particles and transported without sticking together.Type: ApplicationFiled: June 15, 2010Publication date: December 30, 2010Applicant: UOP LLCInventors: James F. McGehee, Ronald S. Smyczynski
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Publication number: 20100096296Abstract: A method is disclosed for treating gaseous effluent from a hydrocarbon pyrolysis unit to provide steam cracked tar of reduced asphaltene and toluene insolubles content. The method is suitable for preparing reduced viscosity tar useful as a fuel blending stock, or feedstock for producing carbon black, while reducing or eliminating the need for externally sourced lighter aromatics additives to meet viscosity specifications. The method comprises drawing steam cracked tar from a separation vessel, e.g., a primary fractionator or tar knock-out drum, cooling the tar, and returning it to the separation vessel to effect lower overall tar temperatures within the separation vessel, in order to reduce viscosity increasing condensation reactions. An apparatus for carrying out the method is also provided.Type: ApplicationFiled: December 21, 2009Publication date: April 22, 2010Inventors: Robert David Strack, Richard C. Stell, John R. Messinger, Dane C. Grenoble, John E. Asplin
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Publication number: 20090301931Abstract: A cost-effective solution is provided for eliminating refinery process waste, including spent catalytic and non-catalytic adsorbent materials, as well as adsorbate process reject materials derived from desorption, while minimizing conventional waste handling demands. An asphalt composition includes asphalt and spent adsorbent material from a solvent deasphalting unit. The asphalt can comprise asphaltic material obtained from a solvent deasphalting unit, and spent adsorbent material in the asphalt composition was previously utilized in the solvent deasphalting unit. The asphalt composition can also include process reject materials.Type: ApplicationFiled: July 2, 2009Publication date: December 10, 2009Inventors: Omer Refa KOSEOGLU, Salman AL-KHALDI, Adnan AL-HAJJI, Ali AL-HAMADH
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Patent number: 7625479Abstract: A binder pitch material includes a petroleum pitch and asphalt fraction obtained from petroleum crude oil and has a significantly lower polycyclic aromatic hydrocarbon composition than a coal tar pitch having a like softening point. The pitch material is useful as a binder material for various applications such as clay pigeons.Type: GrantFiled: June 12, 2008Date of Patent: December 1, 2009Assignee: Marathon Ashland Petroleum LLCInventors: Melvin D. Kiser, David C. Boyer
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Publication number: 20090288983Abstract: A high coking value pitch prepared from coal tar distillate and has a low softening point and a high carbon value while containing substantially no quinoline insolubles is disclosed. The pitch can be used as an impregnant or binder for producing carbon and graphite articles.Type: ApplicationFiled: May 22, 2008Publication date: November 26, 2009Inventors: Douglas J. Miller, Ching-Feng Chang, Irwin C. Lewis, Richard T. Lewis
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Patent number: 7572362Abstract: The present invention is directed to the upgrading of heavy petroleum oils of high viscosity and low API gravity that are typically not suitable for pipelining without the use of diluents. It utilizes a short residence-time pyrolytic reactor operating under conditions that result in a rapid pyrolytic distillation with coke formation. Both physical and chemical changes taking place lead to an overall molecular weight reduction in the liquid product and rejection of certain components with the byproduct coke. The liquid product is upgraded primarily because of its substantially reduced viscosity, increased API gravity, and the content of middle and light distillate fractions. While maximizing the overall liquid yield, the improvements in viscosity and API gravity can render the liquid product suitable for pipelining without the use of diluents.Type: GrantFiled: April 17, 2003Date of Patent: August 11, 2009Assignee: Ivanhoe Energy, Inc.Inventors: Barry Freel, Jerry F. Kriz, Doug Clarke
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Patent number: 7572365Abstract: The present invention is directed to the upgrading of heavy petroleum oils of high viscosity and low API gravity that are typically not suitable for pipelining without the use of diluents. It utilizes a short residence-time pyrolytic reactor operating under conditions that result in a rapid pyrolytic distillation with coke formation. Both physical and chemical changes taking place lead to an overall molecular weight reduction in the liquid product and rejection of certain components with the byproduct coke. The liquid product is upgraded primarily because of its substantially reduced viscosity, increased API gravity, and the content of middle and light distillate fractions. While maximizing the overall liquid yield, the improvements in viscosity and API gravity can render the liquid product suitable for pipelining without the use of diluents.Type: GrantFiled: October 11, 2002Date of Patent: August 11, 2009Assignee: Ivanhoe Energy, Inc.Inventors: Barry Freel, Jerry F. Kriz, Doug Clarke
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Patent number: 7537686Abstract: A method for upgrading heavy oils by contacting the heavy oil with an inhibitor additive and then thermally treating the inhibitor additized heavy oil. The invention also relates to the upgraded product from the inhibitor enhanced thermal treatment process.Type: GrantFiled: May 12, 2005Date of Patent: May 26, 2009Assignee: ExxonMobil Research and Engineering CompanyInventors: Ramesh Varadaraj, Christopher P. Eppig, Douglas W. Hissong, Robert C. Welch
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Patent number: 7393449Abstract: A binder pitch material includes a petroleum pitch and asphalt fraction obtained from petroleum crude oil and has a significantly lower polycyclic aromatic hydrocarbon composition than a coal tar pitch having a like softening point. The pitch material is useful as a binder material for various applications such as clay pigeons.Type: GrantFiled: May 31, 2006Date of Patent: July 1, 2008Assignee: Marathon Ashland Petroleum LLCInventors: Melvin D. Kiser, David C. Boyer
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Patent number: 7374659Abstract: A method for modifying asphalt comprises blowing an oxygen-containing gas through a base asphalt at a high gas flow rate while simultaneously agitating the base asphalt at a high shear rate and at an elevated temperature for a period of time that is effective to substantially improve at least two paving properties of the base asphalt. In preferred embodiments, modified asphalts are produced having both substantially improved rutting resistance and substantially improved fatigue resistance as compared to the base asphalt.Type: GrantFiled: June 21, 2005Date of Patent: May 20, 2008Assignee: Asphalt Technology, LLC.Inventors: Michael V. Burris, Bryan B. Burris, Hossein Ajideh
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Patent number: 7318891Abstract: A process for producing pitch from pitch precursors, such as wood tar, coal tar or petroleum fractions is disclosed. Direct contact heat exchange of the pitch precursor with molten metal, preferably maintained as a metal continuous bath, heats the pitch precursor to a temperature sufficient to induce thermal polymerization reactions and produce a pitch product.Type: GrantFiled: October 8, 2004Date of Patent: January 15, 2008Assignee: DTX Technologies LLCInventor: Donald P. Malone
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Patent number: 7318890Abstract: A process for fractionating crude pitch by direct contact heating with molten metal is disclosed. The crude pitch, which may contain water, contaminants and/or distillables is heated by direct contact heat exchange with molten metal, preferably maintained as a metal continuous bath, operating at a temperature of 100 to 600° C. The molten metal heating zone is maintained at a temperature and pressure sufficient to vaporize a desired amount of contaminants or volatile material from crude pitch to produce pitch product having a desired softening point. New pitch materials, having a softening point above those achievable by conventional techniques, are also produced.Type: GrantFiled: October 8, 2004Date of Patent: January 15, 2008Assignee: DTX Technologies LLCInventor: Donald P. Malone
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Publication number: 20070295640Abstract: deposition in a formation, wellbore, near wellbore region, and production tubing. Compositions of the invention comprise an asphaltene solvent and a viscosity reducing agent, the asphaltene solvent and viscosity reducing agent present in a ratio so as to substantially reduce viscosity of an asphaltene-containing material while substantially negating deposition of asphaltenes either in a reservoir, in production tubing, or both when mixed or otherwise contacting the asphaltene-containing material Methods of the invention comprise forcing a composition comprising an asphaltene solvent and a viscosity reducing agent to contact an asphaltene-containing hydrocarbon in an underground geologic formation, and producing from the formation a production composition comprising at least some of the treatment composition and at least some of the asphaltene-containing hydrocarbon under conditions sufficient to substantially negate deposition of asphaltenes in the formation.Type: ApplicationFiled: June 26, 2006Publication date: December 27, 2007Applicant: Schlumberger Technology CorporationInventors: Jiasen Tan, Ahmed Hammami, Moin Muhammad, Hussein Alboudwarej, Abdel M. Kharrat
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Patent number: 7282135Abstract: A low viscosity, high coking value petroleum tar material having a high coking value as compared to standard petroleum tars and containing at least one biodiesel material dissolved therein, and a method for producing such material, are disclosed.Type: GrantFiled: November 3, 2004Date of Patent: October 16, 2007Assignee: Marathon Ashland Petroleum Co., LLCInventors: Melvin D. Kiser, David C. Boyer
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Patent number: 7279017Abstract: A method for enabling the use of heavy oil residuum by conversion to a useful product. The method, in one embodiment, involves the use of a heavy oil residuum which is substantially non flowable. The viscosity of the residuum is reduced by heat or a combination of heat and a diluent and subsequently mixed with water such that the mixing is high shear mixing. This results in the formation of an emulsion of predispersed residuum in an aqueous matrix. The emulsion is formed such that the aqueous matrix is in a size distribution suitable for use as a combustible fuel.Type: GrantFiled: February 21, 2003Date of Patent: October 9, 2007Assignee: Colt Engineering CorporationInventors: Steve Kresnyak, Edward Warchol
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Patent number: 7252755Abstract: A low-viscosity, high-softening point heavy hydrocarbon material having a viscosity-reducing amount of at least one biodiesel material dissolved in a heavy hydrocarbon, and a method for producing such low-viscosity, high-softening point heavy hydrocarbon material are disclosed.Type: GrantFiled: April 7, 2003Date of Patent: August 7, 2007Assignee: Marathon Ashland Petroleum Co.Inventors: Melvin D. Kiser, David C. Boyer
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Patent number: 7105083Abstract: A method for obtaining activated carbons from a partly mesophased and partly mesogenic pitch containing less than about 40% of the a resins, more than about 40% of type ? resins and between about 5 and 30% of type ? resins by activating the pitch preceded by its optional carbonization.Type: GrantFiled: November 17, 2000Date of Patent: September 12, 2006Assignees: Centre National de la Recherche Scientifique, Manufacture de Vetements Paul BoyeInventors: André Guillot, Xavier Py, Emmanuel Daguerre, Bernard Spinner
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Patent number: 7094331Abstract: A low viscosity, high softening point heavy hydrocarbon material having a viscosity reducing amount of at least one dihydric alcohol dissolved therein, and a method for producing such heavy hydrocarbon material, are disclosed.Type: GrantFiled: November 5, 2003Date of Patent: August 22, 2006Assignee: Marathon Ashland Petroleum LLCInventor: Melvin D. Kiser
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Patent number: 7067050Abstract: A binder pitch material includes a petroleum pitch and asphalt fraction obtained from petroleum crude oil and has a significantly lower polycyclic aromatic hydrocarbon composition than a coal tar pitch having a like softening point. The pitch material is useful as a binder material for various applications such as clay pigeons.Type: GrantFiled: November 14, 2002Date of Patent: June 27, 2006Assignee: Marathon Ashland Petroleum LLCInventors: Melvin D. Kiser, David C. Boyer
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Patent number: 7066997Abstract: A method of making the saturated aircraft brake preform using a coal tar pitch having a softening point in the range of about 160° C. to 240° C. Also, a product having natural rubber in the formulation and the method of making the product using a coal tar pitch having a softening point in the range of about 140° C. to 200° C. A mesophase pitch is formed from quinoline insoluble free coal tar pitch distillate from a high efficiency evaporative distillation process.Type: GrantFiled: May 9, 2002Date of Patent: June 27, 2006Assignee: Koppers Delaware, Inc.Inventors: Thomas A. Golubic, Kenneth C. Krupinski, William E. Saver, David R. Snyder, Robert H. Wombles
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Patent number: 7037955Abstract: Additives and methods for reducing or eliminating odor in oil based media. The additives comprise an essential oil, an essential oil component, or mixtures thereof.Type: GrantFiled: May 2, 2003Date of Patent: May 2, 2006Assignee: Odor Managements, Inc.Inventors: Charles Timcik, John Fergeus
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Patent number: 7008526Abstract: When a pitch composition prepared by mixing 100 parts by weight of mesophase pitch with 10 to 1,000 parts by weight of coal tar pitch, is heat-treated at a temperature of 500° C. or higher, it is possible to produce a high-density coke at a high yield while avoiding the foaming of the mesophase pitch. In addition, when the coke is graphitized at a temperature of 2,000° C. or higher, it is possible to obtain an artificial graphite having a high graphitization degree. Further, when the coke is first pulverized and then graphitized at a temperature of 2,000° C. or higher, it is possible to obtain a high-crystallinity graphite powder which can be suitably used as a carbon material for a negative electrode of non-aqueous solvent type secondary battery having a high discharge capacity and a high charge-discharge efficiency.Type: GrantFiled: August 8, 2001Date of Patent: March 7, 2006Assignee: Mistubishi Gas Chemical Company, Inc.Inventors: Koichi Kanno, Hirotaka Tsuruya, Ryuji Fujiura
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Patent number: 6827841Abstract: A low viscosity, high coking value petroleum tar material having a high coking value as compared to standard petroleum tars and containing at least one biodiesel material dissolved therein, and a method for producing such material, are disclosed.Type: GrantFiled: April 7, 2003Date of Patent: December 7, 2004Assignee: Marathon Ashland Petroleum LLCInventors: Melvin D. Kiser, David C. Boyer
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Publication number: 20040232041Abstract: Fractions derived from a high sulfur content crude oil, having a sulfur content of about 2 wt. % or greater, is hydrotreated to produce a petroleum pitch not only having a low sulfur content of about 1 wt % or less but also a low polycyclic aromatic hydrocarbon (PAH) content of about 13,000 mg/kg or less.Type: ApplicationFiled: May 22, 2003Publication date: November 25, 2004Applicant: Marathon Ashland Petroleum LLCInventors: Melvin D. Kiser, Patricia K. Doolin, David C. Boyer
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Publication number: 20040195150Abstract: A low-viscosity, high-softening point heavy hydrocarbon material having a viscosity-reducing amount of at least one biodiesel material dissolved in a heavy hydrocarbon, and a method for producing such low-viscosity, high-softening point heavy hydrocarbon material are disclosed.Type: ApplicationFiled: April 7, 2003Publication date: October 7, 2004Inventors: Melvin D. Kiser, David C. Boyer
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Publication number: 20040195149Abstract: A low viscosity, high coking value petroleum tar material having a high coking value as compared to standard petroleum tars and containing at least one biodiesel material dissolved therein, and a method for producing such material, are disclosed.Type: ApplicationFiled: April 7, 2003Publication date: October 7, 2004Inventors: Melvin D. Kiser, David C. Boyer
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Publication number: 20040134833Abstract: A description follows of an aqueous dispersion of heavy oil residues, suitable for undergoing combustion with a low emission of SOx, comprising: (a) a heavy oil residue; (b) a dispersing agent; (c) a desulfurizing agent selected from CaCO3, MgCO3, dolomite and relative mixtures; (d) a desulfurizing agent with stabilizing and anti-corrosive properties selected from MgO, Mg(OH)2, CaO, Ca(OH)2 and relative mixtures; (e) water; the weight percentage of (e) with respect of the sum of (a) + (e) being at least 15%.Type: ApplicationFiled: February 11, 2004Publication date: July 15, 2004Inventors: Armando Marcotullio, Riccardo Rausa, Alessandro Lezzi
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Publication number: 20040094454Abstract: A binder pitch material includes a petroleum pitch and asphalt fraction obtained from petroleum crude oil and has a significantly lower polycyclic aromatic hydrocarbon composition than a coal tar pitch having a like softening point. The pitch material is useful as a binder material for various applications such as clay pigeons.Type: ApplicationFiled: November 14, 2002Publication date: May 20, 2004Inventors: Melvin D. Kiser, David C. Boyer
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Patent number: 6717021Abstract: A solvating component for a solvated mesophase pitch. The solvated component includes a mixture of aromatic hydrocarbons having boiling points in the atmospheric equivalent boiling point range of about 285° to about 500° C. (about 550° F.-932° F.). At least 80% of the carbon atoms of the hydrocarbons are aromatic as characterized by carbon 13 NMR. The aromatic hydrocarbons are selected from a group consisting of aromatic compounds having 2 to 5 aromatic rings, substituted aromatic compounds having 2 to 5 aromatic rings wherein said substituents are alkyl groups having 1 to 3 carbons, hydroaromatic compounds having 2 to 5 rings, substituted aromatic compounds having 2 to 5 rings wherein said substituents are alkyl groups having 1 to 3 carbons, and mixtures thereof.Type: GrantFiled: June 4, 2001Date of Patent: April 6, 2004Assignee: ConocoPhillips CompanyInventors: H. Ernest Romine, John A. Rodgers, W. Mark Southard, Edward J. Nanni
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Patent number: 6689295Abstract: The present invention provides a method of manufacturing an exfoliated graphite/phenol resin composite foam of a porosity of 50-95%, a density of 0.1-0.8 g/cm3, by forming under contact pressure or reduced pressure at a temperature of 140-200° C. a mixture comprising 100 parts by weight of powdered and/or crushed exfoliated graphite and 40-240 parts by weight of phenol resin; an exfoliated graphite/phenol resin composite foam obtained by the method; and a method of obtaining an exfoliated graphite/glassy carbon composite foam of a porosity of 50-95%, a density 0.1-0.8 g/cm3 with volumetric baking shrinkage of 10% or less by baking the exfoliated graphite/phenol resin composite foam.Type: GrantFiled: March 21, 2001Date of Patent: February 10, 2004Assignees: Osaka Prefectural Government, E. Tec Co., Ltd.Inventors: Takeshi Hirohata, Shinya Kawakami
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Patent number: 6659684Abstract: A method for repairing a damaged area of a bitutinous wearing course. The method comprises heating the damaged area, applying a liquid to the damaged area that rejuvenates damaged bitumen, adding new material to the damaged area in an amount required to level the area, and compacting the new material. The invention also provides a new composition for rejuvenating damaged bitumen. The composition may comprise an emulsifier, a heavy paraffinic distillate solvent extract, a heavy naphthenic distillate solvent extract and water.Type: GrantFiled: July 2, 2001Date of Patent: December 9, 2003Assignee: Asphalt Systems International LimitedInventors: Jonathan Luke Henry Goodhart, Christopher Paul James Wightman, Gary Alma Porritt
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Patent number: 6530965Abstract: A method for enabling the use of heavy oil residuum by conversion to a useful product. The method, in one embodiment, involves the use of a heavy oil residuum which is substantially non flowable. The viscosity of the residuum is reduced and subsequently mixed with water such that the mixing is high shear mixing. This results in the formation of an emulsion of predispersed residuum in an aqueous matrix. The emulsion is formed such that the aqueous matrix is in a size distribution suitable for use as a combustible fuel.Type: GrantFiled: April 27, 2001Date of Patent: March 11, 2003Assignee: Colt Engineering CorporationInventor: Edward J. Warchol
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Publication number: 20020166794Abstract: The present invention is an energy efficient method for separating petroleum-based waste including sludge, bottoms or used lubricants. By using solid particles and water, and converting them into useable end products, for example gas and gas/oil fractions. The process produces no wasteful by-products like polluted sewage, heavy asphaltenics and tar by-products. Instead, the process eliminates water through selective adsorption by dewatering additives and the process is followed by drying at high temperatures. The dewatering additives are recycled from other processes and are reusable themselves. After skimming the dewatered matter, the remainder is processed by thermocatalytic cracking. Some of the active materials in the cracking reaction are again waste products of other reactions. The gas and gas oil fractions obtained from this process conform to standard specifications. The process uses equipment that is cost-effective and that are routinely produced.Type: ApplicationFiled: January 29, 2001Publication date: November 14, 2002Inventors: Alexander P. Bronshtein, Moshe Gewertz, Vladimir M. Rozhansky
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Patent number: 6478951Abstract: A compatibilizer and process for use in making crumb rubber modified asphalt. The compatibilizer causes the crumb rubber to completely interact with the asphalt, thereby improving the rheological properties of the asphalt and reducing the tendency of pavement made with the asphalt to ravel. The compatibilizer has as its reactive component one or more glycidyl groups; its polymeric backbone can be ethylenic, styrenic, or acrylic or ethylene vinyl acetate (EVA).Type: GrantFiled: April 29, 1996Date of Patent: November 12, 2002Assignee: The United States of America as represented by the Secretary of TransportationInventors: Mohamed E. Labib, Brian H. Chollar, G. Mohammed Memon
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Patent number: 6454934Abstract: A petroleum processing method comprising the steps of: performing an atmospheric distillation of crude oil; collectively hydrodesulfurizing the resultant distillates consisting of gas oil and fractions whose boiling point is lower than that of gas oil in a reactor in the presence of a hydrogenation catalyst at 310 to 370° C. under 30 to 70 kg/cm2G (first hydrogenation step); and further performing hydrodesulfurization at lower temperatures (second hydrogenation step). When the second hydrogenation step is carried out only for the heavy naphtha obtained by separating the distillates after the first hydrogenation step, the second hydrogenation temperature can be in the range of 250 to 400° C.Type: GrantFiled: September 10, 1998Date of Patent: September 24, 2002Assignee: JGC CorporationInventors: Makoto Inomata, Toshiya Okumura, Shigeki Nagamatsu
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Publication number: 20020100711Abstract: The present invention is directed to the upgrading of heavy hydrocarbon feedstock that utilizes a short residence pyrolytic reactor operating under conditions that cracks and chemically upgrades the feedstock. The process of the present invention provides for the preparation of a partially upgraded feedstock exhibiting reduced viscosity and increased API gravity. This process selectively removes metals, salts, water and nitrogen from the feedstock, while at the same time maximizes the yield of the liquid product, and minimizes coke and gas production. Furthermore, this process reduces the viscosity of the feedstock in order to permit pipeline transport, if desired, of the upgraded feedstock with little or no addition of diluents.Type: ApplicationFiled: September 18, 2001Publication date: August 1, 2002Inventors: Barry Freel, Robert Graham
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Patent number: 6383365Abstract: A 40 petroleum pitch is disclosed. A high melting point petroleum pitch is blended with a high boiling normally liquid petroleum derived hydrocarbon stream to form a mixture having a softening point of 35-45 C. as a partial or complete replacement for coal tar pitch used in driveway sealer and other sealer applications. Driveway sealer (an emulsion of clay, water and binder) made with A 40 has excellent durability and can have a greatly reduced amount of, or be essentially free of, coal tar pitch, greatly reducing the toxicity and odor of the sealer.Type: GrantFiled: November 16, 1999Date of Patent: May 7, 2002Assignee: Marathon Ashland Petroleum LLCInventors: D. Chris Boyer, Patricia K. Doolin
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Publication number: 20020027066Abstract: When a pitch composition prepared by mixing 100 parts by weight of mesophase pitch with 10 to 1,000 parts by weight of coal tar pitch, is heat-treated at a temperature of 500° C. or higher, it is possible to produce a high-density coke at a high yield while avoiding the foaming of the mesophase pitch. In addition, when the coke is graphitized at a temperature of 2,000° C. or higher, it is possible to obtain an artificial graphite having a high graphitization degree. Further, when the coke is first pulverized and then graphitized at a temperature of 2,000° C. or higher, it is possible to obtain a high-crystallinity graphite powder which can be suitably used as a carbon material for a negative electrode of non-aqueous solvent type secondary battery having a high discharge capacity and a high charge-discharge efficiency.Type: ApplicationFiled: August 8, 2001Publication date: March 7, 2002Inventors: Koichi Kanno, Hirotaka Tsuruya, Ryuji Fujiura