Processes Patents (Class 209/164)
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Patent number: 6007618Abstract: Kaolin clays are conditioned for the removal of colored titaniferous impurities by (A) first mixing the kaolin clay with a collector to condition the impurities, in the absence of a dispersant, but in the presence of sufficient water to yield a mixture having a solids content of at least 65 percent by weight and (B) then deflocculating the kaolin clay mixture at a pH of at least 4.0 with a dispersant in amounts sufficient to yield a kaolin clay slurry which is suitable for subsequent processing to remove colored titaniferous impurities.Type: GrantFiled: November 10, 1997Date of Patent: December 28, 1999Assignee: Thiele Kaolin CompanyInventors: Joseph Allen Norris, Jorge L. Yordan
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Patent number: 6000551Abstract: A method for rupturing microalgae in an aqueous suspension is disclosed. In one embodiment the aqueous suspension is passed through a constriction into a liquid phase at a pressure sufficient to rupture the cells by circulating the aqueous suspension through a constriction in a pump loop at a pressure and a percent recycle sufficient to rupture the cells. Cells of the alga Dunaliella salina can be ruptured by the method of the invention to promote froth flotation and mechanical filtration of the cells for recovery of mixed carotenoids.Type: GrantFiled: December 20, 1996Date of Patent: December 14, 1999Assignee: Eastman Chemical CompanyInventors: Jeffrey Scott Kanel, Scott Arthur Guelcher
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Patent number: 6000552Abstract: A process for the purification of a fiber suspension (deinking or white water) in which a mixture of fiber suspension and gas bubbles are jtted into a flotation tank in an upwardly directed manner toward the free surface of the pulp at a velocity of greater than Sm/s and the jet ends at or just below the free surface of the mixture.Type: GrantFiled: May 6, 1999Date of Patent: December 14, 1999Assignee: Sunds Defibrator Industries ABInventors: Thomas Eriksson, Borje Fredriksson, Tomas Wikstrom
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Patent number: 5988396Abstract: Processes for treating fly ash to enhance the fly ash as a pozzolan for portland cement mixes and to separate therefrom a substantial carbon compound and/or to increase the fineness of the fly ash include the treatment of a fly ash slurry with ultrasonic energy using ultrasonic horns immersed in a slurry of fly ash and water and imparting to said slurry such ultrasonic energy as to cause microscopic cavities to form and implode with high localized energy to break up fly ash agglomerations along cleavage lines and to break up carbon particles and matrices which have entrapped fly ash microspheres therein to release the microspheres into the slurry. A conditioner agent may be added at or during ultrasonic treatment to enhance the flotation of the carbon compound.Type: GrantFiled: August 18, 1998Date of Patent: November 23, 1999Assignee: ISG Resources, Inc.Inventors: Rafic Y. Minkara, Jerry L. Heavilon
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Patent number: 5936216Abstract: A froth floatation process for separating carbon from coal ash incorporates a step of screening the coal ash before the coal ash is formed into a slurry.Type: GrantFiled: December 1, 1998Date of Patent: August 10, 1999Inventor: Chiung-Hsin Wu
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Patent number: 5925862Abstract: A process for the production of cobalt concentrate from an ore containing metal sulfides including sulfides of lead, zinc, and cobalt. The ore is crushed and subjected to a lead and cobalt flotation to separate the lead and cobalt from the zinc and produce a bulk lead cobalt concentrate. The lead cobalt concentrate is then subjected to a cobalt flotation to separate the cobalt from the lead and produce a cobalt concentrate.Type: GrantFiled: November 21, 1997Date of Patent: July 20, 1999Assignee: The Doe Run CompanyInventors: John C. Morrisey, IV, Quentin J. Schmidt
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Patent number: 5917166Abstract: Methods for washing sawdust are disclosed which include providing a mixture of sawdust and water to a vessel, subjecting the mixture to a reduced pressure so that gases present in the sawdust cause expansion therein and the sawdust rises to the surface of the mixture while the contaminants descend within the vessel, and withdrawing the sawdust from the vessel, in which the sawdust is withdrawn from the vessel at a location above the point where the sawdust and water enter the vessel. Apparatus for carrying out this method is also disclosed.Type: GrantFiled: March 27, 1997Date of Patent: June 29, 1999Assignee: Sunds Defibrator Industries ABInventor: Jan Henriksson
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Patent number: 5916446Abstract: Process and apparatus for the separation of solid matter via flotation. The flotation process for the separation of solid matter from a suspension takes place via the utilization of centrifugal forces wherein the suspension is brought into rotation in a separating zone so that the floated components are particularly effectively routed to and concentrated at the center of the separating space, whereby, when viewed axially, floated components and the remaining portion of the suspension is guided in the same direction and out of the separating zone, with the avoidance of vortexes in the flow stream achieving particularly favorable separation effects. In addition, several apparatuses, for carrying out the process, are also set forth.Type: GrantFiled: April 30, 1997Date of Patent: June 29, 1999Assignee: Sulzer-Escher Wyss GmbHInventors: Herbert Britz, Alexander Peschl
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Patent number: 5910254Abstract: A process for dewatering an aqueous suspension of microalgae is disclosed in which the aqueous suspension of the algae is introduced into a bubble column or a modified bubble column for generating a froth of bubbles and adsorbed algal cells that can be separated from the aqueous suspension. In one advantageous embodiment, the bubble column is a multi-stage loop-flow flotation column that has three loop-flow zones, each of which is defined by a draft tube concentrically mounted in the column to divide each loop-flow zone into a riser and the downcomer. Fine bubbles of gas and brine are in cocurrent upward flow in the riser and in cocurrent downward flow the downcomer. A higher gas holdup is promoted in the riser than in the downcomer, thereby circulating the brine in loop-flow upwardly through the riser and downwardly through the downcomer. Liquid communication between adjacent loop-flow zones is substantially eliminated. A froth enriched in algae is generated that can be separated from the aqueous suspension.Type: GrantFiled: December 20, 1996Date of Patent: June 8, 1999Assignee: Eastman Chemical CompanyInventors: Scott Arthur Guelcher, Jeffrey Scott Kanel
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Patent number: 5909022Abstract: A flash flotation device (1) comprises a tank (2) to contain slurry (3) incorporating minerals to be extracted, a feed inlet (25) for admission of slurry (3) into the tank (2), agitation means (10) to agitate the slurry (3) within the tank (2), aeration means to aerate the slurry (3) whereby floatable minerals in suspension form a surface froth for removal via froth lip (29), a bottom outlet (26) for withdrawal of relatively coarse or dense components of the slurry (3) from the tank (2), and a side outlet (28) to regulate the level of slurry (3) in the tank (2).Type: GrantFiled: April 30, 1997Date of Patent: June 1, 1999Assignee: Outokumpu Mintec OyInventors: Peter Bourke, Jouko Kallioinen
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Patent number: 5902976Abstract: Improved control for the separation of waste materials, or materials having waste components, is provided by the injection of air, or other gas bubbles, into a water-filled tank while simultaneously depositing the waste containing material to be separated onto the top of the water. This method is especially useful where both portions of some or all of the materials to be separated from each other have specific gravities greater than that of pure water. The rapidly rising air bubbles provide turbulence and buoyancy to materials that are slightly heavier than water, such as water-soaked organic products, but do not prevent heavier materials, such as sand and metals from sinking. An apparatus is described which allows for the removal of both the floating and sinking fractions from the floatation tank.Type: GrantFiled: January 30, 1998Date of Patent: May 11, 1999Inventor: Donald R. Beasley
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Patent number: 5900604Abstract: The present invention is a process for recovering valuable minerals using air lift concentration and progressive ore reduction. The ore is ground to a relatively coarse size, the ground ore is classified, and the underflow fraction floated to produce concentrate, middlings, and tailings fractions. The middlings fraction can be reground to liberate the valuable minerals and subjected to further air lift concentration. The classifier overflow fraction is passed through additional classifiers, the underflow fractions of which can be reground and refloated. The overflow fraction of the last classifier can be subjected to flotation to further enhance recovery.Type: GrantFiled: March 18, 1997Date of Patent: May 4, 1999Inventor: Harry L. McNeill
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Patent number: 5876558Abstract: The present invention provides a froth flotation process for the separation of paper and wood fibers from printed and copying inks and other contaminants during the recycling of paper. A liquid solution containing a frothing agent is applied from the top of a froth flotation device, preferably in the form of a spray, to the upper surface or portion of an aqueous pulp slurry present in the device, or of a froth phase produced in the device, prior to or during the froth flotation process.Type: GrantFiled: December 17, 1997Date of Patent: March 2, 1999Assignee: Institute of Paper Science and Technology, Inc.Inventors: Yulin Deng, Junyong Zhu
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Patent number: 5855769Abstract: Hydrophobic material is selectively separated from an aqueous feed by forming gas bubbles in a flow of the feed, forming hydrophobic material/gas bubbles aggregates by motionless mixing and separating the aggregates as a froth by use of centrifugal action.Type: GrantFiled: August 14, 1996Date of Patent: January 5, 1999Assignee: Commonwealth Scientific and Industrial Research OrganisationInventors: Bruce Andrew Firth, Philip Kwadwo Ofori
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Patent number: 5840179Abstract: Processes for treating fly ash to enhance the fly ash as a pozzolan for portland cement mixes and to separate therefrom a substantial carbon compound and/or to increase the fineness of the fly ash include the treatment of a fly ash slurry with ultrasonic energy using ultrasonic horns immersed in a slurry of fly ash and water and imparting to said slurry such ultrasonic energy as to cause microscopic cavities to form and implode with high localized energy to break up fly ash agglomerations along cleavage lines and to break up carbon particles and matrices which have entrapped fly ash microspheres therein to release the microspheres into the slurry. A conditioner agent may be added at or during ultrasonic treatment to enhance the flotation of the carbon compound.Type: GrantFiled: March 17, 1998Date of Patent: November 24, 1998Assignee: JTM Industries, Inc.Inventors: Rafic Y. Minkara, Jerry L. Heavilon
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Patent number: 5814210Abstract: A method and apparatus are disclosed for the microbubble flotation separation of very fine and coarse particles, especially coal and minerals, so as to produce high purity and high recovery efficiency. This is accomplished through the use of a flotation column, microbubbles, recycling of the flotation pulp, and countercurrent wash water to gently wash the froth. Also disclosed are unique processes and apparatus for generating microbubbles for flotation in a highly efficient and inexpensive manner using either a porous tube or in-line static generators.Type: GrantFiled: April 30, 1996Date of Patent: September 29, 1998Assignee: Virginia Tech Intellectual Properties, Inc.Inventors: Roe-Hoan Yoon, Gregory T. Adel, Gerald H. Luttrell
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Patent number: 5807479Abstract: The present invention provides a process that employs both non-selective flotation and oxidative leaching of the resulting concentrates to recover an increased amount of copper from porphyry copper ores. The non-selective flotation step uses collectors and conditions, such as pH, that are conducive to the strong flotation of sulfide minerals generally. In the oxidative leach, the copper sulfide minerals in the concentrate fraction are oxidized to copper compounds, which are soluble in the leach solution. The oxidative leach includes the use of ammonia and sulfite under agitation leaching conditions to convert the copper sulfide minerals into ammonia soluble forms.Type: GrantFiled: July 14, 1995Date of Patent: September 15, 1998Assignee: COPROCO Development CorporationInventor: Nathaniel Arbiter
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Patent number: 5795484Abstract: An ultra-fine coal particle fraction forms a coal product with particles that are dilatant due to the mechanical stripping of the clay contaminates from the coal surface and the subdividing of the clay to clay platelets which are peptized to maintain discreetness in an aqueous slurry. The coal particles are unflocculated and can produce an aqueously permeable barrier on a sieve. The ultrafine coal product has an increase of 100-150 BTU per pound and when combusted reduced Nox production of 20-40% is realized. In a 15.times.0 micron coal fraction, the sulphur content is significantly reduced.Type: GrantFiled: May 8, 1995Date of Patent: August 18, 1998Inventor: Edward H. Greenwald, Sr.
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Patent number: 5776349Abstract: Methods are disclosed for dewatering an aqueous suspension of microalgae, especially Dunaliella salina, with a Jameson cell. The algal cells are ruptured sufficiently to promote froth flotation of the cells from the suspension. The algal suspension is introduced into the top of the Jameson cell downcomer and passed through an orifice plate therein to generate a free liquid jet of the suspension. The jet is plunged downwardly through a gas and the gas is transported with the jet through a gas and liquid interface into the algal suspension. The momentum of the jet is dissipated, which disperses the gas into fine bubbles. The fine bubbles are intimately contacted with the aqueous suspension in cocurrent downward flow in a collection zone to absorb the algal bodies onto the surfaces of the bubbles. A froth of bubble and algal agglomerates is formed and collapsed to obtain a dewatered algal concentrate.Type: GrantFiled: December 20, 1996Date of Patent: July 7, 1998Assignee: Eastman Chemical CompanyInventors: Scott Arthur Guelcher, Jeffrey Scott Kanel
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Patent number: 5762781Abstract: A flotation apparatus including: an elongate vertical riser (142) in which a cocurrent flow of gas/slurry liquid mixture rises upwards to a discharge mouth at its top end; an aeration unit (140) provided at a lower end of the riser; a separation unit (150) provided at the top end of the riser; and wherein the height of the riser is selected to produce substantially turbulence free flow in which a high gas lift occurs in the riser such that a pressure drop between the liquid inlet and the discharge outlet of the aeration unit is sufficient to produce gas particle dispersion and recirculation of the slurry liquid through the flotation apparatus.Type: GrantFiled: May 24, 1996Date of Patent: June 9, 1998Assignee: Atomaer Pty. Ltd.Inventor: George Bodnaras
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Patent number: 5702612Abstract: A flotation method and apparatus for separating a selected constituent from an effluent of an industrial process is provided. The apparatus includes a conditioning tank and a flotation cell. The conditioning tank allows mixing a flotation reagent with an effluent and includes a mechanism for also dissolving gas in the effluent within the conditioning tank. The flotation cell includes a dissolved gas flotation chamber having an overflow for recovering the selected constituent and a tailings drain. In addition, the flotation cell also includes an added gas flotation chamber having a sparger for injecting gas into the effluent, an overflow for recovering the selected constituent and a tailings drain.Type: GrantFiled: July 20, 1995Date of Patent: December 30, 1997Assignee: University of Kentucky Research FoundationInventor: Xiang-Huai Wang
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Patent number: 5690812Abstract: Process and apparatus for the separation of solid matter via flotation. The flotation process for the separation of solid matter from a suspension takes place via the utilization of centrifugal forces wherein the suspension is brought into rotation in a separating zone so that the floated components are particularly effectively routed to and concentrated at the center of the separating space, whereby, when viewed axially, floated components and the remaining portion of the suspension is guided in the same direction and out of the separating zone, with the avoidance of vortexes in the flow stream achieving particularly favorable separation effects. In addition, several apparatuses, for carrying out the process, are also set forth.Type: GrantFiled: November 2, 1995Date of Patent: November 25, 1997Assignee: Sulzer-Escher Wyss GmbHInventors: Herbert Britz, Alexander Peschl
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Patent number: 5685899Abstract: Kaolin clays are conditioned for the removal of colored titaniferous impurities by (A) first mixing the kaolin clay with a collector to condition the impurities, in the absence of a dispersant, but in the presence of sufficient water to yield a mixture having a solids content of at least 65 percent by weight and (B) then deflocculating the kaolin clay mixture at a pH of at least 4.0 with a dispersant in amounts sufficient to yield a kaolin clay slurry which is suitable for subsequent processing to remove colored titaniferous impurities.Type: GrantFiled: July 28, 1995Date of Patent: November 11, 1997Assignee: Thiele Kaolin CompanyInventors: Joseph Allen Norris, Jorge L. Yordan
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Patent number: 5672267Abstract: A method and apparatus for separating particulate material. The method includes the steps of delivering a substantially constant supply of feed to a first aerator, aerating the substantially constant supply of feed in the first aerator, introducing the substantially constant supply of aerated feed to a flotation vessel below a froth/liquid interface within the vessel, so that floatable particulate material entrained by air bubbles from the first aerator can float upwardly to the froth/liquid interface. Air is introduced into the liquid phase in the flotation vessel via a second aerator located below the level at which the aerated feed is introduced into the flotation vessel, so that floatable particulate material not entrained by air bubbles from the first aerator, may be entrained by air bubbles from the second aerator, as the air bubbles from the second aerator rise upwardly through the liquid phase to the froth/liquid interface.Type: GrantFiled: June 5, 1996Date of Patent: September 30, 1997Assignee: Multotec Cyclones (PTY) LimitedInventor: Nardus Terblanche
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Patent number: 5660718Abstract: A suitably conditioned slurry feed is introduced to a trough from which it is distributed into a slurry layer-flow forming chamber provided with a discharge weir which discharges an evenly spread layer of slurry onto an inclined plate feeding into a mixing passage and then into a vessel. Recirculated slurry from the vessel is also fed into the mixing passage via a recycle gate which forms it into a layer of slurry. An array of clean liquid jets accelerates thin gas envelopes and impinges between layers of slurry and causes intensive mixing of all streams in the mixing passage. A high shear rate produces high intensity turbulence and shears gas into very small bubbles. A multiphase mixture flow is discharged from the mixing passage into the vessel, where it flows past one or more longitudinal stabilizing baffles. Gas bubbles loaded with hydrophobic particles disengage from the stream, rise toward the liquid surface and are diverted by bubble-diverting guides toward a froth discharge end of the vessel.Type: GrantFiled: September 13, 1995Date of Patent: August 26, 1997Assignee: M.D. Research Company Pty, Ltd.Inventors: Michael Wenzel Chudacek, Stephen Henry Marshall, Charles Harold Warman
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Patent number: 5653867Abstract: An improved method is provided for separating acrylonitrile butadiene styrene (ABS) and high impact polystyrene (HIPS) plastics from each other. The ABS and HIPS plastics are shredded to provide a selected particle size. The shredded particles of the ABS and HIPS plastics are applied to a solution having a solution density in a predefined range between 1.055 gm/cm.sup.3 and 1.07 gm/cm.sup.3, a predefined surface tension in a range between 22 dynes/cm to 40 dynes/cm and a pH in the range of 1.77 and 2.05. In accordance with a feature of the invention, the novel method is provided for separating ABS and HIPS, two solid thermoplastics which have similar densities by selectively modifying the effective density of the HIPS using a binary solution with the appropriate properties, such as pH, density and surface tension, such as a solution of acetic acid and water or a quaternary solution having the appropriate density, surface tension, and pH.Type: GrantFiled: March 19, 1996Date of Patent: August 5, 1997Assignee: The University of ChicagoInventors: Bassam J. Jody, Bayram Arman, Dimitrios E. Karvelas, Joseph A. Pomykala, Jr., Edward J. Daniels
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Patent number: 5601703Abstract: The present invention is directed to a type of flotation machine that combines three separate operations in a single unit. The flotation machine is a hydraulic separator that is capable of reducing the pyrite and other mineral matter content of a coal. When the hydraulic separator is used with a flotation system, the pyrite and certain other minerals particles that may have been entrained by hydrodynamic forces associated with conventional flotation machines and/or by the attachment forces associated with the formation of microagglomerates are washed and separated from the coal.Type: GrantFiled: December 5, 1995Date of Patent: February 11, 1997Assignee: Electric Power Research Institute, Inc.Inventors: Kazimierz Szymocha, Boleslaw Ignasiak, Wanda Pawlak, Conrad Kulik, Howard E. Lebowitz
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Patent number: 5578198Abstract: The automatic regulator device comprises a channel for measuring the level and density of pulp in the chamber of a floatation machine, in which two bubbling pipes are in communication with a differential pressure pickup connected to the input of a frother flow-rate regulating channel and to one input of a correction unit whose other input is connected to a pressure pickup communicating with one of the bubbling pipes. The output of the correction unit is connected to the input of a circuit designed to regulate the rate of flow of water with frother in a pulp level stabilizing channel, the output of said circuit being connected to an actuator valve installed on a pipeline feeding water with frother and furnishing a control signal with respect to a pulp level deviation from a preset value.Type: GrantFiled: September 21, 1990Date of Patent: November 26, 1996Assignee: Yakutsky Nauchno-Issledovatelsky I Proektny Institut Almazodbyvajuschei PromyshlennostiInventors: Fedor A. Chumak, Vladimir N. Cherednik, Mikhail N. Zlobin
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Patent number: 5573658Abstract: A low brightness pigment and method is provided from a heretofore rejected waste kaolin stream. Kaolin processing rejects are high in iron-stained TiO.sub.2. After separating the stained TiO.sub.2 from the high brightness kaolin and concentrating the resulting fraction, the material can be processed to produce a low brightness pigment suitable of many applications where lower brightness is desirable, such as coating paper board without mottling.Type: GrantFiled: December 28, 1994Date of Patent: November 12, 1996Assignee: J. M. Huber CorporationInventors: Albert C. Kunkle, Robert E. Hardy, Bobby R. Skipper
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Patent number: 5571422Abstract: The present invention concerns a reactor for removing impurities from a liquid, in particular for de-inking, including a tank (1) within which the liquid to be purified together with a gas or air is introduced (2-3); a drain of the purified accepted through an outlet (7) of said tank (1); inlets (8-11, 9-12, 10-13) at different heights of the tank (1) connected to said purified liquid outlet (7) together with the inlet of gas or air; a rotating shaft (18) inside the tank (1) carrying blades (20, 21, 22, 23) at the different heights of the tank within which the liquid together with gas or air is introduced; the blades (20, 21, 22, 23) have progressively increasing heights when moving towards the lower portion of the tank (1). The invention also concerns the method embodied by the above-described reactor.Type: GrantFiled: June 12, 1995Date of Patent: November 5, 1996Assignee: Comer S.p.A.Inventor: Flavio Magaraggia
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Patent number: 5551574Abstract: A method for the separation of components of a slurry by froth flotation are provided. The apparatus includes a flotation column having a slurry feed for introducing slurry into the flotation column, a bubble generator for generating bubbles of gas at the bottom of the flotation column and a froth overflow at the top of the flotation column for collecting and discharging a froth fraction of the slurry. The central portion of the flotation column includes a plurality of vertically-spaced tail ports disposed alternately on opposite sides of the flotation column for discharging a non-float fraction of the slurry. In addition, a single, fluid-impermeable baffle having at least two edges is associated with each tail port. The baffles are of sufficient size to block the vertical flow in at least 50% of the horizontal cross-sectional area of the flotation column to thereby create a quiescent flow zone in the area of each tail port, wherefrom the non-florable fraction of the slurry is removed.Type: GrantFiled: September 18, 1995Date of Patent: September 3, 1996Assignee: The United States of America as represented by the Secretary of the InteriorInventors: Gary W. Hicks, William L. Cornell
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Patent number: 5544759Abstract: The invention relates to a method and an apparatus for the separation of hydrophobic substances by froth flotation that basically consists of feeding pulp in the form of a thin layer on at least a lower gas-permeable slanted surfaces in which low pressure gas is injected generating small bubbles that collect hydrophobic particles. The froth containing concentrate is separated and washed before removal in a froth reservoir formed by a lower gas-permeable slanted surface and a wall at its lower end. At the top of the wall, the froth overflows to a launder for removal. At the bottom of the wall, the pulp containing the tailings discharges through an opening. Froth washing is performed by means of baffles that force the froth to flow underneath water sprays.Type: GrantFiled: April 5, 1995Date of Patent: August 13, 1996Inventor: Daniel F. Urizar
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Patent number: 5522510Abstract: An apparatus for separating impurities from coal, includes a device for removing a predetermined amount of ash-forming substances from the coal and a device for removing a predetermined amount of high specific gravity (e.g., pyrite) from the coal having been processed by the ash-forming substance removing device. The ash-forming substance removing device and the high specific gravity material removing device each possess characteristics that allow them to more efficiently reject different types of mineral impurities from coal.Type: GrantFiled: June 14, 1993Date of Patent: June 4, 1996Assignee: Virginia Tech Intellectual Properties, Inc.Inventors: Gerald H. Luttrell, Roe-Hoan Yoon
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Patent number: 5512133Abstract: A method for producing substantially ink-free pulp from recycle printed paper comprising first pulping the recycle paper in a hydrapulper with at least water and an agglomerating agent thereby producing a pulp. Ink particle agglomerates in the pulp are then removed by screening the pulp through at least one screen and by cleaning the pulp in a cyclone cleaner. Pulp together with small ink particles that escape the prior separation stages is then conducted from the cyclone cleaner through a standpipe at a consistency of about or less than 1% where particles of ink associate with small air bubbles and are elevated to the surface of the pulp where they accumulate as a froth which may be removed by overflowing.Type: GrantFiled: August 1, 1994Date of Patent: April 30, 1996Assignee: International Paper CompanyInventor: Larry D. Markham
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Patent number: 5511669Abstract: A flotation device (1) which includes a tank (2) to contain a slurry (3) incorporating minerals which are to be extracted. Aeration of the slurry (3) by suitable structure in the device produces a zone (11) of mineralised froth above the slurry (3). A launder (15) directs the mineralised froth away from the tank (2). At least one porous diffusion surface (16) in direct contact with the froth dispenses a washing liquid directly into the froth zone (11).Type: GrantFiled: September 2, 1994Date of Patent: April 30, 1996Assignee: Supaflo Technologies Pty. LtdInventor: Peter G. Bourke
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Patent number: 5482535Abstract: In a process for the recovery of silver by flotation from the residue from the wet extraction of zinc, the residue from the neutral wet extraction of zinc, the residue from the neutral wet extraction of zinc is recovered and is subsequently ground in an attritor and the residue which has been ground in an attritor is subjected to a flotation.Type: GrantFiled: July 12, 1994Date of Patent: January 9, 1996Assignee: Metallgesellschaft AktiengesellschaftInventors: Ali-Nagi Beyzavi, Horst Dittmann, Friedrich Rosenstock
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Patent number: 5460270Abstract: Middlings from the primary separation vessel ("PSV") are recycled through a line to the PSV. The middlings are aerated with fine air bubbles using in line eductor/aerator assemblies. The aerated middlings are mixed as they are pumped through a line back to the PSV. Bitumen recovery from the PSV is increased as a result.Type: GrantFiled: September 1, 1993Date of Patent: October 24, 1995Assignees: Alberta Energy Company Ltd., Canadian Occidental Petroleum Ltd., Esso Resources Canada Limited, Gulf Canada Resources Limited, Her Majesty the Queen in right of the Province of Alberta, as represented by the Minister of Energy and Natural Resources, HBOG-Oil Sands Limited Partnership, PanCanadian Petroleum Limited, Petro-Canada Inc., Mocal Energy LimitedInventors: Edward W. Chan, Robert S. MacTaggart
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Patent number: 5456362Abstract: A process for the flotation of coarse potash ore fractions in an aqueous brine containing frother that comprises: (a) using a column flotation device in which air bubbles are generated by a sparger that utilizes high intensity shearing to mix and disperse air into brine containing frother; (b) removing a portion of the suspension at another point in the direction of flow of the suspension to regulate the upward flow rate of the suspension past the point where the air is dispersed into the suspension and thereby reducing fine particles entrainment in the froth product. The suspension can be conditioned with an aqueous composition comprising a hydrocarbon extender oil and a substantially saturated long chain primary mine, optionally comprising an acid, such as a mineral acid or carboxylic acid, to emulsify the oil in the composition, or can be conditioned with an aqueous composition comprising a long chain primary amine having an iodine value ranging from about 20 to about 70 cg/g.Type: GrantFiled: May 26, 1994Date of Patent: October 10, 1995Assignee: The University of British ColumbiaInventors: Janusz S. Laskowski, Qun Wang
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Patent number: 5435443Abstract: The invention proposes using liquefied carbon dioxide as a separation agent for flotation and/or sedimentation separation, which is particularly suitable for separating foodstuff mixtures such as meat components, because it can be maintained in liquid phase at the freezing point of water and is inert with respect to many substances of the mixture. By controlling the pressure and/or the temperature at values of about 26 bar and -14.degree. C., the density of the separation agent can be adjusted to correspond to that of water so that water containing substances of the mixture can be readily separated.Type: GrantFiled: November 3, 1993Date of Patent: July 25, 1995Inventors: Hermann Hohenester, Helmut Reisser
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Patent number: 5417806Abstract: A method of removing fine contaminants from waste paper fibrous material (S) is described with solution (1) and pre cleaning (2) whereupon the fibrous material is first subjected to a washing treatment (3) and then to a flotation treatment (5). The washing filtrate (12) from the washing treatment (3) is cleaned in a filtrate-flotation treatment (4) so that a cleaned fraction (14) can be returned into the useful material (13) of the washing treatment. The so cleaned waste paper fibrous material can be passed to further treatment steps such as flotation, bleaching and/or dispersion. The reject material from the filtrate-flotation (4) is, in one embodiment, again subjected to a flotation treatment.Type: GrantFiled: October 19, 1992Date of Patent: May 23, 1995Assignee: Sulzer-Escher Wyss GmbHInventors: Wolfgang Matzke, Bruno Michelewski
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Patent number: 5413703Abstract: A method and apparatus for dewatering an aqueous coal slurry includes imparting high shear forces to the aqueous coal slurry in the presence of a peptizing agent to render coal particles hydrophobic by stripping clay from the coal particles and peptizing the clay in the aqueous medium of the slurry. The slurry is separating to recover coal particles and the aqueous medium is draining medium from the hydrophobic surface of the coal particles.Type: GrantFiled: July 22, 1993Date of Patent: May 9, 1995Inventor: Edward H. Greenwald, Sr.
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Patent number: 5402893Abstract: A method is described for processing waste materials in the form of filter rods, filter cigarettes and the like comprising filter material with inner hollow volumes accessible from the outside and at least one other material component, in particular paper and tobacco, wherein the following process steps are carried out: the waste material is distributed in a liquid in a pressure vessel. By increasing the pressure or decreasing the temperature an inert gas is dissolved in the liquid. Subsequently the temperature is increased or the pressure decreased so that fine gas bubbles develop within the filter material which permits the latter to float whereby a separation from the further material components to be separated is possible. With this method a separation of the waste material into its individual component parts is possible so that for example valuable filter material in the form of cellulose acetate is obtained in highly pure form and can be used again for the production of filter materials.Type: GrantFiled: July 14, 1993Date of Patent: April 4, 1995Assignee: Rhone-Poulenc Rhodia AktiengesellschaftInventor: Karsten Keller
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Patent number: 5385239Abstract: A low brightness pigment and method is provided from a heretofore rejected waste kaolin stream. Kaolin processing rejects are high in iron-stained TiO.sub.2. After separating the stained TiO.sub.2 from the high brightness kaolin and concentrating the resulting fraction, the material can be processed to produce a low brightness pigment suitable of many applications where lower brightness is desirable, such as coating paper board without mottling.Type: GrantFiled: April 27, 1992Date of Patent: January 31, 1995Assignee: J. M. Huber CorporationInventors: Albert C. Kunkle, Robert E. Hardy, Bobby R. Skipper
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Patent number: 5385600Abstract: The invention relates to a method for fully beneficating nickel sulfide concentrates or other corresponding mixtures, unsuitable for smelting, by combining the use of both pyrometallurgical and hydrometallurgical processes, so that there are formed two separate concentrates, the first of which is suited to pyrometallurgical and the second to hydrometallurgical treatment. In the concentrate going to pyrometallurgical processing, the valuable metal content increases as a consequence of the treatment, and the Fe/MgO ratio of this concentrate is at least 2.6.Type: GrantFiled: June 11, 1993Date of Patent: January 31, 1995Assignee: Outokumpu Harjavalta Metals OyInventor: Seppo S. Jounela
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Patent number: 5376276Abstract: Aerated bitumen froth containing bitumen, water, air and solids is the product of the hot water extraction process for recovering bitumen from oil sand. Measurements related to the water content of the froth can be obtained by measuring its resonant frequency in a calibrated output, open-ended microwave cavity. By also measuring the bulk density of the froth and assuming a constant relationship for the solids content, one can compute from the assembled data the output quality of the froth. The measurements can be taken repetitively at the vessel as the froth is produced and used to almost instantly provide froth quality information.Type: GrantFiled: April 1, 1993Date of Patent: December 27, 1994Assignees: Alberta Energy Company, Ltd., Canadian Occidental Petroleum Ltd., Esso Resources Canada Limited, Gulf Canada Resources Limited, Her Majesty the Queen in right of the Province of Alberta as represented by the Minister of Energy and Natural Resources, Hbog-Oil Sands Limited Partnership, Pancanadian Petroleum Limited, Petro-Canada Inc., Mocal Energy Limited, Murphy Oil Company Ltd.Inventors: Keng H. Chung, Gordon R. Thompson, Wayne B. Jansen, Ethel A. Nakano, Samson Y. Ng
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Patent number: 5368166Abstract: The automatic control device comprises a channel used to measure the level and density of pulp in a chamber of a floatation machine, in which two bubbling tubes communicate with a differential pressure transducer connected to the input of a frother flow control channel and to the input of a correction unit whose other input is connected to a pressure transducer communicating with one of the bubbling tubes. The bubbling tubes are installed in hydrostatic tubes located outside the chamber and communicating therewith at different levels relative to the pulp level. The output of the correction unit is connected to the input of a circuit designed to control the flow rate of water and frother in a pulp level stabilizing channel and having its output connected to an actuator valve of a pipeline feeding water and frother.Type: GrantFiled: September 21, 1990Date of Patent: November 29, 1994Inventors: Fedor A. Chumak, Vladimir N. Cherednik, Mikhail N. Zlobin
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Patent number: 5341938Abstract: A method of separating desired material from undesired material is provided. The method is performed by forming a slurry of material and introducing it into a specially designed flotation reactor chamber. A foam is generated and introduced into the reactor chamber and dispersed into the slurry. A stream of water is provided to separate the undesired portion of the material from the desired portion of the material that has adhered to the bubbles in the foam.Type: GrantFiled: May 13, 1993Date of Patent: August 30, 1994Assignee: Servicios Corporativos Frisco, S.A. de C.V.Inventors: Ulises M. Valenzuela, Guillermo Moguel
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Patent number: 5338337Abstract: The invention relates to a method of ore beneficiation.The process comprises:(1) grinding the ore to produce a first product comprising ground ore and ground gangue,(2) separating the first product into a fraction having particles of a selected size range and a remainder,(3) separating at least a part of the remainder into a ground ore fraction and a ground gangue fraction,(4) combining the particles of selected size range from step (2) with the ground ore fraction of step (3), and(5) autogenously and/or semi-autogenously grinding the combination of step (4).The process is particularly suitable for lead and/or zinc sulphide ores.In step (5) at least 80% of the resulting ore can be ground to a particle size of less than 6 microns.Type: GrantFiled: October 22, 1992Date of Patent: August 16, 1994Assignee: Mount Isa Mines LimitedInventors: Norman W. Johnson, John P. Andreatidis
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Patent number: 5337965Abstract: A method and apparatus for recycling asphalt based roofing material which typically comprises a body of asphalt and fiber, with aggregate on and adhered to the asphalt. The asphalt bodies, with aggregate, are subjected to action to separate or disengage the aggregate from the asphalt body without substantially reducing the size of the aggregate. Disengagement is effected by causing asphalt bodies with aggregate to impact on each other. Disengagement may be effected by placing asphalt bodies with aggregate in water to form in a slurry, which is agitated, as by an impeller. The asphalt bodies float to the top of the liquid, which is a non-solvent for asphalt, and are removed and dewatered; the aggregate of undiminished size is separately recovered.Type: GrantFiled: October 9, 1992Date of Patent: August 16, 1994Assignee: Finoll Recycling Ltd.Inventor: Domenico Chiovitti
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Patent number: 5332100Abstract: A method for the beneficiation of mineral ores by the flotation method whereby a slurry is introduced under pressure into the top of a first column through a downwardly facing nozzle, and air is entrained into the slurry forming a downwardly moving foam bed in the first column. The foam bed passes from the bottom of the first column into a second column where the froth and liquid separate, the froth carrying the values floating upwardly and over a weir and the liquid being drained with the gangue. The liquid/froth interface level in the second column is kept above the bottom of the first column, and the air flow rate into the top of the first column is controlled to keep the first column substantially full of foam.Type: GrantFiled: October 27, 1992Date of Patent: July 26, 1994Assignee: The University of New Castle Research Associates Limited of University of New CastleInventor: Graeme J. Jameson