Abstract: A method of electrolessly gold plating copper on a printed circuit board (PCB). Starting with a copper patterned PCB, steps include: clean with ultrasonic agitation with the PCB initially oriented vertically and gradually moved to a 45° angle; rinse; sulfuric acid bath with ultrasonic and mechanical agitation; rinse; another sulfuric acid bath with ultrasonic and mechanical agitation; plate the copper with palladium with ultrasonic agitation with the PCB initially oriented at a 45° angle and flipped half way through to opposing 45° angle; rinse; post dip in sulfuric acid; rinse; electrolessly nickel plate with mechanical agitation; rinse; nitrogen blow dry; visual inspection for nickel coverage of the copper; hydrochloric acid bath with manual agitation; rinse; if full nickel coverage was not achieved, repeat preceding steps starting with second sulfuric acid bath; gold flash plate to establish a first layer of gold; rinse; autocatalytic gold plate; rinse; and nitrogen blow dry.

Abstract: The object of the invention is to provide a method for sintering bioactive glass or bioactive glass composite. The method according to the invention is characterised in that the sintering is performed with a localised electromagnetic and/or acoustic energy. Other objects of the invention are a method for coating a device with bioactive glass or bioactive glass composite and a method for attaching at least two devices. All these methods use sintering with localised electromagnetic and/or acoustic energy.

Abstract: The present invention has several plausible embodiments. In one embodiment an apparatus for coating a medical device is provided. This apparatus includes a coating chamber, a vibrating structure within the coating chamber the vibrating structure capable of suspending a medical device positioned in the coating chamber, and a coating source, the coating source positioned to introduce coating into the coating chamber. In another embodiment a method of coating a medical device is provided. This method includes moving a medical device into a predetermined coating area, vibrating a structure below the medical device, the vibration of the structure forcing the medical device away from the vibrating structure, and coating at least a portion of the medical device that has moved away from the vibrating structure.

Abstract: A process for depositing metal on microparticulate comprising immersing microparticulate in an autocatalytic plating bath comprising the metal; inducing ultrasonic vibration in the plating bath at a frequency corresponding to resonance frequency of the microparticulate; and inducing a turbulent vibration signal in the plating bath in a direction non-parallel to the ultrasonic vibration. This process results in the autocatalytic plating bath depositing the metal on the microparticulate with uniform thickness. The microparticulate can be spheres, flakes or microfibers, and can be made from a number of materials, such as synthetic polymers (nylon, Kevlar™, Zylon™, and aramid fibers) and biodegradable compounds. A method is disclosed for coating a surface with metallized microparticulate fibers with an orientation perpendicular to the surface.

Abstract: Materials and methods inhibit the localized build-up of material with respect to certain additive manufacturing processes, including those based on ultrasonic consolidation. Where an object is fabricated by consolidating material increments from a feedstock in accordance with a description of the object, the invention prevents the consolidation in specified regions to provide for an intrinsic support or to otherwise build a part or component in accordance with the description. The object being fabricated, the feedstock, or both, may be treated so as to inhibit the consolidation of material increments in the localized area. That is, such treatment may affect the surface chemistry of the feedstock to prevent local bonding, or the treatment may be applied to a previously built surface of the object.

Abstract: A method for making an enameled steel sheet includes the steps of spraying a slurry to form a slurry layer onto a surface of a substrate and firing the slurry layer. In this method, the slurry has a static surface tension of 50 dyne/cm or less and an apparent viscosity of 500 mPa·s that is measured with a model E viscometer at a rotation of 100 rpm. Alternatively, the method includes a step of spraying a slurry for forming an enamel layer onto a surface of a substrate, wherein the substrate is vibrated when the slurry is applied or when the slurry applied is still fluid.

Abstract: The present invention provides a method and apparatus for applying a coating material onto a print substrate mounted on a plate cylinder of a printing press. The method comprising: delivering a supply of the coating material to a distributive surface of an ultrasonic horn, the distributive surface controlling a flow of the coating material to an active edge of the ultrasonic horn, and atomizing the coating material at the active edge of the ultrasonic horn and directing the atomized coating material onto a surface of the print substrate. The present invention also provides a multi-purpose ultrasonic acoustic coating/cleaning system for applying a coating material onto, and cleaning the coating material from, a print substrate.

Abstract: A method of providing a hermetically sealed enclosure for a highly moisture sensitive electronic device including depositing an electrical conductor on the substrate which provides an electrical connection with the electronic device and depositing an electrically insulating thin layer over the electrical conductor; providing a low melting point indium metal or alloy in the form of a wire having diameter ranging from 1 mil to 10 mils on the electrically insulating thin layer on the substrate so that the wire is situated around the periphery of the electronic device; placing an ultrasonic horn over the cover plate so that ultrasonic energy can be delivered through the cover plate to the wire and applying a pressure between 20 and 100 psi; and providing an acoustic wave to melt the wire.

Abstract: A method for locally nickel-plating an aluminum alloy fin structure including placing the aluminum alloy fin structure on a sponge that is located at the bottom of a “zinc” tank containing a volume of zinc chemical solution for zinc plating; and thereafter rotating the aluminum alloy fin structure and immersing the rotated aluminum alloy fin structure in a volume of nickel chemical solution of a “nickel” tank to plate nickel onto the aluminum alloy fin structure.

Abstract: The invention relates to a process for depositing a metal on a material. The process comprises the steps of: immersing the material in a deposition solution comprising the metal; inducing a material vibration in the deposition solution having a frequency corresponding to a resonance frequency of the material; inducing a solution vibration in the deposition solution in a direction non-parallel to the material vibration, said solution vibration having a frequency corresponding to the a resonance frequency of the deposition solution, whereby said metal is deposited onto the material. This process results in deposition of metal from the plating bath on the material in a controlled and substantially uniform thickness.

Abstract: A process for producing a magnetic recording medium is provided in which a magnetic layer including a ferromagnetic powder and a binder is provided on a non-magnetic flexible support. In the process, a magnetic liquid containing mainly a ferromagnetic powder and a binder, and an abrasive liquid paste including an abrasive and a binder are prepared separately, and the abrasive liquid paste is subsequently subjected to an ultrasonic dispersion treatment and then mixed with the magnetic liquid to prepare a magnetic coating solution for the magnetic layer.

Abstract: A process for coating an object formed of magnesium or a magnesium alloy comprising the steps of: immersion coating the object in a sonicated bath to form an undercoat and topcoating the object to form a topcoat. When desirable to protect against topcoat failure, the undercoat may be equally noble or more noble than the topcoat. If topcoat failure is not a concern, the nobility of the topcoat relative to the undercoat need not be considered. The process promotes uniform coating of a magnesium and its alloys.

Abstract: A closed space is formed in a reduced pressure drying station, and the closed space is brought to a vacuum state. In this state, an EB unit irradiates a wafer mounted on a hot plate with an electron beam to foam an insulating film material. Subsequently, the hot plate is raised to a predetermined temperature, and drying processing is performed under a reduced pressure. As described above, since the foaming processing is performed in the reduced pressure drying station, bubbles remain in the insulating film, so that the existence of the bubbles can decrease the relative dielectric constant.

Abstract: An apparatus for repairing a crack in a vehicle windshield includes a high frequency vibration applicator and repair material. The high frequency vibration applicator includes a high frequency vibration generator, an elongate vibration delivery probe, and a handle grip for manipulation of the high frequency vibration applicator by a user. The vibration delivery probe delivers high frequency vibration from the generator to the windshield via a tip of the probe. A method of repairing a crack in a vehicle windshield includes infilling the crack with a repair material, applying to the windshield a tip of an elongate vibration delivery probe of a high frequency vibration applicator, and manipulating the high frequency vibration applicator to track the probe in a longitudinal direction of the crack.

Abstract: A method for fabricating a plated product with a basecoat layer, a metal plating layer, and a topcoat layer that are formed on a surface of a base is provided. The method includes the step of forming the basecoat layer and the metal plating layer on the surface of the base. The step is followed by subjecting the metal plating layer to a cold heat treatment or an ultrasonic wave treatment, thus forming a microcrack in the metal plating layer. Afterwards, the topcoat layer is formed on the surface of the metal plating layer.

Abstract: A method for coating moisture sensitive inorganic particles, such as phosphors, comprising mixing the inorganic particles having a particle size of about 1 to 100 micrometers with nanometer-sized coating particles, and firing the mixture to soften or melt the nanometer-sized particles about the inorganic particles, forming a moisture impervious coating. The coated particles are washed to remove excess particles, and dried. Coated moisture sensitive phosphor particles are impervious to moisture.

Abstract: To prevent blood from clotting or being diluted (which causes inaccuracy in the measurement of the characteristics of blood drawn from a patient), a needle assembly has the interior portion of its cannula and at least one portion of its hub covered by a dry coat of anticoagulant. To provide the dry coat of anticoagulant onto the interior surfaces of the cannula and the hub, a liquid anticoagulant is atomized thereto so that an even coat of the anticoagulant is provided to the interior surfaces of the cannula and hub. The volume and concentration of the anticoagulant atomized to the inside of the needle assembly are controlled as the liquid anticoagulant is ultra-sonically atomized to the interior portion of the needle assembly.

Abstract: A method for rigidifying a fiber-based paper substrate for use in the exhaust system of a combustion device. In the method, a green ceramic fiber-based paper substrate is impregnated with an impregnating material. The impregnated substrate is fired to form a rigidified substrate that is suitable for use in the exhaust system of a combustion device. This rigidification process is performed at least once and, preferably, two or more times.

Abstract: There is provided a process for producing an integrated circuit, wherein not only can conductive fine particles be deposited efficiently and densely in minute wiring channels and connecting holes but also a circuit of low wiring resistance and high density can be formed and wherein a high-degree integration can be achieved to thereby bring about an economic advantage. In particular, there is provided a process for producing an integrated circuit, comprising coating a substrate provided with wiring channels with a coating liquid for integrated circuit formation containing conductive fine particles to thereby form an integrated circuit on the substrate, wherein the coating liquid for integrated circuit formation while being exposed to ultrasonic waves is applied to the wiring channels.

Abstract: Applying materials, e.g. electrolytes and other materials, in the form of a spray during battery manufacture, particularly using a vibratory nebulizer to produce a small droplet, low velocity spray.

Abstract: A method and apparatus apply a lacquer layer to the upper side of a printed medium (i.e. a printed sheet). The method and apparatus form a film of lacquer, in particular a UV lacquer film. Next, the lacquer film is dried or hardened under the action of heat and/or UV radiation. Next, the dried/hardened lacquer film is transferred to the (fresh or still wet) printed upper side of the printed medium, with simultaneous permanent adhesion of the film to this upper side.

Abstract: This invention relates to methods whereby nanoparticle liquid suspensions are used in conventional thermal spray deposition for the fabrication of high-quality nanostructured coatings. Ultrasound is used for disintegration of the as-synthesized particle agglomerates, nanoparticle dispersion in liquid media, and liquid precursor atomization.

Abstract: A fluid treatment device and method for treating moving substrates with fluid as the substrates move through the device at a relatively high rate of travel. Fluid injection in combination with the application of vibration energy (e.g., ultrasonic) results in enhanced fluid treatment of the substrates. In one embodiment, a bifurcated horn is utilized in combination with fluid injector members having pluralities of rows of spaced injector ports, the injectors being strategically positioned relative to the vibrational source. In one example, the device and method may be used for enhanced penetration by dye materials of ceramic substrate surfaces to detect adverse surface conditions (e.g., cracks) and thus potentially defective product.

Abstract: The present invention provides an improved method and apparatus for curing coatings on optical fibers, without creating additional heat and compromising the manufacturing speed of optical fibers. The present invention uses at least one ultrasonic transducer coupled to a component of the optical fiber draw tower, such as the coating die, curing stage device or sheath, to emit ultrasound to the coating of the fiber. The use of ultrasound with current coating cure techniques, such as UV radiation curing, aids in accelerating the coating cure process through the effects of sonolysis, allowing an increase in current manufacturing speeds of optical fibers.

Abstract: A method for making an electrically conductive pattern, including:

Abstract: The method is intended for applying metallic or metal-ceramic coatings to a product surface, particularly during the manufacture and repair of pressurised articles and products which require increased corrosion resistance, heat resistance and other qualities. The method comprises preliminary heating of compressed air to a temperature of from 400 to 700° C., forming a high-velocity air flow in a supersonic nozzle, accelerating by this flow and applying to a product surface a powder material which is a mechanical mixture of ceramic and metal powders, the metal powder being a powder mixture of at least two metals, one of which is zinc powder in an amount of from 20 to 60% of the metal powder total weight. The presence of zinc in the powder material and heating of compressed air up to said temperature assure high-efficient production of coatings having low gas-permeability and high coating-to-substrate bond strength.

Abstract: Wood cellulose is treated with a reactive silicate. The reaction is done to cellulose within the wood and may be catalyzed with acid or base catalysts or a carbon silicon halogen combination which produces in situ acid catalysts or a different combination to produce an in situ base catalyst which replaces some of the molecules or atoms within the cellulose structure with silicon, boron or other hydrophobic or anti-degrading agents. Preferably an organic solvent, such as alcohol is used to accelerate the reaction with the water in the wood. Here, the hydroxyl (OH) group on some or all of the cellulose molecules is partially replaced with silicon or an alternative atom or molecule to changes the character of the wood. The process may be modified to insert a preliminary step of adding a reactive agent to be locked into the wood. Manufacturing techniques to enhance the process using ultrasound or other wave generating techniques are also taught.

Abstract: In general, the present invention is directed to acoustically enhanced deposition processes, and a system for performing same. In one embodiment, the method comprises providing a substrate having a layer of insulating material formed thereabove, the layer of insulating material having a plurality of openings formed therein, performing a deposition process to form a layer of metal at least in the openings in the layer of insulating material, and actuating at least one acoustic generator to generate sound waves during the deposition process. In one illustrative embodiment, the system comprises a deposition tool for receiving a substrate having a layer of insulating material formed thereabove, the layer of insulating material having a plurality of openings formed therein, and performing a deposition process to form a layer of metal at least in the openings in the layer of insulating material, and at least one acoustic generator coupled to the deposition tool to generate sound waves during the deposition process.

Abstract: A coating apparatus for forming a film on a surface of a substrate to be coated, comprises a holding table for holding the substrate to be coated, a discharge head, containing a coating solution and formed with a plurality of discharge holes at a portion thereof opposing the substrate to be coated, for discharging the coating solution, a fine-vibration plate for applying fine vibrations to discharge the coating solution and driving motor for driving the holding table and the discharge head relative to each other.

Abstract: A deposition process for coating a substrate with an ultrasonically generated aerosol spray is described. The resultant droplets are much smaller in size than those produced by conventional processes, thereby providing the present coating having an increased surface area. When the coated substrate is an electrode in a capacitor, a greater surface area results in an increased electrode capacitance. A preferred coating is of a ruthenium-containing oxide.

Abstract: Materials bonded together are separated using electrical current, thermal stresses, mechanical force, any combination of the above methods, or any other application or removal of energy until the bonds disappear and the materials are separated. In one embodiment the original bonding was composed of two layers of material. In another embodiment, the sandwich was composed of three layers. In a further embodiment, the parts of the sandwich are firmly maintained in their respective positions during the application of current so as to be able to subsequently align the materials relative to one another.

Abstract: The present invention is a method of coating a substrate. First, a layer of liquid polymeric coating having a pigment and a solvent is applied to the substrate. An ultrasonic acoustic source is then provided and operated at a frequency of from about above 40 kHz to provide an acoustic pressure field and an acoustic pressure of above 190 dB and directing the main lobe of the acoustic pressure field toward the layer of liquid polymeric coating. This acoustic pressure field reduces the gradient in and smoothes any uneven surface features in the liquid polymeric coating.

Abstract: Methods and devices are disclosed that use focused acoustic energy to generate solid particles containing at least one compound of interest. Focused acoustic radiation serves to eject droplets containing a compound of interest dissolved in a solvent. The droplets are subjected to a condition that allows for the compound of interest to precipitate out of solution, thereby generating solid particles. The particles are typically of controlled size, composition, and/or structure. Often, particles of substantially identical size are generated.

Abstract: The present invention is a method of coating a substrate. First, a layer of liquid polymeric coating having a pigment and a solvent is applied to the substrate. An ultrasonic acoustic source is then provided and operated at a frequency of from about above 40 kHz to provide an acoustic pressure field and an it acoustic pressure of above 190 dB and directing the main lobe of the acoustic pressure field toward the layer of liquid polymeric coating. This acoustic pressure field reduces the gradient in and smoothes any uneven surface features in the liquid polymeric coating.

Abstract: A novel hydrothermal gel process for preparing silicalite particles suitable for use in composite membranes for pervaporation processes is disclosed. A novel process for preparing a silicon-silicalite composite membrane is also disclosed. The novel hydrothermal gel process produces silicalite particles having a diameter from about 0.1 micrometers to about 0.2 micrometers in high yield.

Abstract: The invention relates to a method for coating fibers shaped as fiber strands (roving and mats) using a fluidized bed techniques, wherein (i) the desired composition of the individual coating constituents is directly applied from the fluidized bed without previous compounding and (ii) the individual coating constituents contained in the fluidized bed are additionally mixed in the mass so that dissociation of individual constituents is substantially avoided. The invention also relates to a device for implementing the method.

Abstract: Filter for removal of leucocytes is provided, wherein the filter is coated with a natural polymer of chitosan which has a good blood compatibility and no side effect in human body on an ultrafine non-woven fabric. This blood filter provides a high removal rate of leucocytes as well as good recovery of platelets and red blood cells due to secondary filtration through electrostatic power between a leucocyte and a cationic residue provided by chitosan on the surface of the non-woven fabric.

Abstract: A method of providing a hermetically sealed enclosure for a highly moisture sensitive electronic device including depositing an electrical conductor on the substrate which provides an electrical connection with the electronic device and depositing an electrically insulating thin layer over the electrical conductor; providing a low melting point indium metal or alloy in the form of a wire having diameter ranging from 1 mil to 10 mils on the electrically insulating thin layer on the substrate so that the wire is situated around the periphery of the electronic device; placing an ultrasonic horn over the cover plate so that ultrasonic energy can be delivered through the cover plate to the wire and applying a pressure between 20 and 100 psi; and providing an acoustic wave to melt the wire.

Abstract: A process for coating a moving length of sheet metal is disclosed that includes the steps of 1) cleaning the moving length of sheet metal to remove surface contaminants that may interfere with the coating adhering to the sheet metal; 2) applying an electron beam curable coating to the moving length of sheet metal; and, 3) exposing the coating on the moving length of sheet metal to an electron beam to cure the coating, the cleaning, coating and curing resulting in no emission of pollutants that need to be removed before the emission is released into the atmosphere.

Abstract: In aluminum-based metal pigments produced by physical vapor deposition of a metal film and subsequent crushing of the metal film metal surfaces which are exposed after the operation of crushing the metal film and in particular fracture surfaces thereof are covered with a passivting protective layer to afford corrosion stability of those metal pigments.

Abstract: A method of forming an oriented film. A target is provided and material from the target is ablated onto a substrate to form a film. The film is heated in a synthesis gel of the target material to orient the film.

Abstract: The invention provides a method for generating droplets. Extremely fine droplets may be generated (on the order of 1 picoliter or less) using focused acoustic energy to eject the droplets from a reservoir containing two or more immiscible fluids. The droplets may include immiscible fluids or a single fluid. Typically, the droplets are ejected onto discrete sites on a substrate surface so as to form an array thereon. In some instances, the reservoirs contain layers of immiscible fluids, wherein an upper layer exhibits a nonuniform thickness. In such a case, fluid from a lower fluid layer may be propelled through an aperture region of the upper layer.

Abstract: A deposition process for coating a substrate with an ultrasonically generated aerosol spray of a pseudocapacitive material, or a precursor thereof, contacted to a substrate heated to a temperature to instantaneously solidify the pseudocapacitive material or convert the precursor to a solidified pseudocapacitive metal compound, is described. The ultrasonic aerosol droplets are much smaller in size than those produced by conventional processes and the heated substrate minimizes the possibility of contamination, thereby providing the present coating having an increased surface area. When the coated substrate is an electrode in a capacitor, a greater surface area results in an increased electrode capacitance.

Abstract: A method for fabricating a plated product with a basecoat layer, a metal plating layer, and a topcoat layer that are formed on a surface of a base is provided. The method includes the step of forming the basecoat layer and the metal plating layer on the surface of the base. The step is followed by subjecting the metal plating layer to a cold heat treatment or an ultrasonic wave treatment, thus forming a microcrack in the metal plating layer. Afterwards, the topcoat layer is formed on the surface of the metal plating layer.

Abstract: A novel hydrothermal gel process for preparing silicalite particles suitable for use in composite membranes for pervaporation processes is disclosed. A novel process for preparing a silicon-silicalite composite membrane is also disclosed. The novel hydrothermal gel process produces silicalite particles having a diameter from about 0.1 micrometers to about 0.2 micrometers in high yield.

Abstract: An electrode substrate is brush cleaned with a hydrogen gas dissolved water, which has an oxidation-reduction potential of −860 mV to −400 mV and a pH of 8 to 12, before applying an alignment layer material on the electrode substrate. Thus, it is possible to decrease the manufacturing costs without decreasing the detergency.

Abstract: A method of coating a substrate with an oriented film. A target is ablated to create a plume. The substrate is manipulated, which may be by vibration, in the plume to coat the substrate with a film. The film is heated in a synthesis gel of the target to form the oriented film.

Abstract: A metal shaft is covered with plastic. A metal sleeve is moved relative to the plastic covered shaft. The sleeve and the plastic covered shaft are ultrasoncially vibrated to calibrate the plastic on the shaft.

Abstract: The present invention relates to a method for carrying out a magnesium oxide based deposition on the dielectric surface of a glass plate of a display panel. The method includes the creation of a mist from a metalorganic compound of magnesium dissolved in a solvent, the conveying of the mist to the dielectric surface of the plate, the evaporation the solvent when approaching the dielectric surface of the plate which is taken to a temperature of about 380° to 430°, and the pyrolysis of the metalorganic compound leading to the magnesium oxide based deposit on the surface of the plate and the evaporation of the organic radical of the compound, this deposit being practically waterproof. The method is especially useful in the manufacture of plasma panels.

Abstract: The present invention includes a step of forming an Ni bump by non-electrolytic plating in an opening of a protecting film having an insulating property formed on an electrode pad which is provided on a semiconductor substrate, and a step of removing a plating solution residue remaining in a gap between the Ni bump and the protecting film. The plating solution residue is removed by cleaning in a cleaning solution containing hydrogen peroxide, or by applying an ultrasonic wave in a cleaning solution such as pure water.