With Shaping Of Particulate Material And Subsequent Fusing Of Particles Patents (Class 65/17.3)
  • Patent number: 7788948
    Abstract: To provide a process for producing a reliable substrate in good yield, by suppressing bleeding of boric acid from a green sheet comprising a powder of borosilicate glass to improve printability of a conductive pattern thereby to prevent disconnection. A process for producing a substrate which comprises firing a green sheet comprising a powder of borosilicate glass, wherein the powder is one prepared by holding borosilicate glass before pulverization, at a temperature higher by at least 30° C. than the glass transition temperature and lower by at most 50° C. than the softening point of the borosilicate glass for at least 3 hours in the atmosphere, followed by pulverization.
    Type: Grant
    Filed: December 1, 2006
    Date of Patent: September 7, 2010
    Assignees: Asahi Glass Company, Limited, Asahi Techno Glass Corporation
    Inventors: Jiro Chiba, Atsuo Hiroi, Ryosuke Sugiura, Ryoji Akiyama, Masaya Matsunaga
  • Publication number: 20100192632
    Abstract: A method of manufacturing a resorbable, macroporous bioactive glass scaffold comprising approximately 24-45% CaO, 34-50% SiO2, 0-25% Na2O, 5-17% P2O5, 0-5% MgO and 0-1% CaF2 by mass percent, produced by mixing with pore forming agents and specified heat treatments.
    Type: Application
    Filed: April 6, 2010
    Publication date: August 5, 2010
    Inventors: Jiang Chang, Weiming Gu, Jipin Zhong
  • Patent number: 7754628
    Abstract: The invention relates to a mixture for the production of a vat-dyed amber glass; an amber glass formed from the vitrifiable mixture, based on a silico-sodo-calcic composition; and a method for the production of tubes and blanks (2) for bulbs (1) using said glass. The mixture contains 100% by weight of the following ingredients: 0.01%-1% by weight molybdenum bisulphur and 0.01%-7% strontium sulphur by weight. The glass thus obtained is devoid of harmful products such as cadmium and no additional heat treatment is required in order to obtain the desired colour thereof.
    Type: Grant
    Filed: December 24, 2004
    Date of Patent: July 13, 2010
    Assignee: Vermont
    Inventors: Christian Lefevre, François Lepesqueux
  • Publication number: 20100139549
    Abstract: The present invention is a quartz glass crucible 5 for pulling a silicon single crystal, comprising at least an outer layer portion 23 being a translucent glass layer containing multiple bubbles in it and an inner layer portion 24 being a transparent quartz glass layer having no bubbles and a smooth surface, formed on the inner surface of the outer layer portion 23, wherein the outer layer portion 23 contains bubbles of 0.1 to 0.3 mm in diameter at the density of 1.5 to 5.0×104 bubbles/cm3. Thus, there are provided a quartz glass crucible for pulling a silicon single crystal, the quartz glass crucible being increased in mechanical strength, making it possible to suppress deformation of a quartz glass crucible for pulling a silicon single crystal during a single crystal pulling process, thereby prevent degradation in yield rate due to dislocation in a single crystal and make the manufacture of a silicon single crystal highly efficient and a method of manufacturing the same quartz glass crucible.
    Type: Application
    Filed: May 25, 2006
    Publication date: June 10, 2010
    Applicants: SHIN-ETSU HANDOTAI CO., LTD., SHIN-ETSU QUARTZ PRODUCTS CO., LTD.
    Inventors: Masahiro Sakurada, Susumu Sonokawa, Izumi Fusegawa, Hiroshi Matsui
  • Patent number: 7726153
    Abstract: An object of the present invention is to provide a method for manufacturing a glass particle deposited body in which a taper portion formed at an end portion of the glass particle deposited body is reduced without increasing the number of burners.
    Type: Grant
    Filed: April 18, 2003
    Date of Patent: June 1, 2010
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Toshihiro Ooishi, Motonori Nakamura, Tomohiro Ishihara, Tatsuro Sakai
  • Publication number: 20100126217
    Abstract: A known method for producing a cylinder of quartz glass comprises a method step in which a porous SiO2 body comprising a central inner bore, a lower end and an upper end is sintered in a sintering furnace zone by zone, starting from the upper end, to obtain the quartz glass cylinder, a holding device being used by means of which the SiO2 body is held standing in vertical orientation during a first sintering phase and suspended in a second sintering phase.
    Type: Application
    Filed: June 5, 2008
    Publication date: May 27, 2010
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Frank Hoff, Michael Muschler, Udo Peper, Sven Schmidt, Steffen Zwarg, Hans-Georg Fritsche
  • Patent number: 7716948
    Abstract: A fused glass crucible includes a collar of doped aluminum silica that defines uppermost and outermost surfaces of the crucible. The melt line that defines the surface of molten silicon in the crucible may be substantially at the lower end of the collar or slightly above it. Crystallization of the collar makes it hard and therefore supports the remaining uncrystallized portion of the crucible above the melt line. The melt line may also be below the lower end of the collar, especially if the melt is drawn down or poured early in the process. Because there is little or no overlap or because the overlap does not last long, the doped aluminum collar is not damaged by the heat of from the melt.
    Type: Grant
    Filed: December 18, 2006
    Date of Patent: May 18, 2010
    Assignees: Heraeus Shin-Etsu America, Inc., Shin-Etsu Quartz Products Co., Ltd.
    Inventors: Katsuhiko Kemmochi, Yasuo Ohama
  • Publication number: 20100107691
    Abstract: The disclosed is a method of manufacturing a silica glass crucible for pulling silicon single crystals. In the method, reduced pressure is imparted from the inner surface to the outer surface of a crucible-shaped molded product and the crucible-shaped molded product is arc-fused while rotating the same to form a silica glass crucible with a transparent layer on the inner surface side and a bubble layer on the outer surface side. The inner surface of the wall portion of the silica glass crucible is fused a second time by arc fusion to cause bubbles present in the transparent layer of the inner surface of the wall portion to be displaced toward the bottom portion of the inner surface of the wall portion. The inner surface of the bottom portion of the silica glass crucible is fuse a second time by arc fusion to cause bubbles present in the transparent layer of the inner surface of the bottom portion to be displaced toward the periphery of the inner surface of the bottom portion.
    Type: Application
    Filed: January 9, 2009
    Publication date: May 6, 2010
    Applicant: JAPAN SUPER QUARTZ CORPORATION
    Inventors: Tadahiro SATO, Masaki MORIKAWA
  • Patent number: 7709081
    Abstract: The invention relates to porous bioglass and to the preparation method thereof. More specifically, the invention relates to a solid, porous crystalline or partially-crystalline composition containing at least SiO2, Ca<SB>O</SB>, Na2O, and P2O5, comprising micropores and macropores. The invention is characterised in that: the pore ratio varies between 50% and 80%, preferably between 60 and 75%, and is measured using the geometric method; the average diameter of the macropores varies between 100 and 1250 micrometers, preferably between 150 and 300 micrometers; the average diameter of the micropores is less than or equal to 5 micrometers; and the compression strength varies between 7 MPa and 70 MPa. The invention also relates to the method of preparing one such composition and to such a composition treated with a physiological liquid having an ionic composition similar to that of human plasma. The invention also relates to an implant which is made from one such composition.
    Type: Grant
    Filed: July 25, 2005
    Date of Patent: May 4, 2010
    Assignee: Institut National des Sciences Appliques (INSA)
    Inventors: Rachid Zenati, Gilbert Fantozzi, Jerome Chevalier, Mourad Arioua
  • Patent number: 7686887
    Abstract: An object of the invention is to provide a quartz glass crucible reduced in the generation of vibration occurring on the surface of a silicon melt and free from the generation of rough surface and cristobalite spots, yet capable of pulling up single crystal silicon stably and at high yield even in long-term operations; it is also an object to provide a method for producing the same. In a quartz glass crucible for pulling up single crystal silicon comprising a crucible base body having a bottom part and a straight shell part with an inner layer provided to the inner surface thereof, the quartz glass crucible is characterized by that said inner layer comprises a synthetic quartz glass layer from the lowest end to at least a height of 0.25 H; a naturally occurring quartz glass layer or a mixed layer of naturally occurring quartz glass and synthetic quartz glass extended in a range of from at least 0.5 H to 0.
    Type: Grant
    Filed: July 30, 2003
    Date of Patent: March 30, 2010
    Assignees: Heraeus Quarzglas GmbH & Co. KG, Shin-Etsu Quartz Products Co., Ltd.
    Inventors: Yasuo Ohama, Takayuki Togawa
  • Publication number: 20100071414
    Abstract: Provided is a manufacturing method for a thermal head, which includes: a concave portion forming step of forming a plurality of concave portions on a surface of a collective substrate; a bonding step of thermally fusion bonding an insulating film to the surface of the collective substrate including the plurality of concave portions formed thereon in the concave portion forming step; and a heating resistor forming step of forming a plurality of heating resistors on the insulating film so as to be opposed to the plurality of concave portions, in which the concave portion forming step includes setting any one of the plurality of concave portions as a reference, and setting sizes of the plurality of concave portions other than the any one of the plurality of concave portions so as to become larger as a distance from the any one thereof increases.
    Type: Application
    Filed: July 24, 2009
    Publication date: March 25, 2010
    Inventors: Toshimitsu Morooka, Keitaro Koroishi, Yoshinori Sato, Noriyoshi Shoji, Norimitsu Sanbongi
  • Publication number: 20100071613
    Abstract: A method of manufacturing a fused silica crucible by heating and melting a vitreous silica powder compact shaped into a mold using arc discharge of electrodes arranged around a rotation shaft of the mold, includes the steps of: arranging the electrodes in a ring shape, and setting a ratio W/R of a horizontal distance W between the electrode front end and the surface of the vitreous silica powder compact to a vitreous silica powder compact opening radius R, for at least a predetermined time during arc heating, to be in the range of 0.002 to 0.98.
    Type: Application
    Filed: September 22, 2009
    Publication date: March 25, 2010
    Applicant: JAPAN SUPER QUARTZ CORPORATION
    Inventors: Hiroshi KISHI, Masanori FUKUI, Masaki MORIKAWA
  • Publication number: 20100068521
    Abstract: A process for increasing toughness of glass particulates is provided. The process includes providing an aluminosilicate glass particulate, the glass particulate generally having the form of a sphere, and heating the glass particulate to a temperature greater than 600° C. for a predetermined time. Thereafter, the glass particulate can be cooled to ambient temperature and the heating step can alter the failure mechanism of the glass particulate from a high energy failure that produces generally fine powder to a lower energy failure that produces generally large fragments. The glass particulate can be an amorphous glass particulate and may or may not have a nominal composition that corresponds to rhyolite, basalt, tholeiite, olivine and/or andesite.
    Type: Application
    Filed: August 3, 2009
    Publication date: March 18, 2010
    Applicant: The Penn State Research Foundation
    Inventors: Ryan P. Koseski, John R. Hellmann, Barry E. Scheetz
  • Patent number: 7677058
    Abstract: An apparatus and process for making glass soot sheet and sintered glass sheet. Glass soot particles are deposited on a curved deposition surface of a rotating drum to form a soot sheet. The soot sheet is then released from the deposition surface. The soot sheet can be sintered into a consolidated glass. The soot sheet and the sintered glass can be sufficiently long and flexible to be reeled into a roll.
    Type: Grant
    Filed: May 7, 2007
    Date of Patent: March 16, 2010
    Assignee: Corning Incorporated
    Inventors: Daniel Warren Hawtof, Michael Donovan Brady
  • Patent number: 7661277
    Abstract: As a jig material to use under plasma reaction for producing semiconductors, the present invention provides a quartz glass having resistance against plasma corrosion, particularly corrosion resistance against fluorine-based plasma gases, and which is usable without causing anomalies to silicon wafers; the present invention furthermore provides a quartz glass jig, and a method for producing the same. A quartz glass containing 0.1 to 20 wt % in total of two or more types of metallic elements, said metallic elements comprising at least one type of metallic element selected from Group 3B of the periodic table as a first metallic element and at least one type of metallic element selected from the group consisting of Mg, Ca, Sr, Ba, Sc, Y, Ti, Zr, Hf, lanthanoids, and actinoids as a second metallic element, provided that the maximum concentration of each of the second metallic elements is 1.0 wt % or less.
    Type: Grant
    Filed: December 21, 2007
    Date of Patent: February 16, 2010
    Assignee: Shin-Etsu Quartz Products Co., Ltd.
    Inventors: Tatsuhiro Sato, Nobumasa Yoshida, Mamoru Endo
  • Publication number: 20100006313
    Abstract: The present invention reduces the amount of lead used in a display device and improves its long-term moisture resistance. This display device includes: a panel (1b) provided with a hole (11) formed therein; a phosphate glass member (13); and a tube (12) mounted on the panel (1b) via the glass member (13) so as to cover the hole (11). The glass member (13) is bonded to at least a partial area of the inner wall surface of the tube (12) and to a partial area of the panel (1b), so that the entire periphery of the end face of the tube (12) located on the side of the hole (13) is in contact with the panel (1b).
    Type: Application
    Filed: November 10, 2006
    Publication date: January 14, 2010
    Applicant: MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD.
    Inventors: Yoshiaki Kai, Shinya Hasegawa
  • Publication number: 20090320521
    Abstract: A method of producing a quartz glass crucible for pulling a single crystal comprising: providing a melting mold comprising a wall having passages between outside and inside; providing an outer layer granulation consisting of first coarser SiO2 particles and forming an outer granulation layer from the outer layer granulation on the inside of the melting mold wall; providing a barrier layer granulation consisting of second finer SiO2 particles and forming a barrier granulation layer from the barrier layer granulation on the outer granulation layer; applying a negative pressure to the outside of the melting mold wall; and heating the barrier granulation layer and the outer granulation layer with formation of a quartz glass crucible with transparent inner layer.
    Type: Application
    Filed: June 29, 2009
    Publication date: December 31, 2009
    Applicant: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Walter Lehmann, Achim Hofmann, Thomas Kayser
  • Patent number: 7596968
    Abstract: Glass, glass compositions, methods of preparing the glass compositions, microfluidic devices that include the glass composition, and methods of fabricating microfluidic devices that include the glass composition are disclosed. The borosilicate glass composition includes silicon dioxide (SiO2) in a range from about 60% to 74% by total composition weight; boric oxide (B2O3) in a range from about 9% to 25% by total composition weight; aluminum oxide (Al2O3) in a range from about 7% to 17% by total composition weight; and at least one alkali oxide in a range from about 2% to 7% by total composition weight. In addition, the borosilicate glass has a coefficient of thermal expansion (CTE) that is in a range between about 30×10?7/° C. and 55×10?7/° C. Furthermore, the borosilicate glass composition resists devitrification upon sintering without the addition of an inhibitor oxide.
    Type: Grant
    Filed: January 18, 2008
    Date of Patent: October 6, 2009
    Assignee: Corning Incorporated
    Inventor: Paulo Marques
  • Patent number: 7587912
    Abstract: The present invention refers to a method for producing a quartz glass crucible for use in pulling silicon single crystal, said crucible having at least a double-layer structure comprising a pore-free transparent inner layer and an opaque base body or outer layer having pores, characterized in that at least the base body is formed with a silica powder maintained in a gas having a mixing ratio of 0.0005 to 0.0065 kg/kg (dry gas), and a quartz glass crucible produced by said production method. The obtained crucible has an average OH group concentration of 50 ppm or lower and is capable of suppressing the vibration occurring on the surface of silicon melt during pulling the silicon single crystal. Further the obtained crucible suffers less deformation of the crucible on pulling the silicon single crystal.
    Type: Grant
    Filed: February 20, 2004
    Date of Patent: September 15, 2009
    Assignees: Heraeus Quarzglas GmbH & Co. KG, Shin-Etsu Quartz Products Co., Ltd.
    Inventors: Yasuo Ohama, Hiroshi Matsui
  • Patent number: 7506521
    Abstract: Disclosed are high purity synthetic silica material having an internal transmission at 193 nm of at least 99.65%/cm and method of preparing such material. The material is also featured by a high compositional homogeneity in a plane transverse to the intended optical axis. The soot-to-glass process for making the material includes a step of consolidating the soot preform in the presence of H2O and/or O2.
    Type: Grant
    Filed: June 8, 2005
    Date of Patent: March 24, 2009
    Assignee: Corning Incorporated
    Inventors: Dana Craig Bookbinder, Richard Michael Fiacco, Kenneth Edward Hrdina, Lisa Anne Moore, Susan Lee Schiefelbein
  • Patent number: 7506522
    Abstract: Disclosed are high purity synthetic silica glass material having a high OH concentration homogeneity in a plane perpendicular to the optical axis, and process of making the same. The glass has high refractive index homogeneity. The glass can have high internal transmission of at least 99.65%/cm at 193 nm. The process does not require a post-sintering homogenization step. The controlling factors for high compositional homogeneity, thus high refractive index homogeneity, include high initial local soot density uniformity in the soot preform and slow sintering, notably isothermal treatment during consolidation.
    Type: Grant
    Filed: June 8, 2005
    Date of Patent: March 24, 2009
    Assignee: Corning Incorporated
    Inventors: Daniel Joseph Bleaking, Dana C. Bookbinder, Richard M. Fiacco, Kenneth E. Hrdina, Pushkar Tandon, John E. Maxon, Kimberly Ann Wilbert
  • Patent number: 7507618
    Abstract: A method of making a thin film transistor comprises (a) solution depositing a dispersion comprising semiconducting metal oxide nanoparticles onto a substrate, (b) sintering the nanoparticles to form a semiconductor layer, and (c) optionally subjecting the resulting semiconductor layer to post-deposition processing.
    Type: Grant
    Filed: June 27, 2005
    Date of Patent: March 24, 2009
    Assignee: 3M Innovative Properties Company
    Inventor: Timothy D. Dunbar
  • Publication number: 20090075803
    Abstract: A method of making an article from an aluminum oxide glass is disclosed. The aluminum oxide glass includes zirconium oxide and either calcium oxide or strontium oxide. The aluminum oxide glass has a glass transition temperature and a crystallization temperature, and these temperatures differ by at least 25K. The method includes: providing a glass in a form comprising particles, beads, microspheres, or fibers; heating the glass above the Tg such that the particles, beads, microspheres, or fibers coalesce to form a coalesced shape; and cooling the coalesced shape to form the article.
    Type: Application
    Filed: November 26, 2008
    Publication date: March 19, 2009
    Inventor: Anatoly Z. Rosenflanz
  • Publication number: 20090041960
    Abstract: A rotating mold has a plurality of air channels that communicate with a cavity formed in the mold. Silica grain is deposited in the rotating mold and then formed into the shape of a crucible having a lower portion that comprises a substantially uniformly thick wall. An upper portion of the grain is formed into a substantially narrowed wall portion about the perimeter of the formed shape. The silica grain is heated, and a pump draws gas through the air channels while the silica fuses. There is a pressure drop across the narrowed wall portion. After fusing, the upper portion of the crucible, including the narrowed wall portion, is cut off.
    Type: Application
    Filed: August 8, 2007
    Publication date: February 12, 2009
    Applicants: HERAEUS SHIN-ETSU AMERICA, INC., SHIN-ETSU QUARTZ PRODUCTS CO., LTD.
    Inventors: Katsuhiko Kemmochi, Yasuo Ohama
  • Publication number: 20090035511
    Abstract: Low cost aluminosilicate fibers are used to form a ceramic substrate material using inorganic binders that promote the formation of stable compounds that inhibit the formation of crystal silica, or cristobalite, when the substrate is used or exposed to high operating temperatures. The aluminosilicate fibers are mixed with additives including organic and inorganic binders and a fluid to form a plastic mixture. The plastic mixture is formed into a green substrate, and subsequently cured into the ceramic substrate. The fiber-based constituents permit the formation of rigid porous structures for filtration, insulation, and high temperature processes and chemical reactions.
    Type: Application
    Filed: July 31, 2007
    Publication date: February 5, 2009
    Applicant: GEO2 TECHNOLOGIES, INC.
    Inventors: James Jenq Liu, Bilal Zuberi
  • Publication number: 20090025424
    Abstract: Method of making an article, the method comprising coalescing a plurality of the glass particles. The article may comprise glass, glass-ceramic, and/or crystalline ceramic. Examples of articles include kitchenware (e.g., plates), dental brackets, and reinforcing fibers, cutting tool inserts, abrasives, and structural components of gas engines, (e.g., valves and bearings).
    Type: Application
    Filed: August 2, 2002
    Publication date: January 29, 2009
    Inventor: Anatoly Z. Rosenflanz
  • Publication number: 20080289568
    Abstract: A crucible has a structure where a layer containing a crystallization accelerating component such as aluminum or the like (a crystallization accelerating layer) is inserted inside a quartz glass layer of a crucible straight body part excepting a crucible bottom part. The crucible does not deform and fall inwardly at the straight body part since a part containing a crystallization accelerating component advances to crystallize so as to increase strength at a high temperature when the crucible is used in pulling up silicon single crystal. Therefore, a single crystallization rate can be increased. Further, since the crystallization accelerating layer is inserted inside the quartz glass layer, the crystallization accelerating component, such as aluminum or barium, does not contact with silicon melt or a carbon susceptor, contamination by eluting these metals does not occurs.
    Type: Application
    Filed: May 29, 2008
    Publication date: November 27, 2008
    Applicant: JAPAN SUPER QUARTZ CORPORATION
    Inventors: Minoru Kanda, Masaru Sato
  • Publication number: 20080268201
    Abstract: A fused silica glass having a composition for use in bulk IR optical applications. The fused silica glass has a OH concentration of less than 5 ppm (parts per million) by weight and an absorbance of less than about 50 ppm/cm at a wavelength of about 1.3 ?m. A method of making the fused silica glass is also described.
    Type: Application
    Filed: April 10, 2008
    Publication date: October 30, 2008
    Inventors: Richard Michael Fiacco, Kenneth Edward Hrdina, Daniel Raymond Sempolinski
  • Patent number: 7427387
    Abstract: Subjects for the invention are to obtain a quartz powder having a high purity and high quality and a process for producing the same and to obtain a glass molding formed by melting and molding the powder and extremely reduced in bubble inclusion. The invention provides a quartz powder, preferably a synthetic quartz powder obtained by the sol-gel method, which, upon heating from room temperature to 1,700° C., generates gases in which the amount of CO is 300 nl/g or smaller and the amount of CO2 is 30 nl/g or smaller.
    Type: Grant
    Filed: April 18, 2006
    Date of Patent: September 23, 2008
    Assignee: Mitsubishi Chemical Corporation
    Inventors: Yoshio Katsuro, Keiji Yamahara, Takashi Yamaguchi, Yutaka Mori
  • Patent number: 7416690
    Abstract: The invention provides a method to transform large quantities of fiber glass waste into useful ceramic products by a low-cost manufacturing process. The method consists of reducing the fiber glass waste into a glass powder; mixing the glass powder with additives into a glass-additives mixture; granulating the glass-additives mixture into granulated particles; forming the granulated particles into a green ceramic article; and heating the green ceramic article into the ceramic product. Water and clay can be included in the processing. Only one firing step is needed with a low peak firing temperature of about 700° C. to about 1000° C. The method conserves energy and natural resources compared to clay-based traditional ceramic manufacturing. High-quality impervious ceramic products can be produced by the invention.
    Type: Grant
    Filed: December 1, 2003
    Date of Patent: August 26, 2008
    Inventor: Michael J. Haun
  • Publication number: 20080196449
    Abstract: A zircon composition having a multi-modal particle size distribution is disclosed. The multi-modal zircon composition comprises greater than about 40 parts by weight of a coarse zircon component having a median particle size of from greater than about 3 ?m to about 25 ?m, and less than about 60 parts by weight of a fine zircon component having a median particle size of 3 ?m or less. Methods for manufacturing a green body and a fired refractory ceramic body comprising the multi-modal zircon composition are also disclosed.
    Type: Application
    Filed: February 20, 2007
    Publication date: August 21, 2008
    Inventors: William Peter Addiego, Christopher Raymond Glose
  • Publication number: 20080180018
    Abstract: The present invention has an object to provide a fluorescent substance containing glass sheet which is suppressed attenuation of intensity of wavelength converted light emitted by a sulfide fluorescent substance, able to increase a life of the light emitting device, and does not bring about environmental pollution by lead, its manufacturing method and a light-emitting device using this. A fluorescent substance containing glass sheet formed by mixing an oxide-coated fluorescent substance particle with glass powder that does not substantially include lead, and sintering them, the oxide-coated fluorescent substance particle having been produced by coating a surface of a sulfide fluorescent substance particle, which is excited by light emission from a light-emitting element and which emits wavelength converted light, with an oxide, wherein attenuation of intensity of said wavelength converted light emitted by said sulfide fluorescent substance particle is suppressed by a forming process.
    Type: Application
    Filed: October 16, 2007
    Publication date: July 31, 2008
    Applicant: NEC LIGHTING, LTD.
    Inventors: Maki MINAMOTO, Ryo Yoshimatsu
  • Patent number: 7350378
    Abstract: In a device (5) for the manufacture of a quartz glass crucible (2), one section (14, 15) of a wall (13) of the rotating quartz glass crucible (2) is heated at one time by means of at least two electrode arrangements (7, 8) distributed uniformly at the circumference of the quartz glass crucible (2) and generating a first and another electric arc. By providing several electrode arrangements (7, 8), the cooling-down phase of the sections (14, 15) until their reaching the subsequent heating zone (11, 12) can be shortened, and thus an undesirable high temperature difference of the wall (13) can be avoided. Moreover, the required thermal output of each individual electrode arrangement (7, 8) can be reduced, so that evaporation phenomena and connected bubble formation can be reduced. In addition to the higher quality that can be reached in this way, the duration of the manufacturing process is reduced.
    Type: Grant
    Filed: July 9, 2001
    Date of Patent: April 1, 2008
    Assignee: Heraeus Quarzglas GmbH & Co. KG
    Inventors: Johann Leist, Rolf Göbel, Helmut Fritz
  • Patent number: 7338699
    Abstract: In film-forming devices and plasma-processing devices, filmy matter adheres to the surfaces of the inner parts and it peels to cause dust and particles in the devices. In the devices, the dust and particles contaminate the objects for film formation thereon or the objects to be processed with plasma. For preventing the objects from being contaminated with them, the inner parts of the devices must be frequently exchanged every time when they have received any minor filmy matter thereon, and this lowers the productivity in the devices. When a modified glass part of which the surface is modified with spherical or bell-like island projections having a width and a height of from a few ?m to a few hundreds ?m is used in a film-forming device and in a plasma-processing device, then its ability to hold the filmy substance having adhered thereto is good and its resistance to plasma is also good.
    Type: Grant
    Filed: October 30, 2003
    Date of Patent: March 4, 2008
    Assignee: Tosoh Corporation
    Inventors: Koyata Takahashi, Masanori Kohgo, Osamu Matsunaga
  • Publication number: 20080041103
    Abstract: A process for making inorganic, metal oxide spheres that includes exposing solidified, molded microparticles that include a glass precursor composition to a temperature sufficient to transform the molded microparticles into molten glass and cooling the molten glass to form inorganic, metal oxide spheres.
    Type: Application
    Filed: August 21, 2006
    Publication date: February 21, 2008
    Inventors: David C. Kramlich, John L. Vandenberg, Matthew H. Frey, Scott R. Culler, Kathleen M. Schakel-Carlson
  • Publication number: 20080034794
    Abstract: A reactive liquid ceramic binder suitable for the production of ceramic products from ceramic powders is provided. The reactive liquid ceramic binder contains organo-modified siloxane compounds, wherein the liquid organo-modified siloxane compounds contain organoalkoxysiloxane units according to general formula (I) wherein R1=alkyl radical and/or aryl radical, R2?H and/or alkyl radical with 1 to 4 carbon atoms, a?0 and ?2, and b<0 and ?3, with the proviso that a+b?1 and ?4.
    Type: Application
    Filed: April 26, 2007
    Publication date: February 14, 2008
    Applicant: Goldschmidt GmbH
    Inventors: Thomas Ebbrecht, Tadeusz von Rymon Lipinski, Stefan Silber, Bernd Weyershausen
  • Patent number: 7297646
    Abstract: Ceramics comprising (i) at least one of Nb2O5 or Ta2O5 and (ii) at least two of (a) Al2O3, (b) REO, or (c) at least one of ZrO2 or HfO2. Embodiments of ceramics according to the present invention can be made, formed as, or converted into optical waveguides, glass beads, articles (e.g., plates), fibers, particles (e.g., abrasive particles), and thin coatings.
    Type: Grant
    Filed: September 25, 2006
    Date of Patent: November 20, 2007
    Assignee: 3M Innovative Properties Company
    Inventors: Anatoly Z. Rosenflanz, Craig R. Schardt
  • Patent number: 7178366
    Abstract: A process for producing an SiO2 shaped body which is at least partially vitrified, wherein an amorphous, porous SiO2 green body is sintered or vitrified by contactless heating by means of radiation, while avoiding contamination to the SiO2 shaped body with foreign atoms, wherein the radiation used is the beam of a laser at a subatmospheric pressure below 1000 mbar.
    Type: Grant
    Filed: May 27, 2004
    Date of Patent: February 20, 2007
    Assignee: Wacker Chemie AG
    Inventors: Fritz Schwertfeger, Jens Guenster, Sven Engler, Juergen Heinrich
  • Patent number: 7169725
    Abstract: The invention provides a method to transform large quantities of waste glass into useful ceramic products by a low-cost manufacturing process. The method improves green strength compared to previous methods, and does not require water or any other liquid solvent. Only one firing step is needed with a low peak firing temperature of about 700° C.to about 1000° C. The method conserves energy and natural resources compared to clay-based traditional ceramic manufacturing. High-quality impervious ceramic products can be produced by the invention.
    Type: Grant
    Filed: October 8, 2002
    Date of Patent: January 30, 2007
    Inventor: Michael J. Haun
  • Patent number: 7169721
    Abstract: Disclosed herein are a self-foamed porous ceramic composition and a method for making a porous ceramic using the self-foamed porous ceramic composition. The self-foamed porous ceramic is obtained by fabricating a glass consisting of 41˜47 mole % of calcium oxide (CaO), 41˜47 mole % of silica (SiO2) and 6˜18 mole % of borate (B2O3), pulverizing the glass into a finely-divided glass powder having an average particle size of 1˜10 ?m, molding the glass powder, and sintering the molded glass powder.
    Type: Grant
    Filed: August 27, 2003
    Date of Patent: January 30, 2007
    Assignee: Seoul National University Industry Foundation
    Inventors: Hyun Seung Yu, Kug Sun Hong, Hwan Kim, Dong Ho Lee, Choon Ki Lee, Bong Soon Chang, Deug Joong Kim, Jun Hyuk Seo, Jae Hyup Lee, Ki Soo Park
  • Patent number: 7160387
    Abstract: This invention provides a high purity silica crucible having low impurity concentration in its inner portion, and its production method. The crucible, in which at least each content of Na and Li being contained in the depth of 1 mm from the inside surface is less than 0.05 ppm, is given by a production method of a high purity silica glass crucible, wherein a purity of the melted silica powder layer is increased by applying a voltage between a mold and an arc electrode to move impurity metals being contained in the melted silica glass layer to the outside, when the silica crucible is produced by arc plasma heating a raw material powder of silica in an inside surface of a hollow rotary mold. The method comprises, keeping an arc electrode potential of within ±500 V during an arc melting, applying a voltage of from ?1000 V to ?20000 V to a mold being insulated to the ground, and applying a high voltage to the un-melted silica powder layer of the outside.
    Type: Grant
    Filed: February 20, 2004
    Date of Patent: January 9, 2007
    Assignee: Japan Super Quartz Corporation
    Inventors: Hiroshi Kishi, Masanori Fukui, Yoshiyuki Tsuji
  • Patent number: 7140202
    Abstract: The invention relates to a method for manufacturing optical glasses and colored glasses with the aid of a fluid phase sintering process from a basic material encompassing at least SiO.sub.2 powder as well as additives for reducing the temperature of the fluid phase sintering and/or melting process encompassing the following steps: the starting materials are dissolved in any sequence in a fluid medium to produce a solution as far as is possible and a suspension to the extent that they are not dispersed in solution; a greenbody is produced from the dissolved and dispersed starting materials; the greenbody is dried the dried greenbody is fluid-phase sintered at temperatures below 1200° C., in particular in the temperature range from 600° C. to 1200° C.
    Type: Grant
    Filed: August 20, 2002
    Date of Patent: November 28, 2006
    Assignee: Schott AG
    Inventors: Jochen Freund, Monika Gierke, Uwe Kolberg, Ruediger Hentschel, Rolf Clasen
  • Patent number: 7111476
    Abstract: Cup-shaped porous silica preforms suitable for manufacture of large 24-inch crucibles used in Czochralski crystal-growing furnaces are produced by a unique electrophoretic casting process using a high-purity aqueous silica slip or slurry having a predetermined particle-size distribution, an average particle size of from 6 to 10 microns and a solids content of from 80 to 85 percent by weight. The slurry contains an electrolyte, such as ammonium hydroxide, has a pH of from 7.5 to 8.5, and can be wet milled at a pH of at least 7 in such manner as to provide the micronized silica particles with excellent electrophoretic mobility, thereby providing a superb process for economical mass production of large pure silica preforms using safe voltages, such as 20 to 40 volts. The electrophoretic casting apparatus can be of the type shown in FIGS.
    Type: Grant
    Filed: May 7, 2002
    Date of Patent: September 26, 2006
    Inventors: Ted A Loxley, John F. Blackmer, Klaus-Markus Peters
  • Patent number: 7074731
    Abstract: It is an object of the present invention to provide a hydrogen-doped silica powder that is useful in the formation of a quartz glass crucible that is capable of pulling a silicon single crystal without causing a state having dislocations in the silicon single crystal due to peeling of quartz glass segment. It is a further object of the invention to provide a quartz glass crucible for use in pulling a silicon single crystal whose inner surface is formed by use of the hydrogen-doped silica powder and a producing method of the silica powder.
    Type: Grant
    Filed: May 16, 2003
    Date of Patent: July 11, 2006
    Assignees: Heraeus Quarzglas GmbH & Co. KG, Shin-Etsu Quartz Products Co., Ltd.
    Inventors: Yasuo Ohama, Takayuki Togawa
  • Patent number: 7069746
    Abstract: A method for producing ultra-high purity, optical quality, glass articles is disclosed which involves: 1. compacting metaloxide or metalloidoxide to granules having a mean particle size of less than about 1 millimeter; 2. optionally fully sintering the granules to produce high purity, artificial sand; 3. casting the artificial sand by conventional techniques, such as, slip casting, to form a high density, porous, green body; 4. optionally drying and partially sintering the green body; 5. optionally fully sintering the green body under vacuum; and 6. optionally hot isostatic pressing the green body.
    Type: Grant
    Filed: October 9, 2002
    Date of Patent: July 4, 2006
    Assignee: Degussa AG
    Inventors: Monika Oswald, Gerrit Schneider, Jürgen Meyer
  • Patent number: 7037868
    Abstract: The present invention provides zinc-free glass frits that can be used to formulate glaze compositions that develop glossy surfaces when fired on ceramic products such as floor tile and wall tile. The zinc-free glass frits include, by weight, from about 50% to about 70% SiO2, from about 5% to about 20% CaO, from about 3% to about 15% Al2O3, up to about 20% BaO, up to about 15% B2O3, up to about 10% K2O, up to about 10% Na2O, up to about 10% ZrO2, up to about 5% MgO and up to about 5% PbO and less than 0.5% ZnO. Glaze compositions comprising the zinc-free glass frits can be fired using conventional double fast firing, single fast firing, and gres porcellanato ceramic firing cycles.
    Type: Grant
    Filed: December 10, 2003
    Date of Patent: May 2, 2006
    Assignee: Ferro Corporation
    Inventors: Jose Antonio Pascual Herrero, Juan Uso Villanueva, Antonio Manuel Querol Villalba
  • Patent number: 7007509
    Abstract: A method of making a glass composition consisting essentially by mol percent of about 55<SiO2<75; 5<BaO<30; and 2<MgO<22 for use as a matrix of composite materials. A method of making a glass matrix-ceramic particulate composition useful for sealing electrochemical structures, such as solid oxide fuel cells is also disclosed. Method steps include the admixture of finely divided Mg2SiO4 particulates with the matrix glass, to reach an overall composition by mol percent of about 55<SiO2<65; 5<BaO<15; and 25<MgO<35.
    Type: Grant
    Filed: March 4, 2005
    Date of Patent: March 7, 2006
    Assignee: Ford Global Technologies, LLC
    Inventor: Gary Mark Crosbie
  • Patent number: 7003981
    Abstract: Using sol-gel techniques, an optical gain medium has been fabricated comprising a glass ceramic host material that includes clusters of crystalline oxide material, especially tin oxide, and that is doped with active ions concentrated at the clusters. The active ions are preferentially located at the nanoclusters so that they experience the relatively low phonon energy of the oxide and are insensitive to the phonon energy of the host. A host with a high phonon energy, such as silica, can therefore be used without the usual drawback of reduced carrier lifetimes through enhanced nonradiative decay rates.
    Type: Grant
    Filed: October 1, 2002
    Date of Patent: February 28, 2006
    Assignee: University of Southhampton
    Inventors: Elizabeth Taylor, Gilberto Brambilla, Norberto Chiodini, Alberto Paleari, Giorgio Spinolo, Franca Morazzoni, Roberto Scotti
  • Patent number: 6997015
    Abstract: The invention discloses a method for forming substantially striae-free glass substrates that are suitable for optical applications, including use in forming optical elements or structures such as mirrors and platen stage structures that can be used, for example, in EUV lithography. The method includes forming a mixture of silica soot, binder, lubricant and solvent. The homogenized mixture is then extruded through a slit die or mask into a flat planar pre-form, and the extruded pre-form is then consolidated by heating into a substantially full density, substantially striae-free lithography glass substrate structure. The consolidated perform has a substantially uniform coefficient of thermal expansion and is also substantially void free.
    Type: Grant
    Filed: November 22, 2002
    Date of Patent: February 14, 2006
    Assignee: Corning Incorporated
    Inventors: Bradley F. Bowden, Seann Bishop, Kenneth E. Hrdina, John F. Wight, Jr.
  • Patent number: 6992753
    Abstract: Radiation-induced damage to a lens material in a projection exposure system is reduced by selection of maximum design fluence values HD for lenses and at least one lens made of a material having a characteristic transition point TRC after exposure to a given amount of radiation, wherein, for instance, TRC<0.8. HD among other relationships and/or characteristics of the lenses.
    Type: Grant
    Filed: December 24, 2003
    Date of Patent: January 31, 2006
    Assignee: Carl Zeiss SMT AG
    Inventors: Daniel Krähmer, Eric Eva