With Chemically Reactive Treatment Of Glass Preform Patents (Class 65/30.1)
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Patent number: 7841211Abstract: First of all, there is provided a production process of a synthetic quartz glass which has less impurity, has a high-temperature viscosity characteristic equal to or more than that of a natural quartz glass, and hardly deforms even in a high-temperature environment, and especially a production process of a highly heat resistant synthetic quartz glass which is free from the generation of bubbles and is dense. Secondly, there is provided a highly heat resistant synthetic quartz glass body which is easily obtained by the production process of the present invention, and especially a transparent or black quartz glass body which is free from the generation of bubbles, is dense, has high infrared absorption rate and emission rate, and has an extremely high effect for preventing diffusion of alkali metal. The process is a process of producing a highly heat resistant quartz glass body having an absorption coefficient at 245 nm of 0.Type: GrantFiled: November 28, 2003Date of Patent: November 30, 2010Assignee: Shin-Etsu Quartz Products Co., Ltd.Inventors: Tatsuhiro Sato, Takahiro Kaitou, Akira Fujinoki, Toshiyuki Kato, Tohru Segawa, Nobumasa Yoshida
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Patent number: 7841210Abstract: In a method of manufacturing a glass substrate for an information recording medium including a step for chemically strengthening the glass substrate by contacting the glass substrate with chemical strengthening processing liquid containing chemical strengthening salt, concentration of Fe and Cr is 500 ppb or less in said chemical strengthening salt, respectively. The concentration may be detected by the use of an ICP (Inductively Coupled Plasma) emission spectrometry analyzing method or a fluorescent X-ray spectroscopy analyzing method.Type: GrantFiled: October 5, 2007Date of Patent: November 30, 2010Assignee: Hoya CorporationInventors: Hiroaki Ikeda, Masaru Suzuki, Kazuna Sasaki, Yumi Mukai, Jun Ozawa
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Patent number: 7836727Abstract: A method of cutting a glass substrate to form a plurality of flat panel displays. The method includes forming a scribe line or a line of weakness on a surface of a mother material; treating the mother material with chemical to further weaken the mother material; and cutting the mother material. The scribe line may be formed using a masking technique. The mother material may be treated with chemical by putting the mother material into a chemical solution. Alternatively, the chemical may be sprayed, blown, or exposed to the mother material. The cutting of the mother material may be done by applying mechanical and/or thermal stress along the scribe line.Type: GrantFiled: February 8, 2008Date of Patent: November 23, 2010Assignee: Nishiyama Stainless Chemical Co., Ltd.Inventor: Tomohiro Nishiyama
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Patent number: 7810355Abstract: Methods and apparatus for protecting the thin films during chemical and/or thermal edge strengthening treatment. In one embodiment, a portion of each individual sheet is laminated. Pairs of sheets are then sealed together such that the thin film sides face inward to form a thin film sandwich. In some embodiments, the sandwich in then immersed in a chemical strengthener. In other embodiments, a localized treatment is applied to the unstrengthened edges.Type: GrantFiled: June 30, 2008Date of Patent: October 12, 2010Assignee: Apple Inc.Inventors: Casey J. Feinstein, John Z. Zhong
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Publication number: 20100251771Abstract: The invention relates to a method allowing cost-effective production of doped quartz glass, particularly laser-active quartz glass, that is improved with regard to the homogeneity of the doping material distribution, in that a suspension is provided comprising SiO2 particles and an initial compound for at least one doping material in an aqueous fluid, the fluid being removed under formation of a doped intermediate product comprising particles of the doping material or particles of the precursor substance or the doping material, and the doped quartz glass is formed by sintering the doped intermediate product, wherein at least part of the particles of the doping material or the particles of the precursor substance of the same is generated in the suspension as a precipitate of a pH-value-controlled precipitation reaction of the initial compound.Type: ApplicationFiled: September 18, 2008Publication date: October 7, 2010Applicants: HERAEUS QUARZGLAS GMBH & CO. KG, INSTITUT FUER PHOTONISCHE TECHNOLOGIEN E.V.Inventors: Andreas Langner, Thomas Kayser, Gerhard Schoetz, Mario Such, Johannes Kirchhof, Stephan Grimm, Volker Reichel
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Patent number: 7767607Abstract: A glass substrate of the present invention for magnetic recording media having high heat resistance and easy chemical strengthening ability at once has not been obtained, which is a glass composition essentially comprising 60 to 70 wt % SiO2, 5 to 20 wt % Al2O3, 0 to 1 wt % Li2O, 3 to 18 wt % Na2O, 0 to 9 wt % K2O, 0 to 10 wt % MgO, 1 to 15 wt % CaO, 0 to 4.5 wt % SrO, 0 to 1 wt % BaO, 0 to 1 wt % TiO2 and 0 to 1 wt % ZrO2, wherein the sum of Li2O, Na2O and K2O is from 5 to 25 wt %, and the sum of MgO, CaO, SrO and BaO is from 5 to 20 wt %.Type: GrantFiled: November 1, 2007Date of Patent: August 3, 2010Assignees: Nippon Sheet Glass Co., Ltd., Hoya CorporationInventors: Junji Kurachi, Akihiro Koyama, Nobuyuki Yamamoto
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Patent number: 7755286Abstract: Disclosed is a dense silicon oxide film having a high insulation resistance, which is a glass film having a certain level of thickness. Specifically, disclosed are a silicon oxide film, and a glass film comprising the silicon oxide film and silica particles incorporated in the silicon oxide film. The glass film can be produced by a process comprising the steps of: applying a paste comprising silica particles, an organic silicon compound which is in a liquid form at room temperature and water onto a substrate; and oxidizing the organic silicon compound in the paste.Type: GrantFiled: August 3, 2006Date of Patent: July 13, 2010Assignee: Panasonic CorporationInventors: Tomohiro Okumura, Mitsuo Saitoh, Hironobu Inoue, Motoi Hatanaka
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Patent number: 7749930Abstract: An ideal quartz glass for a wafer jig for use in an environment having an etching effect is distinguished by both high purity and high resistance to dry etching. To indicate a quartz glass that substantially fulfills these requirements, it is suggested according to the invention that the quartz glass is doped with nitrogen at least in a near-surface area, has a mean content of metastable hydroxyl groups of less than 30 wt ppm and that its fictive temperature is below 1250° C. and its viscosity is at least 1013 dPa·s at a temperature of 1200° C. An economic method for producing such a quartz glass comprises the following method steps: melting an SiO2 raw material to obtain a quartz glass blank, the SiO2 raw material or the quartz glass blank being subjected to a dehydration measure, heating the SiO2 raw material or the quartz glass blank to a nitriding temperature in the range between 1050° C. and 1850° C.Type: GrantFiled: March 30, 2006Date of Patent: July 6, 2010Assignee: Heraeus Quarzglas GmbH & Co. KGInventors: Juergen Weber, Tobias Pogge, Martin Trommer, Bodo Kuehn, Ulrich Kirst, Waltraud Werdecker
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Publication number: 20100126218Abstract: A soda-lime-silica glass for solar collector cover plates and solar mirrors has less than 0.010 weight percent total iron as Fe2O3, a redox ratio of less than 0.350, less than 0.0025 weight percent CeO2, and spectral properties that include a visible transmission, and a total solar infrared transmittance, of greater than 90% at a thickness of 5.5 millimeters, and reduced solarization. In one non-limiting embodiment of invention, the glass is made by heating a pool of molten soda-lime-silica with a mixture of combustion air and fuel gas having an air firing ratio of greater than 11, or an oxygen firing ratio of greater than 2.31. In another non-limiting embodiment of the invention, streams of oxygen bubbles are moved through a pool of molten glass. In both embodiments, the oxygen oxidizes ferrous iron to ferric iron to reduce the redox ratio.Type: ApplicationFiled: November 21, 2008Publication date: May 27, 2010Applicant: PPG INDUSTRIES OHIO, INC.Inventors: Larry J. Shelestak, Ronald L. Shewenninger
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Publication number: 20100119846Abstract: [Object] To provide a method of manufacturing a reinforced plate glass by which glass surface strength can be sufficiently increased, and a stable quality reinforced plate glass is manufactured at high production efficiency, and to provide a reinforced plate glass manufactured by the manufacturing method. [Solving Means] A reinforced plate glass (10) is formed of an inorganic oxide glass, and is provided with a compression stress layer by chemical reinforcement on plate surfaces (11, 12) opposed to each other in a plate thickness direction. Plate end faces (13, 14, 15, 16) have regions where a compression stress is formed and regions where no compression stress is formed.Type: ApplicationFiled: March 3, 2008Publication date: May 13, 2010Inventor: Masahiro Sawada
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Patent number: 7712335Abstract: The aim of the invention is to improve a known quartz glass cylinder for the production of an optical component, comprising an inner drilling, which is mechanically machined to size and provided with an etched structure by means of an etching treatment, subsequent to the mechanical machining, such that in the application thereof for production of pre-forms and optical fibers, few bubbles arise along the boundary surface between core and sleeve. Said aim is achieved, whereby the etched structure comprises striations with a maximum depth of 2.0 mm and a maximum width of 100 ?m.Type: GrantFiled: June 2, 2004Date of Patent: May 11, 2010Assignee: Heraeus Quarzglas GmbH & Co. KGInventor: Heinz Fabian
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Publication number: 20100107693Abstract: The invention relates to a method for doping and/or colouring glass. In the method a two- or three-dimensional layer is formed on the surface of the glass, and the layer is further allowed to diffuse and/or dissolve into the glass to change the transmission, absorption, reflection and/or scattering of the electromagnetic radiation of the glass. The layer of nanomaterial includes at least one component that causes the above-mentioned change and at least one component that lowers the melting point of the above-mentioned component causing the change.Type: ApplicationFiled: February 12, 2007Publication date: May 6, 2010Applicant: BENEQ OYInventors: Markku Rajala, Joe Pimenoff, Jussi Wright
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Patent number: 7700205Abstract: A process for manufacturing a glass substrate for a magnetic recording medium comprising polishing a crystallized glass substrate using abrasive grains, and then washing the substrate using an aqueous organic carboxylic acid solution; a glass substrate for a magnetic recording medium which is manufactured by the process; and a magnetic recording medium obtained using the substrate. A glass substrate for a magnetic recording medium is manufactured, whereby the surface roughness is low and the surface defects are minimal for washing after polishing of a crystallized glass substrate, and wherein the Read-Write performance are not impaired when a recording layer including a magnetic film is formed on the magnetic recording medium substrate for manufacturing a magnetic recording medium.Type: GrantFiled: August 4, 2005Date of Patent: April 20, 2010Assignee: Showa Denko K.K.Inventors: Katsuaki Aida, Hiroyuki Machida, Kazuyuki Haneda
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Publication number: 20100089097Abstract: The invention discloses a method for the production of packaging made from borosilicate glass for pharmaceutical products and medical products comprising the steps of: providing a glass tube made from a borosilicate base glass, generating a temporary interface layer on an inner surface of the glass tube, hot-forming the glass tube at a temperature above Tg, and cooling down the glass tube to room temperature.Type: ApplicationFiled: October 7, 2009Publication date: April 15, 2010Inventors: Heike Brack, Uwe Rothhaar, Stephan Tratzky, Juergen Thuerk
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Patent number: 7694530Abstract: Chemical strengthening treatment is performed by first providing a granular chemical strengthening salt so as to prevent spread in atmosphere at the time of introduction of chemical strengthening salt in a treating vessel, introducing the chemical strengthening salt in a treating vessel, melting the chemical strengthening salt into molten chemical strengthening salt and bringing a glass disc into contact with the molten chemical strengthening salt. The granular chemical strengthening salt is, for example, one obtained by forming of a powdery chemical strengthening salt material into grains. A chemically strengthened glass substrate for magnetic disk can be obtained through the process of carrying out chemical strengthening treatment of magnetic disk glass substrates. A magnetic disk can be obtained by forming at least a magnetic layer on the chemically strengthened glass substrate for magnetic disk.Type: GrantFiled: September 28, 2004Date of Patent: April 13, 2010Assignee: Hoya CorporationInventors: Naohiro Kamiya, Hideki Isono
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Publication number: 20100068453Abstract: A processed substrate of the present invention includes a translucent substrate having a plurality of through-holes, in each of which there is a gap from 0 to 5 ?m between (a) a straight line which passes through a central point of an opening plane of the each of the plurality of through-holes and which is perpendicular to the opening plane and (b) a straight line which passes through a central point of the other opening plane of the each of the plurality of through-holes and which is perpendicular to the other opening plane, thereby making it possible to provide (i) a processed substrate having through-holes in each of which central axes are aligned, which can be easily produced with high productivity, and (ii) a production method thereof.Type: ApplicationFiled: September 14, 2009Publication date: March 18, 2010Inventors: Hirofumi IMAI, Koichi Misumi, Takahiro Asai
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Patent number: 7648656Abstract: The invention is directed to a silver-containing polarizing boroaluminosilicate glass composition that has been doped with a noble metal selected from the group consisting of Pt, Pd, Os, Ir, Rh and Ru, including mixtures thereof, to nucleate and precipitate silver ions to silver metal without the need for a reducing atmosphere step. The invention is further directed to a method for making the glass composition of the invention. Using the composition and method of the invention, one can prepare a glass having a selected null transmission range.Type: GrantFiled: November 6, 2008Date of Patent: January 19, 2010Assignee: Corning IncorporatedInventors: Nicholas Francis Borrelli, George Bigelow Hares, David John McEnroe, Joseph Francis Schroeder, III
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Publication number: 20100009154Abstract: A strengthened glass that does not exhibit frangible behavior when subjected to impact or contact forces, and a method of strengthening a glass. The glass may be strengthened by subjecting it to multiple, successive, ion exchange treatments. The multiple ion exchange treatments provide a local compressive stress maximum at a depth of the strengthened layer and a second local maximum at or near (e.g., within 10 ?m) the surface of the glass.Type: ApplicationFiled: July 10, 2009Publication date: January 14, 2010Inventors: Douglas Clippinger Allan, Adam James Ellison, Sinue Gomez
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Patent number: 7635658Abstract: What is disclosed includes OD-doped synthetic silica glass capable of being used in optical elements for use in lithography below about 300 nm. OD-doped synthetic silica glass was found to have significantly lower polarization-induced birefringence value than non-OD-doped silica glass with comparable concentration of OH. Also disclosed are processes for making OD-doped synthetic silica glasses, optical member comprising such glasses, and lithographic systems comprising such optical member. The glass is particularly suitable for immersion lithographic systems due to the exceptionally low polarization-induced birefringence values at about 193 nm.Type: GrantFiled: October 19, 2006Date of Patent: December 22, 2009Inventors: Dana Craig Bookbinder, Richard Michael Fiacco, Ulrich Wilhelm Heinz Neukirch
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Publication number: 20090263662Abstract: A glass composition for chemical tempering includes oxides in wt % ranges of: SiO2 60 to 75; Al2O3 18 to 28; Li2O 3 to 9; Na2O 0 to 3; K2O 0 to 0.5; CaO 0 to 3; MgO 0 to 3; ZrO2 0 to 3; where MgO+CaO is 0 to 6 wt %; Al2O3+ZrO2 is 18 to 28 wt %, and Na2O+K2O is 0.05 to 3.00 wt %. The glass has a log 10 viscosity temperature in the temperature range of 1328° F. (720° C.) to 1499° F. (815° C.); a liquidus temperature in the temperature range of 2437° F. (1336° C.) to 2575° F. (1413° C.), and a log 7.6 softening point temperature in the temperature range of 1544° F. (840° C.) to 1724° F. (940° C.). The chemically tempered glass has, among other properties, an abraded modulus of rupture of 72 to 78 KPSI, and a modulus of rupture of 76 to 112 KPSI.Type: ApplicationFiled: June 26, 2009Publication date: October 22, 2009Applicant: SCHOTT AGInventors: LARRY J. SHELESTAK, George B. Goodwin, Amarendra Mishra, James M. Baldauff
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Publication number: 20090255582Abstract: This invention relates generally to methods of dehydrating glass substrates for use in photovoltaic modules, suitably by reacting moisture on the glass with organosilicon compounds. The invention also relates to methods of preparing thin film photovoltaic modules, which include dehydration of the glass substrates used in the manufacture of the photovoltaic modules.Type: ApplicationFiled: April 10, 2009Publication date: October 15, 2009Applicant: EPV Solar, Inc.Inventor: Masud Akhtar
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Publication number: 20090252947Abstract: A method of loading at least one fused silica article with hydrogen. At least one fused silica article is first loaded with an amount of hydrogen so that the hydrogen concentration at the center of the article exceeds a minimum concentration upon completion of loading. An amount of hydrogen is the removed from the fused silica article so that the fused silica article has an average hydrogen concentration that is less than the maximum average concentration limit. The surface region of the fused silica article is then reloaded to ensure that the hydrogen concentration throughout the article is within a predetermined pressure range. A fused silica article comprising hydrogen is also described.Type: ApplicationFiled: April 8, 2008Publication date: October 8, 2009Inventor: William Rogers Rosch
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Publication number: 20090223699Abstract: The underlying purpose of the invention is to manufacture electrical leadthroughs, which are improved with regard to the temperature resistance thereof. Proposed for this purpose is a method for manufacturing an electrical leadthrough, for which at least one metal tube is fused in a glass insulator, whereby a metal rod is mounted in the metal tube by means of soldering-in, prior to or during the sealing of the tube in the glass insulator.Type: ApplicationFiled: December 12, 2008Publication date: September 10, 2009Applicant: SCHOTT AGInventor: Johann Bernauer
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Publication number: 20090224672Abstract: Disclosed is a dense silicon oxide film having a high insulation resistance, which is a glass film having a certain level of thickness. Specifically, disclosed are a silicon oxide film, and a glass film comprising the silicon oxide film and silica particles incorporated in the silicon oxide film. The glass film can be produced by a process comprising the steps of: applying a paste comprising silica particles, an organic silicon compound which is in a liquid form at room temperature and water onto a substrate; and oxidizing the organic silicon compound in the paste.Type: ApplicationFiled: August 3, 2006Publication date: September 10, 2009Applicant: MATSUSHITA ELECTRIC INDUSTRIAL CO., LTD.Inventors: Tomohiro Okumura, Mitsuo Saitoh, Hironobu Inoue, Motoi Hatanaka
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Publication number: 20090190214Abstract: The invention is directed to a glass composition and articles made from the composition that are both polarizing and photorefractive. The glass has a composition consisting essentially of, in weight percent (“wt. %”) of 70-73 SiO2, 13-17% B2O3, 8-10% Na2O, 2-4% Al2O3, 0.005-0.1% CuO, <0.4% Cl, 0.1-0.5% Ag, 0.1-0.3% Br. The glass can be used make articles or elements that can exhibits both the photorefractive effect and the polarizing effect within a single element or article, and can be used to make a variety of optical elements including Bragg gratings, filtering elements, and beam shaping elements and light collection elements for use in display, security, defense, metrology, imaging and communications applications.Type: ApplicationFiled: January 29, 2008Publication date: July 30, 2009Inventors: Nicholas Francis Borrelli, Joseph Francis Schroeder, III
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Patent number: 7552601Abstract: Starting from an optical component of quartz glass for transmitting ultraviolet radiation of a wavelength between 190 nm and 250 nm, with a glass structure essentially without oxygen defects, a hydrogen content ranging from 0.1×1016 molecules/cm3 to 5.0×1016 molecules/cm3, and with a content of SiH groups of less than 5×1016 molecules/cm3, to provide such a component which is particularly well suited for use with linearly polarized UV laser radiation, the present invention suggests that the component should have a content of hydroxyl groups ranging from 10 to 250 wt ppm and a fictive temperature above 1000° C.Type: GrantFiled: March 30, 2005Date of Patent: June 30, 2009Assignee: Heraeus Quarzglas GmbH & Co. KGInventors: Bodo Kühn, Stephan Thomas, Steffen Kaiser
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Publication number: 20090136762Abstract: The invention relates to a chemical process for obtaining glass with a total or partial satin/matte finish, comprising immersion in an acid solution, for the simultaneous and continuous production of one or more parts and/or sheets of glass having standard, special or variable dimensions, thicknesses, colours, uses and applications. The inventive process can be used to obtain glass with a total or partial satin/matte finish in a simultaneous and continuous manner either on one or both sides of the glass (atmospheric side and tinned side) or of several glass sheets and/or parts at the same time, with different thicknesses, measurements, colours, uses, specifications and characteristics, said process being performed simultaneously by means of immersion. According to the invention, containers of glass sheets are immersed in containers of chemical solutions using a variable-speed transport immersion crane.Type: ApplicationFiled: September 29, 2005Publication date: May 28, 2009Inventor: Juan Luis Rendon Granados
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Publication number: 20090126404Abstract: One embodiment comprises a method for increasing the hydrophobic characteristics of a surface. A coupling agent is applied to the surface, and the surface is subsequently exposed to a first ionizing gas plasma at about atmospheric pressure for a predetermined period of time. The ionizing gas plasma may be formed from a mixture of a carrier gas and a reactive gas. The reactive gas may be comprised of one or more hydrocarbon compound such as an alkane, an alkene, and an alkyne. Alternatively, the reactive gas may be a fluorocarbon or organometallic compound. A lubricant may then be applied to the surface, followed by exposure to second ionizing gas plasma.Type: ApplicationFiled: January 16, 2009Publication date: May 21, 2009Applicant: TriboFilm Research, Inc.Inventors: Vinay G. Sakhrani, Charles Tomasino
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Publication number: 20090098370Abstract: To provide a black synthetic quartz glass with a transparent layer, which has high emissivity in the far infrared region, has excellent light-shielding properties, maintains the same degree of purity as synthetic quartz glass in terms of metal impurities, has high-temperature viscosity characteristics comparable to natural quartz glass, can undergo high-temperature processing like welding, and does not release carbon from its surface; together with a method for the production thereof. A porous silica glass body containing hydroxyl groups is subjected to a gas phase reaction in a volatile organosilicon compound atmosphere at a temperature between 100° C. and 1200° C. and, following the reaction, evacuation is commenced and, on reaching a degree of vacuum exceeding 10 mmHg (1343 Pa), heating is carried out at a temperature between 1200° C. and 2000° C. to produce a compact glass body.Type: ApplicationFiled: October 10, 2008Publication date: April 16, 2009Applicants: HERAEUS QUARZGLAS GMBH & CO. KG, SHIN-ETSU QUARTZ PRODUCTS CO., LTD.Inventors: Tatsuhiro Sato, Nobumasa Yoshida
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Publication number: 20090056379Abstract: The present invention provides an optical element including a silver halide-containing glass material having a concentration of less than 0.001 wt % cerium; and a refractive index pattern formed in the silver halide-containing glass material, the refractive index pattern including regions of high refractive index and regions of low refractive index, the difference between the refractive indices of the high refractive index regions and the low refractive index regions being at least 4×10?5 at a wavelength of 633 nm. The present invention also provides methods for making optical elements from silver halide-containing glass materials.Type: ApplicationFiled: February 27, 2008Publication date: March 5, 2009Inventors: Nicholas F. Borrelli, George B. Hares, Joseph F. Schroeder
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Publication number: 20090034281Abstract: The invention relates to a headlight lens for a vehicle headlight comprising a light source, particularly for a motor vehicle headlight, wherein the headlight lens comprises a transparent lens body made of glass comprising a surface arranged to face the light source and a surface arranged to face away from the light source, and wherein the headlight lens comprises at least with respect to said surface arranged to face away from the light source a layer comprising an aluminum concentration which is higher than an aluminum concentration inside the lens body and/or a sodium concentration which is lower than a sodium concentration inside the lens body.Type: ApplicationFiled: January 25, 2007Publication date: February 5, 2009Inventor: Jan Heiko Hamkens
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Patent number: 7485593Abstract: To provide titania-silica glass which is transparent glass of low thermal expansion, in particular, is of a low thermal expansion coefficient over a wide range of temperatures of 0 to 100° C. (an operating temperature range) when it is used as a photomask or a mirror material in extreme ultraviolet ray lithography, and which is excellent in homogeneity within the field and stability. Titania-silica glass is used which has 8 to 10% by weight of titania and 90 to 92% by weight of silica, where a Ti3+ concentration is 10 to 60 ppm by weight.Type: GrantFiled: October 18, 2007Date of Patent: February 3, 2009Assignee: Covalent Materials CorporationInventors: Masanobu Ezaki, Masashi Kobata, Sachiko Kato
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Patent number: 7468148Abstract: The invention is directed to a silver-containing polarizing boroaluminosilicate glass composition that has been doped with a noble metal selected from the group consisting of Pt, Pd, Os, Ir, Rh and Ru, including mixtures thereof, to nucleate and precipitate silver ions to silver metal without the need for a reducing atmosphere step. The invention is further directed to a method for making the glass composition of the invention. Using the composition and method of the invention, one can prepare a glass having a selected null transmission range.Type: GrantFiled: October 24, 2005Date of Patent: December 23, 2008Assignee: Corning IncorporatedInventors: Nicholas Francis Borrelli, George Bigelow Hares, David John McEnroe, Joseph Francis Schroeder, III
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Publication number: 20080207424Abstract: Bi-containing glass-ceramic material, especially those containing ?-quartz and/or ?-spodumene solid solutions as the predominant crystalline phase, and the precursor glass material as well as process of making such glass-ceramic material and articles. The glass-ceramic can be made to have a dark color, and essentially to be free of V2O5, As2O3 and Sb2O3.Type: ApplicationFiled: February 28, 2007Publication date: August 28, 2008Inventors: Bruce Gardiner Aitken, Lothar Wondraczek
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Publication number: 20080202163Abstract: There is provided a material on which a minute pattern in nanometer order can be formed and capable of providing a glass having transparency and high refractive index. A material for a high refractive index glass according to an embodiment of the present invention includes a polysilane, a silicone compound, and metal oxide nanoparticles. Preferably, the polysilane includes a branched polysilane. Preferably, the polysilane and the silicone compound are contained at a weight ratio of 80:20 to 5:95. Preferably, the metal oxide nanoparticles are formed of at least one metal oxide selected from the group consisting of zircon oxide, titanium oxide, and zinc oxide.Type: ApplicationFiled: August 27, 2007Publication date: August 28, 2008Applicants: RIKEN, NIPPON PAINT CO., LTDInventors: Motoki Okinaka, Kazuhito Tsukagoshi, Yoshinobu Aoyagi, Yoshifumi Ichinose, Toshiyuki Tachibana, Hiroshi Tsushima
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Patent number: 7415841Abstract: Prior to conducting chemical strengthening treatment by contacting a glass with a potassium-containing chemical strengthening treating solution, oxidation treatment is conducted to iron-containing particles adhered to a surface of the glass as a pre-step, and the glass is then chemically strengthened. The oxidation treatment is a heat treatment conducted at 80-400° C. in the air. A glass substrate for an information recording medium is obtained by the method.Type: GrantFiled: March 27, 2003Date of Patent: August 26, 2008Assignee: Hoya CorporationInventors: Yuriko Kudoh, Kazuishi Mitani, Yasuhiro Saito
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Publication number: 20080141724Abstract: In general, in one aspect, the invention features a method that includes exposing a surface to a first gas composition under conditions sufficient to deposit a layer of a first chalcogenide glass on the surface, and exposing the layer of the first chalcogenide glass to a second gas composition under conditions sufficient to deposit a layer of a second glass on the layer of the first chalcogenide glass, wherein the second glass is different from the first chalcogenide glass.Type: ApplicationFiled: June 8, 2007Publication date: June 19, 2008Applicant: OMNIGUIDE, INC.Inventor: Vladimir Fuflyigin
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Publication number: 20080022721Abstract: This invention relates to a method of making glass. In certain example embodiments, a major surface(s) of the glass is treated with aluminum chloride (e.g., AlCl3) at or just prior to the annealing lehr. The aluminum chloride treatment at or just prior to the annealing lehr, in either a float or patterned line glass making process, is advantageous in that it allows the treatment to be performed at a desirable glass temperature and permits exhaust functions in or proximate the annealing lehr to remove byproducts of the treatment in an efficient manner.Type: ApplicationFiled: July 25, 2006Publication date: January 31, 2008Inventors: Bernd Disteldorf, Anthony V. Longobardo, Keith McCrystal
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Patent number: 7312170Abstract: The present invention provides an optical synthetic quartz glass material which substantially does not cause changes in transmitted wave surface (TWS) by solarization, compaction (TWS delayed), rarefaction (TWS progressed) and photorefractive effect when ArF excimer laser irradiation is applied at a low energy density, e.g. at energy density per pulse of 0.3 mJ/cm2 or less. The present invention further provides a method for manufacturing the same. In order to solve the above-mentioned problems, the optical synthetic quartz glass material of the present invention is characterized in that, in a synthetic quartz glass prepared by a flame hydrolysis method using a silicon compound as a material, the followings are satisfied that the amount of SiOH is within a range of more than 10 ppm by weight to 400 ppm by weight, content of fluorine is 30 to 1000 ppm by weight, content of hydrogen is 0.Type: GrantFiled: March 3, 2004Date of Patent: December 25, 2007Assignees: Heraeus Quarzglas GmbH & Co. KG, Shin-Etsu Quartz Products Co., Ltd.Inventors: Hiroyuki Nishimura, Akira Fujinoki
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Publication number: 20070266733Abstract: The invention relates to a method for the manufacture of a lens of synthetic quartz glass with increased H2 content, in particular for a lens for an optical system with an operating wavelength of less than 250 nm, in particular less than 200 nm, with the steps: providing a precursor product of synthetic quartz glass, in particular with a first H2 content of less than 2·1015 molecules/cm3, with a circumferential border surface and two base surfaces lying on opposite sides, wherein at least one partial surface of at least one of said base surfaces has a curvature, and treating the precursor product in an H2-containing atmosphere in order to produce a precursor product of synthetic quartz glass with a second H2 content that is increased in relation to the first H2 content, in particular with a second H2 content of more than 1016 molecules/cm3, and measuring at least one optical property of said precursor product with said second H2 content.Type: ApplicationFiled: May 14, 2007Publication date: November 22, 2007Applicant: Carl Zeiss SMT AGInventor: Eric Eva
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Patent number: 7281394Abstract: In a method of manufacturing a glass substrate for an information recording medium including a step for chemically strengthening the glass substrate by contacting the glass substrate with chemical strengthening processing liquid containing chemical strengthening salt, concentration of Fe and Cr is 500 ppb or less in said chemical strengthening salt, respectively. The concentration may be detected by the use of an ICP (Inductively Coupled Plasma) emission spectrometry analyzing method or a fluorescent X-ray spectroscopy analyzing method.Type: GrantFiled: January 8, 2003Date of Patent: October 16, 2007Assignee: Hoya CorporationInventors: Hiroaki Ikeda, Masaru Suzuki, Kazuna Sasaki, Yumi Mukai, Jun Ozawa
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Patent number: 7226522Abstract: The present invention is directed to method of bonding mineral fibers in a mineral fiber material, according to which an acid is applied to the mineral fiber material in an amount sufficient to dissolve mineral material from the fiber to form a silica containing binder on the mineral fiber, and curing the mineral fiber material to bond the fibers.Type: GrantFiled: December 19, 2002Date of Patent: June 5, 2007Assignee: Paroc Oy ABInventors: Michael Perander, Jean Le Bell
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Patent number: 7197897Abstract: A salt mixture used for chemical strengthening of data recording disks is subjected to sub-micron filtration prior to use to remove certain impurities. Preferably, glass disks are chemically strengthened by ion exchange in a bath of molten sodium nitrate and potassium nitrate. A salt fresh mixture is prepared by starting with high-grade bulk salt in the intended proportions, melting the salt, and filtering the salt in a stainless steel filter, which is preferably approximately 2 micron or smaller. Filtration removes trace amounts of certain contaminants. The salt mixture thus prepared is then used for chemical strengthening of disks in the conventional manner.Type: GrantFiled: April 4, 2002Date of Patent: April 3, 2007Assignee: Hitachi Global Storage Technologies Netherlands B.V.Inventors: Nathan Ellis Jacobson, Terry Lee Jensen, Rick Allan Sprague
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Patent number: 7162894Abstract: The invention relates to the loading of quartz glass objects with hydrogen in an annealing process in a furnace for improving the homogeneity of the refractive index and the laser resistance while, at the same time, maintaining a specified stress birefringence of each of the glass objects. Initially, the distribution of the refractive index, the stress birefringence, the distribution of the hydrogen and the differences in refractive index, which are to the equalized, are determined in the respective glass object, after which the hydrogen change, which is necessary for equalizing the refractive index, is determined. Furthermore, the annealing temperature and its holding time, as well as the hydrogen concentration and the hydrogen pressure in the furnace are adjusted to achieve a sufficiently equalized distribution of refractive index.Type: GrantFiled: August 30, 2002Date of Patent: January 16, 2007Assignee: Schott GlasInventors: Rolf Martin, Gordon Von Der Goenna
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Patent number: 7104090Abstract: Polarizing glass articles and methods of manufacturing polarizing glass articles are disclosed. The method involves forming a polarizing layer on the surface of the glass article by ion-exchanging silver or copper into the surface.Type: GrantFiled: January 24, 2002Date of Patent: September 12, 2006Assignee: Corning IncorporatedInventors: Nicholas F. Borrelli, Donald M. Trotter, Jr.
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Patent number: 7093465Abstract: An object of the present invention is to overcome the problems of the prior art technique, and to provide a heat treatment method as well as a heat treatment apparatus capable of heat treating, with higher efficiency, a synthetic quartz glass for optical use having higher homogeneity and higher purity. Another object of the present invention is to provide and a synthetic quartz glass for optical use.Type: GrantFiled: May 31, 2001Date of Patent: August 22, 2006Assignees: Heraeus Quarzglas GmbH & Co. KG, Shin-Etsu quartz Products Co., Ltd.Inventors: Tetsuji Ueda, Hiroyuki Nishimura, Akira Fujinoki
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Patent number: 7013062Abstract: A material for temperature compensation consists of a sinter produced by baking any of crystalline powder, crystallized glass powder, and partially crystalline glass powder. The sinter has a negative coefficient of thermal expansion and contains anisotropic crystals in terms of thermal expansion.Type: GrantFiled: February 9, 2000Date of Patent: March 14, 2006Assignee: Nippon Electric Glass Co., Ltd.Inventors: Takahiro Matano, Akihiko Sakamoto
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Patent number: 6993934Abstract: Dental glass powders, methods for producing the powders and dental compositions including the glass powders. The powders preferably have a well-controlled particle size, narrow size distribution and a spherical morphology. The method includes forming the particles by a spray pyrolysis technique. The invention also includes dental filler and restorative compositions that include the glass powders.Type: GrantFiled: September 8, 2003Date of Patent: February 7, 2006Assignee: Cabot CorporationInventors: Toivo T. Kodas, Mark J. Hampden-Smith, Quint H. Powell, James H. Brewster, Daniel J. Skamser, Klaus Kunze, Paolina Atanassova, Paul Napolitano
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Patent number: 6992753Abstract: Radiation-induced damage to a lens material in a projection exposure system is reduced by selection of maximum design fluence values HD for lenses and at least one lens made of a material having a characteristic transition point TRC after exposure to a given amount of radiation, wherein, for instance, TRC<0.8. HD among other relationships and/or characteristics of the lenses.Type: GrantFiled: December 24, 2003Date of Patent: January 31, 2006Assignee: Carl Zeiss SMT AGInventors: Daniel Krähmer, Eric Eva
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Patent number: 6946030Abstract: A silica glass crucible is produced by a) providing a porous amorphous silica glass green body, which is infiltrated with at least one substance that promotes crystallization of a silica glass crucible, b) drying the infiltrated silica glass green body, c) filling the green body with a metal or semimetal, and d) heating the filled green body for a period of from 1 h to 1000 h to a temperature of from 900 to 2000° C. to form at least a portion of silica crystalline phase. The process may be continued by further heating to melt the metal or semimetal and pulling a single crystal from the melt.Type: GrantFiled: November 12, 2002Date of Patent: September 20, 2005Assignee: Wacker-Chemie GmbHInventors: Fritz Schwertfeger, Holger Szillat, Christoph Frey, Ulrich Lambert, Axel Frauenknecht