Abstract: A method for isolating a nanoparticle is disclosed. A medium containing a nanoparticle is provided. The medium is acidified with a weak acid. An alcoholic solvent is added to induce the nanoparticle to precipitate from the medium. The precipitated nanoparticles are separated from the medium.

Abstract: Provided is a nanowire manufacturing method, comprising forming a plurality of grid patterns on a substrate, forming a nanowire on the grid patterns, and separating the grid pattern and the nanowire. According to the present invention, the width and height of the nanowire can be adjusted by controlling the wet-etching process time period, and the nanowire can be manufactured at a room temperature at low cost, the nanowire can be mass-manufactured and the nanowire with regularity can be manufactured even in case of mass production.

Abstract: Disclosed is a method of producing low oxygen-content molybdenum powders by reducing molybdenum trioxide, which includes charging a first reducing agent and the molybdenum trioxide, which are in the direct contact with each other on a micro-sieve on an upper portion of a bracket in a body, charging a second reducing agent in the bracket under the micro-sieve, coupling the body with a cover to close the body, and performing a reduction reaction by raising an internal temperature of the body by performing the first reduction reaction due to direct contact between the first reducing agent and the molybdenum trioxide, and performing the second reduction reaction due to evaporation of the second reducing agent. The first and second reduction reactions are performed at a temperature in a range of 550° C. to 650° C., and a temperature in a range of 1000° C. to 1200° C., respectively.

Abstract: A metron refers to a molecule which contains a pre-defined number of high affinity binding sites for metal ions. Metrons may be used to prepare homogenous populations of nanoparticles each composed of a same, specific number of atoms, wherein each particle has the same size ranging from 2 atoms to about ten nanometers.

Abstract: A process for synthesizing metal submicron and nano-scale powders for use in articles of manufacture. In a suitable reactor, single metal or multiple metal complexes are heated to a temperature whereby, upon contact with hydrogen gas, an exothermic reaction begins. The further temperature rise in response to the exothermic reaction is minimized by reducing the external heat input, thereby minimizing the agglomeration or sintering of the metal nano-scale particles resulting from the process. Preferably, after drawing a vacuum on the metal complexes in the reactor, the hydrogen is introduced at about, equal to or below ambient pressure and the reaction is purposely made slow to prevent agglomeration or sintering.

Abstract: Methods of preparing nanowires by reducing metal cations are disclosed and claimed, where the metal cation reduction occurs in at least two stages. Such methods can exhibit improved reproducibility and reduced variability. The product nanowires are useful in, for example, electronics applications.

Abstract: An object of the present invention is to provide a method for producing an alloy recycled material by effectively removing carbon from a carbon-containing alloy, which is produced as scrap or sludge of an R—Fe—B based permanent magnet, a used magnet, or the like. The method of the present invention as a means for resolution is characterized in that a carbon-containing R—Fe—B based permanent magnet alloy is subjected to an HDDR treatment to remove carbon. An alloy recycled material produced by the method of the present invention contains a reduced amount of carbon. Therefore, in the case where it is recycled for the production of a magnet, even when an increased amount is subjected to high-frequency heating in a vacuum melting furnace, a non-negligible increase in the amount of carbon contained in the produced magnet can be avoided.

Abstract: [OBJECT] A composition of a metal nanoparticle is provided in which reproducibility in a method of producing a metal film with excellent low-temperature sinterable properties is improved. An article using the metal nanoparticle composition is also provided. [SOLVING MEANS] A composition of a metal nanoparticle that has a secondary aggregation diameter (median diameter) of 2.0 ?m or less as determined by disk centrifugal-type particle size measurement is used.

Abstract: A method of forming monodispersed metal nanowires comprising: forming a reaction mixture including a metal salt, a capping agent and a quaternary ammonium chloride in a reducing solvent at a first temperature; and forming metal nanowires by reducing the metal salt in the reaction mixture.

Abstract: A method for removing a surfactant from a palladium nanoparticle includes exposing the palladium nanoparticle to hydrogen and removing the surfactant from the palladium nanoparticle. A method includes synthesizing a palladium nanoparticle using a surfactant. The surfactant influences a geometric property of the palladium nanoparticle and bonds to the palladium nanoparticle. The method also includes exposing the palladium nanoparticle to hydrogen to remove the surfactant from the palladium nanoparticle.

Abstract: The invention provides a method for coating fluidic channels, particularly millifluidic channels, with a catalyst coating having controlled dimensions and morphology, and methods for preparing such channels, and devices that can be used in combination with the channels. The invention further provides portable, hand-held millifluidic devices applicable for a wide variety of uses including molecular reduction reactions, in situ material characterization, in situ reaction catalysis characterization, in situ reaction mechanism characterization, nanomaterial synthesis, nanostructured metal and metal oxide growth and coating of channels, continuous flow cell culturing, enzymatic catalysis, biomolecular catalysis, combinatorial chemistry, reactions involving homogeneous catalysts bound to channel walls, peptide synthesis, nucleic acid synthesis, synthesis of pharmaceutical intermediates, biofunctionalization of nanomaterials or a combination thereof.

Abstract: The present invention provides a process for preparing a tantalum powder with high specific capacity, which process comprising the steps of, in sequence, (1) a first reduction step: mixing tantalum oxide powder and a first reducing agent powder homogenously, and then carrying out reduction reaction in hydrogen and/or inert gas or vacuum atmosphere to obtain a tantalum suboxides powder; (2) a second reduction step: mixing the tantalum suboxides powder obtained from the step (1), in which impurities have been removed, and a second reducing agent powder homogenously, and then carrying out reduction reaction in hydrogen and/or inert gas or vacuum atmosphere to obtain a tantalum powder having high oxygen content; (3) a third reduction step: mixing the tantalum powder having high oxygen content obtained from the step (2), in which impurities have been removed, with a third reducing agent powder homogenously, and then carrying out reduction reaction in hydrogen and/or inert gas or vacuum atmosphere to obtain a tanta

Abstract: The present invention relates to a continuous reactor a method for manufacturing nanoparticles. The reactor of the present invention includes: a plurality of first inputs for individually inputting a plurality of reagents; a first mixing part connected to the first inputs to mix the reagents; N number of first reaction units, each comprising a plurality of first diverging channels and a first converging channel to form a channel having the first diverging channels and the first converging channels alternately connected to one another in series for N times of diverging-converging actions, wherein N?1, and the first diverging channels of a 1st one of the first reaction units are connected to the first mixing part; and a first output connected to the first converging channel of an Nth one of the first reaction units, so as to output a product of nanoparticles.

Abstract: There are provided a nickel powder for an internal electrode, synthesized by a vapor phase synthesis method using plasma, more particularly, a nickel powder for an internal electrode, having a favorable crystallite diameter and high density, a method of producing the same, and a multilayer ceramic electronic component including the same. According to the nickel powder for an internal electrode, the method of producing the same, and the multilayer ceramic electronic component including the same, a nickel powder having less impurities, a favorable crystallite diameter, and high density can be produced.

Abstract: The invention relates to a process for producing sinterable molybdenum metal powder in a moving bed, sinterable molybdenum powder and its use.

Abstract: A device for manufacturing finely powdered spherical magnesium includes a gas compressor that compresses argon gas, a gas heating unit that heats the compressed argon gas, and a tundish that receives molten magnesium. The device further includes a reactor having a nozzle injection unit that injects heated argon gas into the reactor, a recovery unit that recovers magnesium powder produced in the reactor, and a first gas cooler that cools the argon gas passing through the recovery unit. The device further includes a filtering unit that filters the cooled argon gas, a buffer tank that receives the filtered argon gas, and a compression blower that adiabatically compresses the argon gas. The device further includes a second gas cooler that cools the compressed argon gas, an adiabatic expansion duct that adiabatically expands the cooled argon gas, supplies the expanded argon gas to the reactor, and cools the magnesium powder.

Abstract: A producing method includes a preparing step of preparing a chemical compound having at least one of elements of alkali metals and alkali earth metals along with platinum, and a reducing step of reducing the prepared chemical compound with a reducing agent to form platinum nanoparticles.

Abstract: A method for the production of iron from an iron oxide-containing material includes contacting an iron oxide-containing material with a particle size distribution range with a ?90 of less than 2 mm, with a carbon-containing material with a particle size distribution range with a ?90 of less than 6 mm, in a commercial scale reactor at a temperature of between 900° C. and 1200° C. for a contact time sufficient to reduce the iron oxide to iron.

Abstract: Embodiments disclosed herein relate to a method for synthesizing self-assembling nanoparticles with defined plasmon resonances. More particularly, certain embodiments disclosed herein relate to an improved method for synthesizing self-assembling gold/gold sulfide nanoparticles by dialyzing samples during the self-assembly process.

Abstract: A method for preparing semiconductor nanocrystals is disclosed. The method comprises adding a precursor mixture comprising one or more cation precursors, one or more anion precursors, and one or more amines to a ligand mixture including one or more acids, one or more phenol compounds, and a solvent to form a reaction mixture, wherein the molar ratio of (the one or more phenol compounds plus the one or more acids plus the one or more amine compounds) to the one or more cations initially included in the reaction mixture is greater than or equal to about 6, and heating the reaction mixture at a temperature and for a period of time sufficient to produce semiconductor nanocrystals having a predetermined composition. Methods for forming a buffer layer and/or an overcoating layer thereover are also disclosed. Semiconductor nanocrystals and compositions including semiconductor nanocrystals of the invention are also disclosed.

Abstract: Provided is a method for producing Ag nanowires, including, heating a precursor solution that includes: an Ag salt; a water-soluble polymer; a surfactant, or a halide of metal ions having a standard reduction potential of ?0.1 to ?0.9V as a metal catalyst; and a reduction solvent, to produce the Ag nanowires. According to this method, a time for synthesizing nanowires may be considerably decreased, and an amount of Ag precursor discarded without reaction may be effectively reduced. As a result, the Ag nanowires may be produced with high efficiency and mass-production thereof through a simple scale-up may be successfully achieved.

Abstract: The present invention discloses a method for recovering rare earth particulate material from an assembly comprising a rare earth magnet and comprises the steps of exposing the assembly to hydrogen gas to effect hydrogen decrepitation of the rare earth magnet to produce a rare earth particulate material, and separating the rare earth particulate material from the rest of the assembly. The invention also resides in an apparatus for separating rare earth particulate material from an assembly comprising a rare earth magnet. The apparatus comprises a reaction vessel having an opening which can be closed to form a gas-tight seal, a separator for separating the rare earth particulate material from the assembly, and a collector for collecting the rare earth particulate material. The reaction vessel is connected to a vacuum pump and a gas control system, and the gas control system controls the supply of hydrogen gas to the reaction vessel.

Abstract: Provided are fine coated copper particles, which are fine with a narrow particle size distribution and superior storability, and which can be sintered at low temperatures. Specifically provided is a method for producing fine coated copper particles which is characterized by including: a step of mixing a copper-containing compound and a reducing compound to form a composite compound that is capable of thermal decomposition to generate copper in an alkylamine; and a step of heating the composite compound in the alkylamine to produce fine copper particles coated with the alkylamine.

Abstract: Copper nanostructures with relatively small dimensions and method for producing such structures are discloses. The ratios of the various reaction products may be adjusted to produce pentagonal nanowires and other structures such as tadpole shaped nanowires, nanocubes or pentagonal bi-pyramids.

Abstract: The present invention relates to a process for forming cobalt nanoparticles and coating them with copper or copper oxide, in which process a copper salt is mixed to a cobalt salt so that the formed salt mixture obtains a cobalt:copper ratio of >1:1, and a reduction is carried out with a reducing gas, whereby nanoparticles are formed while a coating is formed onto their surface.

Abstract: A method of making a nanoscale metallic powder is disclosed. The method includes providing a base material comprising a metallic compound, wherein the base material is configured for chemical reduction by a reductant to form a metallic material. The method also includes forming a powder of the base material, the powder comprising a plurality of powder particles, the powder particles having an average particle size that is less than about 1 micron. The method further includes disposing the powder particles into a reactor together with the reductant under an environmental condition that promotes the chemical reduction of the base material and formation of a plurality of particles of the metallic material.

Abstract: The present invention is directed to a method for producing novel metal nanoparticles and nanomaterials. The method involves mixing one or more metal halide starting materials, one or more lithium reducing agent and one or more solvents. In an exemplary embodiment, the resultant metal nanoparticles are substantially free from impurities and have a novel porous and substantially hollow structure.

Abstract: Disclosed is an iron-based soft magnetic powder obtained by preparing an iron-oxide-based soft magnetic powder through water atomization, and thermally reducing the iron-oxide-based soft magnetic powder. The iron-based soft magnetic powder has an average particle size of 100 ?m or more and has an interface density of more than 0 ?m?1 and less than or equal to 2.6×10?2 ?m?1, where the interface density is determined from a cross-sectional area (?m2) and a cross-sectional circumference (?m) of the iron-based soft magnetic powder. The iron-based soft magnetic powder obtained by preparing an iron-oxide-based soft magnetic powder through water atomization and thermally reducing the iron-oxide-based soft magnetic powder, when used for the production of a dust core, can give a dust core having a low coercive force. Also disclosed is a duct core having a low coercive force and exhibiting superior magnetic properties.

Abstract: A method of fabricating copper nanoparticles includes heating a copper salt solution that includes a copper salt, an N,N-dialkylethylenediamine, and a C6-C18 alkylamine in an organic solvent to a temperature between about 30° C. to about 50° C.; heating a reducing agent solution that includes a reducing agent, an N,N-dialkylethylenediamine, and a C6-C18 alkylamine in an organic solvent to a temperature between about 30° C. to about 50° C.; and adding the heated copper salt solution to the heated reducing agent solution, thereby producing copper nanoparticles. A composition includes copper nanoparticles, a C6-C18 alkylamine and an N,N?-dialkylethylenediamine ligand. Such copper nanoparticles in this composition have a fusion temperature between about 100° C. to about 200° C. A surfactant system for the stabilizing copper nanoparticles includes an N,N?-dialkylethylenediamine and a C6-C18 alkylamine.

Abstract: A method for producing a matrix containing nanostructures. The method includes obtaining a layer having a thickness of 10 nm-100 ?m, wherein the layer contains organic macromolecules arranged in a nanopattern, staining the layer with a solution containing a salt so that a portion of the salt is retained in the layer, and removing the organic mcaromolecules from the layer to form a matrix containing nanostructures. Also within the scope of this invention are nanostructures prepared by this method.

Abstract: A method for manufacturing metal nano particles having a hollow structure is provided. First, a suitable reducing agent is added into a first metal salt solution, and first metal ions are reduced to form first metal nano particles. Next, after the reducing agent is decomposed, a second metal salt solution with a higher reduction potential than that of the first metal is added. Then, the first metal particles are oxidized to form first metal ions when the second metal ions are reduced on the surface of the first metal by electrochemical oxidation reduction reaction, and thus, second metal nano particles having a hollow structure and a larger surface area are obtained. The method is simple and the metal nano particles with uniform particle size are obtained by this method.

Abstract: Processes for producing carboxylic acid-stabilized silver nanoparticles are disclosed. The processes comprise (a) forming a suspension of silver salt particles in a carboxylic acid; (b) forming a solution of an organohydrazine and a first organic solvent; (c) heating the suspension; (d) adding the solution to the suspension to form a mixture; and (e) reacting the mixture to form carboxylic acid-stabilized silver nanoparticles.

Abstract: Process for the production of a powdered spherical tungstic acid by acidification of an aqueous alkaline tungstate solution with mineral acid at elevated temperature, preferably in a continuous stirred tank or a cascade of at least 2 continuous stirred tanks, and tungstic acid obtainable in this way, which is characterized by a high bulk density and spherical morphology.

Abstract: A method of forming monodispersed metal nanowires comprising: forming a reaction mixture including a metal salt, a capping agent and a quaternary ammonium chloride in a reducing solvent at a first temperature; and forming metal nanowires by reducing the metal salt in the reaction mixture.

Abstract: The present invention relates to a process for preparing uniform silver nanoparticles. In particular, the present invention is directed to a process for preparing silver nanoparticles comprising: (i) heating a mixture of a silver precursor and a surfactant under inert atmosphere to prepare silver nanoparticles; and (ii) separating the silver nanoparticles from the reaction products of the step (i).

Abstract: Low temperature gas-phase methods for the preparation of faceted aluminum crystals are disclosed.

Abstract: The invention provides a pollution-free reuse method for iron-based grinding waste, involving the technology of recycling economy, with special reference to the metallurgical industry, iron-based grinding waste green recycling technology. The present invention of the iron grinding waste recycling and reuse methods includes degreasing, heat treatment, sieving, matching, and obtains iron-based alloyed powders, which can be used in SHS lined steel pipe, powder metallurgy structural component, magnetic grinding, thermal spray. More than 95% iron-based alloyed powders can be recycled from wide source of iron-based grinding waste. The invention has the advantage of low cost, no secondary pollution and wide application.

Abstract: A process for production of titanium alloy material has steps of hydrogenating titanium alloy material to generate hydrogenated titanium alloy; grinding, sifting and dehydrogenating the hydrogenated titanium alloy powder to generate titanium alloy powder; adding at least one of copper powder, chromium powder or iron powder to obtain titanium alloy complex powder; consolidating the titanium alloy complex powder by CIP process and subsequent HIP process, or by HIP process after filling the titanium alloy complex powder into a capsule. In addition, titanium alloy complex powder and titanium alloy material produced by the process are provided.

Abstract: A process comprising: (a) preparing a reaction mixture comprising a silver salt, the reducing agent comprising a hydrazine compound, a thermally removable stabilizer, and an optional solvent, to form a plurality of silver-containing nanoparticles with molecules of the stabilizer on the surface of the silver-containing nanoparticles, wherein the reaction mixture generates an acid; and (b) removing the acid to produce the silver-containing nanoparticles substantially free of acid.

Abstract: A powder processing method includes degassing a metallic powder in a rotating chamber that is evacuated to a sub-atmospheric pressure. The method may also include storing the metallic powder in a rotating storage chamber that is pressurized to a super-atmospheric pressure with a dry cover gas.

Abstract: A method of synthesis to produce gram-scale quantities of copper nanowires in an aqueous solution, wherein the copper nanowires are dispersed in said solution. Copper nanowires grow from spherical copper nanoparticles within the first 5 minutes of the reaction. Copper nanowires can be collected from solution and printed to make conductive films (preferably <10,000 ?/sq) that preferably transmit greater than 60% of visible light.

Abstract: A porous tin particle and its preparation method are provided in the present invention. The method includes steps of: (a) performing a reductive (or reductive electrochemical) reaction on a tin particle which simultaneously reacts with lithium ions to form a tin-lithium (Sn—Li) alloy; and (b) performing an oxidative (or oxidative electrochemical) reaction on Sn—Li alloy to release the lithium ions therefrom, and the porous tin particle is formed. The porous tin particle could be further applied in manufacturing the electrochemical electrode for lithium-ion battery with longer cycle life and higher reversibility.

Abstract: Methods of preparing nanowires, compositions, and articles are disclosed. Such methods can provide thin nanowires with reduced nanoparticle contamination. Compositions and articles comprising such nanowires are useful in electronics applications.

Abstract: A method for manufacturing a hollow metal sphere with a mesoporous structure is disclosed, which comprises the following steps: (A) providing a hollow sphere template with a mesoporous structure, wherein the hollow sphere template comprises: a first shell with plural channels penetrating the first shell, the material of the first shell comprises a mesoporous silica material, and the mesoporous silica material has a cubic Ia3d symmetry pore structure; (B) mixing the hollow sphere template with a metal precursor; (C) reducing the metal precursor; and (D) removing the hollow sphere template to obtain a hollow metal sphere with a mesoporous structure. In addition, the present invention also provides a hollow metal sphere with a mesoporous structure prepared by the aforementioned method.

Abstract: Branched nanowire preparation methods, compositions, and articles are disclosed. Such branched nanowires are useful for electronics and optical applications.

Abstract: Nanowire preparation methods, compositions, and articles are disclosed. Such methods which reduce metal ions to metal nanowires in the presence complexes comprising metal-metal bonds, are capable of producing long, narrow, nanowires useful for electronics and optical applications.

Abstract: Methods of preparing metal nanowire are disclosed that employ quaternary phosphonium salts. Such processes can produce long and thin nanowires. Compositions and articles comprising such nanowires are useful in electronics applications.

Abstract: Nanowire preparation methods, compositions, and articles are disclosed. Such methods, which reduce metal ions to metal nanowires in the presence of zero-valent metal atoms, are capable of producing long, narrow, nanowires useful for electronics and optical applications.

Abstract: Methods for preparing metal nanowires in the presence of IUPAC Group 15 ions are disclosed. Such methods are capable of producing high aspect ratio nanowires that are suitable for electronics applications.

Abstract: Methods of preparing nanowires having small diameters and large lengths are disclosed. Such nanowires are useful in electronics applications.