Producing Or Purifying Free Metal Powder Or Producing Or Purifying Alloys In Powder Form (i.e., Named Or Of Size Up To 1,000 Microns In Its Largest Dimension) Patents (Class 75/343)
  • Patent number: 7988761
    Abstract: The present invention relates to a method for manufacturing metal nanoparticles containing rod-shaped nanoparticles, the method including: producing metal oxide nanoparticle intermediates having at least rod-shaped metal oxide nanoparticles by heating a mixture of a nonpolar solvent, a metal precursor and an amine including secondary amine at 60-300° C.; producing metal nanoparticles by adding a capping molecule and a reducing agent to the mixture and heating the result mixture at 90-150° C.; and recovering the metal nanoparticles. According to the present invention, the shape of metal nanoparticle can be controlled by mixing primary amines or secondary amines as proper ratio without using apparatus additionally, as well as, the size of metal nanoparticle can be controlled to several nm.
    Type: Grant
    Filed: November 28, 2007
    Date of Patent: August 2, 2011
    Assignee: Samsung Electro-Mechanics Co., Ltd.
    Inventors: Byung-Ho Jun, Jae-Woo Joung
  • Publication number: 20110179908
    Abstract: Nano-scale particles of materials can be produced by vaporizing material and allowing the material to flow in a non-violently turbulent manner into thermal communication with a cooling fluid, thereby forming small particles of the material that can be in the nano-scale size range. A raw material feeder can be configured to feed raw material toward a heater which vaporizes the raw material. The feeder can include a metering device for controlling the flow of raw material toward the heater. A gas source can also be used to cause gas to flow through a portion of the raw material feeder along with the raw material.
    Type: Application
    Filed: February 24, 2011
    Publication date: July 28, 2011
    Applicant: QUANTUMSPHERE, INC.
    Inventor: Ed Robinson
  • Publication number: 20110167961
    Abstract: It is possible to efficiently obtain a purified material from a material containing a metalloid element such as silicon or metal element as the main component, and an impurity. The method for purifying a material, comprising bringing a material containing a metalloid element or metal element as the main component, and an impurity into contact with a compound represented by the following formula (1): AlX3 ??(1) wherein X is a halogen atom; to remove the impurity from the material.
    Type: Application
    Filed: August 10, 2009
    Publication date: July 14, 2011
    Applicant: SUMITOMO CHEMICAL COMPANY, LIMITED
    Inventors: Kunio Saugusa, Hiroshi Tabuchi, Tomohiro Megumi
  • Patent number: 7976775
    Abstract: Disclosed is a binary aluminum alloy powder sintered material which comprises aluminum and iron, which has a completely crystalline microstructure comprising an aluminum matrix and an ?-Al phase and at least any one phase of an Al6Fe phase or an Al13Fe4 phase mixed in the aluminum matrix as nanocrystalline phases, and which has an extremely high strength and a well-balanced high ductility, though being free from any rare earth element.
    Type: Grant
    Filed: March 25, 2008
    Date of Patent: July 12, 2011
    Assignee: National Institute for Materials Science
    Inventors: Taisuke Sasaki, Kazuhiro Hono, Toshiji Mukai
  • Publication number: 20110162484
    Abstract: Integrated process, in which pure carbonyl iron powder (CIP) is prepared by decomposition of pure iron pentacarbonyl (IPC) in a plant A, carbon monoxide (CO) liberated in the decomposition of the IPC is used in plant A for the preparation of further CIP from iron or is fed to an associated plant B for the preparation of synthesis gas or is fed to an associated plant C for the preparation of hydrocarbons from synthesis gas, and the CIP prepared in plant A is used as catalyst or catalyst component in an associated plant C for the preparation of hydrocarbons from synthesis gas from plant B.
    Type: Application
    Filed: September 2, 2009
    Publication date: July 7, 2011
    Inventors: Jochen Steiner, Ekkehard Schwab, Andreas Keller, Otto Watzenberger, Ulrich Grässle, Manfred Julius
  • Patent number: 7967890
    Abstract: In various aspects provided are methods for producing a nanoparticle within a cross-linked, collapsed polymeric material. In various embodiments, the methods comprise (a) providing a shape-static polymer template with a size in the range between about 1 nm to about 100 nm; (b)) incorporating one or more nanoparticle precursor moieties with the shape-static polymer template; and either (c) oxidizing the precursor moieties to form a composite nanoparticle comprising one or more of an inorganic oxide and hydroxide nanoparticle; or (c) adding an ion with an opposite charge polarity to the at least one nanoparticle precursor moieties to effect formation of a composite nanoparticle.
    Type: Grant
    Filed: December 4, 2009
    Date of Patent: June 28, 2011
    Assignee: Vive Nano, Inc.
    Inventors: Darren Anderson, Jose Amado Dinglasan, Nikolai Loukine
  • Patent number: 7968008
    Abstract: Particles and particle films are provided. In certain examples, particles produced from a single phase process may be used to provide industrial scale synthesis of particles for use in devices such as printed wiring boards.
    Type: Grant
    Filed: August 3, 2006
    Date of Patent: June 28, 2011
    Assignee: Fry's Metals, Inc.
    Inventors: Sachin Parashar, Siuli Sarkar, Oscar Khaselev, Brian G. Lewis, Michael T. Marczi, Bawa Singh, Nitin Desai, Michael Liberatore
  • Patent number: 7964172
    Abstract: A method for synthesis of high surface-area (>100 m2/g) and nanosized (?100 nm) silicon powder by initiation of self-sustained combustion reaction in a mixture of silicon dioxide and magnesium powders in a sealed reactor chamber under pressurized inert gas atmosphere. A specific feature of the method is rapid cooling of the product at a rate of 100 K/s to 400 K/s in the area directly behind the combustion front.
    Type: Grant
    Filed: October 13, 2009
    Date of Patent: June 21, 2011
    Inventors: Alexander Mukasyan, Vasiliy Mukasyan, Mikael Nersesyan
  • Patent number: 7964013
    Abstract: Disclosed herein are methods and processes for making FeRh/FePt nanostructures and the use of these FeRh—FePt nanostructures as a magnetic recording media.
    Type: Grant
    Filed: June 18, 2009
    Date of Patent: June 21, 2011
    Assignee: University of Louisiana at Lafayette
    Inventor: Devesh Kumar Misra
  • Publication number: 20110132144
    Abstract: The invention relates to a process for the preparation of metal nanoparticles, selected from the group consisting of lead, bismuth, zinc, antimony, indium, gold, nickel, cobalt, palladium, platinum, iridium, osmium, rhodium, ruthenium, rhenium, vanadium, chromium, manganese, niobium, molybdenum, tungsten, tantalum, cadmium, silver and/or copper, on a rotating body, characterized in that a reduction of corresponding metal salts, corresponding metal salt complexes, corresponding metal hydroxides and/or corresponding metal oxides by polyols having a number of hydroxyl groups in the polyol of 1 to 10 and a molecular weight of the polyols of 2000 to 18 000 Da is effected.
    Type: Application
    Filed: July 15, 2009
    Publication date: June 9, 2011
    Inventors: Jochen Mezger, Laurent Marc, Simone Klapdohr, Burkhard Walther, Zhizhong Cai, Tobias Austermann, Silke Flakus, Helmut Mack
  • Patent number: 7931855
    Abstract: A method of reducing the oxygen content of a powder is provided. A canister is prepared with a getter, filled with the powder to be densified, sealed and evacuated. The canister is subjected to a hydrogen atmosphere at an elevated temperature whereby hydrogen diffuses into the canister through the walls thereof. The hydrogen forms moisture when reacted with the oxygen of the powder and the moisture in the reacted with the getter in order to remove oxygen from the powder to the getter. The atmosphere outside the canister is then altered to an inert atmosphere or vacuum, whereby hydrogen diffuses out of the canister. A dense body having a controlled amount of oxygen can thereafter be produced by conventional powder metallurgy techniques.
    Type: Grant
    Filed: October 6, 2005
    Date of Patent: April 26, 2011
    Inventors: Roger Berglund, Hans Eriksson, Johan Sundstrom, Per Arvidsson
  • Publication number: 20110088511
    Abstract: The various embodiments herein provide method of producing a rod-shape and branched metal nano-structures with polyol compounds as a reducing agent. The metal nano-structures are produced in a closed chamber of microwave system with variable irradiation power at a designed temperature. The metal nano-structures produced exhibits localized plasmon-polariton resonance, exhibit spectral resonance positions at microwave or radio frequencies and exhibit multiple spectral resonance peak at microwave or radio frequencies. The metal nano-structures produced are suitable as a coating composition material, a coating, a film, a wiring material, an electrode material, a catalyst, a colorant, a cosmetic, a near-infrared absorber, an anti-counterfeit ink and an electromagnetic shielding material, a surface enhanced fluorescent sensor, a biomarker and a nano-waveguide.
    Type: Application
    Filed: August 28, 2010
    Publication date: April 21, 2011
    Inventors: Ghanavi Jalaledin, Mostafavi Mehrnaz
  • Publication number: 20110067527
    Abstract: Process for the production of valve metal powders, in particular niobium and tantalum powder, by reduction of corresponding valve metal oxide powders by means of vaporous reducing metals and/or hydrides thereof, preferably in the presence of an inert carrier gas, wherein the reduction is performed at a vapour partial pressure of the reducing metal/metal hydride of 5 to 110 hPa and an overall pressure of less than 1000 hPa, and tantalum powder obtainable in this way having a high stability of the powder agglomerate particles.
    Type: Application
    Filed: October 22, 2010
    Publication date: March 24, 2011
    Applicants: H. C. Starck GmbH, H. C. Starck Ltd.
    Inventors: Helmut HAAS, Ulrich BARTMANN, Tadashi KOMEYA, Nobuyuki SATO
  • Patent number: 7909907
    Abstract: A system and method for high volume production of nanoparticles, nanotubes, and items incorporating nanoparticles and nanotubes. Microwave, radio frequency, or infrared energy vaporizes a metal catalyst which, as it condenses, is contacted by carbon or other elements such as silicon, germanium, or boron to form agglomerates. The agglomerates may be annealed to accelerate the production of nanotubes. Magnetic or electric fields may be used to align the nanotubes during their production. The nanotubes may be separated from the production byproducts in aligned or non-aligned configurations. The agglomerates may be formed directly into tools, optionally in compositions that incorporate other materials such as abrasives, binders, carbon-carbon composites, and cermets.
    Type: Grant
    Filed: September 2, 2009
    Date of Patent: March 22, 2011
    Assignee: Babcock & Wilcox Technical Services Y-12, LLC
    Inventors: Edward B. Ripley, Jonathan S. Morrell, Roland D. Seals, Gerald M. Ludtka
  • Publication number: 20110059233
    Abstract: A process for preparing stabilized metal nanoparticles, the process comprising reacting a metal compound with a reducing agent in the presence of a stabilizer in a reaction mixture comprising the metal compound, the reducing agent, and the stabilizer, wherein the reaction mixture is substantially free of solvent, to form a plurality of metal-containing nanoparticles during the solvent-free reduction process with molecules of the stabilizer on the surface of the metal-containing nanoparticles.
    Type: Application
    Filed: September 4, 2009
    Publication date: March 10, 2011
    Applicant: XEROX CORPORATION
    Inventors: Ping Liu, Yiliang Wu, Nan-Xing Hu
  • Publication number: 20110020661
    Abstract: The invention relates to a Fe—Si—La alloy having the following atomic composition: (La1-a-a?MmaTRa?)1[(Fe1-b-b,CobMb,)1-x(Si1-cXc)x]13(CdNeH1-d-e)y(R)r(I)r, in which Mm is a mixture of lanthanum, cerium, neodymium and praseodymium in a weight proportion of 22 to 26% of La, 48 to 53% of Ce, 17 to 20% of Nd and 5 to 7% of Pr, wherein said mixture may include up to 1 wt % of impurities, TR is one or more elements of the rare earth family other than lanthanum, M is one or more d-type transition element from layers 3d, 4d and 5d, X is a metalloid element selected from Ge, Al, B, Ga and In, R is one or more element selected from Al, Ca, Mg, K and Na, I is one or two elements selected from O and S, with: 0?a<0.5 and 0?a?<0.2; 0?b?0.2 and 0?b?<0.4; 0?c?0.5 and 0?d?1; 0?e?1 and f?0.1; 0.09?x?0.13 and 0.002?y?4; 0.0001?z?0.01; the indicia b, d, e, x and y being such that the alloy further meets the following condition: 6.143b(13(1?x))+4.437y[1?0.0614(d++e)]?1 Eq.1 d*y?0.005 Eq.2.
    Type: Application
    Filed: December 15, 2008
    Publication date: January 27, 2011
    Applicants: ARCELORMITTAL-STAINLESS & NICKEL ALLOYS, CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
    Inventors: Thierry Waeckerle, Herve Fraisse, Mohamed Balli, Patricia De Rango, Daniel Fruchart, Damien Gignoux, Salvatore Miraglia, Mariana Rosca, Miguel Jose Artigas Alava
  • Publication number: 20110020663
    Abstract: The disclosure relates to metal reduction processes, which comprise adding a mixture comprising at least one metal-containing material, at least one reducing agent, and at least one additive into a reactor, heating the reactor to a selected reduction temperature, moving the mixture through the reactor while stirring the mixture, allowing a reduction period to occur, and obtaining a resulting composition comprising at least one zero-valent metal and a residue. The disclosure also relates to metallurgical processes comprising the metal reduction process, and products made by the metal reduction process. The disclosure further relates to metal reduction apparatuses, as well as metal reduction systems and metallurgical systems comprising the metal reduction apparatuses.
    Type: Application
    Filed: June 28, 2010
    Publication date: January 27, 2011
    Inventor: Bairong LI
  • Publication number: 20100326239
    Abstract: The present invention provides a process for preparing a tantalum powder with high specific capacity, which process comprising the steps of, in sequence, (1) a first reduction step: mixing tantalum oxide powder and a first reducing agent powder homogenously, and then carrying out reduction reaction in hydrogen and/or inert gas or vacuum atmosphere to obtain a tantalum suboxides powder; (2) a second reduction step: mixing the tantalum suboxides powder obtained from the step (1), in which impurities have been removed, and a second reducing agent powder homogenously, and then carrying out reduction reaction in hydrogen and/or inert gas or vacuum atmosphere to obtain a tantalum powder having high oxygen content; (3) a third reduction step: mixing the tantalum powder having high oxygen content obtained from the step (2), in which impurities have been removed, with a third reducing agent powder homogenously, and then carrying out reduction reaction in hydrogen and/or inert gas or vacuum atmosphere to obtain a tanta
    Type: Application
    Filed: June 18, 2010
    Publication date: December 30, 2010
    Applicant: Ningxia Orient Tantalum Industry Co., Ltd.
    Inventors: Wenfeng SHI, Xueqing Chen, Yong Li, Xudong Xi, Tao Guo
  • Publication number: 20100316882
    Abstract: Nanomaterial and methods for generating nanomaterial are described wherein a reaction, for example, decomposition, for generating nanomaterial occurs utilizing a hot wall reactor.
    Type: Application
    Filed: February 25, 2009
    Publication date: December 16, 2010
    Inventors: Andrey V. Filippov, Clinton Damon Osterhout, Martin Andrew Sala, Kamal Kishore Soni, Carlton Maurice Truesdale
  • Publication number: 20100307291
    Abstract: A method of recovering silver from a silver chloride mixture in which hydrogen gas is passed through the mixture to produce a metal chloride hydride which is then heated to dissociate the metal and to release hydrogen chloride gas.
    Type: Application
    Filed: December 9, 2008
    Publication date: December 9, 2010
    Inventors: Philippus Jacobus Mostert, Adalbert Prior
  • Patent number: 7846976
    Abstract: A process for producing metallic fine particles is provided by, the reduction of the metallic ions performed in two steps using two types of reducing agents which significantly differ in reducing ability thereof, in which a reducing agent in which the reduction ability is strong is used in the first reduction step, and a reducing agent in which the reduction ability is weak is used in the second reduction step, and the nano-sized metallic fine particles are produced. An aqueous metallic salt solution containing a surfactant is used and a two-step reduction is performed in the same vessel, in which as the reducing agent of the first reduction process, at least one selected from the group consisting of boron hydride, dimethylamine borane, hydrazine, and ascorbic acid is used, and as the reducing agent of the second reduction process, specific alkylamine or alkanolamine is used.
    Type: Grant
    Filed: December 8, 2005
    Date of Patent: December 7, 2010
    Assignees: Mitsubishi Materials Corporation, Dai Nippon Toryo Co., Ltd.
    Inventors: Daigou Mizoguchi, Yoshiaki Takata, Jun-etsu Satoh, Hiroki Hirata, Masato Murouchi
  • Patent number: 7842274
    Abstract: The invention is directed to a process for manufacture of fine precious metal containing particles, specifically silver-based particles and silver-based contact materials via an intermediate silver(+1)-oxide species. The process comprises in a first step the formation of a thermally instable silver (+1)-oxide species by adding a base to an aqueous silver salt solution comprising an organic dispersing agent. Due to the presence of the organic dispersing agent, the resulting silver (+1)-oxide species is thermally instable, thus the species is decomposing to metallic silver at temperature lower than 100° C. The process optionally may comprise the addition of a powdered compound selected from the group of inorganic oxides, metals, and carbon-based compounds. Furthermore the process may contain additional separating and drying steps. The process is versatile, cost efficient and environmentally friendly and is used for the manufacture of silver-based particles and electrical contact materials.
    Type: Grant
    Filed: March 31, 2006
    Date of Patent: November 30, 2010
    Assignee: Umicore, S.A.
    Inventors: Dan Goia, Sebastian Fritzsche, Bernd Kempf, Peter Braumann, Thierry Charles Simon Vandevelde
  • Patent number: 7828872
    Abstract: There is provided a process comprising mixing a divalent copper oxide with a reducing agent in the presence of a complexing agent and a protective colloid in a liquid medium to thereby produce copper microparticles without formation of a univalent copper oxide from the divalent copper oxide. Further, there is provided a process comprising reducing a divalent copper oxide in the presence of a complexing agent and a protective colloid, such as a protein, to thereby form metallic copper microparticles, adding a protective colloid scavenger, such as a protease, to thereby remove the protective colloid and effect agglomeration of metallic copper microparticles, and filtering the mixture by means of a pressure filter, a vacuum filter, a suction filter, etc.
    Type: Grant
    Filed: August 18, 2005
    Date of Patent: November 9, 2010
    Assignee: Ishihara Sangyo Kaisha, Ltd.
    Inventors: Masanori Tomonari, Masatoshi Honma, Yoshiyuki Kunifusa
  • Publication number: 20100272999
    Abstract: A method and a device are described for the production of metal powder or alloy powder of a moderate grain sizes less than 10 ?m, comprising or containing at least one of the reactive metals zirconium, titanium, or hafnium, by metallothermic reduction of oxides or halogenides of the cited reactive metals with the aid of a reducing metal, wherein said metal powder or alloy powder is phlegmatized by adding a passivating gas or gas mixture during and/or after the reduction of the oxides or halogenides and/or is phlegmatized by adding a passivating solid before the reduction of the oxides or halogenides, wherein both said reduction and also said phlegmatization are performed in a single gas-tight reaction vessel which can be evacuated.
    Type: Application
    Filed: January 8, 2009
    Publication date: October 28, 2010
    Inventor: Ulrich Gerhard Baudis
  • Publication number: 20100269634
    Abstract: A process for the production of metal nanoparticles. The process comprises a rapid mixing of a solution of at least about 0.1 mole of a metal compound that is capable of being reduced to a metal by a polyol with a heated solution of a polyol and a substance that is capable of being adsorbed on the nanoparticles.
    Type: Application
    Filed: July 2, 2010
    Publication date: October 28, 2010
    Applicant: CABOT CORPORATION
    Inventors: Karel Vanheusden, Klaus Kunze, Hyungrak Kim, Aaron D. Stump, Allen B. Schult, Mark J. Hampden-Smith, Chuck Edwards, Anthony R. James, James Caruso, Toivo T. Kodas, Scott Thomas Haubrich, Mark H. Kowalski
  • Publication number: 20100243579
    Abstract: This invention describes a process for producing a nanoscale zero-valent metal, including reduction of a metal ion solution with a dithionite compound, wherein the reduction is carried out under alkaline conditions under substantially an inert atmosphere. A nanoscale zero-valent metal obtainable by this process, and having a new crystalline form, is also described. The nanoscale zero-valent metal produced by the process of the invention is preferably iron, and is advantageously used for the remediation of contaminated water.
    Type: Application
    Filed: February 26, 2010
    Publication date: September 30, 2010
    Applicant: CRC for Waste Management and Pollution Control Limited
    Inventors: Andrew FEITZ, Jing GUAN, David WAITE
  • Publication number: 20100242679
    Abstract: The invention discloses a method for continuously fabricating silver nanowires. The method mixes a glycol solution of a silver salt and a glycol solution of a polyvinyl pyrrolidone, and the mixed solution reacts in a temperature range and a time range to form the silver nanowires. The polyvinyl pyrrolidone has high boiling point and reduction ability so as to reduce the silver salt to the silver nanoparticles, and simultaneously, the polyvinyl pyrrolidone can provide barriers for limiting the particle growth. Besides, the oxygen functional groups on the long chains of the polyvinyl pyrrolidone can keep the stably one-dimensional growth of the silver nanoparticles to form the silver nanowires during the aging process.
    Type: Application
    Filed: March 29, 2009
    Publication date: September 30, 2010
    Inventors: YI-HSIUAN YU, Bao-Yann Lin, Ming-Hsiung Wei, Cheng-En Shen, Lea-Hwung Leu, Kai-Yai Chang, Chen-Chim Ma
  • Patent number: 7799112
    Abstract: It is to propose a method of producing super-micro powders of pure metal-alloy in which cheap materials can be used and the production is efficient. In the production method of pure metal super-micro powder by heating a starting material containing a metal chloride and reducing the resulting vapor of the metal chloride with hydrogen gas, an elementary metal constituting the metal chloride is added to the starting material containing the metal chloride and a metal chloride having a large valence among metal chlorides having two or more valence is used as the metal chloride. Also, in the production method of alloy super-micro powder, a metal chloride is used as one to (number of all alloying components—1) alloying components in the starting material and an elemental metal is used as the other alloying component.
    Type: Grant
    Filed: November 5, 2003
    Date of Patent: September 21, 2010
    Assignees: Ishihara Chemical Co., Ltd., JFE Mineral Company, Ltd.
    Inventors: Yasunori Yonehana, Yoshinao Chisaki, Fumitaka Tsukihashi
  • Publication number: 20100227189
    Abstract: A method of synthesizing ligand-capped metal nanoparticles is disclosed and described. A method of synthesizing ligand-capped metal nanoparticles can comprise reacting a metal salt with 9-borabicyclo [3.3.1] nonane as a reducing agent in the presence of a capping ligand to form the ligand-capped metal nanoparticles. The method can be a single step approach which also significantly broadens choices for capping agents which can be readily incorporated during formation of the metal nanoparticles.
    Type: Application
    Filed: March 9, 2010
    Publication date: September 9, 2010
    Inventors: Jennifer S. Shumaker-Parry, Rajesh Sardar, Patrick M. Shem
  • Publication number: 20100212456
    Abstract: Disclosed is a method of manufacturing a composite ball for electronic parts by preparing a core ball with spherical shape, forming a solder-plated layer encompassing the core ball to obtain a composite ball, and then conducting a smoothing work on the surface of the solder-plated layer, therein the smoothing work is preferably conducted by bringing a medium into contact with the surface of the solder-plated layer.
    Type: Application
    Filed: February 18, 2010
    Publication date: August 26, 2010
    Applicants: HITACHI METALS, LTD., NEOMAX MATERIALS CO., Ltd.
    Inventor: Ken ASADA
  • Patent number: 7776129
    Abstract: An improved method of reducing a mixed metal oxide composition comprising oxides of nickel, cobalt, copper and iron in a hydrogen atmosphere to produce a mixture of the respective metals, the improvement wherein the atmosphere further comprises water vapour at a concentration, temperature and time to effect selective reduction of the oxides of nickel cobalt and copper relative to the iron oxide to produce the metallic mixture having a reduced ratio of metallic iron relative to metallic nickel, cobalt and copper.
    Type: Grant
    Filed: April 24, 2007
    Date of Patent: August 17, 2010
    Assignee: Chemical Vapour Metal Refining Inc.
    Inventors: Walter Curlook, Dmitri Terekhov, Sergiy Kovtun, Olujide Babatunde Olurin, Nanthakumar Victor Emmanuel
  • Publication number: 20100173170
    Abstract: A method of producing titanium metal from a titanium-containing material includes the steps of producing a solution of M?TiF6 from the titanium-containing material, selectively precipitating M?2TiF6 from the solution by the addition of (M?)aXb and using the selectively precipitated M?2TiF6 to produce titanium. M? is a cation of the type which forms a hexafluorotitanate, M? is selected from ammonium and the alkali metal cations, X is an anion selected from halide, sulphate, nitrite, acetate and nitrate and a and b are 1 or 2.
    Type: Application
    Filed: December 8, 2009
    Publication date: July 8, 2010
    Applicant: Peruke Investment Holdings (Proprietary) Limited
    Inventor: Gerard Pretorius
  • Publication number: 20100171072
    Abstract: A method for manufacturing granular metallic iron includes charging a raw-material mixture into a thermal reduction furnace, subjecting the raw-material mixture to thermal reduction to form metallic iron and slag as a by-product, causing metallic iron to coalesce into granules while separating metallic iron from slag, and cooling and solidifying metallic iron. The raw-material mixture contains at least Fe, Ca, Mg, Si, and an alkali metal as constituent elements in such a manner that the slag contains CaO, MgO, SiO2, and an alkali oxide, the alkali oxide is at least one selected from Li2O, Na2O, and K2O, the alkali oxide satisfies at least one of Li2O content?0.03%, Na2O content?0.10%, and K2O content?0.10%, and the basicity of the slag is in the range of 1.3 to 2.3. It is possible to manufacture high-quality granular metallic iron with good productivity by the method.
    Type: Application
    Filed: June 9, 2008
    Publication date: July 8, 2010
    Applicant: Kabushiki Kaisha Kobe Seiko Sho (Kobe Steel, Ltd.)
    Inventors: Takahiro Kudo, Kazutaka Kunii
  • Patent number: 7744954
    Abstract: A core/shell structured powder different in composition between the inside the particle and the surface thereof before sintering, so that it is possible to sinter the powder at lower temperature and give a core/shell structured powder having a shell portion uniform in thickness after sintering; a multilayered ceramic capacitor having a longer lifetime, by preparing the multilayered ceramic capacitor by using a powder having a core/shell structure different in composition between the inside the particle and the surface thereof before sintering; and a method of producing a powder by synthesizing particles in the liquid containing a raw material, wherein particles different in composition at least between the inside the particle and the surface thereof are obtained by adding a composition to be incorporated as a component of the particles to the liquid during the synthetic process so that the composition of the liquid changes continuously or intermittently.
    Type: Grant
    Filed: March 21, 2006
    Date of Patent: June 29, 2010
    Assignee: TDK Corporation
    Inventors: Yoshinori Fujikawa, Satoko Ueda, Kouji Tokita
  • Publication number: 20100158747
    Abstract: A process and system for producing tantalum or other valve metal particles is provided comprising forming tantalum particles in a reduction process carried out in a reactor vessel, and using a siphon to transfer fine tantalum particles out of the reaction mixture to a recovery vessel. This particle transfer can occur while the reaction mixture is agitated. The tantalum particles can be automatically withdrawn when the reaction mixture has a depth level greater than the fluid level of the tantalum fine particle recovery vessel, and outflow automatically stops when the fluid levels of the reactor and particle recovery vessel equilibrate. Tantalum or other valve metal powders made by the processes, and capacitors made with valve metal powders are also provided.
    Type: Application
    Filed: November 20, 2009
    Publication date: June 24, 2010
    Inventor: Hitoshi Iijima
  • Publication number: 20100150826
    Abstract: The present invention relates to hydrogen generating microporous metals, methods for preparing microporous metals, and methods for producing hydrogen from water using the metals and systems of the invention. In particular, microporous metals selected from the group comprising aluminum (Al), magnesium (Mg), silicon (Si), Iron (Fe) and zinc (Zn), capable of producing hydrogen upon reaction of the metal with water having a neutral pH are provided. Methods for preparing microporous metals comprising the steps of selecting a metal that is sufficiently electropositive (i.e. water reactive); and introducing microporosity in the selected metal by means of mechanical deformation, or metallurgical techniques, in order to generate the microporous metal are also provided, as is a method for producing hydrogen comprising reacting a microporous metal powder with water at a pH of between 4 and 10.
    Type: Application
    Filed: August 9, 2006
    Publication date: June 17, 2010
    Applicant: THE UNIVERSITY OF BRITISH COLUMBIA
    Inventors: Tomasz Troczynski, Edith Czech
  • Patent number: 7718094
    Abstract: A method for the formation of metallic nanoparticles, such as gold and silver nanoparticles, which involves, combining in a single solution, solvent, metal ions and copolymers under conditions such that metal nanoparticles are formed. The copolymers have both reducing components and stabilizing components. The method can be used to form metal nanoparticles having a desired shape and size.
    Type: Grant
    Filed: June 20, 2005
    Date of Patent: May 18, 2010
    Assignee: The Research Foundation of State University of New York
    Inventors: Paschalis Alexandridis, Toshio Sakai
  • Patent number: 7708910
    Abstract: The present invention relates to ink jet printing ink consisting of an independently dispersed metal ultrafine particles-containing liquid dispersion in which the metal ultrafine particles having a particle size of not more than 100 nm are independently and uniformly dispersed and which is excellent in characteristic properties required for ink. The ink is used in the printing or the formation of conductive circuits using an ink jet printer.
    Type: Grant
    Filed: October 21, 2001
    Date of Patent: May 4, 2010
    Assignee: ULVAC, Inc.
    Inventors: Noriyuki Abe, Masaaki Oda
  • Publication number: 20100101369
    Abstract: A two-phase reduction method for producing tantalum powder includes loading an unheated reaction vessel with a layer of K2TaF7, then a layer of solid sodium metal, and then followed by a layer of solid diluent salt. A first heating phase is used to promote the solid state reduction of the layer of K2TaF7, which results in the production of very fine tantalum particles while minimizing tantalum crystal growth. A second heating phase is then used to melt the contents of the reactor vessel and react primary quantities of sodium metal and K2TaF7 to produce tantalum powder. In certain embodiments, the fine tantalum particles produced during the first heating phase serve as the nucleation sites needed for tantalum crystal growth in the second heating phase.
    Type: Application
    Filed: October 27, 2008
    Publication date: April 29, 2010
    Applicant: Niotan, Inc.
    Inventor: John CRAWLEY
  • Publication number: 20100095806
    Abstract: Nano-scale particles of materials can be produced by vaporizing material and allowing the material to flow in a non-violently turbulent manner into thermal communication with a cooling fluid, thereby forming small particles of the material that can be in the nano-scale size range. A raw material feeder can be configured to feed raw material toward a heater which vaporizes the raw material. The feeder can include a metering device for controlling the flow of raw material toward the heater. A gas source can also be used to cause gas to flow through a portion of the raw material feeder along with the raw material.
    Type: Application
    Filed: November 2, 2006
    Publication date: April 22, 2010
    Inventor: Ed Robinson
  • Publication number: 20100077888
    Abstract: The present invention is directed to an iron powder commodity and to a process for producing such iron powder commodity comprising dehydrating and de-oiling hot strip mill (HSM) sludge within an inert gas atmosphere contained in a reaction chamber; venting and processing reaction chamber off-gas into a hydrocarbon product; discharging from the reaction chamber a dry de-oiled iron powder commodity that contains nanoparticle and ultrafine particle iron-bearing solids, and beneficiating the discharged iron powder commodity into particles of similar properties.
    Type: Application
    Filed: May 28, 2009
    Publication date: April 1, 2010
    Applicant: Recovery Technology, LP
    Inventor: John D. Lynn
  • Publication number: 20100064852
    Abstract: This invention relates to a method for purifying metal alloy and intermetallic powders. Particularly, the present invention relates to a method for the reduction or elimination of the content of the dissolved oxygen and to remove the metal oxide inclusions from metal alloy and intermetallic powders including the steps of: a) placing the metal in powder form into a reaction apparatus; b) introducing a suitable carrier substance to the metal powder; and c) introducing calcium vapour into the reaction apparatus to create a reaction between the metallic powder and calcium vapour thereby removing inclusions in the metal as shown in FIG. 11.
    Type: Application
    Filed: November 30, 2007
    Publication date: March 18, 2010
    Applicant: WaikatoLink Limited
    Inventor: Deliang Zhang
  • Patent number: 7677255
    Abstract: A method of making intermetallic nanoscale particles comprising iron aluminide and/or iron aluminum carbide comprising the steps of preparing a mixture of a solvent, an iron salt and LiAlH4, and heating the mixture to form the intermetallic nanoscale particles. The intermetallic nanoscale particles, which can comprise intermetallic nanoscale particles of iron aluminide and/or iron aluminum carbide in an alumina matrix, are capable of reducing the amount of 1,3-butadiene in the mainstream smoke of a cigarette.
    Type: Grant
    Filed: December 15, 2005
    Date of Patent: March 16, 2010
    Assignee: Philip Morris USA Inc.
    Inventors: Yezdi B. Pithawalla, Sarojini Deevi
  • Publication number: 20100031773
    Abstract: The present invention provides a compound powder for making magnetic powder cores, a kind of magnetic powder core, and a process for making them. Said compound powder is a mixture composing of powder A and powder B, the content of powder A is 50-96 wt. % and the content of powder B is 4-50 wt. %, wherein powder A is at least one selected from iron powder, Fe—Si powder, Fe—Si—Al powder, Fe-based nanocrystalline powder, Fe-based amorphous powder, Fe—Ni powder and Fe—Ni—Mo powder; powder B bears different requirement characteristics from powder A and is at least one selected from iron powder, Fe—Si powder, Fe—Si—Al powder, Fe-based nanocrystalline powder, Fe-based amorphous powder, Fe—Ni powder and Fe—Ni—Mo powder. Said powder B adopts Fe-based amorphous soft magnetic powder with good insulation property as insulating agent and thus core loss of magnetic powder core decreases.
    Type: Application
    Filed: October 19, 2009
    Publication date: February 11, 2010
    Inventors: Zhichao Lu, Deren Li, Shaoxiong Zhou, Caowei Lu, Feng Guo, Jianliang Li, Jun Wang, Tongchun Zhao, Liang Zhang
  • Publication number: 20100028678
    Abstract: A process for the production of a valve metal oxide powder, in particular an Nb2O5 or Ta2O5 powder by continuous reaction of a fluoride-containing valve metal compound with a base in the presence of water and calcination of the resultant product, wherein the reaction is performed in just one reaction vessel and at a temperature of at least 45° C. Valve metal oxide powders obtainable in said manner which exhibit a spherical morphology, a D50 value of 10 to 80 ?m and an elevated BET surface area.
    Type: Application
    Filed: August 18, 2009
    Publication date: February 4, 2010
    Applicant: H. C. Starck GmbH
    Inventors: Karsten Beck, Hady Seyeda, Klaus Lerch, Bianca Agnes Balan
  • Patent number: 7648554
    Abstract: The main object of the present invention is to manufacture, on an industrial scale, metal nanoparticles with excellent dispersion stability, and therefore provides metal nanoparticles containing a metal component, further containing at least one of phosphorus, nitrogen, and oxygen, and the average particle size being from 1 to 100 nm.
    Type: Grant
    Filed: August 1, 2003
    Date of Patent: January 19, 2010
    Assignees: Daiken Chemical Co., Ltd., Osaka Municipal Technical Research Institute
    Inventors: Masami Nakamoto, Mari Yamamoto, Akio Harada
  • Patent number: 7645318
    Abstract: In various aspects provided are methods for producing a nanoparticle within a cross-linked, collapsed polymeric material. In various embodiments, the methods comprise (a) providing a shape-static polymer template with a size in the range between about 1 nm to about 100 nm; (b)) incorporating one or more nanoparticle precursor moieties with the shape-static polymer template; and either (c) oxidizing the precursor moieties to form a composite nanoparticle comprising one or more of an inorganic oxide and hydroxide nanoparticle; or (c) adding an ion with an opposite charge polarity to the at least one nanoparticle precursor moieties to effect formation of a composite nanoparticle.
    Type: Grant
    Filed: May 7, 2008
    Date of Patent: January 12, 2010
    Assignee: Vive Nano, Inc.
    Inventors: Darren Anderson, Jose Amado Dinglasan, Nikolai Loukine
  • Publication number: 20090325795
    Abstract: A producing method includes a preparing step of preparing a chemical compound having at least one of elements of alkali metals and alkali earth metals along with platinum, and a reducing step of reducing the prepared chemical compound with a reducing agent to form platinum nanoparticles.
    Type: Application
    Filed: June 25, 2009
    Publication date: December 31, 2009
    Applicants: AISIN SEIKI KABUSHIKI KAISHA, Toyota Jidosha Kabushiki Kaisha, THE DOSHISHA
    Inventors: Takeshi Kamizono, Gang Xie, Minoru Inaba
  • Patent number: 7628840
    Abstract: Each of the metal nano-particles present in a dispersion, which comprises at least one metal selected from the group consisting of precious metals and transition metals or an alloy of at least two metals selected from the foregoing metals, comprises a metal particle in which an organic metal compound of a fatty acid and/or an amine-metal complex is adhered to the periphery of the metal particle. This organic metal compound and the amine-metal complex are admixed together in a solvent and then the resulting mixture is subjected to a reducing treatment to thus form a dispersion containing metal nano-particles in a concentration of not less than 5% by mass and not more than 90% by mass. The resulting dispersion is applied onto the surface of a base material, followed by drying the applied layer of the dispersion and then firing the dried layer of the dispersion at a low temperature to thus form a thin metallic wire or a metal film having conductivity.
    Type: Grant
    Filed: September 7, 2004
    Date of Patent: December 8, 2009
    Assignees: ULVAC, Inc., JEMCO, Inc.
    Inventors: Tsutomu Atsuki, Masaaki Oda, Toshiharu Hayashi, Reiko Kiyoshima
  • Publication number: 20090283726
    Abstract: A process for producing metallic fine particles is provided by, the reduction of the metallic ions performed in two steps using two types of reducing agents which significantly differ in reducing ability thereof, in which a reducing agent in which the reduction ability is strong is used in the first reduction step, and a reducing agent in which the reduction ability is weak is used in the second reduction step, and the nano-sized metallic fine particles are produced. An aqueous metallic salt solution containing a surfactant is used and a two-step reduction is performed in the same vessel, in which as the reducing agent of the first reduction process, at least one selected from the group consisting of boron hydride, dimethylamine borane, hydrazine, and ascorbic acid is used, and as the reducing agent of the second reduction process, specific alkylamine or alkanolamine is used.
    Type: Application
    Filed: December 8, 2005
    Publication date: November 19, 2009
    Applicants: Mitsubishi Materials Corporation, Dai Nippon Toryo Co., Ltd.
    Inventors: Daigou Mizoguchi, Yoshiaki Takata, Jun-etsu Satoh, Hiroki Hirata, Masato Murouchi