Abstract: There is disclosed a highly densified, sintered aluminum nitride body having a thermal conductivity in excess of 200 W/m.degree.K. and a strong resistance to attack by hot HC1. There is also disclosed a method of sintering aluminum nitride bodies which employs a variable thermal cycle whereby the body is either heated slowly through a pre-sintering temperature range of 1300.degree. to 1750.degree. C., or held at a temperature within that range for at least a half hour. Optionally, a green aluminum nitride body may be provided with up to 10% by weight of at least one metal fluoride dopant, and may be provided with a sufficient weight to maintain flatness during firing.

Abstract: The present invention is directed to a method for synthesizing fluorine-containing, aluminosilicate crystals having a stoichiometry approximating that of topaz. The method comprises three basic steps:(1) vapors of a readily-oxidizable compound of silicon and of a readily-oxidizable compound of aluminum and fluorine are passed to a flame oxidation burner;(2) amorphous fluorine-containing, aluminosilicate particles resulting from the combustion of those gases are collected; and(3) the collected particles are sintered into an integral body at a temperature between about 650.degree.-925.degree. C.

Abstract: This invention is directed to the preparation of glasses exhibiting a transition temperature below 450.degree. C., a working temperature below 500.degree. C., and excellent resistance to attack by water and mild aqueous alkaline solutions. The glasses consist essentially, in mole percent, of at least 65% total of 23-55% ZnO, 28-40% P.sub.2 O.sub.5, and 10-35% R.sub.2 O, wherein R.sub.2 O consists of at least two alkali metal oxides in the indicated proportions selected from the group consisting of 0-25% Li.sub.2 O, 0-25% Na.sub.2 O, and 0-25% K.sub.2 O, and up to 35% total of optional ingredients in the indicated proportions selected from the group consisting of 0-6% Al.sub.2 O.sub.3, 0-8% B.sub.2 O.sub.3, 0-8% Al.sub.2 O.sub.3 +B.sub.2 O.sub.3, 0-15% Cu.sub.2 O, 0-5% F, 0-35% PbO, 0-35% SnO, 0-35% PbO+SnO, 0-5% ZrO.sub.2, 0-4% SiO.sub.2, and 0-15% MgO+CaO+SrO+BaO+MnO, consisting of 0-10% MgO, 0-10% CaO, 0-10% SrO, 0-12% BaO, and 0- 10% MnO.

Abstract: This invention relates to glasses consisting essentially, by weight, of about 35-72% Ln.sub.2 O.sub.3, 5-37% Al.sub.2 O.sub.3, 29-56% SiO.sub.2, and 4-7.5% N. Up to about one-half of the Ln.sub.2 O.sub.3 on an atomic basis may be replaced with SrO and/or BaO. A transparent glass can be formed which contains about 40-60% on a molar basis of Ln.sub.2 O.sub.3 +SrO and/or BaO and wherein the atomic ratio Sr and/or Ba:Sr and/or Ba+Ln >0.4.

Abstract: This invention relates to glass, glass-ceramic, and/or ceramic vessels which are coated with an organic polymer to reduce breakage and to protect the user from flying fragments when the vessels are broken upon impact. The invention contemplates strongly bonding the organic polymer in a small area around the mouth of the vessel only.

Abstract: The present invention is directed to transparent, essentially haze-free glass-ceramic articles exhibiting moduli of rupture in excess of 10,000 psi which consist essentially, in weight percent, of 3-6% Li.sub.2 O, 17-23% Al.sub.2 O.sub.3, 1-4% B.sub.2 O.sub.3, 60-70% SiO.sub.2, 3-6% TiO.sub.2 and/or ZrO.sub.2, 25-500 ppm Cr.sub.2 O.sub.3, and 1-5 mole percent of a glass modifying oxide selected from the group consisting of 0-3% K.sub.2 O and 0-2.5% SrO and/or BaO.

Abstract: This invention is primarily directed to the production of transformation toughened ZrO.sub.2 -containing ceramic alloys wherein the toughening agent is selected from the group consisting of a rare earth metal vanadate and a magnesium and/or calcium tungstate/molybdate, and SnO.sub.2 can be utilized as a toughening agent and/or a stabilizing agent for ZrO.sub.2.

Abstract: Ultraviolet transmitting glasses exhibiting coefficients of thermal expansion between 46-52.times.10.sup.-7 /.degree.C. and transmittances at a thickness of 1 mm of at least 80% at a wavelength of 254 nm which are essentially free of fluoride and consist essentially, in mole percent, of 60-70% SiO.sub.2, 16-20% B.sub.2 O.sub.3, 1-8% Al.sub.2 O.sub.3, 1-6% Li.sub.2 O, 2.5-5% N.sub.2 O, 0-3% K.sub.2 O, and 0-1.25% Cl, w9herein the mole ratio R.sub.2 O:R.sub.2 O.sub.3 is greater than 0.3, but less than 0.5.

Abstract: There is disclosed a hybrid circuit embodying a crossover formed on a low expansion substrate of aluminum nitride, mullite or a cordierite-type glass-ceramic. The crossover is a thick film dielectric composed of a glass-ceramic having a primary crystal phase of willemite and a secondary phase of cordierite.

Abstract: Ultraviolet transmitting glasses exhibiting coefficients of thermal expansion between 46-52.times.10.sup.-7 /.degree. C. and transmittances at a thickness of 1 mm of at least 80% at a wavelength of 254 nm which are essentially free of fluoride and consist essentially, in mole percent, of 60-70% SiO.sub.2, 16-20% B.sub.2 O.sub.3, 1-8% Al.sub.2 O.sub.3, 1-6% Li.sub.2 O, 2.5-5% N.sub.2 O, 0-3% K.sub.2 O, and 0-25% Cl, wherein the mole ratio R.sub.2 O:R.sub.2 O.sub.3 is greater than 0.3, but less than 0.5.

Abstract: This invention is directed to the preparation of fluoride-containing glasses wherein, when exposed to aqueous solutions, fluoride will be leached therefrom in a controlled manner over a long period of time and which can be melted and formed with little loss of fluorine through volatilization. The glasses are essentially free from alkali metal oxides and heavy toxic metals and consist essentially, in weight percent, of:SiO.sub.2 : 41.4-55.9BaO: 24.7-33.6Al.sub.2 O.sub.3 : 5.6-11B.sub.2 O.sub.3 : 6.5-10.

Abstract: A telescope mirror blank having a supporting network core composed of sintered ceramic struts, and a method of forming such core from a thermally crystallizable, powdered glass and as a separate component from the faceplate, are disclosed. Optionally, the mirror faceplate may be formed in a similar manner.

Abstract: There are disclosed fluoroborosilicate glasses that are particularly adapted to being drawn with lead silicate core glasses to produce clad glass fibers useful in forming fiber optic bundles to be incorporated in night vision equipment. The cladding glass has a refractive index not over about 1.45 and a coefficient of thermal expansion not over about 120.times.10.sup.-7 /.degree.C. The clad fiber has a numerical aperture approximating or equal to one.

Abstract: There is disclosed a maximum reading, temperature measuring device, such as a clinical thermometer, composed of a bulb containing an expandable liquid, such as mercury, an elongated tube with a central bore into which the liquid expands when heated, and a flow control member positioned intermediate the tube and bulb and sealed to each. The flow control member is a short length of tubing having a central bore that is sufficiently small in diameter to form a constriction that inhibits reverse flow of the liquid.

Abstract: This invention is directed to the preparation of glass articles exhibiting a relatively broad band of high contrast polarizing properties in the infrared region of the radiation spectrum from glasses containing silver halide particles selected from the group consisting of AgCl, AgBr, and AgI. The inventive method comprises the following five general steps:(a) melting a batch for a glass containing silver and at least one halide selected from the group consisting of chloride, bromide, and iodide;(b) cooling and shaping said melt into a glass article of a desired configuration;(c) subjecting said glass article to a temperature at least above the strain point, but not in excess of 75.degree. C. above the softening point of the glass, for a sufficient length of time to cause the generation of silver halide particles therein selected from the group consisting of AgCl, AgBr, and AgI, said particles ranging in size between about 200-5000 .ANG.

Abstract: A method is disclosed for constructing a glass mould, and particularly the primary glass mould member, for use in casting multifocal, ophthalmic lenses from organic polymers. The method comprises pressing a glass segment with a cavity, removing the base portion of the segment to form a perforation, mounting the perforated segment on a second glass body, and fusing the assembly to form a blank for finishing. For trifocal lenses, a composite, perforated segment is formed and sealed in a depression on a major element to form a blank.

Abstract: Metallizing pastes, for forming thick film circuitry on low expansion substrates in electronic devices, are disclosed. The paste contains a glass powder that crystallizes on firing to a glass-ceramic in which lead titanate is the primary crystal phase.

Abstract: Secondary discharge slots are cut into the face of newly made or used extrusion dies such that the secondary discharge slots communicate transversely and longitudinally with primary discharge slots but do not communicate with the feed holes. The novel extrusion die arrangement is set forth for the production of ceramic honeycomb structures which produce a greater number of cells per square inch, protrusions on the cell walls, or a combination of both dependent upon the Primary Slots' Volume to Secondary Slots' Volume ratio. The secondary discharge slots can produce honeycomb substrates with much greater surface areas, using an extrusion die with a significantly reduced number of feed holes and a greater number of discharge slots.

Abstract: There is disclosed a family of low dielectric, copper-exuding, boroaluminosilicate glasses particularly adapted to use in forming substrates for electronic devices such as integrated circuits. The glasses are capable of exuding copper oxide, have a coefficient of thermal expansion of 30-35.times.10.sup.-7 at 300.degree. C., a dielectric constant not over 5.0 at 100 KHz, a loss tangent not over 0.003 at 100 KHz and consist essentially, in percent by weight, of 56-64% SiO.sub.2 18-25% B.sub.2 O.sub.3, 3-11% Al.sub.2 O.sub.3, 0-2% CaO, 0-2% Li.sub.2 O, 0-1% K.sub.2 O, the Li.sub.2 O+K.sub.2 O+CaO being 1.5-3% and 1-20% CuO.

Abstract: This invention relates to the production of glass-ceramic materials particularly suitable for use as substrates in integrated circuit packaging. The inventive glass-ceramics can be prepared from thermally crystallizable glass capable of being concurrently sintered and crystallized in situ at temperatures between about 850.degree.-1000.degree. C. to bodies exhibiting dielectric constants less than about 6, linear coefficients of thermal expansion between about 12-60.times.10.sup.-7 /.degree.C. and containing cordierite solid solution as essentially the sole crystal phase. The glass-ceramics are essentially free from Li.sub.2 O and Na.sub.2 O and consist essentially, expressed in terms of weight percent on the oxide basis of 10-25% MgO+ZnO consisting of 2-18% MgO+0-21% ZnO, 20-38% Al.sub.2 O.sub.3, 40-52% SiO.sub.2, and 2-15% total of at least one oxide in the indicated proportion selected from the group consisting of up to 8% of an alkali metal oxide selected from the group consisting of K.sub.2 O, Rb.sub.