Patents Represented by Attorney E. J. Holler
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Patent number: 3975201Abstract: The drying characeteristics of a printing paste comprising a vehicle containing a binder and a low boiling point solvent are improved by substituting a high boiling point solvent for a portion of the low boiling point solvent without substantially adversely affecting the viscosity and flow properties of the paste. The printing paste is advantageously employed in silk screen printing in multiple passes where printed layers must have a uniform degree of wetness. The printing paste and vehicle are especially useful in the manufacture of microelectronic packages.Type: GrantFiled: November 15, 1973Date of Patent: August 17, 1976Assignee: Owens-Illinois, Inc.Inventor: Bernard Greenstein
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Patent number: 3973975Abstract: A sealing glass and a sealing glass paste for sealing the face plate and funnel portion of a color television tube wherein PbO-containing sealing glass frit contains an effective amount of a powder, such as Pb.sub.3 O.sub.4 powder, which powder prevents the reduction of PbO to Pb metal during the sealing process, which reduction would otherwise result in a dielectric breakdown in the seal. Among other powders similarly found to be effective for the purpose of prevention of reduction of PbO in a PbO-containing sealing glass frit are certain other higher oxides of a cation which are selected from a group including, in addition to Pb.sub.3 O.sub.4, such higher oxides of a cation as BaO.sub.2, CrO.sub.3, MnO.sub.2, Mn.sub.2 O.sub.3, Fe.sub.2 O.sub.3, Fe.sub.3 O.sub.4, CuO, Cu.sub.2 O, Tl.sub.2 O.sub.3, Sb.sub.2 O.sub.5, TeO.sub.2, Ta.sub.2 O.sub.5, Nb.sub.2 O.sub.5, V.sub.2 O.sub.5, CeO.sub.2, Bi.sub.2 O.sub.3 and As.sub.2 O.sub.5. A sealing glass paste consisting essentially of a PbO-- B.sub.2 O.sub.Type: GrantFiled: October 22, 1974Date of Patent: August 10, 1976Assignee: Owens-Illinois, Inc.Inventors: Josef Francel, James E. King, John M. Woulbroun
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Patent number: 3970463Abstract: Thermally crystallizable glasses and glass-ceramics having a narrow critical range of compositions coming within the SiO.sub.2 -Al.sub.2 O.sub.3 -Li.sub.2 O and SiO.sub.2 -Al.sub.2 O.sub.3 -Li.sub.2 O-ZnO systems and glass-ceramic products made therefrom including heat exchangers, such as regenerators and recuperators used with gas turbine engines, thermal reactors and catalytic reactors for the gaseous exhausts of combustion engines, and other products which are dimensionally stable at temperatures of at least 1500.degree.F. and above, have very low coefficients of thermal expansion, and have a modulus of rupture of at least about 10,000 psi which is retained when operating at temperatures of at least 1500.degree.F., over an extended period of time.Type: GrantFiled: April 26, 1974Date of Patent: July 20, 1976Assignee: Owens-Illinois, Inc.Inventors: Jerry L. Planchock, Daniel R. Stewart, Thomas W. Brock
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Patent number: 3970603Abstract: The application discloses polymers and methods of making same in which a chlorine atom of a chloromethyl pendant group of a polymer such as a chloromethylated copolymer of styrene and divinylbenzene is substituted with a derivative of malonic acid having a protected amino group on the alpha-carbon atom and two carboxyl groups or precursors thereof to form, via several steps, the alpha-amino acid derivative of the starting polymer. These polymers are used, for instance, as ion exchange resins, as substrates for affinity chromotography, and as a starting resin for solid peptide synthesis. The resultant polymer is also used as a starting material to make a polymer with a pendant group that is a derivative of oxazolidone-2,5-dione, substituted at the 4-position. These polymers are used, for example, as the matrix for solid phase peptide synthesis and as the starting resin for solid phase peptide degradation.Type: GrantFiled: October 15, 1974Date of Patent: July 20, 1976Assignee: Owens-Illinois, Inc.Inventor: Don N. Gray
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Patent number: 3970464Abstract: Zinc borate sealing glasses free of silica, alkali metal oxide and lead are disclosed for use in sealing and encapsulation, particularly in connection with semi-conductor devices and electronic components which are sensitive to alkali metal and lead. The glasses have coefficients of thermal expansion in the range of about 35 to 55 .times. 10.sup..sup.-7 /.degree.C, fiber softening temperatures in the range of about 600.degree. to 675.degree.C and annealing point temperatures in the range of about 500 to 580.degree.C.Type: GrantFiled: February 10, 1975Date of Patent: July 20, 1976Assignee: Owens-Illinois, Inc.Inventor: James Allen Shell
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Patent number: 3967973Abstract: Sealing glass paste for sealing the face plate and funnel portion of a color television tube wherein PbO-containing sealing glass frit contains from at least 0.1 to 1.5% by weight of Pb.sub.3 O.sub.4 powder, which powder prevents the reduction of PbO to Pb metal during the sealing process, which reduction would otherwise result in a dielectric breakdown in the seal. A sealing glass paste consisting essentially of a PbO--B.sub.2 O.sub.3 --ZnO sealing glass frit and containing from at least 0.1 to 1.5% by weight of Pb.sub.3 O.sub.4 powder, based upon the weight of the frit, together with hydroxypropyl cellulose binder for the frit and a solvent for the binder. A method for sealing the face plate of a color television tube to its funnel portion with a PbO-containing solder glass wherein the reduction of PbO to metallic lead during the sealing step is obviated by the addition of a sufficient amount of Pb.sub.3 O.sub.4 powder in the solder glass and paste made therewith, which Pb.sub.3 O.sub.Type: GrantFiled: October 2, 1974Date of Patent: July 6, 1976Assignee: Owens-Illinois, Inc.Inventors: Josef Francel, James E. King, John M. Woulbroun
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Patent number: 3962939Abstract: In a glassmaking process, a pair of reciprocating blades are used to cut a stream of molten glass into discrete charges known as "gobs". The cutting surfaces of the shear blades are maintained in a spaced-apart relationship by pairs of raised portions or rails formed in or on the facing blade surfaces. The raised portions or rails of the blades keep the blades separated a specified distance and thereby extend the wear life of the blades by eliminating friction between the cutting surfaces of the blades. A solid film lubricant is applied to the blades and serves to lubricate both cutting surfaces of the blades, thus the blade surfaces that contact the molten glass stream are lubricated to avoid the possibility of the glass sticking to the shear blades.Type: GrantFiled: May 22, 1975Date of Patent: June 15, 1976Assignee: Owens-Illinois, Inc.Inventor: Edward J. Stengle, Jr.
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Patent number: 3962000Abstract: Disclosed is a method for diffusion doping of silicon and germanium semiconductors by the vapor phase transport of B.sub.2 O.sub.3 from a solid B.sub.2 O.sub.3 source to the semiconductor, wherein the solid B.sub.2 O.sub.3 source comprises a rigid, dimensionally stable, glass-ceramic body formed from certain barium aluminoborosilicate parent glass compositions which in mole percent consist essentially of over 40 and up to 60 SiO.sub.2, 10 to 30 Al.sub.2 O.sub.3, 20 to 40 B.sub.2 O.sub.3 and 3 to 20 alkaline earth oxides including 1 to 15 BaO.Type: GrantFiled: December 20, 1974Date of Patent: June 8, 1976Assignee: Owens-Illinois, Inc.Inventor: James E. Rapp
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Patent number: 3961969Abstract: Disclosed is a method for diffusion doping of silicon and germanium semiconductors by the vapor phase transport of B.sub.2 O.sub.3 from a solid B.sub.2 O.sub.3 source to the semiconductor, wherein the solid B.sub.2 O.sub.3 source comprises a rigid, dimensionally stable, glass-ceramic body formed from certain alkaline earth aluminoborosilicate parent glass compositions. The glass-ceramic bodies contain up to 60 mole % of B.sub.2 O.sub.3 and are dimensionally stable at doping temperatures of 1050.degree.C and higher.Type: GrantFiled: December 23, 1974Date of Patent: June 8, 1976Assignee: Owens-Illinois, Inc.Inventor: James E. Rapp
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Patent number: 3958074Abstract: A high voltage electric power transmission line having an electrical power carrying capacity of 50 megawatts or more. An electrical power conductor is contained within a substantially rigid dielectric casing formed of a plurality of elongated tubular glass casing sections hermetically bonded together linearly end to end forming a continuous elongated casing around the conductor. The casing is loosely contained in an outer duct which permits lateral movement of the casing in the duct but places a maximum limit on such movement.Type: GrantFiled: June 27, 1975Date of Patent: May 18, 1976Assignee: Owens-Illinois, Inc.Inventors: Perry P. Pirooz, Anthony P. Schmid, Dennis T. Sturgill
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Patent number: 3956441Abstract: Plastic containers having internal reinforcing ribs are formed by a molding operation including pre-blow and final-blow steps. The pre-blow step includes inflating a blowable plastic parison into contact with the cavity walls of a first blow mold to form a blown pre-form, the cavity walls of the first blow mold including a plurality of concave grooves to form a pattern of convex or proturburent ribs on the outer periphery of the pre-form. The final-blow step includes positioning the blown, ribbed pre-form within a second or final blow mold having a cavity defined by substantially smooth wall surfaces conforming to the exterior configuration of the desired container. Next, the pre-form is blown to stretch and expand against the cavity walls of the second mold, during which step the convex ribs on the exterior of the pre-form are flattened, forming concave portions intermediate convex reinforcing ribs on the internal wall surface of the container.Type: GrantFiled: September 16, 1974Date of Patent: May 11, 1976Assignee: Owens-Illinois, Inc.Inventor: Albert R. Uhlig
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Patent number: 3956532Abstract: Disclosed is a method for recovering vaporous metal halides, such as tin chloride, from a gaseous stream by introducing volatile amines, such as ammonia, into the stream to form a solid reaction product which is separated and recovered for reuse.Type: GrantFiled: November 29, 1974Date of Patent: May 11, 1976Assignee: Owens-Illinois, Inc.Inventor: Richard H. Russell
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Patent number: 3954486Abstract: Disclosed is a physical blend of particulate lead borate sealing glass and particulate refractory filler for use in forming thermal fusion seals for workpieces having a lower coefficient of thermal expansion than the sealing glass. The particulate refractory filler has a particle size diameter in excess of about 37 microns (i.e. plus 400 U.S. Sieve) to lower the expansion while maintaining adequate flow during fusion. The blend is especially useful as a package sealant for electronic components.Type: GrantFiled: July 30, 1974Date of Patent: May 4, 1976Assignee: Owens-Illinois, Inc.Inventors: Josef Francel, Robert F. Palermo
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Patent number: 3951635Abstract: In accordance with the method and apparatus of this invention, glass-forming materials are subjected to heat and agitation sufficient to form a molten glass having mostly dissolved glass-forming materials, mostly completed chemical reactions between the glass-forming materials and containing a high number of gaseous inclusions, and containing up to 50 volume percent entrapped gases. This glass appears foamy. The molten glass is transferred to a second chamber to complete melting of any unmelted sand grains remaining from the glass-forming materials, and completes the chemical reactions that remain incompleted, and to remove any remaining cords, and to reduce the foamy character of the melt to a dense molten glass which contains only small-sized gaseous inclusions.Type: GrantFiled: November 29, 1974Date of Patent: April 20, 1976Assignee: Owens-Illinois, Inc.Inventor: Robert R. Rough, Sr.
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Patent number: 3949033Abstract: This invention relates to a method of making a blown plastic container having a concave pressure bottom configuration by blowing a pre-form into a container having a flat bottom, then contacting and deforming the flat bottom to reform the flat bottom into the desired pressure bottom configuration. The flat bottom is reformed by blowing, or by mechanical contact, or both blowing and contact, at a temperature conducive to multi-axial orientation to provide a pressure bottom of increased strength. To facilitate the performance of the method utilizing an initial parison formed by free extrusion, the present invention further contemplates smoothing out any pinch flash and distributing it on the bottom of the parison, so that the pinch flash will not interfere with subsequent forming of the bottom of the final container as above described.Type: GrantFiled: November 2, 1973Date of Patent: April 6, 1976Assignee: Owens-Illinois, Inc.Inventor: Albert R. Uhlig
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Patent number: 3949153Abstract: A high voltage electric power transmission line having an electrical power carrying capacity of 50 megawatts or more. An electrical power conductor is contained within a substantially rigid dielectric casing formed of a plurality of elongated tubular glass casing sections hermetically bonded together linearly end to end forming a continuous elongated casing around the conductor. The casing is loosely contained in an outer duct which permits lateral movement of the casing in the duct but places a maximum limit on such movement.Type: GrantFiled: November 14, 1973Date of Patent: April 6, 1976Assignee: Owens-Illinois, Inc.Inventors: Perry P. Pirooz, Anthony P. Schmid, Dennis T. Sturgill
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Patent number: 3949034Abstract: This invention relates to a method of making a blown plastic containeer having an arcuate pressure bottom configuration, preferably provided with integrally formed multiple thickness support walls or "skirts" surrounding the bottom.The method of making such containers is by blowing the container in a blow mold having telescopically movable portions for physically contacting and deforming a blowable parison or preform positioned in the blow mold. The parison contact and deformation aids in forming the bottom and/or the surrounding support walls, while providing a favorable blow-up ratio during the blowing operation. Further, the method can be carried out under conditions causing multi-axial orientation in the final container.Type: GrantFiled: January 30, 1974Date of Patent: April 6, 1976Assignee: Owens-Illinois, Inc.Inventor: Albert R. Uhlig
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Patent number: 3947089Abstract: Disclosed are stable, homogeneous GeO.sub.2 -B.sub.2 O.sub.3 -PbO-Bi.sub.2 O.sub.3 glass compositions having high indices of refraction, low sound velocities, low acoustic loss and high Verdet constants which render them useful in acoustooptic and magnetooptic devices.Type: GrantFiled: May 5, 1975Date of Patent: March 30, 1976Assignee: Owens-Illinois, Inc.Inventor: James E. Rapp
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Patent number: 3947279Abstract: A thermally crystallizable glass of predominantly lead-zinc borate composition is disclosed which is composed of a homogeneous admixture of finely comminuted particles of thermally crystallizable glass and essentially fully crystallized glass particles in a ratio of about 1-10, or more preferably 2-7, parts by weight of crystallized glass particles to one million parts by weight of uncrystallized glass particles and which, in its finely comminuted state, possesses an overall particle size distribution such that it is uniformly composed of particles which are essentially entirely of -100 U.S. Series Sieve screen size and such that between about 65-78 weight percent of such particles are of -325 U.S. Series Sieve screen size.Type: GrantFiled: March 29, 1974Date of Patent: March 30, 1976Assignee: Owens-Illinois, Inc.Inventor: Carl J. Hudecek
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Patent number: 3946128Abstract: A laser assembly and a novel glass laser disc having an annular lead borate glass coating for use in the assembly is disclosed, the annular coating being capable of absorbing energy at a wavelength of 1.06 microns to thereby absorb parasitic oscillations. The outstanding glass coating has an index of refraction not substantially less than the index of refraction of the glass disc, the glass coating containing an effective energy-absorbing amount of a heavy metal oxide, such as Sm.sub.2 O.sub.3 and CuO, for absorbing energy at a wavelength of about 1.06 microns. The heavy metal oxides includes oxides of transition metals of the 3d, 4d, 4f and 5f orbital series.Type: GrantFiled: February 13, 1973Date of Patent: March 23, 1976Assignee: Owens-Illinois, Inc.Inventor: Louis Spanoudis