Patents Represented by Attorney Ernest G. Szoke
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Patent number: 6028231Abstract: A process to obtain 2-methyl-4-(2, 2, 3-trimethyl-cyclopent-3-en-1-yl)-but-2-en-1-ol by reacting campholene aldehyde and propionaldehyde via aldol condensation and further subjecting the resulting reaction mixture to Meerwein-Ponndorf reduction with aluminum alcoholates in the presence of a basic amine compound.Type: GrantFiled: April 20, 1999Date of Patent: February 22, 2000Assignee: Henkel Kommanditgesellschaft auf AktienInventor: Thomas Markert
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Patent number: 6025416Abstract: Two component adhesive/sealing masses based on silane terminated prepolymers contain a component A which is a one-component, humidity hardening adhesive/sealing mass with high initial adhesiveness, and a component B which is a crosslinking agent and/or accelerator for component A are disclosed. These adhesive/sealing masses are suitable for gluing without primer parts made of metals or other materials such as aluminum, steel, glass, wood or plastics. In a particularly preferred embodiment, component B consists of a viscous, stable mixture of plasticisers, water, thickeners and other optional auxiliary substances.Type: GrantFiled: March 24, 1998Date of Patent: February 15, 2000Assignee: Henkel Teroson GmbHInventors: Manfred Proebster, Werner Schumacher
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Patent number: 6025314Abstract: A process for improving the soil release properties of dishwashing machine rinse aid compositions used to rinse dishware and remove starch-containing soils therefrom by adding to the compositions a cationic polymer containing monomer units corresponding to formula I: ##STR1## in which R.sup.1 is hydrogen or a methyl group,R.sup.2, R.sup.3 and R.sup.4 are the same or different and represent hydrogen or a C.sub.1-8 alk(en)yl group, R.sup.8 is a linear, cyclic or branched alkylene group containing 2 to 8 carbon atoms, andX represents a monofunctional anion or the 1/m part of an m-functional anion.Type: GrantFiled: May 6, 1998Date of Patent: February 15, 2000Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Christian Nitsch, Willi Buchmeier, Peter Jeschke, Ludwig Schieferstein, Herbert Fischer
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Patent number: 6015780Abstract: A surfactant composition containing: (a) from 2 to 20% by weight of a betaine having a fatty residue containing exactly 12 carbon atoms; (b) from 3 to 18% by weight of an alkyl and/or alkenyl oligoglycoside; and (c) from 15 to 35% by weight of a fatty alcohol ether sulfate, all weights being based on the weight of the composition.Type: GrantFiled: April 8, 1998Date of Patent: January 18, 2000Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Joaquin Llosas Bigorra, Nuria Bonastre Gilabert, Miguel Osset Hernandez, Xavier Closa Cruxens, Rafael Pi Subirana
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Patent number: 6015865Abstract: A reactive hot melt adhesive contains, as resin component, a reaction product ofa) 30 to 50 wt-% of an epoxy resin, solid at root temperature, prepared from bisphenol A and/or bisphenol F and epichlorhydrin with an epoxide equivalent weight of 400 to 700,b) 10 to 25 wt-% of an epoxy resin, liquid at room temperature, prepared from bisphenol A and/or bisphenol F and epichlorhydrin with an epoxide equivalent weight of 150 to 220 andc) 35 to 50 wt-% amino-terminated polyethylene and/or polypropylene glycols.Type: GrantFiled: October 22, 1997Date of Patent: January 18, 2000Assignee: Henkel-Teroson GmbHInventors: Norman E. Blank, Hubert K. Schenkel
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Patent number: 6013312Abstract: A coating apparatus is disclosed for applying a coating material on one or more zones of a substrate material. In one embodiment, the coating applicators have fluid-wicking strips that apply the coatings directly to the substrate, while in another embodiment, the fluid-wicking strips indirectly apply the coatings to the substrate via feed rolls. Metering mechanisms supply predetermined amounts of coating material to the fluid-wicking strips. Each coating applicator has a housing with a recess for receiving one the fluid-wicking strips therein. One of the fluid-wicking strips is mounted in each housing which has a plurality of transversely spaced passageways. Each passageway of each applicator housing is fluidly coupled to its own separate air actuated metering mechanism which dispenses coating material to the portion of the fluid-wicking strip adjacent thereto. A desired quantity of coating material is simultaneously delivered via the metering mechanisms to each of the applicator housings.Type: GrantFiled: April 20, 1999Date of Patent: January 11, 2000Assignee: Henkel CorporationInventors: Kevin H. Cornell, W. Craig Huffman
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Patent number: 6013750Abstract: The invention pertains to an aerobically curing composition comprising free-radical polymerizable compounds, an activator system, and optionally conventional additives, characterized in that said composition contains as said free-radical polymerizable compounds at least one polyurethane (meth)acrylate one or more (meth)acrylate comonomers; wherein said composition contains from 20 to 80% by weight of said polyurethane (meth)acrylate and from 80 to 20% by weight of said (meth)acrylate comonomer(s), based on the total of polymerizable compounds, and said activator system is a hydrazone activator system, as well as the preparation and use of said composition.Type: GrantFiled: July 9, 1996Date of Patent: January 11, 2000Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Carsten Friese, Frank George, Dieter Rademacher, Thomas Huver, Frank Bergmann
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Patent number: 6013142Abstract: Aluminum alloys that are susceptible to damage by High Temperature Oxidation during solution heat treatment are protected against such damage by a coating containing sodium fluoroborate and/or other fluorine-containing-gas-generating material. The coating can be one suitable for lubrication during cold working of the substrate and can remain in place after the cold working to protect the substrate during subsequent heat treatment.Type: GrantFiled: May 19, 1997Date of Patent: January 11, 2000Assignee: Henkel CorporationInventor: Kenneth J. Hacias
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Patent number: 6013616Abstract: Surfactant mixtures which provide improve dermal compatibility and foam stability contain(a) monoglyceride(ether)sulfates, and(b) fatty acid condensation products selected from(b1) fatty acid isethionates,(b2) fatty acid taurates, and(b3) fatty acid sarcosinates.Type: GrantFiled: March 10, 1997Date of Patent: January 11, 2000Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Bernd Fabry, Ansgar Behler
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Patent number: 6010763Abstract: A fireproofing material is provided in the form of a loose mixture comprising:a. at least one heat-insulating material which is heat resistant at temperatures of up to 1100.degree. C.,b. at least one swelling agent active at elevated temperatures,c. at least one binder active at elevated temperatures, andd. at least one flexibly compliant constituent,wherein the mixture is free from inorganic fibers. The mixture is typically contained in a sealed flexible bag. The flexibly compliant constituent is typically a granular foam or a fiber conglomerate. The flexibly compliant constituent is present in the mixture in quantities of 1 to 30% by weight and preferably 2 to 15% by weight.Type: GrantFiled: January 17, 1996Date of Patent: January 4, 2000Assignee: Grunau IllertissenInventors: Dieter Annemaier, Robert Graf
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Patent number: 6011131Abstract: Process for the preparation of polyamides comprising the steps of A) reacting a soybean oil condensate obtained from the deodorization of refined soybean oil and which contains less than 30% by weight of free and esterified oleic acid based on the total weight of free and esterified fatty acids in said condensate, with a C.sub.1-4 alkanol in the presence of a zinc oxide catalyst to convert free fatty acids and fatty acid glyceride esters to fatty acid C.sub.1-4 alkyl esters;B) removing excess C.sub.1-4 alkanol, volatile reaction by-products, water, and the zinc oxide catalyst from the resulting reaction mixture;C) heating the reaction mixture from step B) under vacuum to obtain a distillate of fatty acid C.sub.1-4 alkyl esters;D) separating the distillate from step C) into a fraction containing mostly C.sub.16-18 saturated fatty acid C.sub.1-4 alkyl esters and a second fraction containing mostly C.sub.16-18 unsaturated fatty acid C.sub.1-4 alkyl esters wherein the oleic acid C.sub.Type: GrantFiled: May 19, 1998Date of Patent: January 4, 2000Assignee: Henkel CorporationInventors: Setsuo Sato, Hercules Peloggia, Tracy Hunt, Joerg Schwarzer, Ramiro Carielo Bueno, Roger A. Lovald
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Patent number: 6008392Abstract: A process for making alkoxylated fatty acid alkyl esters involving: (a) providing a fatty acid alkyl ester; (b) providing an alkylene oxide component; (c) providing a primary catalyst; (d) providing a co-catalyst selected from the group consisting of lithium hydroxide, an alkaline earth metal, a tin salt and mixtures thereof; and (e) reacting (a)-(d) to make the alkoxylated fatty acid alkyl ester.Type: GrantFiled: September 28, 1998Date of Patent: December 28, 1999Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Ansgar Behler, Almud Folge
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Patent number: 6008391Abstract: A process for making alkoxylated fatty acid alkyl esters involving: (a) providing a fatty acid alkyl ester; (b) providing an alkylene oxide component; (c) providing a catalyst component containing a mixture of: (i) a primary catalyst; and (ii) an alkylene glycol having from 2 to 6 carbon atoms; and (d) reacting (a)-(c) to make the alkoxylated fatty acid alkyl ester.Type: GrantFiled: September 25, 1998Date of Patent: December 28, 1999Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Rafael Pi Subirana, Joaquim Llosas Bigorra
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Patent number: 6005668Abstract: A "highlighter" liquid for detecting cosmetic defects in non-metallic surfaces, particularly those intended for high quality automotive finishes comprises organic substances each molecule of which contains at least one continuosly chemically bonded chain or ring of atoms in which there are at least two carbon atoms and at least two oxygen, nitrogen, sulfur, and phosphorus heteroatoms, the carbon atoms and heteroatoms being arranged in such an order along the chain or ring that (i) each heteroatom is bonded to at least one carbon atom and (ii) the chain does not include more than three consecutive continuosly chemically bonded carbon atoms. Particularly suitable materials include glycerin, propylene glycol, low molecular weight glycol condensation polymers, and monoethers of these glycol condensation polymers. Water is also usually present in the highlighter liquid, which has a long open time and does not damage the substrate even if left in place for a day or more.Type: GrantFiled: July 9, 1998Date of Patent: December 21, 1999Assignee: Henkel CorporationInventors: Theodore D. Held, III, Gerald J. Cormier
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Patent number: 6004425Abstract: One-component hot-curing structural adhesives based on liquid rubbers, which may optionally contain functional groups, solid rubbers, thermoplastic polymer powders and sulfur and also vulcanization accelerators are suitable for bonding metal parts. Tensile shear strengths of more than 15 MPa and high breaking elongations of more than 15% can be obtained. These adhesives are substantially free from low molecular weight epoxy resins and are particularly suitable for use in white-shell assembly in the car industry.Type: GrantFiled: July 25, 1997Date of Patent: December 21, 1999Assignee: Henkel-Teroson GmbHInventors: Peter Born, Frank Dittrich
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Patent number: 6003274Abstract: A lightweight structural reinforcement spans a space in a structural member. The reinforcement functions as a web and has a metal plate, a layer of foam and a thin, metal reinforcement selectively positioned at the mid-portion of the reinforcement. Unexpanded foam at the end portions of the plate serve as a n adhesive to bond the reinforcement to the structural member being reinforced.Type: GrantFiled: January 25, 1999Date of Patent: December 21, 1999Assignee: Henkel CorporationInventor: Joseph S. Wycech
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Patent number: 6001186Abstract: A chromium and ferricyanide free aqueous cleaner/deoxidizer for aluminum and titanium and their alloys contains strong acid, fluoride ions, aryl quaternary ammonium ions, and di-anionic functional substituted compounds containing at least two aryl groups per molecule. Excellent cleaning and deoxidizing with substantially no etching is achieved.Type: GrantFiled: June 22, 1998Date of Patent: December 14, 1999Assignee: Henkel CorporationInventors: Philip M. Johnson, Lawrence R. Carlson
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Patent number: 6001791Abstract: The invention concerns a liquid agent in suspension for use in washing-up machines. The aim of the invention is to ensure the consistency of a paste without the need to use thickeners or extenders. This is achieved by using 30 to 60% by weight of water, 15 to 70% by weight of an alkali-metal tripolyphosphate selected from sodium tripolyphosphate, used either in the anhydrous or the partly hydrated form, and potassium tripolyphosphate in the presence of 5 to 30% by weight of an alkali carrier such as an alkali-metal hydroxide, carbonate, or metasilicate, if necessary in the presence of active-chlorine carriers, complex carriers and the other usual auxiliaries.Type: GrantFiled: February 3, 1998Date of Patent: December 14, 1999Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Dieter Hemm, Guenter Hellmann, Klaus Wilbert
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Patent number: 5997944Abstract: The invention is a method for improving the flow of particulate lacquer powders when the lacquer powders are coated on a substrate and the substrate heated to fuse the lacquer particles to provide a finished lacquer surface on the substrate. The flow control agent is an oxazine, oxazoline, oligoxazine or oligoxazoline and salts of the compounds with protonic acids. The flow control agents when included in power lacquer formulations improve the flow of the lacquer when the powder lacquer coated substrate is heated to fuse the coating.Type: GrantFiled: September 5, 1997Date of Patent: December 7, 1999Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Heinz-Guenther Schulte, Paul Birnbrich, Harald Frommelius
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Patent number: D420882Type: GrantFiled: March 1, 1999Date of Patent: February 22, 2000Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Martin Majolo, Roy Edwin van Swieten, Adrianus Petrus Wilhelmus van den Berg