Patents Represented by Attorney Louis Morris
  • Patent number: 5792313
    Abstract: In the evaporation of process wastewater comprising a mixture of different types of wastewater, problems arise due to the formation of reaction products, so-called incrustations, which are difficult to separate. These incrustations clog up the evaporator, thus necessitating frequent stoppages for chemical and mechanical cleaning of the evaporator. The invention concerns an improved method for concentrating process wastewater by evaporation. In this method, one acid process flow and one alkaline process flow are evaporated alternately in one and the same evaporator. With this method, precipitates that are difficult to separate are dissolved in the evaporator during the respective evaporations. As a result, stoppages motivated by the need to clean the evaporator may be avoided to the utmost possible extent, while less and cheaper processing equipment is required.
    Type: Grant
    Filed: June 10, 1996
    Date of Patent: August 11, 1998
    Assignee: Eka Nobel AB
    Inventor: Hans Johansson
  • Patent number: 5789530
    Abstract: The synthesis of an aramid by the catalyzed reaction of carbon monoxide, an aromatic dichloride, such as 1,4-dichlorobenzene, and a diamine, such as 1,4-diaminobenzene, is disclosed. The reaction may be catalyzed by palladium (II) and palladium (0)-containing catalysts with chelating trialkyl phosphines, such as bis(diisopropylphosphino)-propane.
    Type: Grant
    Filed: December 20, 1996
    Date of Patent: August 4, 1998
    Assignee: The Penn State Research Foundation
    Inventors: Ayusman Sen, Jang Sub Kim
  • Patent number: 5788815
    Abstract: A process for the production of paper by mixing an aqueous phase comprising white water with cellulose containing fibres, and optional fillers, in a mixing stage to form an aqueous suspension, draining the suspension in the presence of a drainage or retention aid to form a fibre containing sheet or web and white water, and recirculating at least part of the white water to the mixing stage, whereby at least part of the white water is subject to electrodialysis before the mixing stage.
    Type: Grant
    Filed: January 8, 1997
    Date of Patent: August 4, 1998
    Assignee: Eka Chemicals AB
    Inventors: Maria Norell, Lennart Nilsson
  • Patent number: 5789528
    Abstract: The preparation of polyesters and copolyesters, titanium dioxide precipitates and/or titanium dioxide/silicon dioxide coprecipitates having a composition of TiO.sub.2 :SiO.sub.2 >90:10 mol/mol and/or titanium dioxide/zirconium dioxide coprecipitates having a composition of TiO.sub.2 :ZrO.sub.2 >95:5 mol/mol, which have been obtained by hydrolytic precipitation of the corresponding metal alcoholates formed from mono- or polyhydric alcohols, are proposed as polycondensation catalysts. They offer increased safety for the ecosystem and have a higher catalytic activity than Sb.sub.2 O.sub.3, so that the preferred amount used is only 10 to 100 ppm, based on the esters or oligoesters to be subjected to polycondensation. Their storage stability is good if the catalysts have a water content of from 0 to about 15 weight percent, preferably from 0 to about 5 weight percent based upon the hydrated precipitate or coprecipitate, as determined by Karl Fischer titration.
    Type: Grant
    Filed: March 13, 1997
    Date of Patent: August 4, 1998
    Assignee: Akzo Nobel NV
    Inventors: Michael Martl, Thomas Mezger, Bernard Kuhn, Gerriet Oberlein, Klaus Haferland, Bertram Boehringer, Ulrich Berger
  • Patent number: 5785812
    Abstract: A process for delignifying and bleaching lignocellulose-containing pulp, in which the pulp is delignified with a peracid or a salt thereof, treated with a complexing agent, and subsequently bleached with a chlorine-free bleaching agent. Suitably delignification is carried out with the strongly oxidizing peracetic acid, giving a considerable increase in brightness and a considerable reduction of the kappa number after bleaching with a chlorine-free bleaching agent comprising at least one of a peroxide-containing compound, ozone or sodium dithionite, or optional sequences or mixtures thereof. The brightness increasing effect is highly selective, i.e. the viscosity of the pulp is maintained to a comparatively great extent. Both the delignification and the treatment with a complexing agent are advantageously carried out at a close to neutral pH, thus minimizing the need of pH adjustment and making it possible to use spent bleach liquor internally, e.g. for washing the pulp.
    Type: Grant
    Filed: May 17, 1995
    Date of Patent: July 28, 1998
    Assignee: Eka Nobel AB
    Inventors: Magnus Linsten, Jiri Basta, Ann-Sofie Hallstrom
  • Patent number: 5783730
    Abstract: Styrene phosphonic acid (SPA) can be formed the reaction of phosphorous acid with acetophenone, preferably in the presence of a Lewis acid catalyst, to form a hydroxy adduct intermediate thereof which is then reacted with acetic anhydride to form the acyl derivative of the hydroxy adduct, followed by removal of an acetic acid moiety therefrom, preferably in the presence of an acidic catalyst, to form the styrene phosphonic acid product.
    Type: Grant
    Filed: May 2, 1997
    Date of Patent: July 21, 1998
    Assignee: Akzo Nobel NV
    Inventors: Carl C. Greco, John Tomko
  • Patent number: 5779815
    Abstract: A process and an apparatus for removal of a lumen filler and/or other soluble residues from hollow filament bundles are described. The hollow filament bundles are first roughly cleaned by centrifuging, after which in a process preferably containing multiple steps they are cleaned by spraying and centrifuging. The first spraying step is preferably carried out in a pass-through mode and each of the additional steps under recirculation. After a constant concentration has been attained, the cleaning baths in each case are employed for a lower-order treatment step, the cleaning bath of the first spraying step being fed to a recycling process.
    Type: Grant
    Filed: February 26, 1996
    Date of Patent: July 14, 1998
    Assignee: Akzo Nobel NV
    Inventors: Hans-Gunter Breidohr, Manfred Martin, Bernhard Krautwurst, Martin Konig
  • Patent number: 5776375
    Abstract: The present invention provides an electro-optical device comprising NLO polymer in the active layer with improved stability for light in the wavelength range of 600-1600 nm is guided through the device. The present invention is directed to an electro-optical device comprising two cladding layers and an active layer sandwiched between these cladding layers, with the active layer comprising a non-linear optically active side chain polymer with NLO-chromophores having an N-donor-delocated .pi. system-acceptor structure, the N-donor not being bonded directly to alkyl groups. There are two ways to create NLO-chromophores with N-donors which do not have adjacent linear alkyl groups: The first way is to bond one or two aromatic groups. The N-atom is further bonded to the delocated .pi. system. If only one aromatic group is present, the N-atom is, besides the delocated system, further bonded to a hydrogen or deuterium atom.
    Type: Grant
    Filed: February 13, 1996
    Date of Patent: July 7, 1998
    Assignee: Akzo Nobel N.V.
    Inventors: Johannes Willem Hofstraat, Marinus Cornelis Flipse, Richard Herman Woudenberg
  • Patent number: 5777143
    Abstract: A hydrocarbon-soluble alkylaluminoxane composition, such as, methylaluminoxane or even a modified methylaluminoxane, can be prepared by preparing an alkylaluminoxane precursor via non-hydrolytic means, such as, by treating at least one trialkylaluminum compound with a compound containing an oxygen-carbon bond, adding to that precursor an effective amount of an organoaluminum compound which prevents formation of insoluble species, such as, a trialkylaluminum compound where each alkyl group contains two or more carbon atoms, and converting that modified precursor to an alkylaluminoxane, such as, by thermolysis. In a distinct embodiment of the invention, if an insoluble methylaluminoxane product is formed using the non-hydrolytic technique, it can be solubilized by treatment with a solubilizing amount of an alkylaluminoxane, prepared by either hydrolytic or non-hydrolytic means, wherein the alkyl moieties contain two or more carbon atoms.
    Type: Grant
    Filed: October 25, 1996
    Date of Patent: July 7, 1998
    Assignee: Akzo Nobel NV
    Inventors: Dennis B. Malpass, Stanley W. Palmaka, Gregory M. Smith, Jonathan S. Rogers
  • Patent number: 5777090
    Abstract: Disclosed is carboxymethyl inulin having a degree of substitution (DS) ranging from 0,15 to 2,5, preferably from 0,5 to 1,5, a process for the preparation of said carboxymethyl inulin by reacting inulin at a concentration of at least 100 g/l, preferably at least 200 g/l, at elevated temperature with an aqueous alkaline solution of monochloroacetic acid, followed by working up the reaction mixture according to a method known in the chemical art, and the use of said carboxymethyl inulin as inhibitor for the crystallization of calcium carbonate.
    Type: Grant
    Filed: June 6, 1996
    Date of Patent: July 7, 1998
    Assignee: Akzo Nobel NV
    Inventors: Dorine Lisa Verraest, Jan Gerardus Batelaan, Johannes Andreas Peters, Herman van Bekkum
  • Patent number: 5776354
    Abstract: A method for the use of a porous, preferably dimensionally stable, particulate material in a packed filter bed for separating a disperse liquid phase from a gas and/or separating a disperse liquid phase from a liquid, with the average size of the particles being in the range of from 0.1 to 10 mm and the internal surface area of the material being such that, after it has been filled with the disperse liquid phase to be separated and placed, as a packed bed, at a distance of from R to r from the center in a centrifuge rotating at an angular velocity w, for which it holds that0<w.sup.2 (R.sup.2 -r.sup.2).ltoreq.20 (rad/s).sup.2 m.sup.2,wherein w stands for the angular velocity (in rad/s) and R and r represent the largest and the smallest radius (in m), respectively, of the material in the centrifuge, at least 1% of the liquid will have been separated after 5 minutes, while at least 10% of the liquid will have been separated after 60 minutes is disclosed.
    Type: Grant
    Filed: June 1, 1995
    Date of Patent: July 7, 1998
    Assignee: Akzo Nobel NV
    Inventors: Abele Broer van der Meer, Elwin Schomaker, Johannes Bos, Erik Leonard Middelhoek
  • Patent number: 5776347
    Abstract: The present invention generally relates to a method for reducing the content of organic solvent in an aqueous dispersion of a cellulose-reactive hydrophobing agent, prepared by emulsifying a molten cellulose-reactive hydrophobing agent containing organic solvent in an aqueous solution containing one or more emulsifying agents. The method comprises contacting the aqueous dispersion under agitation with a sorbent, said sorbent having the capacity of absorbing or adsorbing organic molecules, or a gas, whereby the solvent is transferred to the sorbent or the gas.
    Type: Grant
    Filed: July 7, 1995
    Date of Patent: July 7, 1998
    Assignee: Eka Nobel AB
    Inventors: Erik Lindgren, Jeppe Magnusson
  • Patent number: 5772923
    Abstract: A solution which comprises: a non-polar organic solvent, such as an aliphatic hydrocarbon solvent, like hexane; polyaniline; and an effective amount of an amphiphilic phenol-containing reagent, which can be a monomeric compound or a phenol-containing polymer, for the solubilization of the polyaniline in the solvent. The alkyl substituent in the phenol-containing reagent, if monomeric, can contain from about six to about twelve carbon atoms, with a preferred solubilizer being dodecylphenol.
    Type: Grant
    Filed: October 29, 1996
    Date of Patent: June 30, 1998
    Inventor: Kalle M. J. Levon
  • Patent number: 5766564
    Abstract: A process for the production of an aluminosilicate containing at least 9 weight percent alumina, having a BET surface area of 300-600 m.sup.2 /g, and an average pore volume of of 0.2-0.5 ml/g is disclosed. The process includes the steps of preparing an aqueous solution comprising at least one metal silicate, adjusting the pH of said aqueous solution comprising at least one metal silicate with a sufficient amount of an aqueous solution comprising at least one aluminum salt to produce an aqueous solution having a pH of 4.4-7.7, precipitating aluminosilicate from the aqueous solution by concurrently dosing additional aqueous solution comprising at least one metal silicate in such a manner such that the pH is maintained at 4.4-7.7, steps (a)-(c) being carried out at a temperature of 0.degree.-80.degree. C. and isolating said aluminosilicate. The aluminosilicate is useful as a pressure sensitive pigment in carbonless copy paper.
    Type: Grant
    Filed: March 1, 1996
    Date of Patent: June 16, 1998
    Assignee: Akzo-PQ Silica VOF
    Inventors: Ivo Ignatius Maria Tijburg, Abdullah Konuksever
  • Patent number: 5764820
    Abstract: The invention relates to a method of fabricating an electro-optical device which comprises integrating a semiconductor component with a polymeric optical waveguide component. According to the invention, a semiconductor component obtained by epitaxial lift-off (ELO) is embedded in a waveguide device which in addition to a polymeric optical waveguide structure comprises an appropriate cavity. The invention further pertains to an integrated electro-optical device attainable by means of this ELO technique. Notably, it concerns an integrated electro-optical device in which the polymeric waveguide component and the semiconductor component are integrated on a substrate made of a different material from that of the semiconductor component, preferably a material with good heat dissipation, such as silicon. Preferably, the polymeric waveguide component comprises a polymer in which waveguide channels have been provided by bleaching.
    Type: Grant
    Filed: March 17, 1994
    Date of Patent: June 9, 1998
    Assignee: Akzo Nobel NV
    Inventors: Peter M. C. De Dobbelaere, Peter P. van Daele
  • Patent number: 5759348
    Abstract: The aromatic polyamide pulp obtained by the process of this invention is good in dispersibility in water and good in opening property, and excellent in dispersibility of inorganic filler and wettability with and adhesion to a matrix resin such as phenol resin. Hence, an impregnated paper and molded article excellent in homogeneity and mechanical strength can be produced. Also, in the case of friction materials free from paper-making step, the filler-retention of pulp in the production process is good and such a result that the filler-dispersibility and mechanical strength of molded article are excellent is obtained, and the pulp can be utilized particularly effectively in uses as asbestos-substitutes.
    Type: Grant
    Filed: August 27, 1996
    Date of Patent: June 2, 1998
    Assignee: Akzo Nobel nv
    Inventors: Toshiharu Yamabayashi, Kosaku Asagi
  • Patent number: 5760859
    Abstract: The invention is in the field of retardation layers comprising high-molecular weight liquid-crystalline material for liquid-crystalline displays. The invention is directed to a retardation layer for a liquid-crystalline display comprising high-molecular weight liquid-crystalline material, wherein the dispersion has been adapted to that of the active liquid-crystalline cell by varying the mesogenic groups of the high-molecular weight liquid-crystalline material, so that the difference in dispersion between the active cell and the retardation layer in the wavelength area of 400-800 nm is not more than 0.1.
    Type: Grant
    Filed: May 17, 1996
    Date of Patent: June 2, 1998
    Assignee: Akzo Nobel NV
    Inventors: Martin Bosma, Jan-Willem Venema, Stephen James Picken, Gustaaf Ronald Mohlmann
  • Patent number: 5760199
    Abstract: Polysaccharide acid amide compositions are disclosed which contains one extra carbon atom as compared to the polysaccharide and which comprises an acid amide of the formula --C(O)N(R)(R') where R is selected from the group consisting of hydrogen and alkyl of from about one to about four carbon atoms and R' is fatty alkyl of no less than about eight carbon atoms. Disaccharides such as lactose or maltose are preferred. These polysaccharide acid amides are formed by reacting the polysaccharide with a cyanide source, for example, an alkali metal cyanide, such as sodium cyanide, in the presence of an amine reagent containing a fatty alkyl group, such as one which comprises a ammonium ion of the formula H.sub.2 N(R)(R') where R is selected from the group consisting of hydrogen and alkyl of from about one to about four carbon atoms and R' is fatty alkyl of no less than about eight carbon atoms.
    Type: Grant
    Filed: July 13, 1995
    Date of Patent: June 2, 1998
    Assignee: Akzo Nobel nv
    Inventors: Stanley B. Mirviss, Meiylin F. Antezzo
  • Patent number: 5756618
    Abstract: The present invention relates to a polyol(allyl carbonate) based casting composition suitable for forming high quality ophthalmic lenses which contains an epoxy compound in an amount effective to reduce shrinkage during its final polymerization in a mold. The casting composition of the present invention comprising polyol(allyl carbonate) and epoxy compound contains an initiator for the polymerization of the polyol(allyl carbonate), but does not contain a catalyst for polymerization of the epoxy compound.
    Type: Grant
    Filed: February 14, 1997
    Date of Patent: May 26, 1998
    Assignee: Akzo Nobel nv
    Inventors: Kenneth Dixon, Mary Ann Kelly
  • Patent number: 5750030
    Abstract: It is proposed to use a synthetic granulate or powder with a particle size of 0.1 to 10 mm as packing material for the removal of liquid, gaseous and/or dissolved constituents from a process stream, which packing material is made up of a porous, preferably dimensionally stable polymer having an overall porosity of 50 to 95% by volume, which when used as an extracting medium has pores of a diameter of 0.01 to 50 .mu.m, with an extracting liquid immobilised therein, or when used as a coalescence medium has a cellular body/window structure with the diameter of more than 50% by volume of the bodies being in the range of 100 to 700 .mu.
    Type: Grant
    Filed: August 16, 1996
    Date of Patent: May 12, 1998
    Assignee: Akzo Nobelnv
    Inventors: Elwin Schomaker, Johannes Bos, Erik Leonard Middelhoek