Patents Represented by Attorney, Agent or Law Firm Paul W. Zimmerman
  • Patent number: 5708191
    Abstract: The present invention is an ultrasonic fluid densitometer that uses a material wedge having an acoustic impedance that is near the acoustic impedance of the fluid, specifically less than a factor of 11 greater than the acoustic impedance of the fluid. The invention also includes a wedge having at least two transducers for transmitting and receiving ultrasonic signals internally reflected within the material wedge. Density of a fluid is determined by immersing the wedge into the fluid and measuring reflection of ultrasound at the wedge-fluid interface.
    Type: Grant
    Filed: April 5, 1996
    Date of Patent: January 13, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Margaret S. Greenwood, Jason C. Lail
  • Patent number: 5708246
    Abstract: The present invention is the addition of a semiconductor material and energy to the reaction mixture of organic, acid (for example, trifluoroacetate), and oxygen. A transition metal ion may be added to the reaction mixture. The semiconductor material converts energy to oxidants thereby promoting oxidation of the organic. Alternatively, using metal in combination with exposure to light may be used.
    Type: Grant
    Filed: August 28, 1996
    Date of Patent: January 13, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Donald M. Camaioni, Michael A. Lilga
  • Patent number: 5707508
    Abstract: The invention is a method and apparatus using high cerium concentration in the anolyte of an electrochemical cell to oxidize organic materials. The method and apparatus further use an ultrasonic mixer to enhance the oxidation rate of the organic material in the electrochemical cell.
    Type: Grant
    Filed: April 18, 1996
    Date of Patent: January 13, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Jeffrey E. Surma, Garry H. Bryan, John G. H. Geeting, R. Scott Butner
  • Patent number: 5705132
    Abstract: The present invention is a reactor for combustion synthesis of inorganic powders. The reactor includes a reaction vessel having a length and a first end and a second end. The reaction vessel further has a solution inlet and a carrier gas inlet. The reactor further has a heater for heating both the solution and the carrier gas. In a preferred embodiment, the reaction vessel is heated and the solution is in contact with the heated reaction vessel. It is further preferred that the reaction vessel be cylindrical and that the carrier gas is introduced tangentially into the reaction vessel so that the solution flows helically along the interior wall of the reaction vessel. As the solution evaporates and combustion produces inorganic material powder, the carrier gas entrains the powder and carries it out of the reactor.
    Type: Grant
    Filed: December 30, 1994
    Date of Patent: January 6, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Gary D. Maupin, Lawrence A. Chick, Randal P. Kurosky
  • Patent number: 5704890
    Abstract: The invention is a real time sensor for therapeutic radiation. A probe is placed in or near the patient that senses in real time the dose at the location of the probe. The strength of the dose is determined by either an insertion or an exit probe. The location is determined by a series of vertical and horizontal sensing elements that gives the operator a real time read out dose location relative to placement of the patient. The increased accuracy prevents serious tissue damage to the patient by preventing overdose or delivery of a dose to a wrong location within the body.
    Type: Grant
    Filed: May 31, 1995
    Date of Patent: January 6, 1998
    Assignee: Battelle Memorial Institute
    Inventors: Mary Bliss, Richard A. Craig, Paul L. Reeder
  • Patent number: 5697043
    Abstract: The present invention is a novel method for freeform fabrication. Specifically, the method of solid freeform fabrication has the steps of:(a) preparing a slurry by mixing powder particles with a suspension medium and a gelling polysaccharide;(b) making a layer by depositing an amount of said powder slurry in a confined region;(c) hardening a selected portion of the layer by applying a gelling agent to the selected portion; and(d) repeating steps (b) and (c) to make successive layers and forming a layered object. In many applications, it is desirable to remove unhardened material followed by heating to remove gellable polysaccharide then sintering.
    Type: Grant
    Filed: May 23, 1996
    Date of Patent: December 9, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Suresh Baskaran, Gordon L. Graff
  • Patent number: 5694753
    Abstract: The present invention is an automated pruning apparatus that requires little or no follow-up hand pruning and requires no sensors to avoid supportive trunks or posts. The present invention uses at least one pair of flat, close angled toothed, counter rotating blades. Woody branches are directed to the counter rotating blades first with a lifting arm and secondly by a quilled drum.
    Type: Grant
    Filed: March 11, 1996
    Date of Patent: December 9, 1997
    Assignee: Battelle Memorial Institute
    Inventor: Roger D. Dellinger
  • Patent number: 5689966
    Abstract: The present invention is an apparatus and method for de-superheating a primary refrigerant leaving a compressor wherein a secondary refrigerant is used between the primary refrigerant to be de-superheated. Reject heat is advantageously used for heat reclaim.
    Type: Grant
    Filed: March 22, 1996
    Date of Patent: November 25, 1997
    Assignee: Battelle Memorial Institute
    Inventors: James A. Zess, M. Kevin Drost, Charles J. Call
  • Patent number: 5680866
    Abstract: The present invention is a method of diagnosing a cardiopulmonary condition in an individual by comparing data from a progressive multi-stage test for the individual to a non-linear multi-variate model, preferably a recurrent artificial neural network having sensor fusion. The present invention relies on a cardiovascular model developed from physiological measurements of an individual. Any differences between the modeled parameters and the parameters of an individual at a given time are used for diagnosis.
    Type: Grant
    Filed: March 29, 1996
    Date of Patent: October 28, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Lars J. Kangas, Paul E. Keller
  • Patent number: 5652192
    Abstract: The material of the present invention is a mixture of catalytically active material and carrier materials, which may be catalytically active themselves. Hence, the material of the present invention provides a catalyst particle that has catalytically active material throughout its bulk volume as well as on its surface. The presence of the catalytically active material throughout the bulk volume is achieved by chemical combination of catalytically active materials with carrier materials prior to or simultaneously with crystallite formation.
    Type: Grant
    Filed: March 28, 1995
    Date of Patent: July 29, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Dean W. Matson, John L. Fulton, John C. Linehan, Roger M. Bean, Thomas D. Brewer, Todd A. Werpy, John G. Darab
  • Patent number: 5646351
    Abstract: The invention is an ultrasonic surface hardness depth measurement apparatus and method permitting rapid determination of hardness depth of shafts, rods, tubes and other cylindrical parts. The apparatus of the invention has a part handler, sensor, ultrasonic electronics component, computer, computer instruction sets, and may include a display screen. The part handler has a vessel filled with a couplant, and a part rotator for rotating a cylindrical metal part with respect to the sensor. The part handler further has a surface follower upon which the sensor is mounted, thereby maintaining a constant distance between the sensor and the exterior surface of the cylindrical metal part. The sensor is mounted so that a front surface of the sensor is within the vessel with couplant between the front surface of the sensor and the part.
    Type: Grant
    Filed: September 18, 1995
    Date of Patent: July 8, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Morris S. Good, George J. Schuster, James R. Skorpik
  • Patent number: 5645072
    Abstract: The apparatus of the present invention is a combination of a breath interface and an external exposure dosimeter interface to a chemical analysis device, all controlled by an electronic processor for quantitatively analyzing chemical analysis data from both the breath interface and the external exposure dosimeter for determining internal tissue dose. The method of the present invention is a combination of steps of measuring an external dose, measuring breath content, then analyzing the external dose and breath content and determining internal tissue dose.
    Type: Grant
    Filed: September 28, 1995
    Date of Patent: July 8, 1997
    Inventors: Karla D. Thrall, Donald V. Kenny, George W. R. Endres, Daniel R. Sisk
  • Patent number: 5645891
    Abstract: The invention is a mesoporous ceramic membrane having substantially uniform pore size. Additionally, the invention includes aqueous and non-aqueous processing routes to making the mesoporous ceramic membranes. According to one aspect of the present invention, inserting a substrate into a reaction chamber at pressure results in reaction products collecting on the substrate and forming a membrane thereon. According to another aspect of the present invention, a second aqueous solution that is sufficiently immiscible in the aqueous solution provides an interface between the two solutions whereon the mesoporous membrane is formed. According to a further aspect of the present invention, a porous substrate is placed at the interface between the two solutions permitting formation of a membrane on the surface or within the pores of the porous substrate. According to yet another aspect of the present invention, mesoporous ceramic materials are formed using a non-aqueous solvent and water-sensitive precursors.
    Type: Grant
    Filed: November 23, 1994
    Date of Patent: July 8, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Jun Liu, Anthony Y. Kim, Jud W. Virden
  • Patent number: 5637209
    Abstract: The present invention is an apparatus for extracting organic compounds from solid materials. A generator vessel has a removable closure for receiving a solid or liquid solvent which is heated with a resistive heating element to a gaseous or supercritical phase. The removable closure is unencumbered because the side wall is penetrated with an outlet for the gaseous or supercritical solvent. The generator vessel further has a pressure transducer that provides an electronic signal related to pressure of the gaseous or supercritical solvent. The apparatus of the present invention further includes at least one extraction cell having a top and a bottom and a wall extending therebetween, wherein the bottom is sealably penetrated by an inlet for gaseous or supercritical solvent received through a manifold connected to the outlet, the top having an easy-open removable closure cap, and the wall having an outlet port.
    Type: Grant
    Filed: January 18, 1996
    Date of Patent: June 10, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Bob W. Wright, Thomas S. Zemanian, William H. Robins, Leslie J. Woodcock
  • Patent number: 5637875
    Abstract: The present invention is a method of increasing radiation response of a radiation detection material for a given radiation signal by first pressurizing the radiation detection material. Pressurization may be accomplished by any means including mechanical and/or hydraulic. In this application, the term "pressure" includes fluid pressure and/or mechanical stress.
    Type: Grant
    Filed: July 7, 1995
    Date of Patent: June 10, 1997
    Assignee: Battelle Memorial Institute
    Inventor: Steven D. Miller
  • Patent number: 5631820
    Abstract: The invention is an improvement of the PASC inverter, wherein the improvements include the reduction from two shorting gates per transformer to one shorting gate per transformer and replacement of active control of the shorting gate with passive control of the shorting gate. Further advantages are obtained through the use of anti-parallel gate sets.
    Type: Grant
    Filed: September 8, 1995
    Date of Patent: May 20, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Matthew K. Donnelly, Donald J. Hammerstrom
  • Patent number: 5619842
    Abstract: The method of the present invention for bagging pre-silage, has the steps of (a) receiving a bale of pre-silage from a loader, (b) compressing the bale in at least one cross section dimension to fit into a bag, and (c) advancing the compressed bale into the bag. The apparatus of the present invention for bagging baled pre-silage, has (a) a support frame having a plurality of lateral walls. The lateral walls define a rear opening to which a bag is attached, and a front opening through which is received the baled pre-silage. At least one of the lateral walls is reversibly movable in a direction toward an opposite lateral wall for compressing or squeezing the baled pre-silage to a size that will fit into the bag. The front opening has a closure and ram for enclosing the baled pre-silage and applying the ram to advnce the compressed baled pre-silage through the rear opening and into the bag.
    Type: Grant
    Filed: December 22, 1995
    Date of Patent: April 15, 1997
    Inventors: David Brubaker, Darin Boone
  • Patent number: 5611214
    Abstract: The invention is a microcomponent sheet architecture wherein macroscale unit processes are performed by microscale components. The sheet architecture may be a single laminate with a plurality of separate microcomponent sections or the sheet architecture may be a plurality of laminates with one or more microcomponent sections on each laminate. Each microcomponent or plurality of like microcomponents perform at least one unit operation. A first laminate having a plurality of like first microcomponents is combined with at least a second laminate having a plurality of like second microcomponents thereby combining at least two unit operations to achieve a system operation.
    Type: Grant
    Filed: July 29, 1994
    Date of Patent: March 18, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Robert S. Wegeng, M. Kevin Drost, Carolyn E. McDonald
  • Patent number: 5597851
    Abstract: The invention is a method of using enzymes from thiophyllic microbes for selectively breaking the sulfur rubber cross-link bonds in vulcanized rubber. The process is halted at the sulfoxide or sulfone step so that a devulcanized layer is reactive with virgin rubber.
    Type: Grant
    Filed: September 14, 1995
    Date of Patent: January 28, 1997
    Assignee: Battelle Memorial Institute
    Inventors: Robert A. Romine, Lesley J. Snowden-Swan
  • Patent number: 5591420
    Abstract: The invention is the new material, a ternary compound of cesium, silica, and titania, together with a method of making the ternary compound, cesium titanium silicate pollucite. More specifically, the invention is Cs.sub.2 Ti.sub.2 Si.sub.4 O.sub.13 pollucite which is a new crystalline phase representing a novel class of Ti-containing zeolites. Compositions contain relatively high Cs.sub.2 O and TiO.sub.2 loadings and are durable glass and ceramic materials. The amount of TiO.sub.2 and Cs.sub.2 that can be incorporated into these glasses and crystalline ceramics far exceeds the limits set for the borosilicate high level waste glass.
    Type: Grant
    Filed: August 25, 1995
    Date of Patent: January 7, 1997
    Assignee: Battelle Memorial Institute
    Inventor: Mari L. Balmer