Abstract: This invention relates to stable, fluid CaCO.sub.3 -containing dispersions, and the preparations thereof by the high temperature decomposition of a Ca carboxylate such as Ca acetate, etc., in a dispersant-containing fluid.
Abstract: This invention relates to the hydrogenation of tetrahydropyrimidines to yield linear N-substituted diamines which can be reacted with carbonyls to form imines, which imines can be reduced to N,N'-substituted diamines as illustrated by N,N'-substituted 2,4-diamino-2-substituted pentanes. The products of this invention are useful as fuel additives.
Type:
Grant
Filed:
December 30, 1976
Date of Patent:
August 7, 1979
Assignee:
Petrolite Corporation
Inventors:
Bernardus A. Oude Alink, Neil E. S. Thompson
Abstract: Quaternary nitrogen-heterocyclic phosphonates wherein the phosphonate group is ortho- or para- to the nitrogen heterocyclic group, where the compounds are characterized as follows: ##STR1## wherein the dotted line represents a cyclic structure which cyclic structure may be the sole cyclic structure, or may be attached to other cyclic groups, where R is a hydrocarbon or a substituted hydrocarbon group such as alkyl, aryl, alkaryl, aralkyl, etc., and X is an anion such as halogen, a sulfite, a sulfate, a sulfonate-containing group, etc.These nitrogen-heterocyclic phosphonates are prepared by reacting an aromatic nitrogen-heterocyclic compound, wherein the nitrogen atom is in the form of a quaternary alkoxy derivative (N--OR hereinafter defined) with a phosphite salt, preferably in the form of an ester of the phosphite, as exemplified by the following equation: ##STR2## Quaternaries of these compounds are prepared by further reaction with a quaternizing agent.
Abstract: This invention relates to copolymers of alpha-olefins and maleic anhydride reacted with amines in the presence of Lewis acids, preferably BF.sub.3 or a complex thereof; and to the use of these products as anti-static agents in organic liquids, preferably in hydrocarbons. The use of Lewis acid produces a unique reaction product which is superior as to fluidity and/or anti-static properties as compared to the corresponding product produced without Lewis acid. In addition, the use of Lewis acid promotes the rate of reaction thus reducing reaction time.
Abstract: Hydroxyalkylaminoalkylamides, the N-alkylated derivatives thereof, and quaternaries thereof are useful as corrosion inhibitors for metals in an aqueous brine environment.
Abstract: This invention relates to stable, fluid magnesium-containing dispersions and the preparations thereof by the high temperature decomposition of Magnesium salts of carboxylic acids to MgO in a dispersant-containing fluid, where less than a stoichiometric amount of carboxylic acid is employed in forming the magnesium carboxylates, based on Mg(OH).sub.2 or equivalent.
Abstract: This invention relates to substituted pyridines prepared by reacting aldehydes, amines, lower carboxylic acids such as acetic acid in the presence of oxygen. The N-substituted pyridinium salts formed can be converted to pyridines by thermal dealkylation.
Type:
Grant
Filed:
August 14, 1975
Date of Patent:
June 19, 1979
Assignee:
Petrolite Corporation
Inventors:
Bernardus A. Oude Alink, Neil E. S. Thompson
Abstract: This invention relates to a process of removing chlorine (Cl.sub.2) and hydrogen chloride (HCl) from a combustion gas, such as a combustion gas formed from incinerating chlorine-containing organic materials, which comprises:(1) Lowering the temperature of the combustion gas below the melting point of cupric chloride or mixture thereof with other salts;(2) Contacting the cooled combustion gas of step (1), in the presence of oxygen, with copper of lower than a divalent oxidation state, such as a cuprous compound or its equivalent in a quantity sufficient to absorb chlorine and hydrogen chloride present in gas, thereby converting the cuprous compound to cupric chloride (in order to absorb substantially all HCl and Cl.sub.
Abstract: A process for the quality improvement of a nonpetroleum organic liquid (fats, animal and vegetable oils) containing color bodies, moisture and alkali soaps as impurities. The organic liquid is subjected to (1) a refining step using an aqueous alkali reagent, (2) admixing with the organic liquid of a finely dispersed solid adsorbent, (3) elevated temperatures dehydrating and deareating the mixture of the organic liquid and dispersed solid adsorbent, and (4) electrofiltration of the mixture of organic liquid and solid adsorbent to provide a solids-free, soaps-free quality improved organic liquid which is passed to a subsequent utilization (e.g., hydrogenation, deodorization, etc.). Electrofiltration is conducted in an atmosphere substantially devoid of oxygen-containing gases and moisture.
Abstract: Phosphonium compounds of the formula ##STR1## where y is --CH.sub.2 OH or --CH.sub.2 OOCCH.sub.2 PR.sub.3, n is an integer of 2-4, R is a substituted group, preferably hydrocarbon, such as alkyl, cycloalkyl, aryl, etc., and X is a negative ion. These compounds are used in inhibiting the corrosion of metals and particularly in preventing corrosion of metals, particularly iron, steel and ferrous alloys.
Abstract: A desalter/dehydrator having a plurality of electrified coalescing stages in a single vessel, wherein the stages are isolated hydraulically to allow parallel or serial stage operations. In one embodiment, several electrical stages, each separately energized, are operated in parallel to proportionately increase vessel throughput capacity. In another embodiment, series operation is employed, wherein each successive stage receives the product from the preceding stage as feed, with fresh water being added. Placement of electrodes, distributors, collectors, etc. are determined by the type of operation to be performed in the vessel.
Abstract: This invention relates to the use of a water soluble maleate salt, preferably disodium maleate, as a scale converter. Such salts convert scale into a water soluble compound which is capable of aqueous removal without the conventional step of employing either (1) an acid wash or (2) a sequestering agent.
Abstract: This invention relates to N-alkyl sulfone containing quaternary ammonium derivatives of 1,4-thiazines; to the preparation thereof; and to the uses thereof, for example as corrosion inhibitors, microbiocides, etc.
Abstract: A process of converting 2,3,4,5-tetrahydropyrimidines (.DELTA.-1) having at least one hydrogen in the 2-position to 3,4,5,6-tetrahydropyrimidines (.DELTA.-2), which comprises hydrogenating and dehydrogenating said .DELTA.-1 tetrahydropyrimidines. Such hydrogenating and dehydrogenating may be done in either two sequential steps or in one step.Said .DELTA.-1 tetrahydropyrimidines can also be converted to .DELTA.-2 tetrahydropyrimidines by heating in the essential absence of a solvent, and preferably under basic conditions.In addition, corresponding hexahydropyrimidines can be converted to corresponding .DELTA.-2 tetrahydropyrimidines by dehydrogenation.This invention also relates to the use of .DELTA.-2 tetrahydropyrimidines, particularly as corrosion inhibitors.
Abstract: This invention relates to hydroxyalkylaminoalkylamides, the N-alkylated derivatives thereof, and the preparaton and uses thereof. This invention also relates to quaternaries of the abovementioned hydroxyalkylaminoalkylamides.
Abstract: This invention relates to N-alkyl thioethers of quaternary ammonium derivatives of 1,4-thiazines; to the preparation thereof; and to the uses thereof for example as corrosion inhibitors, microbiocides, etc.
Abstract: Substituted 2, 3, 4, 5-tetrahydropyridimines (THP) ##STR1## are prepared as follows: (1) The reaction of a carbonyl compound (ketone or aldehyde) with (NH.sub.3 or NH.sub.4 OH) and a sulfur-containing catalyst.(2) The reaction of an .alpha., .beta.-unsaturated ketone and a carbonyl compound and NH.sub.3 (or NH.sub.4 OH) without a catalyst.(3) Reaction of an .alpha., .beta.-unsaturated ketone, a 1-amino-alcohol and NH.sub.3 (or NH.sub.4 OH) without a catalyst.The compositions of this invention react with carbon disulfide to form xanthates, can be isomerized, converted to pyridines, etc.Thp and derivatives of this invention are useful as biocides, anti-oxidants, oxygen scavengers, corrosion inhibitors, etc.
Abstract: This invention relates to unitized, compact, chew-resistant products with or without structure-supporting fibers. These products are prepared from animal foods which are preferably in a dry, shelf-stable form such as dried meals, dried fish, dried dairy products, fish meal, fish flour, cereals, flours, carbohydrates, dried fruits, etc., with or without food additives or supplements such as vitamins, minerals, medicinals, etc., for example chemicals, enzymes, etc., capable of removing plaque or tartar frm the animal's teeth, etc. These products are prepared by:(1) Adding sufficient water to wet the product without affecting its free flowing character;(2) Compacting the wetted product at high pressure;(3) Baking the product.
Type:
Grant
Filed:
March 22, 1973
Date of Patent:
March 20, 1979
Assignee:
SAID Stanton E. Fisher, by said Bernard W. Weinrich