Abstract: A method for determining the density of an at least flowable, in particular liquid, specimen with a rheometer, in particular a rotational rheometer, includes providing the rheometer with a first measurement component for receiving the at least flowable, in particular liquid, specimen, and a second measurement component with a known volume to be immersed into the specimen. The first and second measurement components are movable relative to one another. The perpendicular force between the two measurement components is measured after the immersion of the second measurement component into the specimen. The measured perpendicular force corresponds to the buoyancy force acting between the specimen and the second measurement component. The density of the specimen is calculated based on Archimedes' principle by reference to the known volume of the second measurement component and the measured perpendicular force. A rheometer for carrying out the method is also provided.

Abstract: An X-ray beam generating system including an X-ray source for generating an original primary X-ray beam, an optics system including a first optics component and at least one second optics component which are movable relative to the X-ray source in order either to bring the first optics component into interaction with the original primary X-ray beam, whereupon a first primary X-ray beam is generated which is deflected at a first deflection angle, or to bring the second optics component into interaction with the original primary X-ray beam, whereupon a second primary X-ray beam is generated which is deflected at a second deflection angle, and a rotating device to rotate the X-ray beam generating system through either a first rotation angle or a second rotation angle to allow either the first primary X-ray beam or the second primary X-ray beam to impinge on a sample region.

Abstract: A device for examining a sample by X-radiation having a radiation generation system for generating primary radiation, a first goniometer arm on which the radiation generation system is mounted and which is pivotable about a goniometer axis, a detection system configured to detect secondary radiation emanating from the sample, a second goniometer arm on which the detection system is mounted and which is pivotable about the goniometer axis, and an evacuable sample chamber within which the sample is arrangeable in a sample region encompassing a portion of the goniometer axis, the sample chamber being delimited by a sample chamber wall which has a transmission region which is transmissive to the primary radiation and is vacuum-tight, in order to allow the primary radiation to penetrate into the sample chamber and to impinge on the sample region at different angles of incidence.

Abstract: Described is a measuring drive for a measuring instrument, in particular a rheometer. The measuring drive has: i) a motor, ii) a shaft, which is coupled to the motor in such a way that the shaft is drivable by the motor, and iii) an ultrasonic device, which is configured to provide ultrasound to the shaft in such a way that at least a part of the shaft is bearable substantially without contact by the ultrasound. Furthermore, the measuring instrument, a method, and a using are described.

Abstract: A device determines an oxygen content of a headspace gas in a liquid-filled container. The device contains a piercer, a sampling tube, a piercing head on which the piercer and the sampling tube are disposed, a pump, a ring line, and a sensor unit disposed within the ring line and used to determine the oxygen content and/or an oxygen partial pressure of the headspace gas of the liquid-filled container. The ring line is configured such that the headspace gas of the liquid-filled container can be sampled via the piercer or the piercing head by use of the pump and can be returned into the headspace of the liquid-filled container via the sampling tube.

Abstract: Described is an apparatus for guiding an electromagnetic microwave, having: antenna surrounding walls, which define an interior space so as to surround therein at least an end region of an antenna of a microwave source, in particular laterally annularly as well as frontally; waveguide boundary walls, at least two of which are arranged in parallel to each other, wherein the waveguide boundary walls form a, in particular cuboid-shaped, waveguide having a substantially rectangular cross-section, wherein a cross-sectional plane is defined by a first direction that extends along a longitudinal direction of the antenna and a second direction that extends perpendicularly to the first direction, wherein it holds: 25>a/b>3, wherein a: is a width of the waveguide along the second direction, b: is a height of the waveguide along the first direction, wherein the apparatus is designed to let proceed a microwave from the interior space of the antenna surrounding walls into the waveguide.

Abstract: A method and a device for measuring an oxygen content of a headspace gas in a beverage can. The beverage can is oriented upside down to allow the headspace gas to collect at the bottom. A hollow piercer on a piercing head forms a sampling opening in the bottom of the can through which the sampling tube penetrates. The liquid level in the beverage can is lowered to establish a direct connection of the gas-filled headspace and the sampling opening. Then the headspace gas is transported from the headspace to a sensor unit via the sampling tube and/or the hollow piercer or the piercing head. The oxygen content and/or an oxygen partial pressure and/or a headspace volume of the headspace gas are determined by the sensor unit. The sampling opening is closed off airtight by sealing elements arranged on the piercer or the piercing head.

Abstract: A rotational viscometer for measuring a viscosity of substances contains a measuring shaft and a hollow shaft which is driven by a drive. The measuring shaft is arranged within the hollow shaft. A measuring body is arranged at one end of the measuring shaft and can be supplied with a sample. A coupling element is provided for connecting the hollow shaft to the measuring shaft. An angle measuring unit is arranged relative to the measuring shaft such that an angular difference and/or a rotational phase difference between the hollow shaft and the measuring shaft can be measured. The hollow shaft and the measuring shaft end opposite the measuring body and protrude into a housing. The coupling element is arranged in the housing, and the housing and the coupling element are connected to the measuring shaft and to the hollow shaft such that the housing is removable from the rotational viscometer.

Abstract: A device is provided for IR-spectroscopy and for determining an impairment of a surface which is exposed to measuring radiation during the IR-spectroscopy. The device includes a radiation source to generate the measuring radiation a detector and a sample receptacle for receiving a sample. The sample receptacle is at least partially delimited by the surface. The detector measures radiation after interaction with the sample. The device is configured to measure an IR-reference spectrum of a reference sample which is received in the sample receptacle, evaluate the reference spectrum, determine an indicator of the impairment, wherein evaluating encompasses an integration of a quantity which is based on the reference spectrum over a predetermined integration spectral range, wherein the indicator is determined dependently on a value of the integration.

Abstract: A cap closes a sample vessel for the microwave treatment of samples. The cap contains a closure body for closing the sample vessel. The closure body is fitted to the sample vessel and closes the sample vessel at a sealing surface. A spring-loaded pressure relief valve and a vent duct are provided. The vent duct, the pressure relief valve and the closure body are configured in such a manner that the vent duct connects the closure body via the pressure relief valve to the surrounding area such that when a defined first pressure level is exceeded at the closure body excess pressure can escape through the vent duct into the area surrounding the cap. A reservoir is provided. The reservoir and the vent duct are configured such that condensate precipitating in the vent duct accumulates in the reservoir when the cap is in the state fitted to the sample vessel.

Abstract: A handling apparatus for handling a measuring probe of a scanning probe microscope is disclosed. The measuring probe has a probe body and a probe tip which is coupled with the probe body by a cantilever. The handling apparatus includes a receiving device for receiving the measuring probe at a receiving area, a guide structure, in which the measuring probe is guidable while at the same time the probe body is at least partially limited and the cantilever and the probe tip are supported without contact, and a transport device for transporting the measuring probe from the receiving area along the guide structure to a target area.

Abstract: A method for determining the viscosity of materials uses a rotation viscosimeter having a measuring shaft connected through a coupling element to a drive and a measuring element on a shaft end applied to a sample. An angle measuring unit measures an angle deflection between drive and shaft. The measuring element is immersed in a measuring container containing the sample. The rotational speed of the shaft increases from a first measuring point at an initial speed in steps to further measuring points and the angle deflection between the drive and the shaft is determined in the measuring points. An estimation function is determined for the rotational speed and the angle deflection for the sample using measured values in the measuring points. An optimum rotational speed is determined based on the estimation function of a previously defined optimum angle deflection and the viscosity measurement of the sample is carried out.

Abstract: An arrangement for heating a sample by microwave radiation is provided. The arrangement includes a container having an inner space for accommodating the sample and having a bottom container wall, a wave guide arranged to guide a microwave having an electric field direction, a waveguide adapter being adapted to couple the microwave from the wave guide into the inner space of the container via the bottom container wall being oriented to be different from perpendicular to, in particular substantially parallel to, the electric field vector direction.

Abstract: A rheometer has rotary rheometer and a linear DM(T)A analysis unit. A measuring shaft of the rotary rheometer carries a measuring part that faces a measuring part carried on an adjusting rod of the linear analysis unit. The sample under test is placed in a measuring gap between the measuring parts. The DM(T)A analysis unit has a linear motor, in particular magnetically operated, with a stator and a slider, and a magnetically-operated gravitational compensation unit, by way of which it is possible to compensate for the weight force of the adjusting rod, the measuring part on the adjusting rod, the slider, and any optional the components fastened to the slider.

Abstract: A rheometer includes a measuring shaft unit being rotatably mounted in a stationary support unit and having a measuring shaft carrying a measuring part. Transmitting units having optical transmitters are disposed on the support unit and receiving units having optical receivers are disposed on the measuring shaft unit for data transmission therebetween. A measuring sensor disposed on the measuring shaft detects at least one parameter. The transmitting and receiving units are disposed between the measuring shaft unit and the support unit and are associated with one another for exchanging data. The optical transmitters on the support unit transmit data and energy to the optical receivers on the measuring shaft unit. The transmitting units feed or transmit to the optical receivers at least energy required by the optical transmitters on the measuring shaft unit and the measuring sensor to output or transmit data to the optical receivers.

Abstract: A scanning probe microscope analyses a sample by moving a probe and the sample relative to one another. The scanning probe microscope includes a detection unit for detecting an image of a gap between the sample and the probe in a substantially horizontal side view.

Abstract: A method and a measuring device measure the density of fluid media with a sensor having a density measuring device. A frequency oscillator with mass balance is used as the density sensor and all components related to the frequency oscillator with mass balance for the oscillation behavior, oscillation excitation and oscillation evaluation, as well as the frequency oscillator with mass balance directly associated with the measuring and sensor electronics, are enclosed in a housing or cartridge. These components are used with the frequency oscillator with mass balance in the cartridge, and/or the frequency oscillator with mass balance together with the cartridge is adjusted or calibrated using measurement standards and adapted as necessary to the specific application. The cartridge with the frequency oscillator with mass balance is releasably or replaceably connected with the measuring device or its base body before the beginning of the measuring operation to investigate the media.

Abstract: A scanning probe microscope, in particular an atomic force microscope, for analyzing a sample by moving a probe and the sample relative to one another, wherein the scanning probe microscope includes a detection unit with a side view camera arranged and configured for detecting an image of the sample in a substantially horizontal side view, and a determining unit for determining information indicative of a profile of at least part of a surface of the sample based on the detected image.

Abstract: A microwave heating system comprises a bowl, dome and rotor device. The dome is fit to the bowl. The bowl and dome form a volume. The bowl is connected to a microwave source such that a microwave field is supplied to the volume. The microwave field is attenuated in a region between the rotor device and the dome compared to a region between the bowl and the rotor device. The rotor device is rotatably supported by the bowl and supports a reaction vessel. The rotor device includes a base plate with a through-hole and a tubular member that receives the reaction vessel. The base plate and tubular member are metal. The rotor device is coupled to the base plate so that a longitudinal axis of the tubular member passes through the through-hole.

Abstract: A fixing device selectively fixes a measuring probe of a scanning probe microscope. The fixing device comprises an inserting unit in which the measuring probe is insertable and a master force unit for selectively exerting a master force onto a fixing mechanism. The fixing mechanism is actuatable without a tool. The fixing mechanism is enabled or disabled to controllably detach or fix the measuring probe when the measuring probe is inserted in the inserting unit.