Patents Assigned to Axens
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Patent number: 11208602Abstract: The invention relates to a process for converting a feedstock comprising pyrolysis oil and a heavy hydrocarbon-based feedstock, with: a) a step of hydroconversion in a reactor; b) a step of separating the liquid effluent obtained from step a) into a naphtha fraction, a gas oil fraction, a vacuum gas oil fraction and an unconverted residue fraction; c) a step of hydrocracking of the vacuum gas oil fraction; d) a step of fractionating the hydrocracked liquid effluent obtained from step c) into a naphtha fraction, a gas oil fraction and a vacuum gas oil fraction; e) a step of steam cracking of a portion of the naphtha fraction obtained from step d); f) a step of fractionating at least a portion of the steam-cracked effluent obtained from step e); g) a step in which the pyrolysis oil fraction obtained from step f) is sent into step a).Type: GrantFiled: July 9, 2020Date of Patent: December 28, 2021Assignee: AXENSInventors: Jacinthe Frecon, Delphine Le Bars, Hong Duc Nguyen
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Publication number: 20210389060Abstract: The invention relates to a heat exchanger plate (A; B) comprising a central panel (A0; B0) with at least four sides (A1, A2, A3, A4; B1, B2, B3, B4), said central panel being preferably quadrilateral, or quadrilateral with truncated corners, said plate having: a first side (A1; B1) of the central panel which is inclined with respect to said central panel (A0; B0) and which forms a first joining panel (JA; JB), the opposite side (A3; B3) to said first side (A1; B1) which is flat.Type: ApplicationFiled: September 20, 2019Publication date: December 16, 2021Applicant: AXENSInventors: Henricus NEEFS, Constantin POPESCU
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Patent number: 11198091Abstract: The present invention proposes to use a dry stream which is rich in C4 to C10 hydrocarbons as stripping agent for improving the regeneration of the liquid desiccant according to the invention. This dry stream rich in C4 to C10 hydrocarbons is extracted from the gas derived from the dehydration, for example during a step of extraction of NGL located downstream of the gas dehydration unit. The stream of stripping agent recovered at the outlet of the liquid desiccant regeneration unit may be recycled into the process of the invention or sent to a unit external to the process according to the invention. For example, this stream of stripping agent recovered at the outlet of the regeneration unit is sent to a unit which can receive wet condensates, such as a three-phase separation unit at the inlet of a crude gas processing plant, a condensate stabilization unit, etc.Type: GrantFiled: May 21, 2019Date of Patent: December 14, 2021Assignee: AXENSInventors: Pierre-Yves Lanfrey, Guillaume Parer, Bernard Chambon
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Patent number: 11154830Abstract: The present invention concerns a device for limiting the entrainment of solid particles placed inside a three-phase fluidized reactor, said device being constituted by an assembly of flat or truncated cone-shaped plates ranked vertically in one or more rows, and the maximum horizontal cross section area of the device being in the range 1 to 10 times the horizontal cross section area of the outlet pipework for the gas effluents. It also concerns a three-phase process employing said device.Type: GrantFiled: November 13, 2015Date of Patent: October 26, 2021Assignee: AXENSInventor: Jean-Francois Le Coz
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Publication number: 20210322942Abstract: The invention relates to a device (D) for distributing a fluid, which is able to be arranged in a fixed catalytic bed (C1, C2) of a reactor (R), said device comprising conveying means for conveying said fluid, comprising a plurality of pipes each directly receiving a distinct share of said fluid, distribution means for distributing said fluid, means for generating a local pressure drop in said fluid, such that: the device comprises manifold means (2a) for collecting said fluid together, and providing the fluidic connection between the pipes of said fluid conveying means and said fluid distribution means, said means for generating a local pressure drop are added on to said conveying or distribution or manifold (2a) means.Type: ApplicationFiled: June 27, 2019Publication date: October 21, 2021Applicant: AXENSInventors: Catherine BOUTROT, Jean-Francois LE COZ
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Patent number: 11110431Abstract: An alumina exhibiting a structure with a porosity such that the volume of the pores having a diameter of between 70 and 2000 ? is between 0.15 and 0.50 ml/g, and comprising at least one alkali metal (M), such that the content by weight of alkali metal, expressed as M2O, is between 400 and 1500 ppm, with respect to the total weight of the alumina, and a process for the transformation of a feedstock comprising at least one alcohol into an olefinic effluent, said process comprising a stage of dehydration of said alcohol in the presence of the alumina according to the present invention, having an acidity and a structure with a porosity which are optimal.Type: GrantFiled: July 25, 2019Date of Patent: September 7, 2021Assignee: AXENSInventors: Christophe Nedez, Olivier Ducreux
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Publication number: 20210261483Abstract: The present invention describes a process for obtaining para-xylene from a feedstock containing xylenes, ethylbenzene and C9+ hydrocarbons, said process comprising a single stage A of separation in a simulated moving bed carried out with a zeolite as adsorbent and a desorbent and making it possible to obtain at least three fractions, a fraction A1 comprising a mixture of para-xylene and of desorbent and two fractions A21, A22 comprising ethylbenzene (EB), ortho-xylene (OX) and meta-xylene (MX) and desorbent, said stage is carried out at a temperature between 20° C. and 250° C., under a pressure between the bubble pressure of the xylenes at the operating temperature and 2.0 MPa, and with a ratio by volume of the desorbent to the feedstock in the unit for separation 2 in a simulated moving bed is between 0.4 and 2.Type: ApplicationFiled: June 21, 2019Publication date: August 26, 2021Applicant: AXENSInventors: Isabelle PREVOST, Jerome PIGOURIER, Gerard HOTIER
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Publication number: 20210253963Abstract: The present invention concerns a process for the treatment of a feed comprising biomass, said process comprising at least the following steps: a) a step for drying said feed at a temperature in the range 20° C. to 180° C. for a period in the range 5 to 180 minutes, b) a step for torrefaction of the dried feed obtained from step a) in order to produce at least one solid torrefied biomass effluent, and c) a step for co-grinding the solid torrefied biomass effluent obtained from step b) in the presence of a second biomass feed in order to obtain a powder.Type: ApplicationFiled: June 12, 2019Publication date: August 19, 2021Applicants: IFP Energies Nouvelles, Axens, Commissariat A L?Energie Atomique Et Aux Energies Alternatives, Total Raffinage Chimie, Thyssenkrupp Industrial Solutions AG, Avril, BionextInventors: Thomas PLENNEVAUX, Jeremy GAZARIAN, Laurent BOURNAY, Norbert ULLRICH, Michael HECQUET
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Publication number: 20210214619Abstract: The present invention relates to the extraction of gasoline from a gas G, with (a) a step of extracting gasoline from the gas to be treated comprising methanol GM obtained from step (d), (b) a step of separating said fluid GL1 partially condensed in step (a), producing a first aqueous liquid phase Al , a first liquid phase H1 of hydrocarbon(s) a gaseous phase G1 obtained from the gas G; (c) a step of contacting a portion of the gas G to be treated with said first aqueous liquid phase A1, producing a second aqueous liquid phase A2, a gaseous phase of gas to be treated comprising methanol GM?; (d) a step of mixing said gaseous phase of gas to be treated comprising methanol GM? with the remainder of the gas G to be treated, producing a gas to be treated comprising methanol GM, (e) a step of stabilizing said first liquid phase H1 of hydrocarbon(s).Type: ApplicationFiled: January 13, 2021Publication date: July 15, 2021Applicant: AXENSInventor: Pierre-Yves LANFREY
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Patent number: 11034895Abstract: The present invention describes a process for the production of base oils having a viscosity of greater than 4 centistokes from waste oils originating from industrial use or engine use, said process using a novel configuration for efficient and effective processing.Type: GrantFiled: January 22, 2020Date of Patent: June 15, 2021Assignee: Axens SAInventors: Trushit Oza, Jerome Bonnardot
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Patent number: 11033876Abstract: A structured packing element has the shape of a rectangular flat plate, and is provided with slots and recesses. The slots are intended for assembly by interlocking the structured packing elements together in order to form the structured packing. The recesses are provided in order to form channels within the structured packing. A packing structure can be obtained by assembling such packing elements. Such a packing can be used for an operation of bringing a gas and a catalyst into contact. A manufacturing process of such a structured packing is also disclosed.Type: GrantFiled: September 11, 2018Date of Patent: June 15, 2021Assignee: AXENSInventor: Nicolas Lambert
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Patent number: 11028330Abstract: A facility and a process for hydrotreatment or hydroconversion, in which a fractionation section comprises a stripper which operates on the overhead fraction obtained from a low pressure separator drum.Type: GrantFiled: December 22, 2016Date of Patent: June 8, 2021Assignee: AXENSInventors: Lajeunesse Odile, Pierre-Yves Alspektor, Paris Packeu, Nicolas Pupat
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Patent number: 11015129Abstract: A naphtha hydrotreating process containing a first step in the presence of the first catalyst containing a support; a second step in the presence of the second catalyst containing a support and an active phase, which active phase contains a Group 9 or 10 metal and a Group 6 metal; a third step in the presence of the third catalyst containing a support and an active phase, which active phase contains a Group 6 metal; wherein the content of Group 6 metal of the third catalyst is less than the content of Group 6 metal of the second catalyst; the ratio of the loaded specific surface area of the first catalyst to that of the second catalyst is greater than or equal to 1.20; the ratio of the loaded specific surface area of the third catalyst to that of the second catalyst is greater than 1.07.Type: GrantFiled: April 10, 2020Date of Patent: May 25, 2021Assignee: AXENSInventors: Geoffrey Dubin, Annick Pucci, Boris Hesse
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Publication number: 20210146273Abstract: The present invention relates to a distributor tray (1) comprising chimneys (2) for the passage of gas and means for the passage of liquid. The distributor tray furthermore has at least one casing (10) for distributing the gas. The casing (10) is arranged around a plurality of chimneys (2), and has gas remixing means and gas redistribution means.Type: ApplicationFiled: July 21, 2018Publication date: May 20, 2021Applicants: IFP Energies nouvelles, AXENS, TOTAL SAInventors: Manel FOURATI, Pascal ALIX, Philippe BEARD, Yacine HAROUN, Gauthier PERDU, Xavier COURTIAL, Claire WEISS, Thomas MAUBERT
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Patent number: 10954176Abstract: The present invention relates to a process for producing high-purity para-xylene, comprising a single step of separation by adsorption in an SMB, with a subsequent step of separation by distillation in a first three-fraction distillation column producing at least two raffinates and optionally of two isomerization steps, making it possible to improve the overall para-xylene yield of the aromatic loop and to minimize the economic impact.Type: GrantFiled: June 27, 2019Date of Patent: March 23, 2021Assignee: AXENSInventors: Isabelle Prevost, Jerome Pigourier, Pierre-Yves Martin, Arnaud Cotte
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Publication number: 20210009907Abstract: The invention relates to a process for converting a feedstock comprising pyrolysis oil and a heavy hydrocarbon-based feedstock, with: a) a step of hydroconversion in a reactor; b) a step of separating the liquid effluent obtained from step a) into a naphtha fraction, a gas oil fraction, a vacuum gas oil fraction and an unconverted residue fraction; c) a step of hydrocracking of the vacuum gas oil fraction; d) a step of fractionating the hydrocracked liquid effluent obtained from step c) into a naphtha fraction, a gas oil fraction and a vacuum gas oil fraction; e) a step of steam cracking of a portion of the naphtha fraction obtained from step d); f) a step of fractionating at least a portion of the steam-cracked effluent obtained from step e); g) a step in which the pyrolysis oil fraction obtained from step f) is sent into step a).Type: ApplicationFiled: July 9, 2020Publication date: January 14, 2021Applicant: AXENSInventors: Jacinthe FRECON, Delphine LE BARS, Hong Duc NGUYEN
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Patent number: 10876051Abstract: The present invention relates to a process and a device for separating a feedstock comprising benzene, toluene and C8+ compounds, by means of at least one “reformate” distillation column (C1), one aromatics extraction unit (P1), one para-xylene separation unit (P2), one xylene isomerization unit (P3) and one transalkylation unit (P4), the effluents of said units being separated in the following distillation columns: purification column (C6), deheptanizer (C7) and toluene column (C10), in which at least one of said distillation columns is suitable for being operated under vacuum so that: the majority of the C7? compounds are recovered in the product at the top of the distillation column operated under vacuum, and the majority of the C8+ compounds are recovered in the product at the bottom of the distillation column operated under vacuum.Type: GrantFiled: May 2, 2019Date of Patent: December 29, 2020Assignee: AXENSInventors: Arnaud Cotte, Jérôme Pigourier, Nicolas Pupat
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Patent number: 10850245Abstract: A radial flow distribution system, a radial flow reactor, and components thereof, including one or more of a scallop, center pipe, and/or outer basket. Each of the scallop, the center pipe, and the outer basket has openings formed therein. wherein the sizes or the shapes of the openings vary along the length or the width of the reactor components such that the openings define a pattern in configured to manipulate and optimize the distribution of flow of feedstock out of the components and through the reactor to maximize the efficiency of the catalyst reaction thereof.Type: GrantFiled: June 3, 2019Date of Patent: December 1, 2020Assignees: Axens SA, Woven Metal Products, Inc.Inventors: Pierre-Yves Le-Goff, Fabian Lambert, Matthew Hutchinson, Russell Hillenburg, Eugene Eberhardt
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Patent number: 10837876Abstract: A device for the sampling and extraction of a granular solid in a pack of granular solids, containing a sampling probe (1), a sample collector (2) connected to said sampling probe (1), and a controller (3), the sampling probe (1) comprising a sampling tube (4) and at least one transfer tube (5), the sampling tube (4) and transfer tube (5) containing at least one central conduit and at least two lateral conduits, wherein the central conduit (6a) of the sampling tube (4) contains a collection chamber (10) containing a system (11) for retaining the granular solid, and the lateral conduits (7a, 7b) of the sampling tube (4) and transfer tube (5) are connected to a source of gaseous fluid (12) which is capable of extracting the granular solid retained in the collection chamber (10) via the lateral conduits (8a, 8b) of the sampling tube (4) and transfer tube (5).Type: GrantFiled: November 8, 2016Date of Patent: November 17, 2020Assignee: AXENSInventor: Yvan Despaux
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Patent number: 10815436Abstract: The present invention relates to a device and a process for hydroconversion or hydrotreatment of a hydrocarbon feedstock, comprising in particular at least one coil-wound heat exchanger (S-1), said coil-wound exchanger being a single-pass heat exchanger formed by a vertical chamber in which one or more bundles of tubes are helically wound around a central core, as numerous superposed layers, for: heating and directly distributing a hydrocarbon feedstock/hydrogen stream mixture to a hydrotreatment or hydroconversion reaction section (R-1), and cooling the reaction effluent from the hydrotreatment or hydroconversion reaction section (R-1). The present invention also relates to a use of a coil-wound heat exchanger (S-1) in a process for hydroconversion or hydrotreatment of a hydrocarbon feedstock.Type: GrantFiled: December 20, 2018Date of Patent: October 27, 2020Assignee: AXENSInventors: Claire Silberstein, Odile Lajeunesse, Jacques Rault, Marielle Gagniere