Abstract: A process for preparing a soft textured high strength Alkali Blue pigment toner comprising preparing an initial mixture from an alkali metal hydroxide, Alkali Blue pigment, resin, oil or varnish, free fatty acid and water and adding a mineral acid to said mixture to precipitate the pigment product.
Abstract: The subject of this invention is elastomers containing polyamide groups and polyurea groups in bonded form, which are prepared by the reaction of(a) at least one organic polyisocyanate and/or a modified polyisocyanate mixture having an NCO content of from 8 to 33.6 weight percent,(b) at least one polyazomethine and(c) at least one alkyl-substituted aromatic polyamine having a molecular weight up to 500,in the presence of or in the absence of(d) catalysts,whereby reaction products of polyoxyalkylenepolyamines, having a functionality of from 2 to 4 and an average molecular weight of from 180 to 10,000 and at least one organic aldehyde and/or preferably ketone, are used as the polyazomethines.
Type:
Grant
Filed:
March 15, 1988
Date of Patent:
December 6, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Guenter Matzke, Peter Horn, Hans U. Schmidt
Abstract: Polyhalocopper phthalocyanine pigments of high color strength are prepared by recrystallizing the finely divided agglomerated crude pigment in a heterogeneous aqueous organic phase at elevated temperatures by a process in which the aqueous organic phase used is a heterogeneous mixture of an aliphatic ketone having a total of 3 to 9 carbon atoms and water. The process gives the pigments in the form of spherical granules which are dust-free or have a low dust content. The pigments give deep, brilliant colorations of pure hues.
Abstract: The invention relates to a thermoplastic molding material of an elastomeric polymer A, a shell B grafted to the polymer A, and a copolymer C as rigid matrix. The amount of polymer A is 1 to 25 percent by weight based on the weight of A+B+C. It has a glass transition temperature, Tg, of less than 0.degree. C. and an average particle size of 200 to 750 nanometers (d.sub.50 value of the integral mass distribution) and is composed of: 50 to 99.9 percent by weight of at least one alkylacrylate with 1 to 8 carbon atoms in the alkyl radical and 0.1 to 5 percent by weight of a polyfunctional monomer which has a crosslinking action. Grafting shell B represents 5 to 40 percent by weight based on A+B+C and is composed of at least one of the monomers of the group of(b.sub.1) vinylaromatic monomers, and(b.sub.2) the ethylenically unsaturated monomers.Grafting shell B is prepared in two stages with 30 to 70 percent by weight of the monomers b.sub.
Type:
Grant
Filed:
April 17, 1987
Date of Patent:
November 29, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Juergen Hambrecht, Burghard Schmitt, Johann Swoboda, Georg Wassmuth, Claus Bernhard, Rudolf Stephan
Abstract: The invention relates to water-dispersible binders which are intended for cationic electropaints and are based on reaction products which are formed from modified epoxy resins and primary and/or secondary amines and which can, if desired, also contain crosslinking agents, pigments, flow-control agents and other customary auxiliaries. They contain as reaction products those which have been prepared by reacting(A) low molecular weight epoxy resins which contain epoxy compound aromatic groups and have an epoxide equivalent weight of less than 375 with(B) aliphatic and/or alicyclic polyfunctional alcohols having hydroxyl groups or carboxylic acids having carboxylic groups and both having a molecular weight of less than 350 and addition of the hydroxyl groups and carboxylic groups to the epoxy groups of (A) in such a way that the reaction products of (A) and (B) contain 10-45% of aromatic groups, calculated as the phenylene group, and have terminal epoxy groups.
Type:
Grant
Filed:
March 3, 1983
Date of Patent:
November 29, 1988
Assignee:
BASF Lacke & Farben AG
Inventors:
Wolfgang Batzill, Horst Diefenbach, Michael Geist, Eberhard Schupp
Abstract: 4-Pentenoates are prepared by isomerization by a process in which isomeric pentenoates are treated with a zeolite of the pentasil type at from 50.degree. to 300.degree. C., and the 4-pentenoate is distilled off from the reaction mixture.
Type:
Grant
Filed:
June 3, 1986
Date of Patent:
November 29, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Wolfgang Hoelderich, Wolfgang Richter, Hubert Lendle, Klaus-Dieter Malsch
Abstract: O-(1-Methoxy-2-chloro)ethoxyphenyl N-methylcarbamate is prepared by reacting pyrocatechol carbonate with methylamine and then reacting the resulting pyrocatechol monomethylcarbamate with 1,2-dichloroethyl methyl ether in the presence of a secondary amine.
Abstract: Wholly aromatic mesomorphic polyester amide imides which form a liquid-crystalline fiber-forming melt below 320.degree. C. and are composed of(a) from 5 to 35 mole % of repeat units of the formula I and/or II ##STR1## where the Xs in the formulae I and II can be identical or different and each is --O--, --S--, --SO.sub.2 --, --CO--, --CH.sub.2 --or .dbd.C(CH.sub.3).sub.2 and n is 0 or 1,(b) from 0 to 30 mole % of repeat units of the formulae III and/or IV ##STR2## (c) a molar amount corresponding to the total amount of components a and b of one or more of the repeat units of the formulae V, VI, VII, VIII and IX ##STR3## (d) if desired from 5 to 25 mole % of one or more of the repeat units of the formulae X, XI and XII ##STR4## (e) repeat units of the formula XIII ##STR5## the mole percentages of components (a), (b), (c), (d) and (e) adding up to 100 mole % in each case,the preparation thereof and fibers, films and moldings prepared therefrom.
Type:
Grant
Filed:
December 4, 1986
Date of Patent:
November 29, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Bernd Hisgen, Michael Portugall, Rolf Steinberger
Abstract: Copolymers of ethylene with acrylates or solutions of free acrylic acid in acrylates are prepared in a continuously operated tubular polymerization system at high pressures and temperatures by feeding a mixture of ethylene, acrylate, initiator and, if appropriate, regulant into the polymerization system in the form of a main stream at the inlet point thereof and at the same time through two or more secondary streams, secondary streams (I) being metered in at points where the reaction temperature has just exceeded a maximum temperature due to the heat of polymerization and secondary streams (II) at points which, relative to the direction of flow of the ethylene, are upstream of the feed points of secondary streams (I) and upstream of the respective maximum temperature.
Type:
Grant
Filed:
April 22, 1987
Date of Patent:
November 29, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Klaus Pfleger, Klaus Boettcher, Oskar Buechner, Friedrich Kanne, Siegfried Kursawe, Wieland Zacher
Abstract: Medicinal white oils and medicinal paraffins are prepared from petroleum fractions containing aromatics and nitrogen, oxygen and sulfur compounds, e.g. light and heavy atmospheric gas oils, vacuum gas oils and residues, which have been pretreated in a first stage by acid treatment or catalytic hydrogenation, by hydrogenation in a second stage over a nickel-containing catalyst under from 50 to 200 bar and at elevated temperatures, by a process in which the catalyst used in the second stage and present in the oxide form is reduced with a hydrogen-containing gas, passivated and then again activated with hydrogen, before the hydrogenation to medicinal white oils or paraffins is carried out.
Type:
Grant
Filed:
August 6, 1987
Date of Patent:
November 22, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Thomas Anstock, Walter Himmel, Matthias Schwarzmann, Heinz Dreyer, Ulrich Lebert, Ansgar Eisenbeis
Abstract: Polymeric compositions which undergo crosslinking after drying at room temperature or elevated temperatures and are dissolved or dispersed in water are prepared by reacting polymeric organic compounds containing carbonyl and carboxyl groups with polyhydrazides in the presence of monoketones or monoaldehydes and are dissolved or dispersed in water by partially or completely neutralizing the carboxyl groups.They are useful as crosslinking agents and as binders for coatings on sheet-like substrates.
Type:
Grant
Filed:
October 10, 1986
Date of Patent:
November 22, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Rainer Blum, Rolf Osterloh, Gerhard Neubert, Gerhard Auchter
Abstract: Process for preparing N,N'-dialkyldiaziridines or bicyclic diaziridines of the general formula I or II: ##STR1## where R.sup.1 and R.sup.2 are each alkyl or aryl, A is a substituted or unsubstituted one-membered carbon bridge and B is a substituted or unsubstituted three-membered methylene bridge, by reacting a mixture of two moles of a monoamine or one mole of a 1,3-diamine with one mole of an aldehyde or ketone at 25.degree.-70.degree. C., preferably 40.degree.-50.degree. C., while thoroughly mixing with one mole of an aqueous solution of an alkali metal or alkaline earth metal salt of hypochlorous acid and extracting with an organic solvent, preferably chloroform, from the reaction mixture, as well as bicyclic diaziridines which have 1,3-diazabicyclo-[3.1.0]-hexane as basic structure and are prepared using 2,2-dimethyl-1,3-propylenediamine.
Abstract: Cavities in mining are filled by introducing a mixture consisting of a slurry or sludge which evolves CO.sub.2, foams and solidifies and predominantly comprises alpha-hemihydrate, alpha-CaSO.sub.4. 0.5 H.sub.2 O, an alkali metal or alkaline earth metal carbonate and water, by a method in which the mixture is mixed with a bisulfate-containing aqueous solution or suspension of one or more metals before being introduced into the cavities to be filled.
Type:
Grant
Filed:
August 6, 1987
Date of Patent:
November 22, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Bernd Leutner, Berthold Mueller, Wilhelm Volkenborn
Abstract: A solid material useful for producing hexagonal ferrites comprises a homogeneous mixture of the cations of the composition (I) and one or more anions comprising one or more thermally decomposable anions.
Abstract: A clamp for flexible strip material, e.g. for a tape reel, is designed to be completely separable from a hub and consists of parts (11, 12) which can be connected to one another and to the tape of strip element outside the hub and can be inserted into the hub.The clamp is suitable in principle for any type of reel for tape-like or strip-like material, in particular for magnetic recording media.
Abstract: Hexamethylenemine is obtained by hydrogenating .epsilon.-caprolactam, the latter being vaporized and hydrogenated under a working pressure of less than 10 bar, the gas phase being unsaturated in respect of caprolactam, and the residence time being short.
Type:
Grant
Filed:
May 9, 1984
Date of Patent:
November 22, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Wolfgang Schroeder, Wolfgang Franzischka, Herbert Mueller
Abstract: Polyvinylpyrrolidone having a Fikentscher K value of from 14 to 95 is prepared at from 50.degree. to 95.degree. C. in aqueous solution with hydrogen peroxide as starter, the solution being maintained at pH 7-11 by means of NaOH, KOH, their carbonates or bicarbonates.
Type:
Grant
Filed:
January 19, 1988
Date of Patent:
November 22, 1988
Assignee:
BASF Aktiengesellschaft
Inventors:
Adolf Nuber, Siegfried Lang, Axel Sanner, Gerd Schroeder