Patents Assigned to HITACHI HIGH-TECH SCIENCE CORPORATION
  • Patent number: 10847355
    Abstract: Disclosed is a mass analysis apparatus and method, wherein the precision of detection of a first material including a second material is improved, without enlarging the apparatus, and the measurement time is reduced. The mass analysis apparatus for analyzing a sample containing a first material including an organic compound and at least one second material including an organic compound and having a mass spectrum peak overlapping that of the first material includes a peak correction unit, wherein, when an intensity ratio (peak B)/(peak A) of peak A, not overlapping that of the first material, and peak B, overlapping that of the first material, is a correction coefficient (W), an intensity of a net peak D of the mass spectrum of the first material is calculated by subtracting W×(intensity of peak A) from an intensity of a peak C of the mass spectrum of the first material in the sample.
    Type: Grant
    Filed: December 6, 2019
    Date of Patent: November 24, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Masahiro Sakuta, Shin Okawa, Yoshiki Matoba
  • Patent number: 10837982
    Abstract: To avoid applying overload on both a probe and a sample surface, and to reduce time for measuring irregular shapes on the sample surface in performing an intermittent measurement method, provided is a scanning probe microscope including: a cantilever having a probe attached thereto, the scanning probe microscope being configured to scan a sample surface by intermittently bringing the probe into contact with the sample surface; and a control device configured to perform a first operation of bringing the probe and the sample surface into contact with each other, and a second operation of separating the probe and the sample surface from each other after the first operation. The control device executes the second operation by thermally deforming the cantilever.
    Type: Grant
    Filed: March 22, 2019
    Date of Patent: November 17, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Masatsugu Shigeno, Hiroyoshi Yamamoto, Kazutoshi Watanabe
  • Patent number: 10832890
    Abstract: To automatically repeat an operation of isolating a sample piece, which is formed by processing a sample with an ion beam, and transferring the sample piece to a sample piece holder, a charged particle beam device includes a computer configured to perform control so that, without rotating a needle with which the sample piece is fixed to the sample piece holder, a deposition film deposited on the needle is irradiated with a charged particle beam from a charged particle beam irradiation optical system.
    Type: Grant
    Filed: March 26, 2019
    Date of Patent: November 10, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Masato Suzuki, Satoshi Tomimatsu, Makoto Sato, Tatsuya Asahata
  • Patent number: 10823686
    Abstract: Detection can be performed even for a thick inspection target object through time delay integration without degradation of spatial resolution. There is provided an X-ray inspection device configured to include: an X-ray source that generates X-rays; a transport unit that performs transporting a sample; a detecting unit that has a time delay integration type detector which detects X-rays generated by the X-ray source and transmitted through the sample transported by the transport unit; and a defect determining unit that processes a signal obtained by detecting the X-rays transmitted through the sample by the time delay integration type detector of the detecting unit and determines a defect in the sample. The transport unit performs transporting the sample while causing the sample to rotate in synchronization with the transporting when the sample passes in front of the time delay integration type detector of the detecting unit.
    Type: Grant
    Filed: May 13, 2016
    Date of Patent: November 3, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Yuta Urano, Kaifeng Zhang, Yoshiki Matoba, Akihiro Takeda
  • Patent number: 10801977
    Abstract: A radiation analyzing apparatus includes a radiation irradiation unit configured to irradiate an object with a first radiation, a radiation detection unit configured to detect a second radiation generated from the object irradiated with the first radiation, a radiation converging unit configured to disposed between the object and the radiation detection unit and to converge the second radiation on the radiation detection unit, a position changing unit configured to vary a relative positional relationship between the radiation converging unit and the radiation detection unit, and a driving unit configured to change the positional relationship.
    Type: Grant
    Filed: March 22, 2017
    Date of Patent: October 13, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Atsushi Nagata, Satoshi Nakayama, Keiichi Tanaka, Kazuo Chinone
  • Patent number: 10790112
    Abstract: The focused ion beam apparatus includes: a vacuum container; an emitter tip disposed in the vacuum container and having a pointed front end; a gas field ion source; a focusing lens; a first deflector; a first aperture; an objective lens focusing the ion beam passing through the first deflector; and a sample stage. A signal generator responding to the ion beam in a point-shaped area is formed between the sample stage and an optical system including at least the focusing lens, the first aperture, the first deflector, and the objective lens, and a scanning field ion microscope image of the emitter tip is produced by matching a signal output from the signal generator and scanning of the ion beam by the first deflector with each other.
    Type: Grant
    Filed: February 13, 2018
    Date of Patent: September 29, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventor: Yoshimi Kawanami
  • Patent number: 10718713
    Abstract: In a standard process for determining an unknown sample, fluorescent substances are determined from respective fluorescence characteristics and model coefficients are calculated from spectrum ranges of the fluorescence characteristics of the determined fluorescent substances. An unknown sample is measured after reading of the model coefficients, whereby a target value of the unknown sample is obtained.
    Type: Grant
    Filed: September 6, 2017
    Date of Patent: July 21, 2020
    Assignee: Hitachi High-Tech Science Corporation
    Inventors: Jun Horigome, Koichi Nakamura, Yoichi Sato, Yusuke Hosen, Michinari Kozuma
  • Patent number: 10712363
    Abstract: Provided is a scanning probe microscope with which measurement data and a distribution image of differential data of the measurement data can be displayed selectively or together, an edge enhancement image can be obtained, and user convenience is improved. A scanning probe microscope (200) includes: a distribution image calculator (40a) configured to calculate a one-dimensional or two-dimensional first distribution image (201) of measurement data, and a one-dimensional or two-dimensional second distribution image (202) of differential data of adjacent data elements of the measurement data; and a display controller (40b) configured to instruct the distribution image calculator to calculate at least one of the first distribution image or the second distribution image, and to display the calculated distribution image on a predetermined display.
    Type: Grant
    Filed: January 25, 2019
    Date of Patent: July 14, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Masayuki Iwasa, Yoshiteru Shikakura, Shinya Kudo, Toshihiro Ueno
  • Patent number: 10692695
    Abstract: Provided is a cross-section processing observation method capable of easily and accurately forming a cross-section used to observe a sample's inside, and a cross-section processing observation apparatus for cross-section processing. The method includes a design data acquisition step acquiring design data of a three-dimensional structure of a sample having three-dimensional structure, a moving step moving the sample based on coordinate information of the design data, a surface observation step acquiring an observation image of a surface of the sample, a cross-section forming step irradiating the sample's surface with an ion beam to form a cross-section of the three-dimensional structure, a cross-section observation step acquiring an observation image of the sample's cross-section, and a display step displaying image data, among pieces of the design data, of surface and cross section corresponding to respective locations of the surface and the cross section.
    Type: Grant
    Filed: November 19, 2018
    Date of Patent: June 23, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventor: Xin Man
  • Patent number: 10692688
    Abstract: A charged particle beam apparatus automatically prepares a sample piece from a sample. The apparatus includes a charged particle beam irradiation optical system that emits a charged particle beam. A sample stage with a sample placed thereon is movable relative to the charged particle beam irradiation optical system. A sample piece transferring device holds and transports a sample piece separated and extracted from the sample, and a holder fixing base holds a sample piece holder to which the sample piece is to be transferred. An electrical conduction sensor detects electrical conduction between the sample piece transferring device and an object, and a computer sets a time management mode when electrical conduction between the sample piece transferring device and the sample piece is not detected when the sample piece transferring device and the sample piece are connected to each other.
    Type: Grant
    Filed: January 15, 2018
    Date of Patent: June 23, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Satoshi Tomimatsu, Makoto Sato, Masato Suzuki
  • Patent number: 10677697
    Abstract: According to one embodiment, an automatic sample preparation apparatus includes: a charged particle beam irradiation optical system configured to perform irradiation with a charged particle beam; a sample stage configured to move with the sample placed thereon; a sample piece transfer device for holding and transferring the sample piece separated and extracted from the sample; a sample piece holder-fixing bed configured to hold a sample piece holder to which the sample piece is transferred; a gas supply portion configured to irradiate gas forming a deposition film with the charged particle beam; and a computer configured to control the charged particle beam irradiation optical system, the sample piece transfer device, and the gas supply portion to transfer and stop the sample piece held by the sample piece transfer device with a gap between the sample piece holder and the sample piece, and connect the sample piece to the sample piece holder.
    Type: Grant
    Filed: September 24, 2018
    Date of Patent: June 9, 2020
    Assignee: Hitachi High-Tech Science Corporation
    Inventors: Atsushi Uemoto, Tatsuya Asahata, Makoto Sato, Yo Yamamoto
  • Patent number: 10658143
    Abstract: Disclosed is a method of manufacturing an emitter in which the tip of the emitter can be formed into a desired shape even when various materials are used for the emitter. The method includes performing an electrolytic polishing process of polishing a front end of a conductive emitter material so that a diameter of the front end is gradually reduced toward a tip; performing a first etching process by irradiating a processing portion of the emitter material processed by the electrolytic polishing process with a charged particle beam; performing a sputtering process by irradiating the pointed portion formed by the first etching process with a focused ion beam; and performing a secondary etching process of further sharpening the tip by an electric field induced gas etching processing while observing a crystal structure of the tip of the pointed portion processed by the sputtering process using a field ion microscope.
    Type: Grant
    Filed: February 20, 2019
    Date of Patent: May 19, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Yoko Nakajima, Yoshimi Kawanami, Hironori Moritani, Hiroshi Oba
  • Patent number: 10658147
    Abstract: A charged particle beam apparatus which automatically prepares a sample piece from a sample, includes: a charged particle beam irradiation optical system configured to perform irradiation of a charged particle beam; a sample stage configured to move, the sample being placed on the sample stage; a sample piece relocation unit configured to hold and transport the sample piece which is separated and picked up from the sample; a holder fixing stage which holds a sample piece holder to which the sample piece is relocated; and a computer which performs positional control in relation to a target object based on a template and positional information which is obtained from an image of the target object, the template being generated based on an absorption current image of the target object which is acquired using the irradiation of the charged particle beam.
    Type: Grant
    Filed: March 24, 2017
    Date of Patent: May 19, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Makoto Sato, Satoshi Tomimatsu, Atsushi Uemoto, Tatsuya Asahata
  • Patent number: 10651018
    Abstract: Disclosed is an apparatus for and a method of mass analysis, the apparatus and the method being capable of improving a detection accuracy of a target substance including impurities, without increasing a size of the apparatus, and shortening measuring time. The apparatus analyzing a sample containing a target substance and one or more interfering substances, which have a peak of a mass spectrum overlapping that of the target substance includes: a peak correction unit calculating an intensity of net peak D of the mass spectrum of the target substance by subtracting a total sum of estimated intensities of the peak B, which are calculated every predetermined time interval according to the intensity of the peak A and a nonlinear relation F between the peak A and the peak B, from an intensity of peak C of a mass spectrum of the target substance of the sample.
    Type: Grant
    Filed: January 10, 2019
    Date of Patent: May 12, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Masahiro Sakuta, Yoshiki Matoba
  • Patent number: 10648081
    Abstract: The invention provides a method of burying trenches of a sample comprises at least the steps of: from the sample having the trenches extending from one surface into a depth direction, cutting a sample piece of a small part including the trenches; and by irradiating an electron beam toward the inside of the trenches from a side surface extending along the depth direction of the sample piece and simultaneously injecting a compound gas into the inside of the trenches from openings on the side of the one surface of the trench, decomposing the compound gas with secondary electrons generated by irradiation of the electron beam and depositing constituents of the compound gas within the trenches. Therefore, the method can bury the trenches uniformly without generating cavities within the trenches even if the trenches of the sample piece have a high aspect ratio deep in a depth direction.
    Type: Grant
    Filed: March 28, 2018
    Date of Patent: May 12, 2020
    Assignee: Hitachi High-Tech Science Corporation
    Inventor: Shota Torikawa
  • Patent number: 10651006
    Abstract: According to an embodiment of the present invention, an ion beam apparatus switches between an operation mode of performing irradiation with an ion beam most including H3+ ions and an operation mode of performing irradiation with an ion beam most including ions heavier than the H3+.
    Type: Grant
    Filed: March 26, 2018
    Date of Patent: May 12, 2020
    Assignee: Hitachi High-Tech Science Corporation
    Inventors: Shinichi Matsubara, Yoshimi Kawanami, Hiroyasu Shichi
  • Patent number: 10636619
    Abstract: Disclosed is a charged particle beam apparatus including a stage supporting a sample holder; a stage driving mechanism; a sample chamber; a focused ion beam column; an electron beam column; a detector detecting secondary ions or secondary electrons generated from the sample; a reading unit reading identification information attached to the sample holder; a memory unit storing holder shape information indicating a correspondence relationship between the identification information and a shape of the sample holder, and design information that is shape information of an internal structure of the sample chamber; and a stage driving range limiting unit limiting a driving range of the stage supporting the sample holder on the basis of the shape of the sample holder that is acquired from the identification information read by the reading unit and the holder shape information, and on the basis of a shape of the internal structure.
    Type: Grant
    Filed: February 19, 2019
    Date of Patent: April 28, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventor: Hiroyuki Suzuki
  • Patent number: 10636615
    Abstract: A composite beam apparatus includes an electron beam column for irradiating an electron beam onto a sample, a focused ion beam column for irradiating a focused ion beam onto the sample to form a cross section, and a neutral particle beam column having an acceleration voltage set lower than that of the focused ion beam column for irradiating a neutral particle beam onto the sample to perform finish processing of the cross section. The electron beam column, the focused ion beam column, and the neutral particle beam column are arranged such that the beams of the columns cross each other at an irradiation point. A controller controls the electron beam column to irradiate and scan the electron beam on the sample during cross section processing by the focused ion beam column and during finish processing by the neutral particle beam column.
    Type: Grant
    Filed: February 8, 2019
    Date of Patent: April 28, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventor: Tatsuya Asahata
  • Patent number: 10629411
    Abstract: (Task) To repeatedly perform an operation of extracting a sample piece formed by processing a sample with an ion beam and of transferring the extracted sample piece to a sample piece holder. (Problem Solving Means) A charged particle beam apparatus includes a computer that sets a shaping processing region including a bottom portion of sample piece in a thickness direction of the sample piece corresponding to a depth direction at the time of processing a sample after a needle holds the sample piece, and controls a focused ion beam irradiation optical system to irradiate the shaping processing region with a focused ion beam to thereby shape the sample piece.
    Type: Grant
    Filed: November 15, 2018
    Date of Patent: April 21, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Satoshi Tomimatsu, Tatsuya Asahata, Makoto Sato, Masato Suzuki
  • Patent number: 10622187
    Abstract: Disclosed are a charged particle beam apparatus wherein the charged particle beam apparatus can efficiently performs finish processing of a sample and acquisition of a high-precision SEM image of a processing surface of the sample in a short time, and a sample processing observation method using the same. The charged particle beam apparatus includes: a gallium ion beam column radiating a gallium ion beam toward a sample to form a cross-section of the sample; an electron beam column having a semi-in-lens type objective lens and radiating an electron beam toward the sample; a gas ion beam column radiating a gas ion beam toward the sample to perform finish processing of the cross-section of the sample, wherein the gas ion beam has a beam diameter larger than a maximum diameter of the cross-section of the sample.
    Type: Grant
    Filed: February 19, 2019
    Date of Patent: April 14, 2020
    Assignee: HITACHI HIGH-TECH SCIENCE CORPORATION
    Inventors: Yo Yamamoto, Shota Torikawa, Hidekazu Suzuki, Hiroyuki Suzuki, Mamoru Okabe, Tatsuya Asahata