Patents Assigned to Midwest Research Institute
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Patent number: 5785837Abstract: A process for the preparation by electrodeposition of metal oxide film and powder compounds for ferroelectric memory materials and ferrites wherein the metal oxide includes a plurality of metals. The process comprises providing an electrodeposition bath, providing soluble salts of the metals to this bath, electrically energizing the bath to thereby cause formation of a recoverable film of metal on the electrode, recovering the resultant film as a film or a powder, and recovering powder formed on the floor of the bath. The films and powders so produced are subsequently annealed to thereby produce metal oxide for use in electronic applications. The process can be employed to produce metal-doped metal oxide film and powder compounds for transparent conductors. The process for preparation of these metal-doped metal oxides follows that described above.Type: GrantFiled: January 2, 1996Date of Patent: July 28, 1998Assignee: Midwest Research InstituteInventors: Raghu Nath Bhattacharya, David S. Ginley
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Patent number: 5785852Abstract: A process and apparatus for pretreating microbial sludges in order to enhance secondary anaerobic digestion. The pretreatment process involves disrupting the cellular integrity of municipal sewage sludge through a combination of thermal, explosive decompression and shear forces. The sludge is pressurized and pumped to a pretreatment reactor where it is mixed with steam to heat and soften the sludge. The pressure of the sludge is suddenly reduced and explosive decompression forces are imparted which partially disrupt the cellular integrity of the sludge. Shear forces are then applied to the sludge to further disrupt the cellular integrity of the sludge. Disrupting cellular integrity releases both soluble and insoluble organic constituents and thereby renders municipal sewage sludge more amenable to secondary anaerobic digestion.Type: GrantFiled: April 6, 1995Date of Patent: July 28, 1998Assignee: Midwest Research InstituteInventors: Christopher J. Rivard, Nicholas J. Nagle
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Patent number: 5785769Abstract: A substrate for a photovoltaic device wherein the substrate is the base upon which photosensitive material is to be grown and the substrate comprises an alloy having boron in a range from 0.1 atomic % of the alloy to 1.3 atomic % of the alloy and the substrate has a resistivity less than 3.times.10.sup.-3 ohm-cm.Type: GrantFiled: January 27, 1995Date of Patent: July 28, 1998Assignee: Midwest Research InstituteInventor: Theodore F. Ciszek
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Patent number: 5776819Abstract: A method of producing hydrogenated amorphous silicon on a substrate by flowing a stream of safe (diluted to less than 1%) silane gas past a heated filament.Type: GrantFiled: May 25, 1994Date of Patent: July 7, 1998Assignee: Midwest Research InstituteInventors: Archie Harvin Mahan, Edith C. Molenbroek, Brent P. Nelson
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Patent number: 5757474Abstract: A method and apparatus for measuring characteristics of a piece of material, typically semiconductor materials including photovoltaic devices. The characteristics may include dislocation defect density, grain boundaries, reflectance, external LBIC, internal LBIC, and minority carrier diffusion length. The apparatus includes a light source, an integrating sphere, and a detector communicating with a computer. The measurement or calculation of the characteristics is calibrated to provide accurate, absolute values. The calibration is performed by substituting a standard sample for the piece of material, the sample having a known quantity of one or more of the relevant characteristics. The quantity measured by the system of the relevant characteristic is compared to the known quantity and a calibration constant is created thereby.Type: GrantFiled: June 28, 1995Date of Patent: May 26, 1998Assignee: Midwest Research InstituteInventors: Bhushan L. Sopori, Larry C. Allen, Craig Marshall, Robert C. Murphy, Todd Marshall
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Patent number: 5747967Abstract: A method and apparatus for maximizing the electric power output of a photovoltaic array connected to a battery where the voltage across the photovoltaic array is adjusted through a range of voltages to find the voltage across the photovoltaic array that maximizes the electric power generated by the photovoltaic array and then is held constant for a period of time. After the period of time has elapsed, the electric voltage across the photovoltaic array is again adjusted through a range of voltages and the process is repeated. The electric energy and the electric power generated by the photovoltaic array is delivered to the battery which stores the electric energy and the electric power for later delivery to a load.Type: GrantFiled: February 22, 1996Date of Patent: May 5, 1998Assignee: Midwest Research InstituteInventors: Eduard Muljadi, Roger W. Taylor
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Patent number: 5747099Abstract: A vertical two chamber reaction furnace. The furnace comprises a lower chamber having an independently operable first heating means for heating the lower chamber and a gas inlet means for admitting a gas to create an ambient atmosphere, and an upper chamber disposed above the lower chamber and having an independently operable second heating means for heating the upper chamber. Disposed between the lower chamber and the upper chamber is a vapor permeable diffusion partition. The upper chamber has a conveyor means for conveying a reactant there through. Of particular importance is the thallinating of long-length thallium-barium-calcium-copper oxide (TBCCO) or barium-calcium-copper oxide (BCCO) precursor tapes or wires conveyed through the upper chamber to thereby effectuate the deposition of vaporized thallium (being so vaporized as the first reactant in the lower chamber at a temperature between about 700.degree. and 800.degree. C.Type: GrantFiled: January 5, 1996Date of Patent: May 5, 1998Assignee: Midwest Research InstituteInventor: Richard D. Blaugher
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Patent number: 5731031Abstract: A process for chemical bath deposition of selenide and sulfide salts as films and powders employable as precursors for the fabrication of solar cell devices. The films and powders include (1) Cu.sub.x Se.sub.n, wherein x=1-2 and n=1-3; (2) Cu.sub.x Ga.sub.y Se.sub.n, wherein x=1-2, y=0-1 and n=1-3; (3) Cu.sub.x In.sub.y Se.sub.n, wherein x=1-2.27, y=0.72-2 and n=1-3; (4) Cu.sub.x (InGa).sub.y Se.sub.n, wherein x=1-2.17, y=0.96-2 and n=1-3; (5) In.sub.y Se.sub.n, wherein y=1-2.3 and n=1-3; (6) Cu.sub.x S.sub.n, wherein x=1-2 and n=1-3; and (7) Cu.sub.x (InGa).sub.y (SeS).sub.n, wherein x=1-2, y=0.07-2 and n=0.663-3.Type: GrantFiled: December 20, 1995Date of Patent: March 24, 1998Assignee: Midwest Research InstituteInventors: Raghu Nath Bhattacharya, Rommel Noufi, Li Wang
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Patent number: 5730837Abstract: A method for separating lignocellulosic material into (a) lignin, (b) cellulose, and (c) hemicellulose and dissolved sugars. Wood or herbaceous biomass is digested at elevated temperature in a single-phase mixture of alcohol, water and a water-immiscible organic solvent (e.g., a ketone). After digestion, the amount of water or organic solvent is adjusted so that there is phase separation. The lignin is present in the organic solvent, the cellulose is present in a solid pulp phase, and the aqueous phase includes hemicellulose and any dissolved sugars.Type: GrantFiled: December 2, 1994Date of Patent: March 24, 1998Assignee: Midwest Research InstituteInventors: Stuart K. Black, Bonnie R. Hames, Michele D. Myers
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Patent number: 5726053Abstract: The invention relates to microorganisms which normally do not ferment pentose sugar and which are genetically altered to ferment pentose sugar to produce ethanol, and fermentation processes utilizing the same. Examples include Zymomonas mobilis which has been transformed with combinations of E. coli genes for xylose isomerase, xylulokinase, transaldolase, transketolase, L-arabinose isomerase, L-ribulokinase, and L-ribulose-5-phosphate 4-epimerase. Expression of the added genes are under the control of Zymomonas mobilis promoters. These newly created microorganisms are useful for fermenting pentoses and glucose, produced by hydrolysis of hemicellulose and cellulose, to produce ethanol.Type: GrantFiled: April 14, 1995Date of Patent: March 10, 1998Assignee: Midwest Research InstituteInventors: Stephen K. Picataggio, Min Zhang, Christina K. Eddy, Kristine A. Deanda
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Patent number: 5716736Abstract: The present invention relates to the composition of a solid lithium-ion electrolyte based on the Li.sub.2 O--CeO.sub.2 --SiO.sub.2 system having good transparent characteristics and high ion conductivity suitable for uses in lithium batteries, electrochromic devices and other electrochemical applications.Type: GrantFiled: October 6, 1995Date of Patent: February 10, 1998Assignee: Midwest Research InstituteInventors: Ji-Guang Zhang, David K. Benson, C. Edwin Tracy
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Patent number: 5712187Abstract: A method of depositing a semiconductor material on a substrate. The method sequentially comprises (a) providing the semiconductor material in a depositable state such as a vapor for deposition on the substrate; (b) depositing the semiconductor material on the substrate while heating the substrate to a first temperature sufficient to cause the semiconductor material to form a first film layer having a first grain size; (c) continually depositing the semiconductor material on the substrate while cooling the substrate to a second temperature sufficient to cause the semiconductor material to form a second film layer deposited on the first film layer and having a second grain size smaller than the first grain size; and (d) raising the substrate temperature, while either continuing or not continuing to deposit semiconductor material to form a third film layer, to thereby anneal the film layers into a single layer having favorable efficiency characteristics in photovoltaic applications.Type: GrantFiled: November 9, 1995Date of Patent: January 27, 1998Assignee: Midwest Research InstituteInventors: Xiaonan Li, Peter Sheldon
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Patent number: 5712133Abstract: The invention relates to microorganisms which normally do not ferment pentose sugar and which are genetically altered to ferment pentose sugar to produce ethanol, and fermentation processes utilizing the same. Examples include Zymomonas mobilis which has been transformed with combinations of E. coli genes for xylose isomerase, xylulokinase, transaldolase, transketolase, L-arabinose isomerase, L-ribulokinase, and L-ribulose 5-phosphate 4-epimerase. Expression of the added genes are under the control of Zymomonas mobilis promoters. These newly created microorganisms are useful for fermenting pentoses and glucose, produced by hydrolysis of hemicellulose and cellulose, to produce ethanol.Type: GrantFiled: April 14, 1995Date of Patent: January 27, 1998Assignee: Midwest Research InstituteInventors: Stephen K. Picataggio, Min Zhang, Christina K. Eddy, Kristine A. Deanda, Mark Finkelstein, Ali Mohagheghi, Mildred M. Newman, James D. McMillan
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Patent number: 5712142Abstract: The gene encoding Acidothermus cellulolyticus E1 endoglucanase is cloned and expressed in Pichia pastoris. A new modified E1 endoglucanase enzyme comprising the catalytic domain of the full size E1 enzyme demonstrates enhanced thermostability and is produced by two methods. The first method of producing the new modified E1 is proteolytic cleavage to remove the cellulose binding domain and linker peptide of the full size E1. The second method of producing the new modified E1 is genetic truncation of the gene encoding the full size E1 so that the catalytic domain is expressed in the expression product.Type: GrantFiled: February 22, 1996Date of Patent: January 27, 1998Assignee: Midwest Research InstituteInventors: William S. Adney, Steven R. Thomas, John O. Baker, Michael E. Himmel, Yat-Chen Chou
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Patent number: 5711803Abstract: A process for the preparation of a semiconductor film. The process comprises depositing nanoparticles of a semiconductor material onto a substrate whose surface temperature during nanoparticle deposition thereon is sufficient to cause substantially simultaneous fusion of the nanoparticles to thereby coalesce with each other and effectuate film growth.Type: GrantFiled: September 29, 1995Date of Patent: January 27, 1998Assignee: Midwest Research InstituteInventors: Martin Pehnt, Douglas L. Schulz, Calvin J. Curtis, David S. Ginley
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Patent number: 5705369Abstract: The invention relates to the prehydrolysis of lignocellulose by passing an acidic or alkaline solution through solid lignocellulosic particles with removal of soluble components as they are formed. The technique permits a less severe combination of pH, temperature and time than conventional prehydrolysis. Furthermore, greater extraction of both hemicellulose and lignin occurs simultaneously in the same reactor and under the same conditions.Type: GrantFiled: May 18, 1995Date of Patent: January 6, 1998Assignee: Midwest Research InstituteInventors: Robert W. Torget, Kiran L. Kadam, Teh-An Hsu, George P. Philippidis, Charles E. Wyman
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Patent number: 5692491Abstract: An unglazed transpired solar collector using solar radiation to heat incoming air for distribution, comprising an unglazed absorber formed of low thermal-conductance material having a front surface for receiving the solar radiation and openings in the unglazed absorber for passage of the incoming air such that the incoming air is heated as it passes towards the front surface of the absorber and the heated air passes through the openings in the absorber for distribution.Type: GrantFiled: April 19, 1996Date of Patent: December 2, 1997Assignee: Midwest Research InstituteInventors: Craig B. Christensen, Charles F. Kutscher, Keith M. Gawlik
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Patent number: 5679580Abstract: Dissolved components of a liquid sample are recovered for analysis by delivering the sample to a concentrator comprising a cylindrical receptacle into which an uncontaminated gas, such as air, is introduced in a direction tangentially of the cylindrical wall. The gas is under sufficient pressure to effect swirling of the gas and liquid sample and atomization of the sample to rapidly evaporate the same and cause a residue containing the dissolved components to be deposited on the interior surface of the wall. A reconstituting solvent is then admitted to the receptacle to dissolve the residue and provide a reconstituted, concentrated sample for analysis. If desired, the sample may be concentrated to a given volume rather than to complete dryness. In nonlaboratory applications, a dilute liquid substance may be processed by rapid evaporation to provide a final product of desired concentration.Type: GrantFiled: September 14, 1995Date of Patent: October 21, 1997Assignee: Midwest Research InstituteInventors: Carroll E. Ball, Paul G. Gorman, Michael F. Fischer, Brian R. Cage, David H. Steele
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Patent number: 5661670Abstract: The present invention is a system and method for simulating the performance of a cooling tower. More precisely, the simulator of the present invention predicts values related to the heat and mass transfer from a liquid (e.g., water) to a gas (e.g., air) when provided with input data related to a cooling tower design. In particular, the simulator accepts input data regarding: (a) cooling tower site environmental characteristics; (b) cooling tower operational characteristics; and (c) geometric characteristics of the packing used to increase the surface area within the cooling tower upon which the heat and mass transfer interactions occur. In providing such performance predictions, the simulator performs computations related to the physics of heat and mass transfer within the packing.Type: GrantFiled: May 25, 1995Date of Patent: August 26, 1997Assignee: Midwest Research InstituteInventors: Desikan Bharathan, A. Vahab Hassani
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Patent number: 5643485Abstract: A cooking utensil with improved heat retention includes an inner pot received within an outer pot and separated in a closely spaced-apart relationship to form a volume or chamber therebetween. The chamber is evacuated and sealed with foil leaves at the upper edges of the inner and outer pot. The vacuum created between the inner and outer pot, along with the minimum of thermal contact between the inner and outer pot, and the reduced radiative heat transfer due to low emissivity coatings on the inner and outer pot, provide for a highly insulated cooking utensil. Any combination of a plurality of mechanisms for selectively disabling and re-enabling the insulating properties of the pot are provided within the chamber.Type: GrantFiled: November 21, 1994Date of Patent: July 1, 1997Assignee: Midwest Research InstituteInventors: Thomas F. Potter, David K. Benson, Steven D. Burch