Abstract: A process for producing calcium hypochlorite from lime containing insoluble impurities comprises reacting the lime with an aqueous solution of hypochlorous acid to form a reaction mixture comprised of coarse dibasic calcium hypochlorite crystals and fine insolubles comprised of fine dibasic calcium hypochlorite crystals, insoluble impurities, and unreacted lime. Coarse dibasic calcium hypochlorite crystals are separated from the reaction mixture, leaving a slurry comprised of an aqueous calcium hypochlorite solution containing fine insolubles. The slurry of fine insolubles is separated and the resulting clarified aqueous calcium hypochlorite solution is used to wash occluded fine insolubles from the coarse dibasic crystals. The resulting wash solution is combined with fine insolubles and the resulting slurry is reacted with hypochlorous acid and filtered to remove insoluble lime impurities.

Abstract: An apparatus and process for operating a rolling mill having at least two rolls rotating at different speeds to produce a continuous strip material having a substantially constant final thickness comprises a mechanism for controlling the magnitude of the compressive force between the rolls in response to the ratio of the incoming strip speed to the outgoing strip speed. A mechanism is provided for comparing the ratio of the strip speeds to a ratio of the roll speeds and for adjusting the compressive force magnitude until the two speed ratios are substantially equal. In this manner, the amount of off-stage strip material produced during mill start-up is reduced and process stability and gage control during steady state operation is enhanced.

Abstract: An electromagnetic casting system for casting materials comprising the apparatus and process for electromagnetically containing and forming molten material during a casting run into a desired shape. During the casting run, a liquid-solid interface defines molten material head and solid material portions of the casting. The electromagnetic containing and forming device includes an inductor applying a magnetic field to the molten material. The magnetic field defines a containment zone for the molten material. An alternating current is applied to the inductor to generate the magnetic field. The improvement comprises controlling the location of the liquid-solid interface in the containment zone. The location of the liquid-solid interface along the periphery of the casting is monitored.

Abstract: A duplex rolling process and apparatus for working a metal or alloy subject to the formation of strain induced martensite. The metal or alloy is first worked at an elevated temperature wherein the formation of strain induced martensite is substantially suppressed or eliminated. The metal or alloy is then worked at a lower temperature wherein the formation of strain induced martensite is promoted whereby working is carried out more efficiently.

Abstract: An electrochemical oxidation treatment for monolithic cathode structures having a Beta phase Raney nickel alloy surface thereon is disclosed. When a freshly leached structure is made the anode in an electrochemical cell, which is operated at a current density of between about 40 and about 60 mA/cm.sup.2 until the polarization voltage is reduced from the open circuit value of about -1250 mV by about 500 to about 700 mV, the treated structure is free of subsequent problems with pyrophoricity. Cathodic structures treated this way show substantially no difference in hydrogen overvoltage characteristics and long-term stabilities when compared to chemically depyrophoricized materials of the same composition and structure.

Abstract: A disposable bed filter for removing particulate matter and/or reducing oxygen in a poured metal melt is located within a trough. The bed filter preferably comprises discrete layers of bed media located in a trough between entry and exit baffle plates. The layers of bed media include a layer of coarse media and a layer of fine media. The trough is preferably provided with a closeable lid to permit removal of the bed media and to compensate for buoyancy of the bed media if present. In its preferred use, the bed filter forms part of a process for making a metal alloy wherein the bed filter simultaneously reduces the oxygen content of the melt and filters particulate matter from the melt.

Abstract: This invention relates to a rolling mill apparatus and process which utilizes the creation of a differential friction force in at least the most downstream one of a plurality of roll bites for a variety of purposes. In a first embodiment, a differential friction force is created at the most downstream roll bite for reducing the maximum strip tension and forward strip tension thereby increasing the maximum attainable reduction in strip thickness per pass and reducing the size of the recoiler used for applying the forward tension. In a second embodiment, differential friction forces are created at the most upstream roll bite and the most downstream roll bite for increasing strip tension at all of the roll bites while decreasing the separating force required to obtain given strip reductions without increasing the maximum strip tension.

Abstract: The disclosure teaches improved cast copper alloys exhibiting surprisingly good hot rollability and a method of processing copper base alloys to provide cast structures having good hot rollability, especially those containing silicon and tin. In accordance with the method of the invention, ingots are direct chill cast in a mold from liquid metal wherein the melt temperature entering the mold is 100.degree. to 350.degree. C. in excess of the liquidus temperature.

Abstract: A process for restructuring thin strip semiconductor material is disclosed. It comprises the steps of providing relative movement between the thin strip material and the heating station. The thin strip material is heated at the heating station to a desired temperature between the recrystallization temperature and the melting temperature. The strip is maintained at the desired temperature whereby preferred recrystallization and stress relief occurs within the material. In addition, the thin strip material may be elongated through elevating the temperature of the thin strip and/or increasing the longitudinal tension on the strip.

Abstract: A casing for an electrical component comprises a metal base member. A metal housing member is mounted on the base member to provide a hollow enclosed casing for receiving the electrical component. A metal lead frame is provided within the enclosed casing and is electrically connected to the electrical component. The lead frame has terminal leads projecting between the base member and the housing member external to the casing. The improvement comprises a device extending from the base member for strengthening the base member and providing additional heat transfer from the casing. Also, an adhesive seals and bonds the terminal leads to both the base member and to the housing member to form the enclosed casing.

Abstract: An apparatus for measuring the liquid level adjacent the bottom of a slurry vessel is provided with a liquid level indicator that works in conjunction with a flow conduit which passes through a container with an imperforate side surface that covers a first open-topped fluid retaining container to permit the liquid within the slurry vessel to enter the open-top first fluid retaining container and the flow conduit in response to the level of liquid within the slurry vessel.

Abstract: An electrolytic diaphragm cell for the electrolysis of an aqueous solution of an alkali metal chloride is comprised of a cell body having a porous diaphragm separating the cell body into an anode compartment and a cathode compartment. The anode compartment contains at least one anode and the cathode compartment contains at least one cathode. The cathode is comprised of a formaminous metal conductor and a reticulate cathode, with the reticulate cathode being positioned between and in contact with the porous diaphragm and the foraminous metal conductor. The cell has means adapted to supply electric current to the anodes and the cathodes, nd inlets and outlets in the cell body adapted to supply and remove fluids. The electrolytic diaphragm cell of the present invention operates at reduced electrical power consumption by employing three dimensional cathodes having increased internal surface area and increased porosity.

Abstract: An electrical connector arrangement comprises a first element adapted to be in contact for substantial periods of time with a second element. The first element comprises a first metal substrate having an outer layer of a copper base alloy comprising from about 2 to about 12% aluminum, about 0.001 to about 3% silicon, and the balance essentially copper. The second element comprises a second metal substrate having a gold or gold base alloy contact surface.

Abstract: Described are selected siloxane adducts of tris(2-hydroxyethyl)isocyanurate having the formula: ##STR1## wherein each R and R' is individually selected from lower alkyl groups having 1 to 4 carbon atoms and lower alkoxy groups having 1 to 4 carbon atoms; and the sum of m, n, and p is from 0 to about 20; with the proviso that each R' is a lower alkoxy group when the sum of m, n, and p is 0. These siloxane adducts are also described as good functional fluids, particularly as lubricants and lubricant additives.

Abstract: A fire and heat resistant container having at least the sidewall partially formed from fibrous material with an inner surface and an outer surface that has a plurality of laminae of predetermined composition and thickness arrayed in a specific manner therebetween is provided to protect an object or substance adjacent the inner surface from a fire or heat generating source adjacent the outer surface. The laminae are bonded together by a fire resistant bonding agent of predetermined thickness.

Abstract: An improved cathode with a conductive metal core and a Raney-type catalytic surface predominantly derived from an adherent Beta Nickel (NiAl.sub.3) crystalline precursory outer portion of the metal core is disclosed. The precursory outer portion preferably has molybdenum added to give a precursor alloy having the formula Ni.sub.x Mo.sub.1-x Al.sub.3 where x is within the range of from about 5 to about 15 weight percent. Also disclosed is a method of producing a low overvoltage cathode. The method includes the steps of taking a Ni-Mo core or substrate having about 5-20 weight percentage of Mo and coating it with aluminum then heat treating to form a Ni-Mo-Al alloy with mostly a Beta Nickel structure and then leaching out the Al to produce a Raney surface.

Abstract: Selective heating of edge and near-edge portions of a strip material is used to increase the ductility of the strip material at these portions and to improve the cold rollability and/or strip annealability of the strip material. The selective heating may be performed either by radiant heating or by induction heating.

Abstract: Disclosed is a process for making potassium ferrate (K.sub.2 FeO.sub.4) by reacting substantially pure KOH, C1.sub.2, and a ferric salt in the presence of a stabilizing proportion of at least one ferrate-stabilizing compound (e.g., a combination of an alkali metal silicate and an alkali metal iodine-containing salt). The formed K.sub.2 FeO.sub.4 is separated and recovered from other reaction co-products [KCl, H.sub.2 O, KOCl, and Fe(OH).sub.3 ] and excess KOH. Other specific improvements include the following:(i) returning KCl co-product back to a chlor/alkali membrane-type electrolytic cell and then making very pure KOH and Cl.sub.2 ;(ii) recylcing excess KOH back to the ferrate-forming reaction; and(iii) recovering a substantially pure dry solid K.sub.2 FeO.sub.4 product by washing the above-noted K.sub.2 FeO.sub.4 product in DMSO or its equivalent; and then washing with methanol or its equivalent, before drying.

Abstract: A process is described for reducing the concentration of oxyhalogen impurities in an alkali metal halide brine recovered from an electrolytic cell which comprises circulating the alkali metal halide brine to a treatment zone outside of the electrolytic cell. Within the treatment zone, the alkali metal halide brine is reacted with oxalic acid while maintaining the alkali metal halide brine at a pH of less than about 4.5. A purified brine having a substantially reduced concentration of oxyhalogen impurities is recovered from the treatment zone. The process may be employed in treating brines recovered from mercury cells and membrane cells for the production of chlorine and alkali metal hydroxides and its employment results in a substantial reduction in the amount of concentrated acid required in brine treatment and a reduction in energy costs for brine purification.

Abstract: An improved cathode with a conductive metal core and a Raney-type catalytic surface predominantly derived from an adherent .[.NiAl.sub.3 .]. .Iadd.Beta Nickel (NiAl.sub.3) .Iaddend.crystalline precursory outer portion of the metal core is disclosed. The precursory outer portion preferably has molybdenum added to give a precursor alloy having the formula Ni.sub.x Mo.sub.1-x Al.sub.3 where x is within the range of from about .[.5.]. .Iadd.95 .Iaddend.to about 15 weight percent. Also disclosed is a method of producing a low overvoltage cathode. The method includes the steps of taking a Ni-Mo core or substrate having about 5-20 weight percentage of Mo and coating it with aluminum then heat treating to form a Ni-Mo-Al alloy with mostly .[.NiAl.sub.3 .]. .Iadd.a Beta Nickel .Iaddend.structure and then leaching out the Al to produce a Raney surface.