Abstract: An apparatus and process for the preparation of colloidal dispersions of sodium metallo silicates, useful as coagulant aids, are disclosed. The dispersions are prepared by the controlled sequential mixing of separate streams of water, sodium silicate and a metal salt in a mixing block that has no moving parts. The apparatus and process are also useful in the mixing of other reactive solutions and fluids.
Type:
Grant
Filed:
August 3, 1977
Date of Patent:
April 3, 1979
Assignee:
PQ Corporation
Inventors:
Robert J. Kovanda, Serge Maliar, Jr., Robert W. Spencer
Abstract: Hydrophilic, silane-zeolite compositions, their preparation, properties and applications are disclosed. These unique composites are formed by condensing a hydrophilic silane onto the surface of a hydrated zeolite. The properties of the silane-zeolite composite are surprisingly similar to those of the zeolite without the surface modification of the silane. These composites are useful in numerous applications of zeolite, particularly in aqueous environments. The composites are particularly suited to be included in detergent compounds as the builder since they do not agglomerate with other detergent ingredients as do zeolites.
Type:
Grant
Filed:
September 14, 1977
Date of Patent:
February 6, 1979
Assignee:
PQ Corporation
Inventors:
Elliot P. Hertzenberg, Howard S. Sherry
Abstract: The alkali rich raw material batch required to produce soluble alkali metal silicate glass is effectively agglomerated by contacting a concentrated alkali metal silicate solution with the agitating raw materials. Hard agglomerates that are free-flowing, storable and provide important process advantages are formed.
Abstract: Alkaline silicates such as sodium metasilicate are prepared by a method that prevents unreacted batch ingredients to come in contact with furnace walls. The method also prevents any molten material from contacting the floor of the furnace. The raw materials and unreacted melt are confined to the central portion of the furnace by maintaining vigorous bubbling around the periphery of the melting furnace. The vigorous bubbling action prevents migration of unreacted raw material to the furnace walls. The bubbling eminates from means that extend up from the furnace floor and therefore, the portion of the material in the lower part of the furnace bed is in the solid state.
Type:
Grant
Filed:
June 7, 1977
Date of Patent:
October 3, 1978
Assignee:
PQ Corporation
Inventors:
Frank J. Lazet, D. John Meador, Richard G. Webster
Abstract: A process for the preparation of finely divided dispersible alpha-alumina monohydrate (boehmite) from alumina trihydrate is disclosed. The alumina trihydrate is calcined thereby increasing the surface area through a partial dehydration. The calcined intermediate is slurried in water and autoclaved to achieve crystallization and rehydration. Conventional drying methods are used to obtain the particles. The particle size of the product is much smaller than that of the starting raw material.
Type:
Grant
Filed:
March 21, 1977
Date of Patent:
September 26, 1978
Assignee:
PQ Corporation
Inventors:
Elliot P. Hertzenberg, Irwin Jerry Itzkovitch, Ivan H. Joyce
Abstract: A free-falling curtain of molten glass that is uniform in thickness and temperature is formed by flowing the glass over the lip of a forehearth after conditioning the glass in said forehearth. The forehearth is constructed to provide an increasing rate of fall as the glass travels, flows from the furnace through the forehearth and progressively cools. The floor of the forehearth is essentially the mirror image of the viscosity versus temperature curve of the material being treated.Other molten materials that become viscous as they cool can also be treated by the method of my invention to provide a uniform falling curtain of said material.