Patents Examined by Brian D Walck
  • Patent number: 11535906
    Abstract: The present disclosure provides a method that ensures easily manufacturing an alloy ribbon piece having excellent soft magnetic properties. The method is a method for manufacturing an alloy ribbon piece obtained by crystallizing an amorphous alloy ribbon piece and including: increasing a temperature of the amorphous alloy ribbon piece to a crystallization starting temperature; and increasing the temperature of the amorphous alloy ribbon piece from the crystallization starting temperature to a crystallization process termination temperature equal to or less than a crystallization completion temperature.
    Type: Grant
    Filed: May 12, 2020
    Date of Patent: December 27, 2022
    Assignee: TOYOTA JIDOSHA KABUSHIKI KAISHA
    Inventors: Osamu Yamashita, Shinichi Hiramatsu
  • Patent number: 11530466
    Abstract: A low thermal expansion alloy having a high rigidity and a low thermal expansion coefficient comprising, by mass %, C: 0.040% or less, Si: 0.25% or less, Mn: 0.15 to 0.50%, Cr: 8.50 to 10.0%, Ni: 0 to 5.00%, and Co: 43.0 to 56.0%, S: 0 to 0.050%, and Se: 0 to 0.050% and having a balance of Fe and unavoidable impurities, the contents of Ni, Co, and Mn represented by [Ni], [Co], and [Mn] satisfying 55.7?2.2[Ni]+[Co]+1.7[Mn]?56.7 and the structure being an austenite single phase.
    Type: Grant
    Filed: April 3, 2018
    Date of Patent: December 20, 2022
    Assignee: SHINHOKOKU MATERIAL CORP.
    Inventors: Naoki Sakaguchi, Haruyasu Ohno
  • Patent number: 11524486
    Abstract: It is an object to provide a method for producing a substrate for epitaxial growth having a higher degree of biaxial crystal orientation without forming an irregular part a3. The method for producing a substrate for epitaxial growth comprising a step of laminating a metal base material and a copper layer having an fcc rolling texture by surface-activated bonding, a step of applying mechanical polishing to the copper layer, and a step of carrying out orientation heat treatment of the copper layer, wherein the copper layer is laminated in such a way that, when ratios of the (200) plane of the copper layer before laminated and of the copper layer after laminated when measured by XRD are I0Cu and I0CLAD, respectively and ratios of the (220) plane of the copper layer before laminated and of the copper layer after laminated are I2Cu and I2CLAD, respectively, I0Cu<20%, I2Cu=70 to 90%, and I0CLAD<20%, I2CLAD=70 to 90% and I0CLAD?I0Cu<13%.
    Type: Grant
    Filed: October 21, 2016
    Date of Patent: December 13, 2022
    Assignees: TOYO KOHAN CO., LTD., SUMITOMO ELECTRIC INDUSTRIES, LTD.
    Inventors: Teppei Kurokawa, Yusuke Hashimoto, Hironao Okayama
  • Patent number: 11525172
    Abstract: A nickel-niobium intermetallic alloy contains, in weight percent, silicon from about 1.5 to about 3.5 percent; chromium from 5 to about 15 percent; nickel from about 45 to about 75 percent; niobium from about 14 to about 30 percent; cobalt up to about 7 percent; and iron up to about 10 percent; wherein the nickel plus niobium content is about 70 to about 90 percent and the total silicon, chromium, cobalt and iron content is about 10 to about 30 percent. The alloy can have a cast microstructure of at least 95 volume percent intermetallic phases and no more than about 5 volume percent solid solution phases. The intermetallic phases can include rod-like intermetallic phases of Ni3Nb and Ni8Nb7. The microstructure can be a lamellar microstructure and/or the microstructure can have less than 5 volume percent Ni—Fe and Ni—Co rich intermetallic phases.
    Type: Grant
    Filed: December 1, 2021
    Date of Patent: December 13, 2022
    Assignee: L.E. Jones Company
    Inventors: Cong Yue Qiao, David M. Doll
  • Patent number: 11512371
    Abstract: Disclosed are a BCC dual phase refractory superalloy with high phase stability and a manufacturing method therefor, the alloy comprising one or more of Ti, Zr, and Hf as Group 4 transition metals, one or more of Na and Ta as Group 5 transition metals, and Al, and having a structure of a BCC phase, wherein the BCC phase is composed of a disordered BCC phase and an ordered BCC phase, and wherein the ordered BCC phase is formed by allowing Al, which is a BCC phase forming element, to be soluted in an area of the BCC phase where the contents of the Group 5 transition metals are more than those of the Group 4 transition metals, so that the present disclosure provides a BCC dual phase refractory superalloy with high phase stability, characterized in that when a BCC dual phase with the ordered BCC phase and the disordered BCC phase separated from each other is formed by aging, the aging condition is precisely controlled through the apex temperature (Tc) of the BCC phase miscibility gap, expressed by (Equation 1) bel
    Type: Grant
    Filed: August 18, 2020
    Date of Patent: November 29, 2022
    Assignee: SEOUL NATIONAL UNIVERSITY R&DB FOUNDATION
    Inventors: Eun Soo Park, Sang Jun Kim, Ji Young Kim, Hyun Seok Oh, Kook Noh Yoon
  • Patent number: 11512370
    Abstract: This free-cutting copper alloy contains Cu: 58.5 to 63.5%, Si: more than 0.4% and 1.0% or less, Pb: 0.003 to 0.25%, and P: 0.005 to 0.19%, with the remainder being Zn and inevitable impurities, a total amount of Fe, Mn, Co and Cr is less than 0.40%, a total amount of Sn and Al is less than 0.40%, a relationship of 56.3?f1=[Cu]?4.7×[Si]+0.5×[Pb]?0.5×[P]?59.3 is satisfied, constituent phases of a metal structure have relationships of 20?(?)?75, 25?(?)?80, 0?(?)<2, 20?(?)1/2×3+(?)×(?0.5×([Si])2+1.5×[Si])?78, and 33?(?)1/2×3+(?)×(?0.5×([Si])2+1.5×[Si])+([Pb])1/2×33+([P])1/2×14, and a compound including P is present in ? phase.
    Type: Grant
    Filed: December 11, 2019
    Date of Patent: November 29, 2022
    Assignee: MITSUBISHI MATERIALS CORPORATION
    Inventors: Keiichiro Oishi, Kouichi Suzaki, Hiroki Goto
  • Patent number: 11512380
    Abstract: The present invention provides a method for manufacturing more beautiful black coated steel sheets by uniformly blackening the coating layer. Specifically, the present invention provides a method for manufacturing black coated steel sheets, which brings Zn—Al—Mg alloy coated steel sheets (1) into contact with steam in a closed container (10), wherein said closed container (10) can maintain a predefined internal pressure through variable control of the amount of steam flowing into said closed container (10) and/or the amount of steam flowing out of said closed container (10), and in said closed container (10) that can maintain said predefined pressure, said Zn—Al—Mg alloy coated steel sheets (1) have contact with the steam introduced into said closed container (10).
    Type: Grant
    Filed: January 17, 2018
    Date of Patent: November 29, 2022
    Assignee: NIPPON STEEL NISSHIN CO., LTD.
    Inventors: Masaki Yamamoto, Tadashi Nakano, Ichiro Takahashi, Hiroyuki Nakamizo, Toshiaki Sato, Yoshinobu Kurisu, Yuuki Sakuraba, Yoshitaka Yukura, Tsutomu Ohta, Shinichi Kajimoto, Noboru Suzuki, Masahiko Tsuchiyama, Yuusuke Murai
  • Patent number: 11512369
    Abstract: A method for manufacturing an ingot made of titanium-based metallic compound, includes providing raw material fragments; melting the raw material fragments into a liquid metal in at least one basin; keeping in the molten state the liquid metal in the at least one basin; pouring the liquid metal from the at least one basin into a crucible by overflow from the at least one basin into the crucible; forming an ingot by cooling of the liquid metal into the crucible; wherein the method further includes preheating the raw material fragments before the melting of the raw material fragments with a preheating temperature higher than or equal to 75% of the liquidus temperature of the raw material fragments, and lower less than the liquidus temperature of the raw material fragments.
    Type: Grant
    Filed: June 24, 2019
    Date of Patent: November 29, 2022
    Assignee: SAFRAN AIRCRAFT ENGINES
    Inventors: Bruno Vitorino Lopes, Laurent Ferrer
  • Patent number: 11504768
    Abstract: A method for producing hard metal powder suitable for manufacturing hard metal products including metal carbides and a binder is provided. An easy to carry out method that provides high quality hard metal powder includes: a) dissolving in water, water soluble raw materials and a binder source to form an aqueous solution, b) drying the aqueous solution to form a precursor powder having the raw materials homogenously distributed throughout the precursor powder, c) decomposing the precursor powder by heating the powder in an inert atmosphere to remove gas evolved in the decomposition of the raw materials, d) grinding the precursor powder and mixing it with a liquid media to produce a suspension, e) spray drying the suspension to agglomerate the precursor powder, and f) heat treating the agglomerated precursor powder to form a hard metal powder containing agglomerates of carbides evenly distributed and bonded to a metallic matrix.
    Type: Grant
    Filed: February 16, 2018
    Date of Patent: November 22, 2022
    Assignee: TEKNOLOGIAN TUTKIMUSKESKUS VTT OY
    Inventors: Juha Lagerbom, Marjaana Karhu, Hanna-Mari Sinilehto, Ulla Kanerva
  • Patent number: 11505858
    Abstract: Provided is a Zn—Al—Mg-based alloy-plated steel material that can be used in automobiles and home appliances and the like and, more particularly, to a Zn—Al—Mg-based alloy-plated steel material that can suppress the generation of cracks in a plating layer that are generated during processing.
    Type: Grant
    Filed: December 21, 2017
    Date of Patent: November 22, 2022
    Inventors: Il-Ryoung Sohn, Tae-Chul Kim, Jong-Sang Kim
  • Patent number: 11504770
    Abstract: Systems and methods are disclosed for fabricating a metal or ceramic component using a 3D printer. An entire 3D printed piece, including both the metal or ceramic component and one or more support structures, is created of a first metal or ceramic material. A sensitization layer is applied to all or part of the 3D printed piece to chemically alter portions of the first metal or ceramic material near the surface making those portions of the material more sensitive to the etching process. The etching process causes the affected material to deplete and separates the component from the support structures without requiring mechanical machining.
    Type: Grant
    Filed: February 16, 2017
    Date of Patent: November 22, 2022
    Assignees: ARIZONA BOARD OF REGENTS ON BEHALF OF ARIZONA STATE UNIVERSITY, THE PENN STATE RESEARCH FOUNDATION
    Inventors: Owen Hildreth, David Wright, Abdalla Nassar, Tim Simpson, Christopher Lefky
  • Patent number: 11499205
    Abstract: Suggested is a method for recovering precious metals from secondary resources comprising or consisting of the following steps: (a) providing a source of solid waste material comprising precious metals in an amount of at least 0.0001% b.w.; (b) bringing said waste material into contact with heterotrophic micro-organisms capable of producing and releasing hydrocyanic acid; (c) adding a solvent or an aqueous nutrient solution capable of serving as a nutrient source for said micro-organisms to the mixture; (d) depleting said waste materials from the precious metals contained therein by complexation of the metals with said hydrocyanic acid released by said micro-organisms; (e) separating the depleted solid waste material from the liquid containing the metal-cyano complexes; (f) recovering the precious metals from their cyano-complexes in known manner.
    Type: Grant
    Filed: June 7, 2018
    Date of Patent: November 15, 2022
    Assignee: BRAIN AG
    Inventors: Ester Gabor, Yvonne Tiffert, Guido Meurer
  • Patent number: 11499201
    Abstract: A process for the production of direct reduced iron (DRI), with or without carbon, using hydrogen, where the hydrogen is produced utilizing water generated internally from the process. The process is characterized by containing either one or two gas loops, one for affecting the reduction of the oxide and another for affecting the carburization of the DRI. The primary loop responsible for reduction recirculates used gas from the shaft furnace in a loop including a dry dedusting step, an oxygen removal step to generate the hydrogen, and a connection to the shaft furnace for reduction. In the absence of a second loop, this loop, in conjunction with natural gas addition, can be used to deposit carbon. A secondary carburizing loop installed downstream of the shaft furnace can more finely control carbon addition. This loop includes a reactor vessel, a dedusting step, and a gas separation unit.
    Type: Grant
    Filed: June 2, 2020
    Date of Patent: November 15, 2022
    Assignee: Midrex Technologies, Inc.
    Inventors: Todd Michael Astoria, Gregory Darel Hughes, Enrique Jose Cintron, Keith Marshall Bastow-Cox
  • Patent number: 11493273
    Abstract: A method for measuring the softening and melting performances of iron ore in blast furnace is disclosed, which is implemented by a device including a high temperature furnace, gas supply system, a loading system and a weighing system. The method includes: step 1: the dried coke and iron ore specimen are placed in the graphite crucible in a specified way; step 2: the graphite crucible is placed in the high temperature furnace, and N2 is continuously fed into the high temperature furnace to reach an airtightness requirement; step 3: a vacuum pump is used to extract mixed gas in a hearth of the high temperature furnace and heating process is started; step 4: both the composition of mixed gas and pressure imposed on the iron ore are controlled according to the designed temperature variation; step 5: data are acquired to calculate.
    Type: Grant
    Filed: July 10, 2020
    Date of Patent: November 8, 2022
    Inventors: Shengfu Zhang, Chenguang Bai, Rongjin Zhu, Cheng Yin, Qingyu Deng, Liangying Wen, Jian Xu, Jie Dang, Zhixiong You, Wenzhou Yu, Liwen Hu
  • Patent number: 11495377
    Abstract: Provided is a soft magnetic alloy which has high saturation flux density and low coercivity and is represented by the compositional formula (Fe(1?(?+?))X1?X2?)(1?(a+b+c+d+e+f))MaPbSicCudX3eBf, wherein X1 is at least one element selected from the group consisting of Co and Ni, X2 is at least one element selected from the group consisting of Ti, V, Mn, Ag, Zn, Al, Sn, As, Sb, Bi, and rare earth elements, X3 is at least one element selected from the group consisting of C and Ge, and M is at least one element selected from the group consisting of Zr, Nb, Hf, Ta, Mo, and W, and wherein 0.030?a?0.120, 0.010?b?0.150, 0?c?0.050, 0?d?0.020, 0?e?0.100, 0?f?0.030, ??0, ??0, and 0??+??0.55.
    Type: Grant
    Filed: February 15, 2019
    Date of Patent: November 8, 2022
    Assignee: TDK CORPORATION
    Inventors: Hajime Amano, Akihiro Harada, Kenji Horino, Hiroyuki Matsumoto, Kazuhiro Yoshidome, Akito Hasegawa, Kensuke Ara, Masakazu Hosono
  • Patent number: 11492681
    Abstract: A method for extracting base and precious metals, all contained in refractory minerals, using aqueous media. The method includes mixing the mineral (Cu2S, CuS, CuFeS2, Cu5FeS4, FeS2, FeAsS.NiS, (Ni,Fe)xSy), ground to an appropriate size (2.5 centimetres), with a specific dose of solid reagent in a rotary agglomeration drum and then adding slightly acidified water to obtain a defined water content (5-8%) depending on the type of gangue contained in the metal-containing solid, thereby forming an agglomerate that will form a heap, which is subsequently allowed to stand for a period of several days (20-60 days), during which the conditions required to transform the refractory matrix into a highly soluble solid will be generated. Finally, appropriately regulated irrigation is applied, thus resulting in extraction of the metal by simple aqueous washing.
    Type: Grant
    Filed: September 5, 2018
    Date of Patent: November 8, 2022
    Inventor: Eduardo Luis Patino Martinez
  • Patent number: 11486012
    Abstract: An inoculant for the manufacture of cast iron with spheroidal graphite is disclosed, the inoculant has a particulate ferrosilicon alloy having between 40 and 80% by weight of Si; 0.02-8% by weight of Ca; 0-5% by weight of Sr; 0-12% by weight of Ba; 0-15% by weight of rare earth metal; 0-5% by weight of Mg; 0.05-5% by weight of Al; 0-10% by weight of Mn; 0-10% by weight of Ti; 0-10 by weight of Zr; the balance being Fe and incidental impurities in the ordinary amount, wherein the inoculant additionally contains, by weight, based on the total weight of inoculant: 0.1 to 15% of particulate Sb2S3, and optionally between 0.1 and 15% of particulate Bi2O3, and/or between 0.1 and 15% of particulate Sb2O3, and/or between 0.1 and 15% of particulate Bi2S3, and/or between 0.1 and 5% of one or more of particulate Fe3O4, Fe2O3, FeO, or a mixture thereof, and/or between 0.1 and 5% of one or more of particulate FeS, FeS2, Fe3S4, or a mixture thereof, a method for producing such inoculant and use of such inoculant.
    Type: Grant
    Filed: December 21, 2018
    Date of Patent: November 1, 2022
    Assignee: ELKEM ASA
    Inventors: Emmanuelle Ott, Oddvar Knustad
  • Patent number: 11486017
    Abstract: A cold rolled and annealed steel sheet includes by weight: 0.6<C<1.3%,15.0<Mn<35%, 6.0<Al<15%, Si<2.40%, S<0.015%, P<0.1%, N<0.1%, iron and inevitable impurities, optionally one or more of Ni, Cr and Cu in an individual amount of up to 3% and optionally one or more of B, Ta, Zr, Nb, V, Ti, Mo, and W in a cumulated amount of up to 2.0%, a microstructure of the sheet comprising at least 0.1% of intragranular kappa carbides, at least 80% of the kappa carbides have an average size below 30 nm, the remainder being made of austenite, an average grain size of the austenite being below 6 ?m, an average aspect ratio of the austenite being between 1.5 and 6, an average grain size of the ferrite, when present being below 5 ?m, and an average aspect ratio of the ferrite, when present, being below 3.0.
    Type: Grant
    Filed: May 23, 2017
    Date of Patent: November 1, 2022
    Assignee: ArcelorMittal
    Inventors: Michel Soler, Ian Alberto Zuazo Rodriguez, Irène De Diego Calderon
  • Patent number: 11486011
    Abstract: An inoculant for the manufacture of cast iron with spheroidal graphite is disclosed, the inoculant has a particulate ferrosilicon alloy having between 40 and 80% by weight of Si; 0.02-8% by weight of Ca; 0-5% by weight of Sr; 0-12% by weight of Ba; 0-15% by weight of rare earth metal; 0-5% by weight of Mg; 0.05-5% by weight of Al; 0-10% by weight of Mn; 0-10% by weight of Ti; 0-10 by weight of Zr; the balance being Fe and incidental impurities in the ordinary amount, wherein the inoculant additionally contains, by weight, based on the total weight of inoculant: 0.1 to 15% of particulate Sb2S3, and optionally between 0.1 and 15% of particulate Bi2O3, and/or between 0.1 and 15% of particulate Sb2O3, and/or between 0.1 and 15% of particulate Bi2S3, and/or between 0.1 and 5% of one or more of particulate Fe3O4, Fe2O3, FeO, or a mixture thereof, and/or between 0.1 and 5% of one or more of particulate FeS, FeS2, Fe3S4, or a mixture thereof, a method for producing such inoculant and use of such inoculant.
    Type: Grant
    Filed: December 21, 2018
    Date of Patent: November 1, 2022
    Assignee: ELKEM ASA
    Inventor: Oddvar Knustad
  • Patent number: 11479828
    Abstract: An inoculant for the manufacture of cast iron with spheroidal graphite is disclosed, the inoculant has a particulate ferrosilicon alloy having between 40 and 80% by weight of Si; 0.02-8% by weight of Ca; 0-5% by weight of Sr; 0-12% by weight of Ba; 0-15% by weight of rare earth metal; 0-5% by weight of Mg; 0.05-5% by weight of Al; 0-10% by weight of Mn; 0-10% by weight of Ti; 0-10 by weight of Zr; the balance being Fe and incidental impurities in the ordinary amount, wherein the inoculant additionally contains, by weight, based on the total weight of inoculant: 0.1 to 15% of particulate Sb2S3, and optionally between 0.1 and 15% of particulate Bi2O3, and/or between 0.1 and 15% of particulate Sb2O3, and/or between 0.1 and 15% of particulate Bi2S3, and/or between 0.1 and 5% of one or more of particulate Fe3O4, Fe2O3, FeO, or a mixture thereof, and/or between 0.1 and 5% of one or more of particulate FeS, FeS2, Fe3S4, or a mixture thereof, a method for producing such inoculant and use of such inoculant.
    Type: Grant
    Filed: December 21, 2018
    Date of Patent: October 25, 2022
    Assignee: ELKEM ASA
    Inventors: Emmanuelle Ott, Oddvar Knustad