Abstract: In one aspect, the present disclosure pertains to methods of making various noble metal nanoprisms, e.g., gold nanoprisms. In various aspects, the methods can comprise incubating, under dark conditions, a growth solution comprising: (a) a plurality of gold seed structures; (b) a gold precursor, and (c) a photocatalytic intermediary, such that during the incubating step multiply-twinned gold seed structures in the growth solution are preferentially enlarged. The disclosed methods can comprise separating the multiply-twinned gold seed structures from the growth solution based upon the size of the gold seed structures to produce an enriched growth solution. In some aspects, the methods comprise irradiating the enriched growth solution to produce the gold nanoprisms. In some aspects, the disclosed nanoprisms comprise silver.
Type:
Grant
Filed:
May 24, 2017
Date of Patent:
April 26, 2022
Assignee:
University of Florida Research Foundation, Inc.
Abstract: The present invention provides a high strength, high toughness, heat-cracking resistant bainite steel wheel for rail transportation and a manufacturing method thereof. Components are: carbon 0.10-0.40%, silicon 1.00-2.00%, manganese 1.00-2.50%, copper 0.20-1.00%, boron 0.0001-0.035%, nickel 0.10-1.00%, phosphorus ?0.020%, and sulphur ?0.020%, where the remaining is iron and unavoidable residual elements, 1.50%?Si+Ni?3.00%, and 1.50%?Mn+Ni+Cu?3.00%. Compared with the prior art, in the present invention, by using design of the chemical compositions of steel and wheel manufacturing processes, especially a heat treatment process and technology, a rim of the wheel obtains a carbide-free bainite structure, and a web and a wheel hub obtain a metallographic structure based on granular bainite and a supersaturated ferritic structure.
Abstract: The present invention relates to an aluminum alloy for the manufacture of thick blocks comprising (as a percentage by weight), Zn: 5.3-5.9%, Mg: 0.8-1.8%, Cu: <0.2%, Zr: 0.05 to 0.12%, Ti<0.15%, Mn<0.1%, Cr<0.1%, Si<0.15%, Fe<0.20%, impurities having an individual content of <0.05% each and <0.15% in total, the rest aluminum, The alloy may be used in a process comprising the steps of: (a) casting a thick block of an alloy according to the invention (b) solution heat treating said cast block at a temperature of 500 to 560° C. for 10 minutes to 20 hours, (c) cooling said solution heat treated block to a temperature below 100° C., (d) tempering said solution heat treated and cooled block by heating to 120 to 170° C. for 4 to 48 hours, In this process, said block is not subjected to any significant deformation by working between the casting and the tempering.
Type:
Grant
Filed:
December 6, 2011
Date of Patent:
April 19, 2022
Assignees:
CONSTELLIUM VALAIS SA (AG, LTD), CONSTELLIUM ISSOIRE
Abstract: Provided are methods for preparing iron nanoparticles and to iron nanoparticles produced by those methods. The invention also provides methods for coating the iron nanoparticles with oxides and functionalizing the iron nanoparticles with organic and polymeric ligands. Additionally, the invention provides methods of using such iron nanoparticles.
Type:
Grant
Filed:
May 12, 2017
Date of Patent:
March 29, 2022
Assignees:
University of Maryland, College Park, University of Maryland, Baltimore
Abstract: An aluminum alloy contains 0.7% to 1.8% of silicon, 0.5% to 2.1% of copper, 0.4% to 1.8% of manganese, 0.6% to 1.6% of magnesium, and 0.1% to 0.7% of zinc in terms of mass ratio and the balance aluminum with inevitable impurities.
Abstract: The invention relates to a method for producing an engine component, in particular a piston for an internal combustion engine, wherein an aluminum alloy is cast in the gravity die casting process and wherein the aluminum alloy has 7 to <14.5 wt % silicon, >1.2 to ?4 wt % nickel, >3.7 to <10 wt % copper, <1 wt % cobalt, 0.1 to 1.5 wt % magnesium, 0.1 to ?0.7 wt % iron, 0.1 to ?0.7 wt % manganese, >0.1 to <0.5 wt % zirconium, ?0.1 to ?0.3 wt % vanadium, 0.05 to 0.5 wt % titanium, and 0.004 to ?0.05 wt % phosphorus as alloying elements and aluminum and unavoidable contaminants as the remainder. The aluminum alloy can optionally comprise beryllium, wherein the calcium content is limited to a low level.
Type:
Grant
Filed:
May 11, 2015
Date of Patent:
March 22, 2022
Assignee:
Federal-Mogul Nurnberg GmbH
Inventors:
Roman Morgenstern, Stephan Silvio, Scott Kenningley, Philipp Koch, Isabella Sobota, Klaus Lades, Martin Popp, Rainer Weiss, Robert Willard
Abstract: The mechanical properties and thermal resistance of a sintered component made from an Al—Cu—Mg—Sn alloy powder metal mixture can be improved by doping the Al—Cu—Mg—Sn alloy powder metal mixture with a silicon addition. Silicon is added as a constituent to the Al—Cu—Mg—Sn alloy powder metal mixture. The Al—Cu—Mg—Sn alloy powder metal mixture is compacted to form a preform and the preform is sintered to form the sintered component.
Type:
Grant
Filed:
November 29, 2018
Date of Patent:
March 15, 2022
Assignee:
GKN Sinter Metals, LLC
Inventors:
Donald Paul Bishop, Richard L. Hexemer, Ian W. Donaldson, Randy Williams Cooke
Abstract: Disclosed herein are embodiments of methods, devices, and assemblies for processing feedstock materials using microwave plasma processing. Specifically, the feedstock materials disclosed herein pertains to scrap materials, dehydrogenated or non-hydrogenated feed material, and recycled used powder. Microwave plasma processing can be used to spheroidize and remove contaminants. Advantageously, microwave plasma processed feedstock can be used in various applications such as additive manufacturing or powdered metallurgy (PM) applications that require high powder flowability.
Type:
Grant
Filed:
March 23, 2020
Date of Patent:
March 15, 2022
Assignee:
6K Inc.
Inventors:
John Barnes, Aaron Bent, Kamal Hadidi, Makhlouf Redjdal, Scott Turchetti, Saurabh Ullal, Ning Duanmu, Michael C. Kozlowski
Abstract: Disclosed herein are methods of making a plurality of metal particles, the methods comprising: injecting a metal particle precursor, a capping material, and a reducing agent into an inlet of a continuous flow microwave reactor, thereby forming a mixture within the continuous flow microwave reactor, wherein the inlet of the continuous flow microwave reactor is fluidly connected to an outlet of the continuous flow microwave reactor through a reaction vessel; flowing the mixture through the reaction vessel, wherein the metal particle precursor is reduced within the reaction vessel, thereby forming the plurality of metal particles; and collecting the plurality of metal particles from the outlet of the continuous flow microwave reactor.
Type:
Grant
Filed:
March 16, 2018
Date of Patent:
March 15, 2022
Assignee:
Board of Regents, the University of Texas System
Abstract: An aluminum alloy material of the present disclosure has an alloy composition containing Mg: 0.50% by mass or more and 6.0% by mass or less, Fe: 0% by mass or more and 1.50% by mass or less, Si: 0% by mass or more and 1.0% by mass or less, one or more selected from Cu, Ag, Zn, Ni, Ti, Co, Au, Mn, Cr, V, Zr and Sn: 0% by mass or more and 2.0% by mass or less in total, with the balance being Al and inevitable impurities. The aluminum alloy material has a fibrous metallographic structure in which crystal grains extend so as to be aligned in one direction, and an average value of sizes perpendicular to longitudinal direction of the crystal grains is 310 nm or less in a cross section parallel to the one direction.
Abstract: This invention relates to the field of welding high strength aluminum structures, and more particularly to the alloy filler metal composition, its resultant microstructure, and the physical and mechanical properties which are obtained in the weld bead during fusion welding. A composition for producing small diameter aluminum welding filler metal wires having a chemistry comprising Si varying from approximately 0.3 to 0.9 wt. %, Mn varying from approximately 0.05 to 1.2 wt. %, Mg varying from approximately 2.0 to 7.0 wt. %, Cr varying from approximately 0.05 to 0.30 wt. %, Zr varying from approximately 0.05 to 0.30 wt. %, Ti varying from approximately 0.003 to 0.20 wt. %, and B varying from approximately 0.0010 to 0.030 wt. %, and a remainder of aluminum and various trace elements.
Abstract: A method for producing nickel nanopowder is introduced. For this, the present invention relates to a method for producing nickel nanopowder, including: (a) a step of preparing nickel oxide configured in the form of an oxide; (b) a nickel oxide nanopowder production step of pulverizing the nickel oxide so as to produce nano-sized nickel oxide nanopowder; (c) a step of drying the nickel oxide nanopowder; (d) a step of heat-treating the nickel oxide nanopowder so as to produce natural metal nickel nanopowder; and (e) a step of crushing the heat-treated nickel oxide nanopowder.
Abstract: A method for preparing copper nanocubes with specific facets and uniform size, the method comprising combining a copper complex solution in a reaction mixture with a ligand. Using a ligand of pure, unoxidized tributylphosphine, uniform copper nanocubes with six facets are prepared.
Abstract: A shaped charge liner may include an apex portion and a skirt portion extending from the apex portion. The skirt portion may include a body connected to the apex portion, a perimeter spaced apart from the apex portion, and a carbide layer extending between and spaced apart from the perimeter and the apex portion. A shaped charge for creating a perforation hole in a wellbore casing may include a shaped charge liner having at least one material having hardness that is greater than a corresponding hardness of the wellbore casing. The at least one material is configured to bond to at least one of an outer surface and an inner surface of the perforation hole upon detonation of the shaped charge and penetration of the casing by a perforation jet.
Type:
Grant
Filed:
March 29, 2021
Date of Patent:
February 22, 2022
Assignee:
DynaEnergetics Europe GmbH
Inventors:
Joern Olaf Loehken, Liam McNelis, Bernd Fricke
Abstract: A method of forming a high strength aluminum alloy. The method comprises subjecting an aluminum material containing at least one of magnesium, manganese, silicon, copper, and zinc at a concentration of at least 0.1% by weight to an equal channel angular extrusion (ECAE) process. The method produces a high strength aluminum alloy having an average grain size from about 0.2 ?m to about 0.8 ?m and a yield strength from about 300 MPa to about 650 MPa.
Type:
Grant
Filed:
March 16, 2020
Date of Patent:
February 15, 2022
Assignee:
Honeywell International Inc.
Inventors:
Stephane Ferrasse, Susan D. Strothers, Patrick K. Underwood, Marc D. Ruggiero, Wayne D. Meyer, Lucia M. Feng, Frank C. Alford
Abstract: An aluminum-based composite material includes an aluminum parent phase, and stick-shaped or needle-shaped dispersive matter of aluminum carbide dispersed in the aluminum parent phase. A method of manufacturing the aluminum-based composite material includes a step of mixing aluminum powder having a purity of 99% by mass or higher with a stick-shaped or needle-shaped carbon material, and pressing and molding a resulting mixture, so as to prepare a compacted powder body. The manufacturing method further includes a step of heating the compacted powder body at 600C to 660C to react the carbon material with aluminum in the aluminum powder, so as to disperse the stick-shaped or needle-shaped dispersive matter of aluminum carbide in the aluminum parent phase.
Abstract: The present invention provides a preparation method for gold nanoparticles based on functionalized ionic liquid. The method comprises synthesizing a functionalized ionic liquid, 3-(12-bromo-dodecyl)-1-(3-pyrrole propyl)-imidazole bromide, as a stabilizer for synthesizing gold nanoparticles, adjusting the concentration of the ionic liquid and the dosage of the reducing agent, thereby successfully preparing the icosahedral gold nanoparticles, and characterizing the morphology thereof by TEM, XRD and SEM. In the present invention, the method employed for preparing the stabilizer is simple, non-toxic, harmless and pollution-free, moreover the preparation of gold nanoparticles by aqueous phase has the advantages of mild conditions, short reaction time, simple operation, green and pollution-free, and belongs to the environment-friendly preparation.
Abstract: The present disclosure concerns embodiments of aluminum alloy compositions exhibiting superior microstructural stability and strength at high temperatures. The disclosed aluminum alloy compositions comprise particular combinations of components that contribute the ability of the alloys to exhibit improved microstructural stability and hot tearing resistance as compared to conventional alloys. Also disclosed herein are embodiments of methods of making and using the alloys.
Type:
Grant
Filed:
May 12, 2017
Date of Patent:
February 8, 2022
Assignees:
UT-Battelle, LLC, FCA US LLC, Nemak USA, Inc.
Inventors:
Amit Shyam, James A. Haynes, Adrian S. Sabau, Dongwon Shin, Yukinori Yamamoto, Christopher R. Glaspie, Jose A. Gonzalez-Villarreal, Seyed Mirmiran, Andres F. Rodriguez-Jasso
Abstract: A deployable manufacturing center (DMC) system includes a foundry module containing a metallurgical system configured to convert a raw material into an alloy powder, and an additive manufacturing (AM) module containing an additive manufacturing system configured to form the alloy powder into metal parts. The deployable manufacturing center (DMC) system can also include a machining module containing a machining system configured to machine the metal parts into machined metal parts, and a quality conformance (QC) module containing an inspection and evaluation system configured to inspect and evaluate the metal parts. A process for manufacturing metal parts includes the steps of providing the deployable manufacturing center (DMC) system; deploying the (DMC) system to a desired location; forming an alloy powder from a raw material using the deployable foundry module; and then forming the metal parts from the alloy powder using the additive manufacturing (AM) module.
Type:
Grant
Filed:
September 19, 2018
Date of Patent:
February 1, 2022
Assignee:
MolyWorks Materials Corp.
Inventors:
Andrew VanOs LaTour, Christopher Eonta, Matthew Charles, Scott Steiner, Joel Cheng
Abstract: The purpose of the present invention is to provide novel solid gold-nickel alloy nanoparticles and a production method thereof. Provided are solid gold-nickel alloy nanoparticles having a particle diameter of 500 nm or less. In particular, gold-nickel alloy nanoparticle are provided in which the concentration of nickel in the gold-nickel alloy is 2.0-92.7 wt %, and the main component is a gold-nickel alloy in which gold and nickel are in a nano-level fine mixed state. The gold-nickel alloy particles have as the main component a substitutional solid solution of gold and nickel. These gold-nickel alloy particles are optimally formed by mixing and discharging gold ions, and a substance having reducing characteristics in the thin film fluid occurring between processing surfaces which are arranged facing each other, which can move towards and away from each other, and at least one of which rotates relative to the other.