Abstract: A process is provided for recovering uranium comprising (A) bringing a solution (A) into contact with a resin (A) to produce a mixture of solution (B) and resin (B), wherein the solution (A) is an aqueous solution comprising dissolved sodium carbonate, sodium bicarbonate, or a mixture thereof, and wherein the resin (A) is a strong acid cation exchange resin that comprises one or more cationic moiety that comprises uranium and one or more cationic moiety that comprises iron, and (B) separating the solution (B) from the resin (B).
Abstract: To provide a fine nickel powder for an internal electrode paste of an electronic component, the nickel powder obtained by a wet method and having high crystallinity, excellent sintering characteristics, and heat-shrinking characteristics. The nickel powder is obtained by precipitating nickel by a reduction reaction in a reaction solution including at least water-soluble nickel salt, salt of metal nobler than nickel, hydrazine as a reducing agent, and alkali metal hydroxide as a pH adjusting agent and water; the reaction solution is prepared by mixing a nickel salt solution including the water-soluble nickel salt and the salt of metal nobler than nickel with a mixed reducing agent solution including hydrazine and alkali metal hydroxide; and the hydrazine is additionally added to the reaction solution after a reduction reaction initiates in the reaction solution.
Type:
Grant
Filed:
March 14, 2017
Date of Patent:
July 5, 2022
Assignees:
SUMITOMO METAL MINING CO., LTD., MURATA MANUFACTURING CO., LTD.
Abstract: The present disclosure is related to a method to control sizes of core-shell nanoparticles comprising the steps of: manufacturing slurry by irradiating ultrasonic waves to a dispersion solution containing a reducing solvent, a carbon support, a transition metal precursor and a precious metal precursor; manufacturing a solid by filtering the manufactured slurry, followed by washing and drying; and manufacturing a nanoparticle of a transition metal core and a platinum shell by heat-treating the dried solid at a temperature of 450 to 900° C. and a pressure of 1 to 90 bar for 0.5 to 10 hours under N2 atmosphere.
Type:
Grant
Filed:
June 30, 2020
Date of Patent:
July 5, 2022
Assignee:
KOREA INSTITUTE OF ENERGY RESEARCH
Inventors:
Gu-gon Park, Hyun-uk Park, Won-yong Lee, Sung-dae Yim, Min-jin Kim, Young-jun Sohn, Byungchan Bae, Seung-gon Kim, Dongwon Shin, Hwanyeong Oh, Seung Hee Woo, So Jeong Lee, Hyejin Lee, Yoon Young Choi, Seok-hee Park, Tae-hyun Yang
Abstract: The invention regards a method for the synthesis of Zero-Valent metal micro- and nanoparticles, in which a first aqueous solution (SOL1) of a salt of a noble metal (A) is mixed with a third neutral or basic aqueous solution (SOL3) of an inorganic sulphur-based reducing agent (C), and wherein the mixture thus obtained is added to a second aqueous solution (SOL2) of a salt of a transition metal (B) and a second aliquot of the inorganic reducing agent; such method provides that the amount of the inorganic reducing agent (C) is in a stoichiometric excess in the reduction reaction to Zero-Valent of both the salt of the noble metal (A) contained in the first solution (SOL1) and the salt of the transition metal (B) contained in the second solution (SOL2). The invention also regards Zero-Valent micro and nanoparticles, preferably bimetallic, obtained with the above method.
Type:
Grant
Filed:
November 27, 2018
Date of Patent:
June 28, 2022
Assignee:
POLITECNICO DI TORINO
Inventors:
Rajandrea Sethi, Carlo Bianco, Andrea Gallo, Tiziana Anna Elisabetta Tosco, Alberto Tiraferri
Abstract: A method of producing a magnetic powder and a magnetic powder is provided. The method of producing a magnetic powder according to an exemplary embodiment of the present disclosure includes: producing an iron powder by a reduction reaction of iron oxide, producing a magnetic powder using a molded body obtained by press molding a mixture including the iron powder, a rare earth oxide, boron, and calcium at a pressure of 22 MPa or more, and coating a surface of the magnetic powder with ammonium fluoride.
Type:
Grant
Filed:
August 14, 2019
Date of Patent:
June 21, 2022
Inventors:
Ingyu Kim, Soon Jae Kwon, Ikjin Choi, Hyounsoo Uh
Abstract: A sputtering target comprising a forged aluminum material having an average grain size between about 15 and 55 microns. The aluminum material has at least one of the following: a homogeneous texture with minimal texture banding as measured by banding factor B below about 0.01; a texture gradient H of less than 0.2; or either weak (200) texture or near random texture characterized by maximum intensity of inverse pole figure less than 3 times random in multiple directions.
Type:
Grant
Filed:
July 26, 2016
Date of Patent:
June 14, 2022
Assignee:
Honeywell International Inc.
Inventors:
Stephane Ferrasse, Suresh Sundarraj, Frank C. Alford, Jeffrey J. Schaefer, Susan D. Strothers
Abstract: Provided is a method of inhibiting degradation of an extractant by an anhydrous environment avoiding and metal stripping, the method including the steps of: (a) stopping the addition of soda ash (Na2CO3) to an extracting reaction tank; (b) starting solution recirculation and stopping solvent recirculation of a settler; (c) supplying a solvent from a loaded organic tank to a scrubbing reaction tank, in which the scrubbing reaction tank, stripping reaction tank and extracting reaction tank are connected for circulation and operating stirrers of the scrubbing reaction tank, stripping reaction tank and extracting reaction tank; (d) supplying a sulfuric acid solution having a controlled concentration with a diluting solution to the stripping reaction tank; (e) transferring the solvents of the settler, the loaded organic tank and all the pipes to the scrubbing reaction tank; and (f) stopping the step (e) and initiating solvent recirculation.
Type:
Grant
Filed:
September 4, 2019
Date of Patent:
June 14, 2022
Assignee:
KOREA RESOURCES CORPORATION
Inventors:
Jeon Woong An, Youn Kyu Yi, Kyung Bae Jung, Seung Ho Lee
Abstract: Provided is a method for producing an aluminium alloy strip from a non-precipitation-hardenable aluminium alloy having the following alloying constituents in wt %: 3.6%?Mg?6%, Si?0.4%, Fe?0.5%, Cu?0.15%, 0.1%?Mn?0.4%, Cr?0.05%, Zn?0.20%, Ti?0.20%, with the remainder Al and unavoidable impurities, individually at most 0.05 wt %, in total at most 0.15 wt %. In the method, a rolling ingot is cast. The rolling ingot is homogenised and then hot rolled into a hot strip. Then, the strip is cold rolled before a last intermediate annealing. The intermediate annealing is carried out to produce a recrystallised microstructure. The intermediate-annealed aluminium alloy strip is cold rolled to a final thickness, and the aluminium alloy strip is reverse annealed in the coil to a final thickness.
Abstract: The present disclosure relates to a method for synthesizing Pd nanocubes having an average size less than 10 nm. The reaction temperature, reaction time, and molar ratios of TOP/Pd-OLA can be used to control size and formation of the Pd nanocubes. The present disclosure is also directed to Pd nanocubes, less than 10 nm, having face centered cubic structures. Pd nanocubes of the present disclosure are an effective catalyst for CO2 reduction reaction with excellent selectivity for CO. Small sized Pd nanocubes can be used not only as the seeds to prepare other metal nanocubes, but can also as powerful catalysts for a wide variety of reactions in different industrial processes.
Abstract: A method of forming one of a plurality of encapsulated crystalline particles includes feeding a coaxial feed wire downwardly such that a first wire end of the coaxial feed wire is positioned at a heating source. The coaxial feed wire includes a crystalline wire core, and an amorphous shell surrounding the crystalline wire core. The first end of the coaxial feed wire is heated at the heating source, thereby forming a molten pendant drop at the first wire end. The plurality of encapsulated crystalline particles are emitted from the molten pendant drop onto a collector located below the molten pendant drop.
Type:
Grant
Filed:
September 26, 2019
Date of Patent:
May 17, 2022
Assignee:
WESTERN NEW ENGLAND UNIVERSITY
Inventors:
Jingzhou Zhao, Max Aaron Martel, Yuri Andrew Gulak
Abstract: Nanocages are formed by etching nanocubes. The nanocubes are added to an aqueous system having an amphiphilic lipid dissolved in an organic solvent (e.g. a hydrophobic alcohol) to form reverse micelles. As the water evaporates the micelles shrink as etching of the flat surface of the nanocubes occurs. In this fashion hollow nanocages are produced. In one embodiment, the nanocage is covalently attached to a polymer shell (e.g. a dextran shell).
Type:
Grant
Filed:
May 18, 2020
Date of Patent:
May 10, 2022
Assignee:
Research Foundation of the City University of New York
Abstract: A method for producing aluminum strips for lithographic printing plate supports, wherein the aluminum strip is produced from a rolling ingot, which after optional homogenizing is hot-rolled to a thickness of 2 mm to 7 mm and cold-rolled to a final thickness of 0.15 mm to 0.5 mm provides for an aluminum strip having a thickness of 0.15 mm to 0.5 mm and a printing plate support produced from the aluminum strip.
Type:
Grant
Filed:
April 21, 2017
Date of Patent:
May 10, 2022
Assignee:
Hydro Aluminium Deutschland GmbH
Inventors:
Bernhard Kernig, Henk-Jan Brinkman, Jochen Hasenclever, Christoph Settele, Gerd Steinhoff
Abstract: A micro/nanoparticle-reinforced composite solder for low-temperature soldering and a preparation method thereof belong to the manufacturing field of lead-free low-temperature soldering solders. Micro/nanoparticle-reinforced tin-based alloy solder powder is formed by diffusely mixing micro/nano-sized Cu, Ag and Sb particles with a molten metal tin and atomizing the mixture, and then blended with low-melting-point SnBi-based alloy solder powder and a conventional flux to prepare a micro/nanoparticle-reinforced composite solder. In soldering at a temperature below 200° C.
Type:
Grant
Filed:
December 7, 2017
Date of Patent:
May 10, 2022
Assignee:
Shenzhen Fitech Co., Ltd.
Inventors:
Pu Xu, Siyuan Wang, Daoke Yu, Kui Chen, Jianhao Shi
Abstract: A preparation method of indium oxide with stable morphology includes: (1) mixing indium oxide powder and bismuth oxide powder according to a mass ratio of 1:0.1-0.5 to obtain a powder mixture; (2) putting the powder mixture into a ball mill for ball milling at room temperature to obtain a uniform powder mixture; (3) putting the obtained uniform powder mixture into a muffle furnace and calcining at 700-1000° C.; and (4) obtaining the indium oxide with cubic stable morphology after the muffle furnace naturally cools to room temperature. The method has advantages of simple synthesis process, short synthesis period, high sample yield, no need of complicated equipment, and morphology of the obtained indium oxide can be maintained after being heated at a high temperature within 1000° C. for 2 hours. An electrochemical sensor prepared by using the indium oxide obtained by the method has better selectivity to nonane.
Abstract: The present disclosure relates to an aluminum alloy for die casting, more particularly, to an aluminum alloy for die casting which has high corrosion resistance, strength and castability. The embodiments of the present disclosure provide an aluminum alloy for die casting comprising a composition ratio having an aluminum (Al) content which occupies almost the composition ratio of the aluminum alloy; a magnesium (Mg) content of 2.5˜3.0%; a silicon (Si) content of 9.6˜0.5%; a zinc (Zn) content of 0.5% or less; and a copper (Cu) content of 0.15% or less.
Abstract: To provide a method for efficiently producing metal microparticles having a particle diameter of 1 ?m to 10 ?m, and a device for producing the same. A metal microparticle production method is used, which includes a particle generating step of generating primary particles by irradiating a metal lump in a solvent in a first tank with an ultrasonic wave, and a particle splitting step of irradiating the primary particles with an ultrasonic wave in a solvent in a second tank and splitting the primary particles to produce secondary particles.
Abstract: Aluminum alloys having improved properties are provided. The alloy includes about 13 to about 17 weight percent silicon, about 0.3 to about 0.6 weight percent magnesium, and at least 75 weight percent aluminum. The alloy may include copper up to about 2.0 weight percent; iron up to about 0.8 weight percent; manganese up to about 1.0 weight percent; nickel up to about 1.0 weight percent; zinc up to about 0.8 weight percent; titanium up to about 0.5 weight percent; zirconium up to about 0.5 weight percent; vanadium up to about 0.5 weight percent; and other trace elements up to about 0.1 weight percent. In addition, the alloy may contain about 50 to about 1000 ppm of strontium and about 10 about 100 ppm phosphorus. Also disclosed is a die cast article, such as transmission clutch housing.
Abstract: Systems, methods, and devices are disclosed for producing quantum particles (e.g., quantum dots) having a uniform size by vaporization of molten precursor droplets. More particularly, the present technology produces quantum dots by melting or liquefying solid and substantially pure precursor materials followed by production of uniformly sized droplets of molten precursor by use of a droplet maker into a microwave generated plasma torch.
Abstract: Disclosed herein are embodiments of mechanically alloyed powder feedstock and methods for spheroidizing them using microwave plasma processing. The spheroidized powder can be used in metal injection molding processes, hot isostatic processing, and additive manufacturing. In some embodiments, mechanical milling, such as ball milling, can be used to prepare high entropy alloys for microwave plasma processing.
Type:
Grant
Filed:
April 29, 2020
Date of Patent:
April 26, 2022
Inventors:
Sunil Bhalchandra Badwe, Makhlouf Redjdal, Scott Joseph Turchetti