Patents Examined by John P Sheehan
  • Patent number: 7955443
    Abstract: A permanent magnet material is prepared by covering an anisotropic sintered magnet body of formula: R1x(Fe1-yCoy)100-x-z-aBzMa wherein R1 is a rare earth element, M is Al, Cu or the like, with a powder comprising an oxide of R2, a fluoride of R3 or an oxyfluoride of R4 wherein R2, R3, and R4 are rare earth elements, and having an average particle size up to 100 ?m, heat treating the powder-covered magnet body in a hydrogen gas-containing atmosphere for inducing disproportionation reaction on R12Fe14B compound, and continuing heat treatment at a reduced hydrogen gas partial pressure for inducing recombination reaction to said compound, thereby finely dividing said compound phase to a crystal grain size up to 1 ?m, and for effecting absorption treatment, thereby causing R2, R3 or R4 to be absorbed in the magnet body.
    Type: Grant
    Filed: April 11, 2007
    Date of Patent: June 7, 2011
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Hajime Nakamura, Takehisa Minowa, Koichi Hirota
  • Patent number: 7955442
    Abstract: The present invention provides a method for producing a sintered magnet, which can have a sufficient sintered density even when the magnet has a low-R composition. The method is for producing a sintered magnet comprising R (R: one or more rare-earth elements), T (T: one or more transition metal elements essentially comprising Fe, or Fe and Co) and B (boron) as the main components, wherein a starting alloy prepared by strip casting is pulverized to a given particle size to form a fine powder, where the starting alloy comprises discolored deposit 1 on the surface and the area ratio of the discolored deposit 1 is 1.5% or less, the resulting fine powder is compacted in a magnetic field to prepare a compact, and the compact is sintered.
    Type: Grant
    Filed: November 16, 2004
    Date of Patent: June 7, 2011
    Assignee: TDK Corporation
    Inventors: Tetsuya Hidaka, Chikara Ishizaka
  • Patent number: 7942984
    Abstract: A steel pipe blank having a composition containing 0.5% or less C and 85% or more Fe in terms of mass percent is heated, and stretch-reducing is then performed so that the diameter decrease ratio is 15% or more and the rolling finishing temperature is (the Ar3 transformation point?10)° C. or lower. Consequently, a structure in which the ratio of X-ray diffraction intensity obtained from the plane in which the <100> direction of crystal grains is preferentially oriented parallel to the circumference direction and the <011> direction of crystal grains is preferentially oriented parallel to the rolling direction of the steel pipe to that obtained for a three-dimensionally randomly oriented sample is 3.0 or more is formed, and the r-value is increased, thereby improving the magnetic properties of the steel pipe.
    Type: Grant
    Filed: September 1, 2005
    Date of Patent: May 17, 2011
    Assignee: JFE Steel Corporation
    Inventors: Yasuhide Ishiguro, Yoshikazu Kawabata, Kei Sakata, Masayuki Sakaguchi, Masayoshi Ishida, Motoaki Itadani, Yasue Koyama
  • Patent number: 7942985
    Abstract: A soft magnetic alloy for perpendicular magnetic recording medium excellent in saturation magnetic flux density, amorphousness and atmospheric corrosion resistance. The alloy is an Fe—Co based alloy and comprises Fe in an amount satisfying 0.25 to 0.65 of Fe/(Fe+Co) ratio, which is an atomic ratio of Fe and Fe+Co; Zr+Hf in an amount of 6 to 100 at %; Na+Ta in an amount of 0 to 2 at %; Al and/or Cr in an amount of 0 to 5 at %; and the balance Co and unavoidable impurities. A part of Zr and/or Hf can be replaced by B, provided that the amount of B to replace Zr and/or Hf is double in at % of the total amount of Zr and Hf to be replaced and that the total amount of Zr and Hf after replacement is 4 at % or more.
    Type: Grant
    Filed: May 1, 2008
    Date of Patent: May 17, 2011
    Assignee: Sanyo Special Steel Co., Ltd.
    Inventors: Toshiyuki Sawada, Akihiko Yanagitani
  • Patent number: 7942982
    Abstract: Grain-oriented electrical steel sheet excellent in coating adhesion is provided. The steel sheet contains Si: 2 to 7% mass % and has a primary coating composed mainly of forsterite on its surface. A compound (A) containing one or more elements selected from among Ca, Sr and Ba, at least one rare earth metal, and sulfur is incorporated in the primary coating so as to reside in the interface layer between the primary coating and the steel sheet. As a result, occurrence of primary coating exfoliation at regions that are strongly worked during manufacture of a wound core transformer or the like is prevented.
    Type: Grant
    Filed: November 15, 2007
    Date of Patent: May 17, 2011
    Assignee: Nippon Steel Corporation
    Inventors: Yuji Kubo, Eiichi Nanba, Satoshi Arai, Hotaka Honma, Kazumi Mizukami, Koki Tanaka
  • Patent number: 7942981
    Abstract: A seamless, rotationally symmetrical hollow blank formed by a non-cutting operation from a deformable permanently magnetic alloy is provided, said alloy consisting essentially of 5.0 to 20.0 percent by weight cobalt, 20.0 to 35.0 percent by weight chromium, for the remainder iron and impurities caused by melting and/or by chance. The seamless hollow body is suitable in particular for use in hysteresis clutches, hysteresis brakes, and position measuring devices. Furthermore, non-cutting shaping processes for producing the seamless rotationally symmetrical hollow body are provided, with roller spinning being preferred.
    Type: Grant
    Filed: September 19, 2007
    Date of Patent: May 17, 2011
    Assignee: Vacuumschmelze GmbH & Co. KG
    Inventors: Ottmar Roth, Hartwin Weber, Lutz Hinrich, Jens Diehl
  • Patent number: 7938915
    Abstract: A method for producing a rare-earth alloy based binderless magnet according to the present invention includes the steps of: (A) providing a rapidly solidified rare-earth alloy magnetic powder; and (B) compressing and compacting the rapidly solidified rare-earth alloy magnetic powder by a cold process without using a resin binder, thereby obtaining a compressed compact, 70 vol % to 95 vol % of which is the rapidly solidified rare-earth alloy magnetic powder.
    Type: Grant
    Filed: August 3, 2006
    Date of Patent: May 10, 2011
    Assignees: Hitachi Metals, Ltd., Nippon Kagaku Yakin Co., Ltd.
    Inventors: Hirokazu Kanekiyo, Toshio Miyoshi, Katsunori Bekki, Ikuo Uemoto, Kazuo Ishikawa
  • Patent number: 7934309
    Abstract: The method of fabricating an exchange-coupling film in accordance with the present invention comprises a multilayer body forming step of forming a multilayer body having an antiferromagnetic layer and a ferromagnetic layer laminated on the antiferromagnetic layer; and an annealing step of annealing the multilayer body in a magnetic field with a maximum temperature higher than a blocking temperature of the multilayer body by 15 to 60° C.
    Type: Grant
    Filed: December 26, 2007
    Date of Patent: May 3, 2011
    Assignee: TDK Corporation
    Inventors: Keita Kawamori, Satoshi Miura
  • Patent number: 7935196
    Abstract: A soft magnetic ribbon that especially in a relatively low magnetic field region of 500 A/m or less, is high in the squareness of magnetic flux density-magnetization curve. There is disclosed a soft magnetic ribbon of 100 ?m or less thickness comprising a parent phase structure in which by volume ratio, 30% or more of crystal grains of 60 nm or less (not including 0) crystal grain diameter are dispersed in an amorphous phase and comprising an amorphous layer disposed on the surface side of the parent phase structure. Preferably, the soft magnetic ribbon is represented by the composition formula Fe100-x-yCuxXy (wherein X is at least one element selected from among B, Si, S, C, P, Al, Ge, Ga and Be), in which the atomic percents (%) satisfy the relationships 0<x?5 and 10?y?24.
    Type: Grant
    Filed: March 4, 2008
    Date of Patent: May 3, 2011
    Assignee: Hitachi Metals, Ltd.
    Inventors: Motoki Ohta, Yoshihito Yoshizawa
  • Patent number: 7931756
    Abstract: A method of making a rare-earth alloy granulated powder according to the present invention includes the steps of: preparing a rare-earth alloy powder; generating remnant magnetization in the powder; and granulating the powder by utilizing agglomeration force produced by the remnant magnetization of the powder. Since the agglomeration force produced by the remnant magnetization is utilized, the addition of a granulating agent may be omitted.
    Type: Grant
    Filed: October 5, 2009
    Date of Patent: April 26, 2011
    Assignee: Hitachi Metals, Ltd.
    Inventors: Futoshi Kuniyoshi, Tomoiku Otani
  • Patent number: 7922832
    Abstract: A permanent magnet material is prepared by machining an anisotropic sintered magnet body having the compositional formula: Rx(Fe1-yCoy)100-x-z-aBzMa wherein R is Sc, Y or a rare earth element, M is Al, Cu or the like, to a specific surface area of at least 6 mm?1, heat treating in a hydrogen gas-containing atmosphere at 600-1,100° C. for inducing disproportionation reaction on the R2Fe14B compound, and continuing heat treatment at a reduced hydrogen gas partial pressure and 600-1,100° C. for inducing recombination reaction to the R2Fe14B compound, thereby finely dividing the R2Fe14B compound phase to a crystal grain size ?1 ?m.
    Type: Grant
    Filed: April 6, 2007
    Date of Patent: April 12, 2011
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Hajime Nakamura, Takehisa Minowa
  • Patent number: 7918946
    Abstract: The invention provides an amorphous alloy with good soft magnetic properties, namely an Fe-based amorphous alloy having excellent soft magnetic properties comprising, in at. %, Fe: 78 to 86%, P: 6 to 20%, C: 2 to 10%, one or both of Si and Al: 0.1 to 5%, and a balance of unavoidable impurities. P or C can as required be partially or totally replaced with B: 1 to 18%.
    Type: Grant
    Filed: December 27, 2007
    Date of Patent: April 5, 2011
    Assignee: Nippon Steel Corporation
    Inventor: Yuichi Sato
  • Patent number: 7914628
    Abstract: A magnetic material comprising a NaZn13 type crystal structure with uniform and fine microstructure exhibiting excellent characteristics as a magnetic refrigeration material, and a method of manufacturing the magnetic refrigeration material are provided. An alloy composition for forming magnetic material of the NaZn13 type crystal structure was melted comprising 0.5 atomic percent to 1.5 atomic percent of B to molten metal. The molten metal is rapidly cooled and solidified by a forced cooling process. Then, a rapidly cooled alloy having the NaZn13 type crystal structure was obtained. In this manner, magnetic materials comprising the NaZn13 type crystal structure phase, or the NaZn13 type crystal structure phase accompanied with other phases such as ?-Fe phase having very small phase regions was manufactured without requiring heat treatment for a long time. As the result, productivity of manufacturing the magnetic refrigeration material is remarkably enhanced.
    Type: Grant
    Filed: March 2, 2006
    Date of Patent: March 29, 2011
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Hideyuki Tsuji, Akiko Saito, Tadahiko Kobayashi
  • Patent number: 7909945
    Abstract: Disclosed are soft magnetic alloys that consist essentially of 10% by weight ?Co?22% by weight, 0% by weight ?V?4% by weight, 1.5% by weight ?Cr?5% by weight, 1% by weight ?Mn?2% by weight, 0% by weight ?Mo?1% by weight, 0.5% by weight ?Si?1.5% by weight, 0.1% by weight ?Al?1.0% by weight, rest iron. Also disclosed are methods of making the alloys, and products containing them, such as actuator systems, electric motors, and the like.
    Type: Grant
    Filed: July 27, 2007
    Date of Patent: March 22, 2011
    Assignee: Vacuumschmelze GmbH & Co. KG
    Inventors: Witold Pieper, Joachim Gerster
  • Patent number: 7892365
    Abstract: A method of making a magnetically anisotropic magnet powder according to the present invention includes the steps of preparing a master alloy by cooling a rare-earth-iron-boron based molten alloy and subjecting the master alloy to an HDDR process. The step of preparing the master alloy includes the step of forming a solidified alloy layer, including a plurality of R2Fe14B-type crystals (where R is at least one element selected from the group consisting of the rare-earth elements and yttrium) in which rare-earth-rich phases are dispersed, by cooling the molten alloy through contact with a cooling member.
    Type: Grant
    Filed: December 5, 2007
    Date of Patent: February 22, 2011
    Assignee: Hitachi Metals, Ltd.
    Inventors: Hiroyuki Tomizawa, Yuji Kaneko
  • Patent number: 7887645
    Abstract: The present invention provides a method of producing a high permeability grain oriented electrical steel having excellent mechanical and magnetic properties. A hot band having a thickness of about 1.5 to about 4.0 mm has a chemistry comprising about 2.5 to about 4.5% silicon, about 0.1 to about 1.2% chromium, about 0.02 to about 0.08% carbon, about 0.01 to about 0.05% aluminum, up to about 0.1% sulfur, up to about 0.14% selenium, about 0.03 to about 0.15% manganese, up to about 0.2% tin, up to about 1% copper, and balance being essentially iron and residual elements, all percentages by weight. The band has a volume resistivity of at least about 45 ??-cm, an austenite volume fraction (?1150° C.) of at least 20% and the strip has an isomorphic layer thickness of at least about 2% of the total thickness on at least one surface of the hot processed band. The band is rapidly cooled after the anneal prior to cold rolling at a rate of at least 30° C./second from 875-950° C. to a temperature below 400° C.
    Type: Grant
    Filed: May 2, 2001
    Date of Patent: February 15, 2011
    Assignee: AK Steel Properties, Inc.
    Inventors: Jerry W. Schoen, Norris A. Dahlstrom, Robert J. Comstock, Jr.
  • Patent number: 7887647
    Abstract: A soft magnetic material includes a plurality of composite magnetic particles each including a metal magnetic particle and an insulating coating film covering the metal magnetic particle. Each of the plurality of composite magnetic particles has a ratio Rm/c of a maximum diameter to a circle-equivalent diameter of more than 1.15 and not more than 1.35. The insulating coating film is composed of a thermosetting organic material and has a pencil hardness of 5H or higher after thermosetting. With this material, an eddy current loss can be reduced, and a compact with a high strength can be formed.
    Type: Grant
    Filed: September 8, 2006
    Date of Patent: February 15, 2011
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Toru Maeda, Yasushi Mochida, Takao Nishioka
  • Patent number: 7887646
    Abstract: The present invention provides oriented magnetic steel plate with excellent coating adhesion, in particular coating edge peeling resistance, that is, oriented magnetic steel plate with excellent coating adhesion containing, by mass %, Si: 1.8 to 7% and having a primary coating having forsterite as its main ingredient on its surface, said oriented magnetic steel plate characterized in that said primary coating contains one or more of Ce, La, Pr, Nd, Sc, and Y in an areal weight per side of 0.001 to 1000 mg/m2; characterized in that said primary coating contains Ti in an areal weight per side of 1 to 800 mg/m2; and characterized in that said primary coating contains one or more of Sr, Ca, and Ba in an areal weight per side of 0.01 to 100 mg/m2.
    Type: Grant
    Filed: May 19, 2006
    Date of Patent: February 15, 2011
    Assignee: Nippon Steel Corporation
    Inventors: Eiichi Nanba, Yuji Kubo, Kazutoshi Takeda, Satoshi Arai, Hotaka Honma, Kenichi Murakami, Hideyuki Kobayashi
  • Patent number: 7883587
    Abstract: A rare earth permanent magnet is prepared by providing a sintered magnet body consisting of 12-17 at % of rare earth, 3-15 at % of B, 0.01-11 at % of metal element, 0.1-4 at % of O, 0.05-3 at % of C, 0.01-1 at % of N, and the balance of Fe, disposing on a surface of the magnet body a powder comprising an oxide, fluoride and/or oxyfluoride of another rare earth, and heat treating the powder-covered magnet body at a temperature below the sintering temperature in vacuum or in an inert gas, for causing the other rare earth to be absorbed in the magnet body.
    Type: Grant
    Filed: November 16, 2007
    Date of Patent: February 8, 2011
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Hajime Nakamura, Koichi Hirota, Takehisa Minowa
  • Patent number: 7871475
    Abstract: The object of the present invention is to provide a rare earth magnet which enables to achieve a good balance between high coercive force and high residual magnetic flux density, and its manufacturing method. The present invention provides a rare earth magnet in which a layered grain boundary phase is formed on a surface or a potion of a grain boundary of Nd2Fe14B which is a main phase of an R—Fe—B (R is a rare-earth element) based magnet, and wherein the grain boundary phase contains a fluoride compound, and wherein a thickness of the fluoride compound is 10 ?m or less, or a thickness of the fluoride compound is from 0.1 ?m to 10 ?m, and wherein the coverage of the fluoride compound over a main phase particle is 50% or more on average.
    Type: Grant
    Filed: August 3, 2009
    Date of Patent: January 18, 2011
    Assignee: Hitachi, Ltd.
    Inventors: Matahiro Komuro, Yuichi Satsu