Abstract: A method of making a ?-SiAlON is described in involves mixing nanoparticles of AlN, Al2O3, and SiO2 with particles of Si3N4 and spark plasma sintering the mixture. The sintering may be at a temperature of 1450-1600° C. or about 1500° C. The particles of Si3N4 may be nanoparticles comprising amorphous Si3N4, or 25-55 ?m diameter microparticles comprising ?-Si3N4.
Type:
Grant
Filed:
August 2, 2019
Date of Patent:
October 25, 2022
Assignee:
KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
Inventors:
Abbas Saeed Hakeem, Anwar Ul-Hamid, Oki Muraza, Muhammad Ali Ehsan
Abstract: The method of making carbon-zinc oxide (C—ZnO) nanoparticles includes grinding a mixture of zinc nitrate hexahydrate (Zn(NO3)2.6H2O) and furfural (C4H3OCHO) to produce a ground mixture. As a non-limiting example, the zinc nitrate hexahydrate (Zn(NO3)2.6H2O) and the furfural (C4H3OCHO) may be placed in a mortar and ground, by hand with a pestle, for approximately 10 minutes. The ground mixture is then heated to produce the C—ZnO nanoparticles. As a non-limiting example, the ground mixture may be heated in a quartz tube at a temperature of approximately 500° C.
Type:
Grant
Filed:
February 6, 2021
Date of Patent:
October 18, 2022
Assignee:
KING FAISAL UNIVERSITY
Inventors:
Sajid Ali Ansari, Nazish Parveen, Abdullah Aljaafari, Adil Ahmed Al Shoaibi
Abstract: A solid particulate reactive sorbent for decontaminating toxic chemical and biological agents and its method of making. The reactive sorbent comprising a plurality of aggregates formed from linked hydrophilic nanoparticles and individual nanoparticles that bind at least one detoxifier, such that the sorbent absorbs the agents, allowing the detoxifier to oxidize and decontaminate the agents for removal. More preferably, the hydrophilic nanoparticles comprise fumed silica and the detoxifier comprises hydrogen peroxide.
Type:
Grant
Filed:
December 11, 2018
Date of Patent:
October 11, 2022
Assignee:
The United States of America as Represented by the Secretary of the Army
Abstract: A method of applying a NOx degrading composition on a concrete element, including providing a concrete element having a surface, and applying a composition including photocatalytic titanium dioxide particles dispersed in a continuous phase on the surface of said concrete element. Also, a concrete element having NOx degrading properties. Also, a concrete element having photocatalytic titanium dioxide particles dispersed thereon.
Type:
Grant
Filed:
April 11, 2014
Date of Patent:
October 11, 2022
Assignee:
Photocat A/S
Inventors:
Henrik Jensen, Karsten Felsvang, Michael Humle
Abstract: The invention discloses a preparation method of high-absorptivity silica as lutein carrier. The method includes adding sodium silicate into a synthesis kettle, introducing steam for heating while stirring, adding water, stirring for reaction to obtain a reaction substrate A, and adding sulfuric acid to the reaction substrate A to obtain reaction solution B; simultaneously adding sulfuric acid and sodium silicate into the reaction solution B, performing synthesis reaction for a given period of time, stopping feeding of sodium silicate, adding sulfuric acid only for post-acidification, and aging to obtain dilute slurry D; and filtering the dilute slurry D, washing, slurrying, drying and packaging to obtain silica microspheres as lutein carrier. The invention accurately controls each process so that the prepared high-absorptivity silica as lutein carrier has high adsorption and good dispersibility and flowability after adsorbing lutein.
Type:
Grant
Filed:
May 7, 2019
Date of Patent:
September 13, 2022
Assignee:
SHANDONG LINK SCIENCE AND TECHNOLOGY CO., LTD.
Abstract: The present invention relates to a mixed oxide with enhanced resistance and NOx storage capacity. The mixed oxide may be used as a component of a NOx trap material in an exhaust system of an internal combustion engine. The invention also relates to a method for treating an exhaust gas from an internal combustion engine using the mixed oxide.
Abstract: A system and a method for producing silicon from a SiO2-containing material that includes solid SiO2. The method uses a reaction vessel including a first section and a second section in fluid communication with said first section. The method includes: heating the SiO2-containing material that includes the solid SiO2 to a SiO2-containing material that includes liquid SiO2, at a sufficient temperature to convert the solid SiO2 into the liquid SiO2; converting, in the first section, the liquid SiO2 into gaseous SiO2 that flows to the second section by reducing the pressure in the reaction vessel to a subatmospheric pressure; and reducing, in the second section, the gaseous SiO2 into liquid silicon using a reducing gas. The reducing of the pressure is performed over a continuous range of interim pressure(s) sufficient to evaporate contaminants from the SiO2-containing material, and removing by vacuum, the one or more evaporated gaseous contaminants.
Abstract: Granular and/or shaped hydrophobic silica useful for thermal insulation materials are prepared by mixing hydrophilic silica with a hydrophobicizing agent at low temperature so the hydrophobicizing agent does not appreciably react, followed by deaeration and compaction.
Type:
Grant
Filed:
February 27, 2017
Date of Patent:
July 5, 2022
Assignee:
WACKER CHEMIE AG
Inventors:
Konrad Hindelang, Dominik Jantke, Richard Weidner
Abstract: A porous carbon-based metal catalyst, a preparation method and application thereof are provided. The preparation method includes: successively performing activation, surface corrosion, nitrogen-doping treatment and graphitization treatment on washed micro-grade porous carbon, then performing sensitization treatment, and subsequently carrying out loading, reduction and other treatments of catalytic metal, so as to finally obtain the porous carbon-based metal catalyst. The porous carbon-based metal catalyst provided by the present application has excellent catalytic performance, is especially suitable for producing hydrogen by efficiently catalytically decomposing ammonia borane, is not prone to inactivation, and is easy to regenerate after inactivation. Meanwhile, the preparation method is environmental-friendly, is suitable for large-scale production and has a wide application prospect in the fields such as hydrogen fuel batteries.
Abstract: The present invention relates to a general field of machine building and provides a composition for coating friction surfaces usable for coating friction surfaces to de-crease wear and to reduce the friction coefficient. Also uses of the composition are within the scope of the present invention.
Abstract: The present invention relates to a catalyst comprising a carrier substrate of the length L extending between substrate ends a and b and three washcoat zones A, B and C wherein washcoat zone A comprises one or more first platinum group metals and extends starting from substrate end a over a part of the length L, washcoat zone C comprises one or more first platinum group metals and extends starting from substrate end b over a part of the length L, and washcoat zone B comprises the same components as washcoat zone A and in addition, one or more second platinum group metals and extends between washcoat zones A and C, wherein L=LA+LB+LC, wherein LA is the length of washcoat zone A, LB is the length of substrate length B and LC is the length of substrate length C.
Type:
Grant
Filed:
September 6, 2018
Date of Patent:
May 17, 2022
Assignee:
UMICORE AG & CO. KG
Inventors:
Ryan J. Andersen, John G. Nunan, Curt M. Ellis, Geon Seog Son
Abstract: The present invention provides a polycrystalline silicon rod whose rod surface portion has a phosphorus concentration of 0.015 ppba or less, in which the ratio (P2/P1) of the phosphorus concentration (P2) of the rod center portion to the phosphorus concentration (P1) of the rod surface portion is within the range of 2 or lower. The present invention also provides a method for producing a polycrystalline silicon rod by the Siemens method that assembles a polycrystalline silicon seed rod in a reactor, then heats the seed rod up to a temperature of 1000° C. or more and less than the melting point of silicon by energization heating, and supplies a raw material gas including trichlorosilane gas and hydrogen gas as the main components to the reactor at the heating temperature to deposit and grow silicon on the seed rod surface.
Abstract: The invention relates to a method for preparing a hydrogenation catalyst or catalyst precursor comprising a catalytically active material and a carrier material. The method involves the mixing of an acidic solution comprising metal ions of a metal selected from the IUPAC group 8, 9 or 10 metals, preferably cobalt, a suspension comprising the carrier material and an alkaline solution. The invention also relates to a precursor of a hydrogenation catalyst wherein the precursor comprises crystallites of metal oxides having an average size of max. 8 nm.
Type:
Grant
Filed:
December 20, 2016
Date of Patent:
April 12, 2022
Assignee:
SHELL OIL COMPANY
Inventors:
Andreas Klemt, László Domokos, Frank Peter Friedel, Stefan Boettcher, Erwin Roderick Stobbe
Abstract: Methods for synthesizing a water-soluble titanium-silicon complex are disclosed herein. The titanium-silicon complex can be utilized to produce titanated solid oxide supports and titanated chromium supported catalysts. The titanated chromium supported catalysts subsequently can be used to polymerize olefins to produce, for example, ethylene based homopolymer and copolymers.
Type:
Grant
Filed:
March 6, 2019
Date of Patent:
April 12, 2022
Assignee:
Chevron Phillips Chemical Company LP
Inventors:
Max P. McDaniel, Kathy S. Clear, Eric D. Schwerdtfeger, Jeremy M. Praetorius
Abstract: An exhaust gas purifying catalyst for 2-stroke general-purpose engines, which is characterized in that: the exhaust gas purifying catalyst includes a base and a coat layer on the base; the coat layer contains noble metals and metal oxides; the noble metals include palladium and one or more elements selected from among platinum and rhodium; the zirconia content in the coat layer is 0.07 mole or less per 100 g of the metal oxides contained in the coat layer; and the total content of one or more metal oxides selected from among lanthana and alkaline earth metal oxides in the coat layer is 0.05 mole or more per 100 g of the metal oxides contained in the coat layer.
Abstract: A process for producing a metal-molybdate material is provided. The process includes a step of reacting a metal molybdenum (Mo) material in a liquid medium with a first acid to provide a Mo composition and combining the Mo composition with a metal source to provide a metal-Mo composition. The metal-Mo composition can be pH adjusted with a base to precipitate a plurality of metal-Mo particulates.
Type:
Grant
Filed:
February 22, 2018
Date of Patent:
March 29, 2022
Assignee:
BWXT Isotope Technology Group, Inc.
Inventors:
William Earl Russell, II, Earl Brian Barger, Benjamin I. Bishop, Barbara B. Bohannon, Christopher Sean Fewox, James B. Inman, Erik T. Nygaard, Timothy A. Policke, Stephen D. Preite, Roger D. Ridgeway, Steve W. Schilthelm, Bryan Blake Wiggins
Abstract: The present invention relates to a novel process for oxidative esterification, generally for reaction of aldehydes with alcohols in the presence of oxygenous gases directly to give the corresponding ester in the presence of a heterogeneous catalyst, by means of which, for example, (meth)acrolein can be converted to methyl (meth)acrylate. The new catalyst has titanium dioxide as the main component of the support material. The catalysts are especially notable for high mechanical and chemical stability and for good catalytic performance even over very long periods. The process is an improvement in the catalyst service life, activity and selectivity over prior art catalysts which lose activity and/or selectivity relatively quickly in continuous operation in media having even a small water content.
Abstract: A method for producing a dispersion of metal-containing particles includes contacting a metal-supported material obtained by supporting a metal and/or a metal compound on a carrier with a polymeric protective agent showing affinity for the metal and/or the metal compound in a solvent to obtain a dispersion of metal-containing particles in which the metal and/or the metal compound is dispersed in the solvent in the form of particles.
Abstract: A manufacturing system and method for recycling and smelting crushed silica from silicon plants, including a crushed silica storage device, granulator, submerged arc furnace, transfer device, forming device and cooling system. Firstly silicon waste is collected, then crushed silica is output to a granulator. The granulator mixes the waste irregular crushed silica with water, and granulates and produces small particles having an uniform grain size as the raw material for smelting. The raw material is smelted in the submerged arc furnace. The forming device evenly pours the silicon liquid into the cooling system according to a set flow rate. The silicon liquid is solidified to form silicon pellets, and then a lift system is used to lift the formed silicon pellets, wherein the silicon liquid poured into the cooling system has a uniform diameter. The system can rapidly and efficiently smelt the silicon waste from the silicon plants.
Abstract: A method for oxidizing water including fabricating a working electrode using an electrocatalyst, preparing an electrochemical cell by putting the working electrode, a counter electrode, and a reference electrode in an electrolyte, and performing an oxygen evolution reaction (OER) by applying an electrical potential between the working electrode and the counter electrode. The electrocatalyst includes a nickel-calcium-iron layered double hydroxide (NiCaFe-LDH) nanoparticle, the NiCaFe-LDH nanoparticle has a formula of [Fex)NiCa(1-x](OH)2(NO3)x.nH2O, where: 0.2?x?0.4 and 0?n?2.5.