Patents Examined by Nazmun Nahar Shams
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Patent number: 12233463Abstract: A composition for pressure bonding contains a metal powder and a solid reducing agent and has a compressibility of 10% to 90%, the compressibility being expressed by a relationship formula using the thickness A of a dried coating film formed by drying the composition in an air atmosphere at 110° C. under atmospheric pressure for 20 minutes and the thickness B of a sintered body formed by treating the dried coating film in a nitrogen atmosphere at 280° C. under a pressure of 6 MPa for 20 minutes. The solid reducing agent may be BIS-TRIS. Also provided is a bonded structure of conductors in which a bonding portion via which two conductors are bonded together is formed by treating, under pressure, the two conductors and a coating film formed of the composition for pressure bonding provided therebetween.Type: GrantFiled: March 25, 2020Date of Patent: February 25, 2025Assignee: Mitsui Mining & Smelting Co., Ltd.Inventors: Kei Anai, Shinichi Yamauchi, Jung-Lae Jo
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Patent number: 12218322Abstract: A manganese-lithium separation process and a pre-extraction solution preparation process in comprehensive recovery of ternary battery wastes, and a method for comprehensive recovery of cobalt, nickel, manganese and lithium elements from the ternary battery wastes, relates to a method for recycling battery wastes. According to the present disclosure, cobalt and nickel ions are separated from an impurity-removed solution by a hydrolysis method; manganese, lithium and other ions in the impurity-removed solution are free from an extraction procedure, so that most manganese ions are separated and removed by a wet method before extraction, to prevent the manganese ions from entering the extraction system; nickel ions are free from an extraction procedure of full extraction and full back-extraction; and nickel hydroxide is directly precipitated after related impurities are removed by extraction.Type: GrantFiled: January 6, 2022Date of Patent: February 4, 2025Assignee: HUNAN JIN YUAN NEW MATERIALS JOINT STOCK COMPANY LIMITEDInventors: Xunbing Liu, Jianjun Ouyang, Xijuan Liu, Shanmu Wu, Xiangping Zhao, Xiongwu Dong, Chaowen Zhang, Quncheng Zhou, Chun Luo, Sanxian Chen
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Patent number: 12203159Abstract: A method of producing a wrought aluminum alloy product is disclosed comprising Cu, Mn, Zr, Sc and Ti. The method includes casting an unwrought billet, ingot or shape from a liquid metal bath, and homogenizing the unwrought billet, ingot or shape at an equivalent time at temperature. The homogenization process includes first stage heating within a relatively low temperature range, second stage heating within an intermediate temperature range, and third stage heating at a relatively high temperature. After homogenizing, the billet, ingot or shape is worked into an extruded product, solution heat treated, quenched, stretched to a permanent set, and artificially aged. The extruded aluminum alloy product has desirable mechanical properties and electrical conductivity.Type: GrantFiled: April 25, 2022Date of Patent: January 21, 2025Assignee: Universal Alloy CorporationInventors: Baptiste Thomas Jean Rouxel, Thomas Henri Dorin, Timothy J. Langan, Justin D. Lamb
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Patent number: 12205738Abstract: A method of producing a sintered magnet is disclosed herein. In some embodiments, a method of producing a sintered magnet comprises, sintering a R—Fe—B based magnetic powder to produce a sintered magnet; wherein the R is Nd, Pr, Dy, Ce or Tb, and infiltrating a eutectic alloy into the sintered magnet, wherein the eutectic alloy contains Pr, Al, Cu and Ga, and wherein infiltration the eutectic alloy includes applying the eutectic alloy to the sintered magnet and heat-treating the sintered magnet to which the eutectic alloy is applied.Type: GrantFiled: October 7, 2020Date of Patent: January 21, 2025Assignee: LG Chem, Ltd.Inventors: Tae Hoon Kim, Soon Jae Kwon, Hyounsoo Uh, Ikjin Choi, Jinhyeok Choe, Ingyu Kim, Eunjeong Shin, Nakheon Sung
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Patent number: 12202046Abstract: Methods and systems for producing feedstock powders, suitable for use in laser-based additive manufacturing, use laser ablation to vaporize a source material, which may be in bulk solid or solid coarse grain form. The source material is vaporized by a laser (or other focused energy source) in a vaporization chamber that is temperature controlled to provide a vertical thermal gradient. The vertical thermal gradient may be controlled to, in turn, control the nucleation, coagulation, and agglomeration of the vaporized molecules, enabling formation of microparticles that may then be used as feedstock powders in laser-based additive manufacturing. The produced feedstock powder particles may be of uniform composition, of uniform shape (e.g., substantially spherical), and of uniform phase or homogeneously mixed phases.Type: GrantFiled: December 22, 2020Date of Patent: January 21, 2025Assignee: Battelle Energy Alliance, LLCInventors: Robert C. O'Brien, Owen O. Abe
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Patent number: 12194531Abstract: This application describes kits, methods, and systems of three dimensional printing. In some examples, described herein are three-dimensional object printing kits comprising a metallic or a ceramic build material, a polymeric binder dispersed in an aqueous liquid vehicle, and a boundary fluid comprising thermally expandable particles.Type: GrantFiled: April 29, 2019Date of Patent: January 14, 2025Assignee: Hewlett-Packard Development Company, L.P.Inventor: James P Shields
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Patent number: 12194530Abstract: The present invention relates to an additive manufacturing powder material including Fe alloy particles each having an oxide film on a surface thereof, in which the Fe alloy particles satisfy d?15 and I/d?0.025, where d [nm] represents a thickness of the oxide film, and a peak intensity ratio I represents an intensity ratio IB/IA of a peak B in a region B of a Raman shift of 1,309 to 1,329 cm?1 to a peak A in a region A of a Raman shift of 657.5 to 677.5 cm?1 in a Raman spectrum.Type: GrantFiled: November 29, 2022Date of Patent: January 14, 2025Assignee: DAIDO STEEL CO., LTD.Inventors: Daisuke Kanai, Yuki Matsuoka
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Patent number: 12180560Abstract: The present invention relates to a solid-liquid-solid hydrometallurgical method in the presence of hydrated and/or non-hydrated salts in an oversaturation conditions, which is achieved by the intentional and repetitive application of drying and wetting steps, enhancing the chemical and physical phenomena on the mineral or concentrate, thus provoking the crystallization, recrystallization, and release of copper in a non-stoichiometric decomposition of the sulfide and its subsequent precipitation with chloride. The invention is made up of 3 steps called: (a) Wetting, (b) Drying and Oversaturation, (c) Washing and re-wetting, and these are conducted at temperatures ranging from 20-40° C. regardless of the redox potential with a minimum consumption of water and acid without requiring the addition of oxygen. The method allows diminishing the water and acid consumption, since the transformation of the sulfide can be carried out only in the presence of hydrated salts and/or the minimal addition of acid and water.Type: GrantFiled: October 29, 2019Date of Patent: December 31, 2024Assignee: NOVA MINERALIS S.A.Inventor: Rodrigo Andrés Cortés Cortés
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Patent number: 12180572Abstract: The steel plate has a specific chemical composition, and a microstructure where a volume fraction of martensite at a depth of 1 mm from a surface of the steel plate is 95% or more, and at a depth of 1 mm from a surface of the steel plate, a Vickers hardness at 400° C. is 288 or more, and a Brinell hardness at 25° C. is 360 HBW10/3000 to 490 HBW10/3000.Type: GrantFiled: August 17, 2020Date of Patent: December 31, 2024Assignee: JFE STEEL CORPORATIONInventors: Naoki Takayama, Shigeki Kitsuya, Yoshiaki Murakami
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Patent number: 12180558Abstract: A method for manufacturing a grain-oriented electrical steel sheet includes: a silicon steel material production process of producing a silicon steel material; a hot rolling process of obtaining a hot rolled sheet by subjecting the silicon steel material to hot rolling; a cold rolling process of obtaining a steel sheet of a final sheet thickness by subjecting the hot rolled sheet to a single cold rolling process or multiple cold rolling processes having intermediate annealing performed between the cold rolling processes; a decarburization annealing process of subjecting the steel sheet to decarburization annealing; and a final annealing process of applying an annealing separator containing alumina as a main component to the steel sheet and subjecting the steel sheet to final annealing.Type: GrantFiled: January 16, 2020Date of Patent: December 31, 2024Assignee: NIPPON STEEL CORPORATIONInventors: Yoshiyuki Ushigami, Shuichi Nakamura, Hiroyasu Fujii, Norikazu Fujii
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Patent number: 12168256Abstract: The disclosure relates to a method for forming a metal article by additive manufacturing and related apparatus for performing the method. A metal particle suspension including a UV-curable polymeric resin liquid medium, and metal particles distributed throughout the liquid medium is deposited and cured by spatially selective exposure to UV radiation in a layer-by-layer process. Metal particle size can be selected in combination with the applied layer thickness to ensure complete cure throughout the applied layer while providing a high print speed and high spatial resolution. Intermittent or periodic partial curing of an applied layer can be used to maintain a homogeneous distribution of metal particles in the applied layer prior to full curing. The final product is achieved after sintering, which removes the cured binder in a debinding step and also provides the desired final article at close to the full density.Type: GrantFiled: April 22, 2022Date of Patent: December 17, 2024Assignee: BOARD OF TRUSTEES OF MICHIGAN STATE UNIVERSITYInventors: Haseung Chung, Patrick Kwon
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Patent number: 12170161Abstract: A process and a system for producing a stock solution for production of a ferrofluid is provided. The process includes contacting an acidic solution in a reaction container filled with an excess of a bulk material containing Fe(III) and optionally Fe(II). The acid reacts with the bulk material to form the stock solution (Ls) having dissolved ferric (Fe(III)) and optionally ferrous (Fe(II)) ions which is then separated from the bulk material.Type: GrantFiled: March 27, 2020Date of Patent: December 17, 2024Assignees: URBAN MINING CORP B.V., TECHNISCHE UNIVERSITEIT DELFTInventors: Piotr Jakub Glazer, Ronald Alphons Penners, Simon Petrus Maria Berkhout, Peter Carlo Rem
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Patent number: 12146211Abstract: A cryogenic pressure vessel of formed of an ASTM A553 Type 1 cryogenic steel alloy including in wt. %: C: 0.01-0.04; Mn: up to 2.0; P: up to 0.02; S: up to 0.15; Si: up to 1.0; Ni: 7-11; Cr: up to 1.0; Mo: up to 0.75; V: up to 0.2; Nb: up to 0.1; Al: up to 0.1; and N: up to 0.01. The steel alloy may have an ultimate tensile strength of at least 900 MPa, a total elongation of at least 20%; a microstructure including between 5 and 20 area % reverted austenite and the remainder tempered martensite; a transverse Charpy impact energy of at least 27 J at ?196° C.; and a lateral expansion of at least 0.381 mm at ?196° C.Type: GrantFiled: November 21, 2019Date of Patent: November 19, 2024Assignee: ArcelorMittalInventors: George Jay Fraley, Frederick Fletcher
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Patent number: 12131850Abstract: A NdFeB rare earth magnet includes a main phase and a grain boundary phase including a white grain boundary phase and a gray grain boundary phase. In a microstructure observation area of the rare earth magnet, an area of the white grain accounts for 1˜3% of a total area of the microstructure observation area, and an area of the gray grain boundary phase accounts for 2˜10% of the total area of the microstructure observation area.Type: GrantFiled: June 24, 2021Date of Patent: October 29, 2024Assignees: SANVAC (BEIJING) MAGNETICS CO., LTD., BEIJING ZHONG KE SAN HUAN HI-TECH CO., LTD.Inventors: Guoan Chen, Haojie Wang, Bin Fang, Fei Du, Zhan Wang, Yugang Zhao
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Patent number: 12116657Abstract: A predetermined chemical composition is contained, and a predetermined relationship of the contents of Ag, B and REM is satisfied.Type: GrantFiled: June 4, 2020Date of Patent: October 15, 2024Assignee: JFE STEEL CORPORATIONInventors: Akito Mizutani, Mitsuyuki Fujisawa
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Patent number: 12112884Abstract: A method for improving the corrosion resistance of NdFeB materials is provided. The method includes in-situ growing a layer of oxide, nitride, or oxynitride on the surface of NdFeB magnet correspondingly by performing at least one of an oxidation treatment and a nitridation treatment at low temperature in a range of 200˜400° C., thereby significantly improving the corrosion resistance of the magnet. The method is simple to operate, low-cost, green, safe, and efficient. Depending on the parameters of the low-temperature oxidation and/or nitridation treatment, the thickness of the oxide, nitride, or oxynitride layer is adjustable from 10 nm to 100 ?m, which can improve the corrosion resistance of the magnet while maintaining excellent magnetic properties. Moreover, the thin surface layer is in-situ grown on the NdFeB substrate, which is strong and stable over a long service period and can be applied for mass production.Type: GrantFiled: April 1, 2022Date of Patent: October 8, 2024Assignee: ZHEJIANG UNIVERSITYInventors: Mi Yan, Jiaying Jin, Wang Chen, Chen Wu
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Patent number: 12090553Abstract: A manufacturing method of alloy powder comprises a liquid film forming step, a supplying step and a dividing step. In the liquid film forming step, a high speed fluid made of coolant liquid is shaped into a liquid film which has a predetermined thickness of 0.1 mm or more and receives a predetermined acceleration of 2.0×104G or more along a thickness direction. In the supplying step, molten alloy which is not divided into a size of the predetermined thickness or less is supplied to the liquid film. In the dividing step, the molten alloy is divided into the size of the predetermined thickness or less by the high speed fluid to make alloy particles and keeping the alloy particles in the liquid film by the predetermined acceleration so that the alloy particles are continuously cooled in the high speed fluid.Type: GrantFiled: June 29, 2022Date of Patent: September 17, 2024Assignee: TOKIN CORPORATIONInventors: Yosuke Imano, Akiri Urata, Masato Kuno
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Patent number: 12084736Abstract: A manufacturing method of a grain-oriented electrical steel sheet according to an embodiment of the present invention includes: manufacturing a cold-rolled sheet; forming a groove in the cold-rolled sheet; removing an Fe—O oxide formed on a surface of the cold-rolled sheet; primary recrystallization annealing the cold-rolled sheet; and applying an annealing separating agent to the primary recrystallized cold-rolled sheet, and secondary recrystallization annealing it, wherein a close contacting property coefficient calculated by Formula 1 below is 0.016 to 1.13. close contacting property coefficient (Sad)=(0.8×R)/Hhill-up??[Formula 1] (In Formula 1, R represents the average roughness (?m) of the surface of the cold-rolled sheet after the removing of the oxide, and Hhill-up represents the average height (?m) of the hill-up present on the surface of the cold-rolled sheet after the removing of the oxide.).Type: GrantFiled: December 18, 2019Date of Patent: September 10, 2024Assignee: POSCO CO., LTDInventors: Oh-Yeoul Kwon, Woo-Sin Kim, Dae-Uk Kim, Jong-Tae Park
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Patent number: 12059729Abstract: An object of the present invention is to provide a method for manufacturing a metal printed object that can reduce the generation of sputters, and the present invention provides a method for manufacturing a metal printed object in which, in the presence of a shielding gas supplied around metal powder in a chamber, heat is supplied to the metal powder using energy rays to form a metal layer and laminate the metal layer, wherein the mass per unit volume of the shielding gas at a temperature of 25° C. and a pressure of 0.1 MPa is 1.30×10?3 g/cm3 or less.Type: GrantFiled: April 17, 2019Date of Patent: August 13, 2024Assignee: TAIYO NIPPON SANSO CORPORATIONInventors: Yusuke Yamaguchi, Toyoyuki Sato, Tomoaki Sasaki, Hiroki Amano
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Patent number: 12049683Abstract: Methods for recovering metals from metal-containing materials are provided. The metal-containing material comprises either Co and Li (e.g., an electrode material from a spent lithium ion battery) or Fe and Al (e.g., bauxite). The metal-containing material is exposed to a leaching solution comprising ammonium hydrogen oxalate, oxalic acid, or both, to provide a solid composed of either cobalt oxalate or iron oxalate, and a solution of either lithium oxalate or aluminum oxalate. The solid is processed to provide either cobalt oxide or iron oxide; the solution is processed to provide either a lithium precipitate or an aluminum precipitate, and a filtrate comprising an oxalate; and the filtrate comprising the oxalate is processed to recover ammonium hydrogen oxalate, oxalic acid, or both. The method further comprises repeating the digestion step with the recovered ammonium hydrogen oxalate, the recovered oxalic acid, or both.Type: GrantFiled: October 22, 2019Date of Patent: July 30, 2024Assignee: University of KansasInventors: Mark Brandon Shiflett, David Richard Corbin, Ankit Verma