Abstract: The present invention relates to a preparation method of fluorinated graphene. The method for preparing fluorinated graphene, including the following steps: S1), under the protection of inert gas, the graphene undergoes a fluorination reaction with a first fluorinating agent, the reaction temperature is 150-550° C., the reaction time is 2-20 h, and a fluorinated graphene crude product is obtained. The graphene is graphene powder, or a graphene film; the first fluorinating agent includes fluorine gas; S2), under the protection of inert gas, the fluorinated graphene crude product undergoes a fluorination reaction with a second fluorinating agent, the reaction temperature is 150-400° C., the reaction time is 2-10 h, and a fluorinated graphene is obtained. The second fluorinating agent is gas-phase fluoride. By using the method, fluorinated graphene having a high fluorine content can be prepared, the fluorine content is close to the theoretical level, and the defect density is low.

Abstract: A system and method for synthesizing a nanoparticle material includes dissolving a metal nitrate in deionized water, adding a hydrogel precursor in the deionized water containing the dissolved metal nitrate to create an aqueous solution, heating the aqueous solution, cooling the aqueous solution to create a solid gel, and calcinating the solid gel to create a metal oxide nanoparticle material. The metal oxide nanoparticle material may include a zinc oxide-based nanoparticle material. The hydrogel precursor may include an agarose gel. The solid gel may be calcinated at approximately 600° C. The solid gel may be calcinated for approximately five hours in the presence of air. The aqueous solution may be heated to a boil. The aqueous solution may be heated at a temperature of ?100° C.

Abstract: A method and a device for the production of graphene or graphene-like material are provided. The method can comprise the following steps: providing particles of a crystalline graphitic material; dispersing the particles in a solvent or surfactant mixture; submitting the mixture to a cavitation force such that cavitation bubbles are present; and submitting the mixture to high shear agitation. The cavitation and high shear agitation steps can be simultaneous, in particular in the same enclosed vessel. The device for the production of graphene or graphene-like material can comprise a reactor having an enclosed vessel for receiving a solvent or surfactant mixture with dispersed particles of a crystalline graphitic material. The reactor can be arranged for: submitting the mixture in the enclosed vessel to a cavitation force such that cavitation bubbles are present and, simultaneously in the same enclosed vessel, submitting the mixture to high shear agitation.

Abstract: A method for recovering ammoniacal nitrogen, in the form of ammonium carbonate and/or ammonium bicarbonate, from an ammoniacal nitrogen-containing vapor that comprises introducing said vapor into at least one pressurizable ammonia scrubbing vessel containing water, simultaneously introducing a carbon dioxide-containing vapor into at least one pressurizable carbon dioxide scrubbing vessel containing water, and simultaneously pumping the solutions created in said scrubbers via hydrologic connections between said scrubbers to mix the solution to create an ammonium carbonate and/or ammonium bicarbonate containing mixture, all while maintaining independent and unmixed vapor streams throughout the entire process. The method further involves recovering ammonium carbonate and/or ammonium bicarbonate from the mixture for further use.

Abstract: Suggested is a carbon black composition showing a narrow Aggregate Size Distribution (ASD) characterized by a ?D50/Dmode value of about 0.58 to about 0.65 and a Relative Span (D90?D10)/D50 of about 0.5 to about 0.8, which is obtainable by means of a modified furnace reactor. The composition shows superior additive performance and allows producing e.g. bus or truck tires with improved wear resistance and reinforcement.

Abstract: Provided is a method of producing graphene from a microwave-expandable un-exfoliated graphite or graphitic carbon, comprising: (a) feeding a powder of the microwave-expandable material onto a non-metallic solid substrate, wherein the powder is in a ribbon shape having a first ribbon width and a first ribbon thickness; (b) moving the ribbon-shape powder into a microwave applicator chamber containing a microwave power zone having a microwave application width (no less than the first ribbon width) and a microwave penetration depth (no less than the first ribbon thickness) so that the entire ribbon-shape powder receives and absorbs microwave power with a sufficient power level for a sufficient length of time to exfoliate and separate the powder for producing graphene sheets; and (c) moving the graphene sheets out of the microwave chamber, cooling the graphene sheets, and collecting the graphene sheets in a collector container or for a subsequent use.

Abstract: According to the present invention, a carbon nanotube structure can be manufactured by merely a simple process in which carbon nanotubes are pulverized and mixed in a dispersion solvent without a dispersant, followed by freezing, and then the dispersion solvent is removed. Such a method does not require a dispersant and a binder so that the manufactured carbon nanotube structure can be composed of only carbon nanotubes, and does not depend on the other additives to form the carbon nanotube structure so that there is little possibility of damage and contamination of the structure during the collection procedure of the structure after the formation of the structure.

Abstract: The invention provides a method for making multiporous carbon material from a bio-oil produced by a biomass thermochemical process. The bio-oil is blended with a resin and a Zinc Oxide (ZnO) template as a major component of a precursor. The pore sizes of the carbon material made by the invention comprise mesopores and micropores to form the multiporous carbon material. The main production steps include: (1) mixing the precursor with a crusher, (2) packing the precursor, (3) heating for carbonization: holding 350° C. for 1 hour then holding 900° C. for 2 hours, and (4) washing the ZnO with hydrochloric acid by adjusting the pH value to less than 1.

Abstract: Methods, apparatuses, and systems to collect fine particle coal are provided herein. For example, these methods, apparatuses, and systems may be incorporated into a coal processing plant to collect a portion of the fine particle coal that is normally lost in the system. A fine particle coal also is provided. The fine particle coal may have a particle size of 1000 ?m or smaller and a water content of from about 5% to about 20%, by weight.

Abstract: Thermochemical storage materials having the general formula AxA?1-xByB?1-yO3-?, where A=La, Sr, K, Ca, Ba, Y and B=Mn, Fe, Co, Ti, Ni, Cu, Zr, Al, Y, Cr, V, Nb, Mo, are disclosed. These materials have improved thermal storage energy density and reaction kinetics compared to previous materials. Concentrating solar power thermochemical systems and methods capable of storing heat energy by using these thermochemical storage materials are also disclosed.

Abstract: Provided is a mounting member that is excellent in low dusting property and hardly contaminates an object to be mounted while being excellent in gripping force and heat resistance. In one embodiment of the present invention, the mounting member includes an aggregate of carbon nanotubes for forming amounting surface, wherein a standard deviation of diameters of the carbon nanotubes is 3 nm or less. In one embodiment of the present invention, the mounting member includes an aggregate of carbon nanotubes for forming a mounting surface, wherein the aggregate of the carbon nanotubes includes carbon nanotubes each having a multi-walled structure, and wherein a standard deviation of wall numbers of the carbon nanotubes is 3 or less.

Abstract: The present invention is a process, a method, and system for recovery and concentration of dissolved ammonium bicarbonate from a wastewater containing ammonia (NH3) using gas separation, condensation, filtration, and crystallization, each at controlled operating temperatures. The present invention includes 1) removal of ammonia from waste (sludges, semi-solids, and solids and liquids) without the use of chemicals at a temperature of at least 80 degrees Celsius, 2) mixing of the gaseous ammonia with carbon dioxide and water vapor and concentrating dissolved ammonium carbonate and ammonium bicarbonate using reverse osmosis at a temperature of between about 35 and 50 degrees Celsius, and 3) crystallizing concentrated dissolved ammonium carbonate and ammonium bicarbonate at a temperature of less than about 35 degrees Celsius to form solid ammonium bicarbonate and ammonium carbonate.

Abstract: Graphene production methods are described based on subjecting non-covalent graphite intercalated compounds, such as graphite bisulfate, to expansion conditions such as shocks of heat and/or microwaves followed by turbulence-assisted exfoliation to produce few-layer, high quality graphene flakes. Depending on the approach selected for the exfoliation step, free-flowing graphene powder, graphene slurry, or an aqueous graphene mixture can be obtained. Surfactants can aid in dispersion, and graphene inks can be formed. The parameters of the process are simple, efficient and low-cost enabling therefore the scale-up of production. Applications include electrodes and energy storage devices.

Abstract: The invention relates to the field of carbon structure production and, in particular, to a method for synthesis of graphene oxide which is widely used in electronics, medicine, pharmacology and construction industries. Provided is a method for synthesis of graphene oxide that includes oxidizing ground graphite with sulfuric acid and at least one oxidizer in a medium of supercritical fluid, wherein the method includes providing a mixture of sulfuric acid and dry ice in an amount sufficient for the mixture to solidify, and a mixture of at least one oxidizer and dry ice, wherein at least one of said mixtures contains ground graphite; introducing the provided mixtures into a high pressure autoclave; and further mixing the reagents. Thus, the claimed invention is a method for synthesis of graphene oxide that allows achieving the technical result consisting in safe production of high quality graphene oxide, wherein the time cost is relatively low and the consumption of sulfuric acid is significantly reduced.

Abstract: A hollow porous carbon nitride nanospheres composite loaded with AgBr nanoparticles, preparation method thereof, and its application in dye degradation are disclosed. Using silica nanosphere with core-shell structure as a template and hydrogen cyanamide as precursor, melting to enter the pores of mesoporous silica, after calcination, the silica template is etched with ammonium bifluoride to obtain hollow porous carbon nitride nanospheres; dispersing hollow porous carbon nitride nanospheres in deionized water, adding silver nitrate and sodium bromide in sequence, and obtaining silver bromide nanoparticles by in-situ ion exchange method, stirring, washing and centrifuging to obtain the hollow porous carbon nitride nanospheres composite. The hollow porous carbon nitride prepared by the template method has good photocatalytic effect on dye degradation after composite with silver bromide; and it has the advantages of easy production of raw materials, good stability, reusability, etc.

Abstract: This invention relates to a method for the preparation of lithium carbonate from lithium chloride containing brines. The method can include a silica removal step, capturing lithium chloride, recovering lithium chloride, supplying lithium chloride to an electrochemical cell and producing lithium hydroxide, contacting the lithium hydroxide with carbon dioxide to produce lithium carbonate.

Abstract: Provided are a method for producing a graphite oxide derivative capable of simply producing a high-quality graphite oxide derivative, and a high-quality graphite oxide derivative. The present invention relates to a method for producing a graphite oxide derivative, the method including the steps of oxidizing graphite; and preparing a graphite oxide derivative by reacting graphite oxide in a reaction liquid containing graphite oxide obtained in the oxidation step or graphite oxide in a graphite oxide-containing composition that is separated from the reaction liquid with a compound reactive with an oxygen-containing functional group of the graphite oxide, the method not including the step of purifying and drying the graphite oxide-containing reaction liquid between the oxidation step and the graphite oxide derivative preparation step.

Abstract: A process for producing crystalline sodium bicarbonate, comprising: providing an aqueous sodium-bicarbonate containing liquor originating from a reactive crystallization step in which first sodium bicarbonate crystals are produced and recovered; feeding at least a portion of said aqueous sodium-bicarbonate containing liquor to a cooling crystallization unit to form second sodium bicarbonate crystals and produce a crystals slurry comprising the second sodium bicarbonate crystals; and withdrawing a portion of the crystals slurry from the cooling crystallization unit for the withdrawn second sodium bicarbonate crystals to be further processed. A portion of the second sodium bicarbonate crystals withdrawn from the cooling crystallization unit may be fed to a sodium bicarbonate reactive crystallization unit, to a caustic unit, or may be separated and dried.

Abstract: A method for making a carbon nanotube composite structure includes the following steps: dispersing a plurality of carbon nanotubes in water, to form a carbon nanotube dispersion; adding an aniline solution into the carbon nanotube dispersion, to form a mixed solution; adding an initiator into the mixed solution, to form a carbon nanotube composite structure preform; freeze-drying the carbon nanotube composite structure preform in a vacuum environment; and carbonizing the carbon nanotube composite structure preform in a protective gas after freeze-drying. The present application also relates to the carbon nanotube composite structure.

Abstract: The disclosure provides a system and method for production of activated carbon from a coal-originating particulate feed material. Feed material and activating gas are introduced into a reaction chamber, the activating gas being introduced at a velocity above the average terminal velocity of particles within the feed material. Feed material is then entrained in the activating gas such that a recirculating flow path for the feed material is established within the reaction chamber. Activated material may then be recovered from the chamber.