Abstract: A method for curing a resin includes the steps of placing the resin into a reaction vessel, drawing a vacuum in the reaction vessel, positioning the reaction vessel in a gaseous coupling fluid, and applying ultrasonic energy to the coupling fluid.

Abstract: Polyacetylinic oligomers suitable for high-temperature polymer-matrix composites are provided. The polyacetylinic oligomers have the formula: D-A-D wherein D is an endcap including at least one crosslinking functionality; and A is backbone selected from the group consisting of imidesulfone; ether; ethersulfone; amide; imide; ester; estersulfone; etherimide; amideimide; oxazole; oxazole sulfone; thiazole; thiazole sulfone; imidazole; and imidazole sulfone. At least one ethynyl functional group, however, is incorporated into the backbone such that crosslinking is not only realized at the endcaps but also at the ethynyl groups within the backbone of the oligomer itself.

Abstract: An oligomer having di-phenylethynyl endcaps is disclosed. The capped oligomer has the formula: D-A-D wherein D is a di-phenylethynyl endcap; and A is an oligomer selected from the group consisting of imidesulfone; ether; ethersulfone; amide; imide; ester; estersulfone; etherimide; amideimide; oxazole; oxazole sulfone; thiazole; thiazole sulfone; imidazole; and imidazole sulfone.

Abstract: A method and composition for corrosion protection of a structure is provided. In one disclosed embodiment, a polysiloxane ureide which inhibits corrosion formation on a surface of a physical object is provided. The polysiloxane ureide has a backbone including, (i) at least one diamine-terminated polysiloxane as disclosed; (ii) at least one aromatic diamine; and, (iii) at least one diisocyanate. In another disclosed embodiment, there is provided a polyureide which inhibits corrosion formation on a surface of a physical object. The polyureide comprises: (i) at least one aliphatic diamine; (ii) at least one aromatic diamine; and, (iii) at least one diisocyanate.

Abstract: A filter membrane includes a substrate, a polymer layer provided on the substrate and a plurality of filter openings each having a width of from about 2 nanometers to about 5 nanometers provided in the polymer layer. A method of controlling pore size of a filter membrane and a method of decontaminating a filter membrane are also disclosed.

Abstract: The present invention is directed to a method for applying to a substrate, in the form of a seal, a polysiloxane-containing coating, preferably a polysiloxane(amide-ureide) coating capable of inhibiting corrosion as well as the accumulation of ice. One embodiment of the present invention is directed to a polysiloxane(amide-ureide) that forms a durable, long lasting, anti-corrosive and anti-ice coating when applied to a substrate as a seal.

Abstract: A method of improving the material properties of a composite by electrodepositing various polymers, organic compounds or inorganic compounds onto each individual carbon (graphite) fiber strand, whether individual fiber or as a fabric to form an homogeneous chemically-bonded composite as opposed to the formation of a heterogeneous, non-chemically bonded composite. Thus, electrodeposition forms a unique discrete interface at the molecular layer (nanolayer) between the reinforcement (fiber) and the matrix (resin) over as opposed to any previous resin infusion process.

Abstract: A test method for determining, quantifying, and qualifying the stress-relaxation characteristics of a sealant material compound comprising applying a sealant material layer between a first plate and a second plate, disposing a fastener assembly through the plates, and providing tension preload upon the fastener assembly so as to compress the plates together. The elongation of the fastener assembly is measured and the test assembly is heated and cooled under controlled parameters and the elongation of the fastener assembly is again measured. The stress-relaxation of the sealant material compound is correlated to the corresponding change in fastener assembly elongation for the purposes of measuring, quantifying, and qualifying the sealant material compound.

Abstract: A test method for determining, quantifying, and qualifying the flow characteristics of a sealant material compound comprising the steps of applying a uniform layer of known initial mass of sealant material between two test surfaces and compressing the sealant material between the surfaces at a specific pressure for a specific length of time, and at a specific temperature, causing an amount of sealant to be extruded from between the test surfaces. The amount of the extruded sealant is measured and compared to the total mass of initial sealant material to determine the ratio of the extruded to initial sealant material. Based upon the mass ratio of extruded sealant material versus the initial sealant material, the flow characteristics of the sealant material may be expressed for any given combination of temperature, pressure, and duration and compared to other sealant materials.

Abstract: The present invention is directed to a method for applying to a substrate having a faying surface, a polysiloxane-containing coating, preferably a polysiloxane(amide-ureide) coating capable of inhibiting corrosion as well as the accumulation of ice. One embodiment of the present invention is directed to a polysiloxane(amide-ureide) that forms a durable, long lasting, anti-corrosive and anti-ice coating when directed to a substrate faying surface.

Abstract: A surface coating which inhibits the formation of ice upon the surface of a substrate comprising a polysiloxane(amide-ureide) having the general formula: wherein R1 and R2 are independently selected from the group consisting of C1 to C10 alkyls, aryls, and polyaryls; R3 and R4 are independently selected from the group consisting of hydrogen, C1 to C6 alkyls, aryls, C3 to C6 cycloaliphatics, and C3 to C6 heterocycles; A1 and A2 are independently selected from the group consisting of hydrogen, C1 to C6 alkyls, aryls, polyaryls, C3 to C6 cycloaliphatics, and C3 to C6 heterocycles; x is a number from 1 to 1000; and Y is selected from a dicarboxyl residue and a non-linear diisocyanate residue. The polysiloxane(amide-ureide) is formed by reacting at least one diamine terminated polysiloxane, at least one halide substituted dicarboxylic acid, and at least one non-linear diisocyanate.

Abstract: The present invention is directed to a method for applying to a substrate, in the form of a seal, a polysiloxane-containing coating, preferably a polysiloxane(amide-ureide) coating capable of inhibiting corrosion as well as the accumulation of ice. One embodiment of the present invention is directed to a polysiloxane(amide-ureide) that forms a durable, long lasting, anti-corrosive and anti-ice coating when applied to a substrate as a seal.

Abstract: A surface coating which inhibits the formation of ice upon the surface of a substrate comprising a polysiloxane(amide-ureide) having the general formula: 1

Abstract: A surface coating which inhibits the formation of ice upon the surface of a substrate comprising a polysiloxane(amide-ureide) having the general formula: 1

Abstract: The present invention is directed to a method for applying to a substrate having a faying surface, a polysiloxane-containing coating, preferably a polysiloxane(amide-ureide) coating capable of inhibiting corrosion as well as the accumulation of ice. One embodiment of the present invention is directed to a polysiloxane(amide-ureide) that forms a durable, long lasting, anti-corrosive and anti-ice coating when directed to a substrate faying surface.

Abstract: An aluminum-alloy, aircraft structural component having a faying surface prepared by treating with one or more curable organic coatings, one or more of which is optionally in an encapsulated state, and delivering a uniform coating on demand by rupturing and curing the encapsulated coating.

Abstract: An aluminum-alloy, aircraft structural component having a faying surface prepared by treating with one or more curable organic coatings, one or more of which is optionally in an encapsulated state, and delivering a uniform coating on demand by rupturing and curing the encapsulated coating.

Abstract: An aluminum-alloy, aircraft structural component having a faying surface prepared by treating with one or more curable organic coatings, one or more of which is optionally in an encapsulated state, and delivering a uniform coating on demand by rupturing and curing the encapsulated coating.

Abstract: An aluminum-alloy, aircraft structural component having a faying surface prepared by treating with one or more curable organic coatings, one or more of which is optionally in an encapsulated state, and delivering a uniform coating on demand by rupturing and curing the encapsulated coating.

Abstract: An improved, pre-coated aluminum-alloy aircraft component prepared by providing an aluminum-alloy component precursor to a coating apparatus having a fluidized-bed or mist apparatus, suspending the components in the fluidized-bed apparatus vertically at a distance from the bottom of the apparatus and introducing a coating to the apparatus to coat the components while being suspended in the airstream flowing through the apparatus. The non-contact, fluidized-bed or mist coating method allows for the coating of increased batch sizes in shorter coating times with decreased variations in coating thickness and uniformity.