Abstract: A method of manufacturing a component for a gas turbine engine. The method may include the steps of: providing a forged preform of the component that is made from a stainless steel alloy; identifying two non-overlapping portions of the component that together form a whole of the component: a target portion and a remainder portion; and treating the component with a regionally selective tempering process in which a treated region receives a tempering process while an untreated region is excluded from receiving the tempering process. The target portion may be the treated region while the remainder portion is the untreated region. The tempering process of the regionally selective tempering process may be configured to appreciably increase a hardness of the target portion of the component relative to a hardness of the remainder portion of the component.

Abstract: Rail manufacturing method performs, on at least a head of the rail that is hot after hot-rolled at an austenite region temperature or higher or after heated to the austenite region temperature or higher, forced cooling: for 10 seconds from start of the forced cooling so that a cooling rate at a surface of the head becomes 1° C./s to 20° C./s; during a period after a lapse of 10 seconds from the start until heat generation during transformation begins at the surface so that the cooling rate becomes 1° C./s to 5° C./s; during transformation from beginning to end of the heat generation during transformation so that the cooling rate becomes lower than 1° C./s or a temperature-rising rate becomes 5° C./s or lower; and during a period after the end of the heat generation during transformation until temperature at the surface becomes 450° C. or lower so that the cooling rate becomes 1° C./s to 20° C./s.

Abstract: Methods for recovering gold from gold-bearing materials are provided. The methods rely upon on the self-assembly of KAuBr4 and ?-cyclodextrin (?-CD) in aqueous solution to form a co-precipitate, a 1:2 complex, KAuBr4•(?-CD)2 (“?•Br”), either alone or in an extended {[K(OH2)6][AuBr4]?(?-CD)2}n chain superstructure (FIG. 1). The co-precipitation of ?•Br is selective for gold, even in the presence of other metals, including other square-planar noble metals. The method enables one to isolate gold from gold-bearing materials from diverse sources, as further described.

Abstract: Disclosed is a method for producing and identifying a Weyl semimetal. Identification is enabled via a combination of the vacuum ultraviolet (low-photon energy) and soft X-ray (SX) angle resolved photoemission spectroscopy (ARPES). Production generally requires providing high purity raw materials, creating a mixture, heating the mixture in a container at a temperature sufficient for thermal decomposition of an impurity while preventing the possible reaction between the side walls of the container and the raw materials, depositing the resulting compound and a transfer agent onto the bottom surface of the ampule, differentially heating the ampule, and allowing a chemical vapor transport reaction to complete.

Abstract: In a method for controlling energy damping in a shape memory alloy, provided is a shape memory alloy having a composition including at least one of: Cu in at least about 10 wt. %, Fe in at least about 5 wt. %, Au in at least about 5 wt. %, Ag in at least about 5 wt. %, Al in at least about 5 wt. %, In in at least about 5 wt. %, Mn in at least about 5 wt. %, Zn in at least about 5 wt. % and Co in at least about 5 wt. %. The shape memory alloy is configured into a structure including a structural feature having a surface roughness and having a feature extent that is greater than about 1 micron and less than about 1 millimeter. Energy damping of the structural feature is modified by exposing the structural feature to process conditions that alter the surface roughness of the structural feature.

Abstract: The present invention relates to a heat treatment method for increasing the depth of hardening layer in a steel rail, and belongs to the field of steel rail production process. The technical problem to be solved in the present invention is to provide a heat treatment method for increasing the depth of hardening layer in a steel rail and a steel rail obtained with the method. The method comprises the following steps: cooling a finished rolling steel rail by natural cooling, till the temperature at the center of rail head surface is 660˜730° C.; cooling the steel rail by accelerated cooling at 1.5˜3.5° C./s cooling rate, till the temperature at the center of rail head surface is 500˜550° C.; increasing the cooling rate by 1.0˜2.0° C./s and further cooling down the steel rail, till the temperature at the center of rail head surface is 450° C. or lower; then, stopping the accelerated cooling, and cooling down the steel rail by air cooling to room temperature.

Abstract: Articles of bulk-solidifying amorphous alloys such as a golf club face insert with improved durability and fatigue resistance, and more specifically articles of bulk-solidifying amorphous alloys subjected to a surface treatment, such as shot-peening, which creates deformations in the exterior surface, and methods of improving the durability and fatigue resistance of bulk-solidifying amorphous alloys using a surface treatment, such as shot-peening.

Abstract: Composite structures and methods of their manufacture are provided. In one embodiment, the composite structure includes a substrate which includes a relatively soft material, and nanoparticles which include a relatively hard material and which are embedded (i) within at least a surface region of the substrate, or (ii) uniformly within and throughout the substrate, in an amount effective to improve the wear resistance of the substrate. Methods for forming these composite structures include a hot-rolling process, a roll-bonding process, or a combination thereof.

Abstract: An aluminum alloy and a method for improving the ability of a semi-finished or finished product to age artificially, includes an age-hardenable aluminum alloy on an Al—Mg—Si, Al—Zn, Al—Zn—Mg or Al—Si—Mg basis, wherein the aluminum alloy is transformed to a solid solution state, in particular by solution heat treatment (1), is quenched and subsequently forms precipitations by a process of natural aging (3), the method involving at least one measure for reducing a negative effect of natural aging (3) of the aluminum alloy on artificial aging (4) thereof.

Abstract: A method for machining a wall of a cylinder of an internal combustion engine, in which recesses in the wall are introduced by mechanical machining. The invention is characterized in that the wall is radiated with a medium under high pressure after the mechanical machining in order to introduce micro-recesses.

Abstract: A first stage turbine nozzle includes a first stage hub portion extending axially along a central axis, a first stage disk portion attached to the first stage hub portion and centered on the central axis, and a plurality of first stage vanes positioned radially around and attached to the first stage disk portion. Each vane extends a vane height H away from the first stage disk portion and each vane has a first end positioned at a diameter D away from the central axis. The first stage turbine nozzle also includes a plurality of first stage throats defined between radially adjacent first stage vanes. Each first stage throat has a throat width W between radially adjacent first stage vanes. The first stage turbine nozzle also includes a coating on a sidewall of each first stage vane.

Abstract: A workpiece made from a self passivating metal and having one or more surface regions defining a Beilby layer as a result of a previous metal shaping operation is activated for subsequent low temperature gas hardening by exposing the workpiece to the vapors produced by heating an oxygen-free nitrogen halide salt.

Abstract: Systems are provided that include one or more retractable deposition source assemblies that eliminate the need for a bellows, but do not require breaking the ultra-high vacuum of a growth module for source replacement or recharging with deposition material. Systems of the present invention may include source heads that allow for a differential pumping option that provides marked improvement in base pressure around the source head (and material) that provides longer lifetimes for sources in corrosive, reactive or oxidizing environments. In addition, systems of the invention do not require an entire growth module to be vented to refill or repair an effusion source. Instead, for maintenance events that are tied to a specific source, a retractable source assembly of the present invention allows the sources to be withdrawn from the system, isolated from the growth environment, and removed without venting the entire chamber of the growth module.

Abstract: A method for depositing tungsten includes arranging a substrate including a titanium nitride layer in a substrate processing chamber and performing multi-stage atomic layer deposition of tungsten on the substrate using a precursor gas includes tungsten chloride (WClx) gas, wherein x is an integer. The performing includes depositing the tungsten during a first ALD stage using a first dose intensity of the precursor gas, and depositing the tungsten during a second ALD stage using a second dose intensity of the precursor gas. The first dose intensity is based on a first dose concentration and a first dose period. The second dose intensity is based on a second dose concentration and a second dose period. The second dose intensity is 1.5 to 10 times the first dose intensity.

Abstract: A deposition apparatus for performing a deposition process by using a mask with respect to a substrate, the deposition apparatus includes a chamber, a support unit in the chamber, the support unit including first holes and being configured to support the substrate, a supply unit configured to supply at least one deposition raw material toward the substrate, and movable alignment units through the first holes of the support unit, the alignment units being configured to support the mask and to align the mask with respect to the substrate.

Abstract: A reactive material stack with tunable ignition temperatures is provided by inserting a barrier layer between layers of reactive materials. The barrier layer prevents the interdiffusion of the reactive materials, thus a reaction between reactive materials only occurs at an elevated ignition temperature when a certain energy threshold is reached.

Abstract: A tool has a main part of hard metal, cermet, ceramic, steel, high-speed steel, and a single or multilayer wear protection coating applied onto the main part by CVD and which has a thickness from 3 ?m to 25 ?m. The wear protection coating has at least one Ti1?xAlxCyNz layer with stoichiometric coefficients 0.70?x<1.0?y<0.25 and 0.75?z<1.15 and a thickness from 1.5 ?m to 17 ?m. The T1?xAlxCyNz layer has a lamellar structure with lamellae with thickness of no more than 150 nm, preferably no more than 100 nm, particularly preferably no more than 50 nm. Lamellae are made of periodically alternating regions of the Ti1?xAlxCyNz layer with alternatingly different stoichiometric proportions of Ti and Al, having the same crystal structure (crystallographic phase), and the Ti1?xAlxCyNz layer has at least 90% vol. % of face centered cubic (fcc) crystal structure.

Abstract: A process for conducting vapor phase deposition is disclosed. The process separates a series of reactions through a sequence of reaction reservoirs. The reactor includes a reactive precursor reservoir beneath a powder reservoir separated by valve means. A reactive precursor is charged into the reactive precursor reservoir and a powder is charged into the powder reservoir. The pressures are adjusted so that the pressure in the reactive precursor reservoir is higher than that of the powder reservoir. The valve means is opened, and the vapor phase reactant fluidized the powder and coats its surface. The powder falls into the reactive precursor reservoir. The apparatus permits vapor phase deposition processes to be performed semi-continuously.

Abstract: A method of fabricating a PCD cutter element including a diamond table including a plurality of coated diamond particles fabricated using an atomic layer deposition (ALD) process.

Abstract: The invention relates to an apparatus and to a method for providing an ALD coating to a surface of a substrate. The apparatus includes at least one ALD coating unit for coating the surface of the substrate, a first reel for unwinding the substrate to be coated, a second reel for rewinding the coated substrate, one or more primary support structures provided on the same side of the substrate as the surface to be coated or the coated surface for forming a substrate transport path from the first reel through the at least one primary support structure to the second reel, and an interleave web in connection with each of the one or more primary support structures.

Abstract: Substrate treating apparatus including a cover that covers a substrate on a plate. The cover undersurface is substantially horizontal and adjacent to a surface of the substrate. Through a gas flow path, a treatment gas is supplied to the substrate. The gas flow path includes a swirl chamber, a diameter contraction chamber, and a diameter expansion chamber. In the swirl chamber, the treatment gas flows around the central axis. The diameter contraction chamber is disposed below and in communication with the swirl chamber, and has an inner diameter that decreases from its upper end toward its lower end. The diameter expansion chamber is disposed below and in communication with the diameter contraction chamber, and has an inner diameter that increases from its upper end toward its lower end. The lower end of the diameter expansion chamber includes an opening on the undersurface of the cover.

Abstract: Methods and apparatus relating to aluminum nitride baffles are provided herein. In some embodiments, a baffle for use in semiconductor process chambers may include a body comprising aluminum nitride and a metal oxide binding agent, wherein a ratio of aluminum nitride to metal oxide on a surface of the body is greater than or equal to the ratio within the body. In some embodiments, the body may have a center stem and an outer annulus coupled to and extending radially outwards from a lower portion of the center stem. In some embodiments, a method of fabricating a baffle may include sintering aluminum, nitrogen, and a metal oxide binding agent to form a body of the baffle, the body having excess metal oxide binding agent disposed on a surface thereof; and removing a bulk of the excess metal oxide binding agent from a surface of the body.

Abstract: An apparatus for depositing film stacks in-situ (i.e., without a vacuum break or air exposure) are described. In one example, a plasma-enhanced chemical vapor deposition apparatus configured to deposit a plurality of film layers on a substrate without exposing the substrate to a vacuum break between film deposition phases, is provided. The apparatus includes a process chamber, a plasma source and a controller configured to control the plasma source to generate reactant radicals using a particular reactant gas mixture during the particular deposition phase, and sustain the plasma during a transition from the particular reactant gas mixture supplied during the particular deposition phase to a different reactant gas mixture supplied during a different deposition phase.

Abstract: A deposition system can conduct ALD or CVD deposition and can switch between the deposition modes. The system is capable of depositing multi-metal films and multi-layer films of alternating ALD and CVD films. Reactant supplies can be bypassed with carrier gas flow to maintain pressure in a reactor and in reactor supply lines and purge reactants.

Abstract: The present invention concerns anti-corrosive coating compositions, in particular coating compositions for protecting iron and steel structures. In particular, the present invention relates to silicate-based coating compositions comprising particulate zinc, conductive pigments, and glass hollow microspheres. The invention furthermore concerns a kit of parts containing the composition, a method for its application, as well as metal structures coated with the composition.

Abstract: A sacrificial galvanic anode, an anodic assembly including the sacrificial anode, and a method of cathodically protecting steel reinforcement in concrete structures from corrosion is provided. The sacrificial galvanic anode comprises at least one sacrificial metal helical coil. The galvanic anode is easily fabricated and occupies a minimum volume within a steel reinforced concrete structure while providing maximum surface area for sacrificial corrosion.

Abstract: A hydrogen generation system includes a pulsed drive signal generator to generate a pulsed drive signal, a hydrogen generation chamber to receive the pulsed drive signal and generate hydrogen from a feedstock material contained therein based on the pulsed drive signal and a controllable reactive circuit coupled between the pulsed drive signal generator and the hydrogen generation chamber. A hydrogen detection device is coupled to the hydrogen generation chamber to detect the generated hydrogen. A controller controls the controllable reactive circuit based on detection of the generated hydrogen.

Abstract: An electrolyzer operates within an energy system, for example to provide grid services, energy storage or fuel, or to produce hydrogen from electricity produced from renewable resources. The electrolyzer may be configured to operate at frequently or quickly varying rates of electricity consumption or to operate at a specified power consumption. In one process of operating an electrolyzer, a series of dispatches is received indicating a specified power consumption for a period of time. The dispatches may occur at least once every 30 minutes. The electrolyzer is operated according to the dispatches. Hydrogen produced by the electrolyzer is discharged to a natural gas system.

Abstract: An electrode of an embodiment includes a base material, and a catalyst layer provided on the base material and having a porous structure. When a sum of heights of all peaks belonging to Ir oxide is I0, the height of a peak of IrO2 (110) is I1, and the height of a peak of IrO2 (211) is I2, a ratio of (I1+I2)/I0, which is a ratio of spectra obtained by X-ray diffraction measurements using K? rays of Cu in the catalyst layer, is 50% or more and 100% or less in a range of a diffraction angle of 20 degrees or more and 70 degrees or less.

Abstract: A coated metal component includes an aluminum alloy substrate and a protective aluminum coating on a substrate. An interfacial boundary layer between the coating and substrate enhances coating adhesion. The boundary layer includes isolated regions of copper or tin produced by a double zincating process. The protective aluminum coating exhibits improved adhesion and is formed by electrodeposition in an ionic liquid.

Abstract: A composite component and a plated polymer component are disclosed. The composite component may comprise a body portion formed from an organic matrix composite, a first metal coating applied to a surface of the body portion, and an outer metal layer on the first metal coating that is erosion-resistant. The plated polymer component may comprise a polymer substrate, a metal plating layer applied to a surface of the polymer substrate, and at least one selectively thickened region in the metal plating layer. The at least one selectively thickened region may assist in protecting the plated polymer component against wear and/or erosion.

Abstract: A method of forming a thermal barrier coating onto a surface of a ferrous alloy or nickel alloy component part involves depositing a layer of hollow microspheres to a surface of the component part or to a previously deposited layer of hollow microspheres through heating and cooling of a metallic precursor setting layer composed of copper, a copper alloy, or a nickel alloy. Once deposited in place, the layer(s) of hollow microspheres are heated to sinter the hollow microspheres to each other and to the surface of the ferrous alloy or nickel alloy component part to form an insulating layer.

Abstract: Certain embodiments herein relate to a method of electroplating copper into damascene features using a low copper concentration electrolyte having less than about 10 g/L copper ions and about 2-15 g/L acid. Using the low copper electrolyte produces a relatively high overpotential on the plating substrate surface, allowing for a slow plating process with few fill defects. The low copper electrolyte may have a relatively high cloud point.

Abstract: Methods of preparing metal and metal alloys with partially microcrystalline anodic coatings are disclosed. Associated article therefrom are correspondingly disclosed. The partially microcrystalline anodic coatings exhibit fade and pattern removal resistance when subjected to sterilization processes. Partially microcrystalline anodic coating can be prepared by impregnation of micropores of a metal or metal substrate with metal precursor species, conversion of the metal precursor species into metal hydroxides, and one or more additional treatments to promote phase transformation of the metal hydroxide product into metal oxides solids and bonding with metastable metal oxide substance in the pore structure of the metal or metal alloy substrate.

Abstract: Various embodiments herein relate to methods and apparatus for electroplating metal onto substrates. In various cases, a reference electrode may be modified to promote improved electroplating results. The modifications may relate to one or more of the reference electrode's shape, position, relative conductivity compared to the electrolyte, or other design feature. In some particular examples the reference electrode may be dynamically changeable, for example having a changeable shape and/or position. In a particular example the reference electrode may be made of multiple segments. The techniques described herein may be combined as desired for individual applications.

Abstract: Various embodiments herein relate to methods and apparatus for electroplating metal onto substrates. In various cases, a reference electrode may be modified to promote improved electroplating results. The modifications may relate to one or more of the reference electrode's shape, position, relative conductivity compared to the electrolyte, or other design feature. In some particular examples the reference electrode may be dynamically changeable, for example having a changeable shape and/or position. In a particular example the reference electrode may be made of multiple segments. The techniques described herein may be combined as desired for individual applications.

Abstract: A substrate holder for holding a substrate, such as a wafer, is disclosed. The substrate holder includes a seal ring which can be brought into contact with a peripheral portion of the substrate, a support ring supporting the seal ring, and a fixing ring pressing the seal ring against the support ring. The fixing ring includes an annular portion having an inner circumferential surface and an outer circumferential surface, each of which is constituted by a tapered surface. The fixing ring further includes a seal-ring pressing portion connected to the annular portion, and a regulation ring projecting radially inwardly from the seal-ring pressing portion. The regulation ring has an inside diameter which is smaller than an inside diameter of the seal ring.

Abstract: The invention relates to a one-piece metal component including an electroformed metal body, the external surface of the body including, only over or to a predetermined depth, less trapped hydrogen than the rest of the electroformed metal body causing a hardening relative to the rest of the body in order to improve the wear resistance of the one-piece component while preserving a relative magnetic permeability of less than 10 and the ability to be driven or pressed fit.

Abstract: A system for recycling machined metal produced by an electrochemical material removal process. The system includes a machining unit and an electrowinning unit. The machining unit includes an anode to receive a workpiece, a cathode tool, and a first pulse generator to provide a voltage or current waveform between the anode and the cathode tool. The electrowinning unit includes an electrowinning cathode, an electrowinning anode, and a second pulse generator to provide a voltage or current waveform between the electrowinning anode and the electrowinning cathode. The machining unit is in fluid communication with the electrowinning unit.

Abstract: The present invention relates to additive manufacturing methods, in which crystalline materials can be formed by using a liquid precursor. In particular embodiments, the crystalline material is a perovskite. The methods include the use of a thermal voxel, which can be translated to form any arbitrary pattern of initial crystalline seed structure(s). Then, the seed structure can be incubated to promote crystal growth and/or crystal dissolution, thereby providing a patterned crystalline material.

Abstract: The present invention relates a method for controlling a growth interface shape while growing a monocrystal ingot by a Czochralski method, the method including a step of starting a growth of the monocrystal ingot after setting a control condition of a monocrystal growing process so that an interface of the ingot becomes a target shape; a step of deriving a measurement value by measuring a weight of the ingot grown for a predetermined time by means of a load cell disposed on an upper portion the monocrystal ingot; a step of deriving a theoretical value of the weight of the monocrystal ingot through a diameter of the monocrystal ingot measured by a diameter measuring camera disposed outside of a process chamber for a predetermined time and a height of the monocrystal ingot grown for the predetermined time; a step of predicting a growth interface shape of a growing monocrystal ingot by deriving a difference between the measurement value and the theoretical value; and changing process conditions during growth of

Abstract: A method of processing a super-hard material having a Vickers hardness of no less than 2000 kg/mm2, the method comprising: (a) forming a surface of the super-hard material to have a first surface profile within a first root mean square deviation being no more than 5 ?m; (b) analyzing said surface of the super-hard material to detect a plurality of protruding regions on said surface; and (c) selectively processing over only the protruding regions on the surface of the super-hard material to form a second surface profile within a second root mean square deviation from the smooth target surface profile, said second root mean square deviation being no more than 100 nm.

Abstract: Acrylic compositions comprising a hindered amine light stabilizer are described herein. The acrylic composition may be in the form of a fiber, thread, yarn, and/or fabric. Also described herein are methods of making and using the acrylic compositions and articles comprising an acrylic composition as described herein.

Abstract: A textile stuffer box comprises a housing assembly having a yarn entrance and a yarn exit, and cooperating interior chamber-forming surfaces. The chamber-forming surfaces defines a multi-stage internal crimping chamber for receiving and accumulating a moving length of ply-twisted yarn between the entrance and exit of the housing assembly. The crimping chamber comprising an upstream fixed-volume stage and a downstream adjustable-volume stage. A weight-balanced gate selectively adjusts a volume of the downstream adjustable-volume stage of the crimping chamber, thereby controlling axial compression of yarn accumulating inside the upstream fixed-volume stage of the crimping chamber.

Abstract: The present invention discloses high modulus single twisted nylon 6.6 yarns having a tensile stress value between 2.0 and 2.8 cN/dtex at 4% elongation. The single twisted yarns are prepared from a raw polyamide 6.6 yarn. The single twisted yarns are used as reinforcement in shaped rubber composites. The minimum heat shrinkage of the cords is 4% and maximum heat shrinkage is 7%.

Abstract: A preform manufacturing apparatus comprising a supply of fiber strip, a moveable positive fiber strip delivery mechanism coupled between a desired lay down location and the supply of fiber strip to positively deliver and orient the supply of fiber strip to the desired lay down location, and an electronic unwinder coupled to the supply of fiber strip is described herein. The electronic unwinder is configured to interact with the moveable positive fiber strip delivery mechanism.

Abstract: A method of producing a sandwich panel core of mineral wool fibers from a cured mineral fiber product includes the steps of providing a cured mineral fiber product with a dual density having a top layer with mineral fibers with a first density and a base layer having mineral fibers with a second density, the second density is at least two times lower than said first density. The top layer and the base layer have different fiber orientations. Further steps including cutting the mineral fiber product into a plurality of lamellae, rotating the lamellae 90 degrees, and re-joining the lamellae so that the top layers with the first density are vertically oriented.

Abstract: A needle inserter comprising an elongated handle having a first end portion and a second end portion, a releasable support at the first end portion and an elongated element extending perpendicularly from the first end portion and includes a perpendicular extending distal end. The needle inserter operates such that an embroidery needle is supported on the needle inserter by the releasable support and by the distal end. The needle inserter further operates to allow a user to hold the needle inserter to move the embroidery needle such that the embroidery needle engages with the retaining member such that the embroidery needle is retained in its proper orientation and alignment and to allow the user to move the needle inserter such that the embroidery needle disengages from the needle inserter.

Abstract: A washing machine may include a cabinet, a tub, a drum, a driving module for rotating the drum, a water supply module for supplying the wash water to the tub, a drainage module for discharging the wash water from the tub, a drying module at the cabinet for supplying heated air into the tub from an upper side of the tub to dry the laundry, and an exhaust duct coupled to the tub for discharging a fluid in the tub out of the cabinet.

Abstract: A control method of a washing machine may include supplying water to a predetermined unbalance induction water level into a wash tub configured to accommodate fabric, the wash tub being rotated about a vertical axis, rotating a pulsator inside the wash tub, sensing an amount of fabric, rotating the wash tub at a constant acceleration, determining unbalance based on a current value applied to a motor in a state in which a rotational speed of the wash tub falls in a given range and the sensed amount of fabric while the wash tub is rotated at the constant acceleration, and supplying water to a first water supply level into the wash tub when the unbalance is greater than a reference value, and supplying water to a second water supply level, which is higher than the first water supply level, when the unbalance is smaller than the reference value.