Patents Issued in May 12, 2020
  • Patent number: 10647875
    Abstract: Provided is a thermally curable coating composition for alloy substrates, comprising: curable components, comprising an epoxy resin and a multifunctional (meth)acrylate; latent curing agents, which crosslink with the curable components upon heating, and comprise an isocyanate having at least two NCO groups and an amino resin; a curing promoter, comprising an aromatic phosphate comprising at least one hydroxy group connected with the phosphorous atom; and an organic solvent. Also provided are a method for providing a coating layer onto an alloy substrate and a coating layer thus obtained.
    Type: Grant
    Filed: October 21, 2015
    Date of Patent: May 12, 2020
    Assignee: Hewlett-Packard Development Company, L.P.
    Inventors: Yong-Jun Li, Steven Zhu, Army Zhang, Herbert Liu
  • Patent number: 10647876
    Abstract: An RMA crosslinkable composition having at least one crosslinkable component including reactive components A and B each including at least 2 reactive groups, the at least 2 reactive groups of component A being acidic protons (C—H) in activated methylene or methine groups and the at least 2 reactive groups of component B are activated unsaturated groups (C?C) and a base catalyst (C) which reactive components A and B crosslink by Real Michael Addition (RMA) reaction under action of the base catalyst, characterised in that the at least one crosslinkable component including reactive components A and B in the composition have a total hydroxy number of less than 60, preferably less than 40 and more preferably less than 20 mg KOH/g solids. Further, specific resins A and B having a low hydroxy number for use in RMA cross-linkable compositions and a process for the manufacture thereof.
    Type: Grant
    Filed: February 6, 2018
    Date of Patent: May 12, 2020
    Assignee: Allnex Netherlands B.V.
    Inventors: Richard Hendrikus Gerrit Brinkhuis, Antonius Johannes Wilhelmus Buser, Petrus Johannes Maria David Elfrink, Ferry Ludovicus Thys, Nicole Mangnus-Verhagen, Elwin Aloysius Cornelius Adrianus De Wolf
  • Patent number: 10647877
    Abstract: A curable composition includes specific amounts of a ketone, a curable component, and particulate poly(phenylene ether) having a mean particle size of 3 to 12 micrometers and a particle size relative standard deviation of 20 to 60 percent. The composition has a low viscosity that facilitates wetting of reinforcing structures, and composites formed from the composition and a reinforcing structure cure to form a dielectric material with a low dielectric constant and loss tangent.
    Type: Grant
    Filed: September 24, 2015
    Date of Patent: May 12, 2020
    Assignee: SABIC GLOBAL TECHNOLOGIES B.V.
    Inventors: Eylem Tarkin-Tas, Edward Norman Peters
  • Patent number: 10647878
    Abstract: The invention is directed to curable polyurethane coating compositions which may be used to form fouling release coatings, e.g., for use in protecting boat hulls. The curable polyurethane coating compositions of the invention comprise (a) a prepolymer made by reacting at least one polyisocyanate with (i) at least one monocarbinol-terminated poly(dimethylsiloxane), (ii) at least one methoxy-terminated poly(ethylene glycol), or (iii) mixtures thereof, (b) at least one polyol, and (c) at least one polyisocyanate crosslinker. The invention also relates to the prepolymer used in the curable coating compositions. The invention further relates to methods for reducing or preventing biofouling of a surface exposed to an aqueous environment comprising the steps of coating the surface with a curable coating composition of the invention to form a coated surface, and curing the coating coating composition on the coated surface.
    Type: Grant
    Filed: June 1, 2016
    Date of Patent: May 12, 2020
    Assignee: NDSU RESEARCH FOUNDATION
    Inventors: Dean C. Webster, Teluka Galhenage
  • Patent number: 10647879
    Abstract: A polymerizable liquid, or resin, useful for the production by additive manufacturing of a three-dimensional object of polyurethane, polyurea, or a copolymer thereof, is described. The resin includes at least one of (i) a blocked or reactive blocked prepolymer, (ii) a blocked or reactive blocked diisocyanate, or (iii) a blocked or reactive blocked diisocyanate chain extender.
    Type: Grant
    Filed: April 26, 2018
    Date of Patent: May 12, 2020
    Assignee: Carbon, Inc.
    Inventors: Jason P. Rolland, Kai Chen, Justin Poelma, James Goodrich, Robert Pinschmidt, Joseph M. DeSimone, Lloyd M. Robeson
  • Patent number: 10647880
    Abstract: A method of forming a three-dimensional object of polyurethane, polyurea, or copolymer thereof is carried out by: (a) providing a carrier and an optically transparent member having a build surface, the carrier and the build surface defining a build region therebetween; (b) filling the build region with a polymerizable liquid, the polymerizable liquid including at least one of: (i) a blocked or reactive blocked prepolymer, (ii) a blocked or reactive blocked diisocyanate, or (iii) a blocked or reactive blocked diisocyanate chain extender; (c) irradiating the build region with light through the optically transparent member to form a solid blocked polymer scaffold and advancing the carrier away from the build surface to form a three-dimensional intermediate having the same shape as, or a shape to be imparted to, the three-dimensional object, with the intermediate containing the chain extender; and then (d) heating or microwave irradiating the three-dimensional intermediate sufficiently to form from the three-dime
    Type: Grant
    Filed: February 7, 2019
    Date of Patent: May 12, 2020
    Assignee: Carbon, Inc.
    Inventors: Jason P. Rolland, Kai Chen, Justin Poelma, James Goodrich, Robert Pinschmidt, Joseph M. DeSimone, Lloyd M. Robeson
  • Patent number: 10647881
    Abstract: A polyimide precursor composition in which a resin and an organic amine compound are dispersed in an aqueous solvent, wherein the aqueous solvent contains 50% by weight or more of water and at least one organic solvent selected from a solvent group A consisting of a urea solvent, an amide solvent containing an alkoxy group, and an amide solvent containing an ester group in an amount of 5% by weight or more with respect to the total amount of the aqueous solvent, and the resin has a repeating unit represented by the following formula (I): wherein A indicates a tetravalent organic group, and B indicates a bivalent organic group.
    Type: Grant
    Filed: February 23, 2016
    Date of Patent: May 12, 2020
    Assignee: FUJI XEROX CO., LTD.
    Inventors: Tomoya Sasaki, Tsuyoshi Miyamoto, Kana Miyazaki, Katsumi Nukada
  • Patent number: 10647882
    Abstract: Porous air permeable expanded PTFE composite with enhanced mechanical and thermal properties are described. The node and fibril microstructure of expanded PTFE is coated on and within the node and fibril microstructure with a suitably chosen polymer to impart property enhancement while maintaining porosity. The coating polymer content of the composite is maintained between 3 and 25 weight percent of the composite and the areal mass of the composite is less than 75 gm/m2. Exemplary enhancement to properties may include, among others, Average Tensile Strength (ATS) (in MPa)×Z strength (in MPa) of 50 MPa2 or greater, preferably 100 MPa2 or greater, with air flow less than 500 Gurley seconds. Coating polymers with appropriate temperature resistance provides composites which further exhibit shrinkage of less than 10% at temperatures up to 300° C. with air flow of less than 500 Gurley seconds.
    Type: Grant
    Filed: February 6, 2018
    Date of Patent: May 12, 2020
    Assignee: W. L. Gore & Associates, Inc.
    Inventors: Anit Dutta, Leslie N. Rikleen
  • Patent number: 10647883
    Abstract: The present invention relates to a polyimide-based solution that can be used to produce an isotropic transparent polyimide-based film with high heat resistance and excellent mechanical properties as well as high transmittance. A coating of the polyimide-based solution on a substrate has a haze of 1% or less after storage at a temperature of 30° C. and a humidity of 70% for 30 minutes.
    Type: Grant
    Filed: October 31, 2018
    Date of Patent: May 12, 2020
    Assignee: LG CHEM. LTD.
    Inventors: Cheolmin Yun, BoRa Shin, Hye Won Jeong, Kyungjun Kim, HangAh Park
  • Patent number: 10647884
    Abstract: A hydrophobic and oleophobic coating composition includes at least a polysilazane polymer and a fluoroacrylate copolymer. The coating composition can be applied to a substrate in a single-step process as a thick and durable polymeric layer. Methods for making the coating composition and related articles are also provided.
    Type: Grant
    Filed: June 8, 2018
    Date of Patent: May 12, 2020
    Inventor: Steven Martin Johnson
  • Patent number: 10647885
    Abstract: Provided herein is a method of coating a surface. A silicon-based coating composition is coated onto a surface. The composition comprises 5% to 80% polysilazane, 20% to 60% polysiloxane, and polysilane of a formula (R1R2Si)n, wherein n is greater than 1, and wherein R1 and R2 are the same or different and are chosen from alkyl, alkenyl, cycloalkyl, alkylamino, aryl, aralkyl, or alkylsilyl, which polysilane has a weight average molecular weight of more than 50,000, and optionally organic solvent. The coating is cured ambiently to provide a non-ceramic clear coating having a thickness ranging between 0.1 mil and 1.5 mil, a hardness ranging between 2H and 9H in accordance with ASTM 3363 for film hardness by pencil test, and a kinetic coefficient of friction between 0.03 and 0.04. Also provided are silicon-based coating compositions and cured coatings from those compositions using the provided method.
    Type: Grant
    Filed: April 10, 2019
    Date of Patent: May 12, 2020
    Assignee: Burning Bush Group, LLC
    Inventors: Chris Fish, Jerry Kilby
  • Patent number: 10647886
    Abstract: A water-based hydrogel polymer coating and a method of application to natural rubber or other elastomeric latex products are provided. The water-based hydrogel polymer is mixed with a blend of at least one elastomeric material to provide a hydrogel polymer blend composition. The water-based hydrogel polymer blend composition is applied in a single application to an elastomeric article, such as gloves, without additional solvents in the polymer blend composition and without a separate acid or chemical priming step. The water-based hydrogel coating herein provides increased lubricity to facilitate improved wet and dry donning of the elastomeric article.
    Type: Grant
    Filed: October 18, 2016
    Date of Patent: May 12, 2020
    Assignee: Allegiance Corporation
    Inventors: Choon Kong Woo, Chuang Sim Chong, Nujalee Dangseeyun, Panor Wannawong
  • Patent number: 10647887
    Abstract: The invention provides a chemical-mechanical polishing composition comprising a) surface-modified colloidal silica particles, comprising a negatively-charged group on the surface of the particles, wherein the surface-modified colloidal silica particles have a negative charge, a particle size of about 90 nm to about 350 nm, and a zeta potential of about ?5 mV to about ?35 mV at a pH of about 3, b) an iron compound, c) a stabilizing agent, d) a corrosion inhibitor, and e) an aqueous carrier. The invention also provides a method suitable for polishing a substrate.
    Type: Grant
    Filed: January 8, 2018
    Date of Patent: May 12, 2020
    Assignee: Cabot Microelectronics Corporation
    Inventors: Kevin P. Dockery, Pankaj K. Singh, Steven Grumbine, Kim Long
  • Patent number: 10647888
    Abstract: Provided is an adhesive composition which exhibits excellent water resistance and warm-water resistance without impairing instantaneous adhesiveness. The 2-cyanoacrylate adhesive composition contains a 2-cyanoacrylic acid ester, and a specific phthalic anhydride derivative, in which the content of the phthalic anhydride derivative is from 0.01 to 5% by mass, relative to the total amount of the adhesive composition. Preferably, the adhesive composition further contains an elastomer.
    Type: Grant
    Filed: February 18, 2016
    Date of Patent: May 12, 2020
    Assignee: Toagosei Co., LTD.
    Inventors: Masaru Ando, Norifumi Yoshida, Hiroyuki Terai
  • Patent number: 10647889
    Abstract: A two-component (meth) acrylic adhesive excellent in peel strength at low temperature and impact resistance is provided. A composition comprising components of (1) to (4): (1) a polymerizable vinyl monomer comprising (1-1) to (1-4); (2) a polymerization initiator; (3) a reducing agent; and (4) an elastomer having no polymerizable unsaturated double bond at the end and having 10 to 30 mol % of a (meth) acrylonitrile. A composition comprising components of (1) to (4): (1) a polymerizable vinyl monomer comprising (1-1) to (1-4); (2) a polymerization initiator; (3) a reducing agent; (4) an elastomer having a polymerizable unsaturated double bond at the end and having 10 to 30 mol % of a (meth) acrylonitrile; and (5) an elastomer having no polymerizable unsaturated double bond at the end.
    Type: Grant
    Filed: July 28, 2016
    Date of Patent: May 12, 2020
    Assignee: DENKA COMPANY LIMITED
    Inventors: Hayato Miyazaki, Kenji Fukao, Hiroki Uno, Yoshitsugu Goto
  • Patent number: 10647890
    Abstract: The present application relates to an adhesive composition comprising a curable oligomer and a polymer derived from butylene, an adhesive film comprising same, an organic electronic device comprising same, and a lighting apparatus and a display device comprising same. The adhesive film comprising the adhesive composition shows excellent moisture-blocking properties and enables an organic electronic device to have flexibility as well as excellent and reliable durability at high temperature and high humidity.
    Type: Grant
    Filed: June 9, 2016
    Date of Patent: May 12, 2020
    Assignee: LG CHEM, LTD.
    Inventors: Kyung Yul Bae, Yoon Gyung Cho, Hyun Jee Yoo, Se Woo Yang
  • Patent number: 10647891
    Abstract: Provided is a PSA sheet that has a high level of moisture resistance while maintaining good holding power with reduced gas emission. The PSA sheet provided by this invention comprises a moisture-impermeable layer and a PSA layer provided to one face of the moisture-impermeable layer. The PSA layer comprises a polymer A having a weight average molecular weight of 5×104 or higher as a base polymer and a polymer B having a number average molecular weight of 1000 or higher and a weight average molecular weight lower than 5×104.
    Type: Grant
    Filed: March 18, 2019
    Date of Patent: May 12, 2020
    Assignee: NITTO DENKO CORPORATION
    Inventors: Kenji Furuta, Akira Hirao, Tatsuya Suzuki
  • Patent number: 10647892
    Abstract: Provided is an adhesive that can provide quick bonding between thermoplastic resins and excellent bond strength, a structure having adhesion provided by the adhesive, and an adhesion method using the adhesive. The adhesive bonds a first member (11) containing a thermoplastic resin or a carbon fiber reinforced thermoplastic resin and a second member (12) containing the thermoplastic resin or the carbon fiber reinforced thermoplastic resin. The adhesive includes a thermoplastic resin as a main component containing a metal nano material that absorbs electromagnetic waves and generates heat.
    Type: Grant
    Filed: February 9, 2016
    Date of Patent: May 12, 2020
    Assignees: MITSUBISHI HEAVY INDUSTRIES, LTD., AKITA UNIVERSITY, TSUCHIYA CO., LTD.
    Inventors: Toshiyuki Takayanagi, Naomoto Ishikawa, Hideki Horizono, Nobuyuki Kamihara, Mikio Muraoka, Hiroaki Hayashi, Osamu Yoshida, Kotaro Tsuji
  • Patent number: 10647893
    Abstract: Aqueous-based adhesive composition comprising a mixture of polycholorprenes, at least one self-crosslinkable agent of alkyd type and at least one filler, 2) use of such a composition as contact adhesive, 3) multilayer structure assembled with the aid of the adhesive composition 1).
    Type: Grant
    Filed: February 8, 2016
    Date of Patent: May 12, 2020
    Assignee: BOSTIK SA
    Inventors: Jessie Casimiro, Mélanie Nataf
  • Patent number: 10647894
    Abstract: Provided is an adhesive composition for an optical use, including: a first isobutylene-isoprene-based rubber having a weight average molecular weight (Mw) of 100,000 g/mol to 1,000,000 g/mol; and a second isobutylene-isoprene-based rubber having a weight average molecular weight (Mw) of 5,000 g/mol to 100,000 g/mol, in which the first isobutylene-isoprene-based rubber and the second isobutylene-isoprene-based rubber each include a hydroxy group. Further, provided is an adhesive layer including a thermally cured product of the adhesive composition for optical use.
    Type: Grant
    Filed: April 4, 2017
    Date of Patent: May 12, 2020
    Assignee: LG Chem, Ltd.
    Inventors: Kwang Su Seo, Eun Kyung Park, Seung Won Lee, Jang Soon Kim, Tae Yi Choi
  • Patent number: 10647895
    Abstract: The present invention aims to provide an interlayer filling material for a touch panel which is used for filling an interlayer space between a touch panel and another component or an interlayer space between transparent conductive films included in the touch panel in production of a personal digital assistant, is less likely to cause cracks or breakage in a surface protection panel or a glass substrate, and enables production of a touch panel laminate that is not likely to display images with color irregularity. The present invention also aims to provide a touch panel laminate produced using the interlayer filling material for a touch panel.
    Type: Grant
    Filed: October 6, 2016
    Date of Patent: May 12, 2020
    Assignee: SEKISUI CHEMICAL CO., LTD.
    Inventors: Juichi Fukatani, Kiyomi Uenomachi, Takazumi Okabayashi, Ryousuke Ebina, Atsushi Wada
  • Patent number: 10647896
    Abstract: The present invention relates to a hydrogenated petroleum resin, and to a manufacturing method and use thereof. More specifically, it relates to a hydrogenated petroleum resin manufactured by subjecting dicyclopentadiene and an olefinic monomer to thermal polymerization and then carrying out a hydrogenation reaction, and to a manufacturing method and use therefor. The hydrogenated petroleum resin has the advantage of being useful in practical applications, since the petroleum resin is manufactured via thermal polymerization using inexpensive raw materials and on the contrary to conventional catalytic polymerization, a catalyst elimination process can be excluded. The hydrogenated petroleum resin produced in this way can be applied to, for example, an adhesive agent used in environmentally friendly sanitary goods, because the petroleum resin has excellent compatibility, adhesiveness and heat resistance, and has no bad odor.
    Type: Grant
    Filed: June 28, 2016
    Date of Patent: May 12, 2020
    Assignee: KOLON INDUSTRIES, INC.
    Inventors: Sang Hyun Lee, Min Sik Cho, Jun Hyo Park, Joong Suk Lee
  • Patent number: 10647897
    Abstract: The present disclosure is directed to a precursor composition for a curable adhesive, the precursor comprising: a) a part (A) comprising: i. a first epoxy curing agent comprising at least one polyether amine and having an amine equivalent weight of at least 45 grams per mole of amine equivalents; ii. a second epoxy curing agent distinct from the first epoxy curing agent; iii. a metal nitrate catalyst; iv. optionally, a metal triflate catalyst; and b) a part (B) comprising: i. an epoxy resin; ii. a filler material; iii. an epoxy-based reactive diluent; and iv. optionally, a core-shell polymer toughening agent; and wherein the amount of filler material is selected such as to provide the part (B) with a hysteresis area of at least 30 Pa×1/s, when measured at 23 C according to the test method described in the experimental section.
    Type: Grant
    Filed: October 21, 2016
    Date of Patent: May 12, 2020
    Assignee: 3M Innovative Properties Company
    Inventor: Mareike Bardts
  • Patent number: 10647898
    Abstract: Disclosed are an adhesive composition for polarizing plates, a polarizing plate using the same, a method for preparing the same, and an optical member including the same. The adhesive composition includes (A) a (meth)acrylic radical compound, (B) a cationic epoxy compound, (C) a phenoxy resin, and (D) a photoinitiator.
    Type: Grant
    Filed: August 29, 2018
    Date of Patent: May 12, 2020
    Assignee: Cheil Industries, Inc.
    Inventors: Mi Yeon Yu, Tae Hyun Lee, Do Heon Lee, Ik Hwan Cho, In Cheon Han
  • Patent number: 10647899
    Abstract: Provided are a heat-curable fluoropolyether-based adhesive composition capable of being cured and adhering to various kinds of base materials made of, for example, a metal, ceramic and/or plastic in a short period of time; and an electric/electronic component employing the same. The composition is a heat-curable fluoropolyether-based adhesive composition having, as an adhesion imparting agent, an alicyclic epoxy group-containing and fluorine-containing organohydrogensiloxane having in one molecule: a monovalent perfluoroalkyl or perfluorooxyalkyl group(s), or a divalent perfluoroalkylene or perfluorooxyalkylene group(s); and at least one silicon atom-bonded hydrogen atom (SiH group).
    Type: Grant
    Filed: May 1, 2018
    Date of Patent: May 12, 2020
    Assignee: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: Hidenori Koshikawa
  • Patent number: 10647900
    Abstract: A chemical-mechanical polishing (CMP) composition is provided comprising (A) one or more compounds selected from the group of benzotriazole derivatives which act as corrosion inhibitors and (B) inorganic particles, organic particles, or a composite or mixture thereof. The invention also relates to the use of certain compounds selected from the group of benzotriazole derivatives as corrosion inhibitors, especially for increasing the selectivity of a chemical mechanical polishing (CMP) composition for the removal of tantalum or tantalum nitride from a substrate for the manufacture of a semiconductor device in the presence of copper on said substrate.
    Type: Grant
    Filed: July 1, 2014
    Date of Patent: May 12, 2020
    Assignee: BASF SE
    Inventors: Robert Reichardt, Martin Kaller, Michael Lauter, Yuzhuo Li, Andreas Klipp
  • Patent number: 10647901
    Abstract: Provided is a refrigerating machine oil composition for a mixed refrigerant comprising difluoromethane, the composition comprising a polymer (A) below and an ester (B) of polyhydric alcohol(s) with aliphatic monocarboxylic acid(s). The polymer (A): a polymer which is obtained by polymerizing monomer(s) consisting of at least one monomer of monosubstituted ethylenes and disubstituted ethylenes, and in which a ratio of a monomer represented by the following general formula (I): wherein R1 represents an alkyl group having 1 to 14 carbon atoms, R2 represents hydrogen or an alkyl group having 1 to 4 carbon atoms, and the sum of carbon numbers in R1 and R2 is 2 to 14, is 75 to 100% by mass based on a total mass of monomers constituting the polymer.
    Type: Grant
    Filed: September 29, 2016
    Date of Patent: May 12, 2020
    Assignee: KH NEOCHEM CO., LTD.
    Inventors: Takahiro Sawada, Junya Kishi, Aya Okita
  • Patent number: 10647902
    Abstract: The present invention discloses temporary plugging agent for drilling fluid and preparation method thereof, and water-based drilling fluid and use thereof. The temporary plugging agent for drilling fluid is obtained by controlling gelatinized starch and a vinyl grafted monomer to have a polymerization reaction in an activator solution in the presence of a cross-linking agent and an initiator; the vinyl grafted monomer comprises acrylic acid, acrylamide, and 2-acrylamide-2-methyl propanesulfonic acid; the gelatinized starch is obtained by adding starch into deionized water to have a gelatinization reaction.
    Type: Grant
    Filed: April 25, 2019
    Date of Patent: May 12, 2020
    Assignee: CHINA UNIVERSITY OF PETROLEUM (EAST CHINA)
    Inventors: Weian Huang, Jingwen Wang, Ming Lei, Jiaqi Zhang, Gongrang Li, Kaihe Lv, Xiongjun Wu, Zhengsong Qiu
  • Patent number: 10647903
    Abstract: The present application discloses drilling fluid compositions, methods for making drilling fluids, and methods for drilling subterranean wells utilizing the drilling fluids. According to one embodiment, a drilling fluid composition may include an oil phase, an aqueous phase, an emulsifier, and a rheology modifier. The emulsifier may include an amino amide, and the rheology modifier may include a layered double hydroxide, such as Mg/Al-Myristate layered double hydroxide.
    Type: Grant
    Filed: August 9, 2018
    Date of Patent: May 12, 2020
    Assignees: Saudi Arabian Oil Company, Durham University, M-I Drilling Fluids UK Ltd
    Inventors: Musarrat Halima Mohammed, Andrew Whiting, Mona Al Batal, Manohara Gudiyor Veerabhadrappa, Hugh Christopher Greenwell, John Adrian Hall, Gasan Selman Alabedi, Michael Hayward Hodder
  • Patent number: 10647904
    Abstract: The present invention provides for a compressible grout mix for filling an annular gap between a tunnel rock wall surface and a tunnel liner of a tunnel in a rock formation subject to time dependent deformation after excavation and a method of filling the annular gap between a tunnel rock wall surface and a funnel liner of a tunnel in a rock formation subject to time dependent deformation after excavation utilizing the compressible grout mix for resilient absorption of forces in the hardened state of the compressible grout mix exerted by the time dependent deformation of the rock wall surface into the tunnel opening. The method includes: a. providing a compressible grout mix comprising hydraulic binding agent, bentonite clay, polymer foam particles, water, and one or more additives selected from water-reducing admixture and/or setting retarding admixture, aggregate materials, anti-wash agents and air, b.
    Type: Grant
    Filed: June 10, 2019
    Date of Patent: May 12, 2020
    Inventor: Tony Dimillo
  • Patent number: 10647905
    Abstract: Methods and systems are presented in this disclosure for evaluating performance of cement fluid-loss-control additives and generating cement slurries with controlled fluid losses for cementing operations. A normalized pressure along a wellbore length can be first specified based on properties of the proposed cement slurry formulation and properties of the wellbore in a subterranean formation. A volume loss of a fluid of the proposed cement slurry formulation can be calculated using a model associated with the fluid obtained based at least in part on the normalized pressure and properties of the fluid. The proposed cement slurry formulation can be manipulated by adding one or more fluid-loss control additives to the proposed cement slurry formulation based on the calculated volume loss of the fluid to produce a preferred cement slurry.
    Type: Grant
    Filed: August 5, 2015
    Date of Patent: May 12, 2020
    Assignee: HALLIBURTON ENERGY SERVICES, INC.
    Inventors: Elias D. Rodrigues, Rafael M. Oliveira, Flavio H. Marchesini
  • Patent number: 10647906
    Abstract: Compositions may include a wax modifier that is the product of a reaction between a polysaccharide having a number of sugar subunits in the range of 2 to 60 and one or more fatty acid reagents, and a reservoir fluid produced from a subterranean formation comprising one or more components capable of producing waxes. Methods may include contacting a hydrocarbon fluid with a wax modifier, wherein the wax modifier is the product of the reaction of a polysaccharide and one or more fatty acid reagents. Methods may also include introducing a wax modifier into a wellbore penetrating a subterranean formation, wherein the wax modifier is the product of a reaction between a polysaccharide and one or more fatty acid reagents; producing hydrocarbons from the subterranean formation; and allowing the wax modifier to inhibit the precipitation of a wax.
    Type: Grant
    Filed: December 11, 2017
    Date of Patent: May 12, 2020
    Assignee: M-I L.L.C.
    Inventors: Pradyumna Avinash Deshpande, Chandrashekhar Yeshwant Khandekar
  • Patent number: 10647907
    Abstract: Compositions and methods for increasing recovery, or flowback, of hydrocarbon compounds from hydrocarbon-containing subterranean reservoirs. The compositions include a dialkyl dimethyl ammonium surfactant, an amphoteric surfactant, and a solvent. The concentrated compositions are storage stable and easily diluted with a water source such as produced water to form injectates suitable for injecting into one or more hydrocarbon-bearing subterranean reservoirs. The injectates convert oil-wet rocks to water-wet but do not cause formation of emulsions with hydrocarbon compounds within the subterranean environment. Injection of the injectates into a reservoir results in an increase in the yield of hydrocarbons recovered, in particular from low permeability, low porosity reservoirs such as those formed by or encountered in hydraulic fracturing and/or in certain geographic locations.
    Type: Grant
    Filed: July 3, 2018
    Date of Patent: May 12, 2020
    Assignee: Ecolab USA Inc.
    Inventors: Duy T. Nguyen, Tzu-Ping Hsu
  • Patent number: 10647908
    Abstract: Provided is a composition for preparing injection fluid in oil and gas recovery comprising an inverse emulsion of a water-soluble polymer A comprising acrylamide monomer units, and solid particles of a water-soluble polymer, wherein water-soluble polymer B is obtained by a polymerization step of at least acrylamide and 1 and 15 mol % of acrylamido tertiary butyl sulfonic acid (ATBS), and/or salts thereof, and a subsequent post treatment step of the resulting polymer. Also provided is a method of treating a portion of subterranean formation comprising providing the composition, preparing an injection fluid with at least the composition, introducing the injection fluid into portion of the subterranean formation. The composition is particularly useful to prepare fracturing fluid in fracturing operations.
    Type: Grant
    Filed: July 26, 2019
    Date of Patent: May 12, 2020
    Assignee: S.P.C.M. SA
    Inventor: Cédrick Favero
  • Patent number: 10647909
    Abstract: A fracturing fluid including a base fluid including salt water, a polymer, a crosslinker, and a nanomaterial. The crosslinker may include a Zr crosslinker, a Ti crosslinker, an Al crosslinker, a borate crosslinker, or a combination thereof. The nanomaterial may include ZrO2 nanoparticles, TiO2 nanoparticles, CeO2 nanoparticles; Zr nanoparticles, Ti nanoparticles, Ce nanoparticles, metal-organic polyhedra including Zr, Ti, Ce, or a combination thereof; carbon nanotubes, carbon nanorods, nano graphene, nano graphene oxide; or any combination thereof. The viscosity and viscosity lifetime of fracturing fluids with both crosslinkers and nanomaterials are greater than the sum of the effects of crosslinkers and nanomaterials taken separately.
    Type: Grant
    Filed: January 13, 2016
    Date of Patent: May 12, 2020
    Assignee: Saudi Arabian Oil Company
    Inventors: Leiming Li, Feng Liang, Ghaithan A. Al-Muntasheri, Amy J. Cairns
  • Patent number: 10647910
    Abstract: The present disclosure relates to oil and gas well proppant compositions and methods for enhancing the conductivity of a propped fracture formed during a hydraulic fracturing operation. The method introduces a micro-proppant slurry prepared with slickwater containing both a low-density and a conventional micro-proppant during injection of the pad fluid stages to prop the natural and induced microfractures open and then injecting a proppant slurry prepared with slickwater containing low-density proppant and conventional frac sand during proppant slurry stage to prop the dominant fractures or large branches, provide open flow paths to keep them connective with the wellbore.
    Type: Grant
    Filed: October 19, 2018
    Date of Patent: May 12, 2020
    Assignee: HALLIBURTON ENERGY SERVICES, INC.
    Inventors: Philip D. Nguyen, Baidurja Ray, Vishwajit Manajirao Ghatge, Larry Steven Eoff, Christopher Austin Lewis
  • Patent number: 10647911
    Abstract: Disclosed are coated particles. The coated particles include substrate particles and a coating disposed over at least a portion of the substrate particles. The coating includes a condensation reaction product of a reaction mixture that includes a liquid isocyanate-functional component and an isocyanate-reactive composition. Also disclosed are methods for making such particles and methods for using such particles as proppants in hydraulic fracturing.
    Type: Grant
    Filed: July 2, 2019
    Date of Patent: May 12, 2020
    Assignee: Covestro LLC
    Inventors: Stephen J. Harasin, Kenneth R. Riddle, Michael T. Wellman
  • Patent number: 10647912
    Abstract: A carbon-coated vanadium dioxide particle includes a vanadium dioxide particle; and a coating layer containing amorphous carbon on a surface of the vanadium dioxide particle, the amorphous carbon being derived from carbon contained in an oxazine resin, and having a peak intensity ratio of a G band to a band of 1.5 or greater as determined from a Raman spectrum. The coating layer has an average thickness of 50 nm or less. The coating layer has a coefficient of variation (CV value) of thickness of 7% or less.
    Type: Grant
    Filed: March 22, 2017
    Date of Patent: May 12, 2020
    Assignee: SEKISUI CHEMICAL CO., LTD.
    Inventors: Ren-de Sun, Shoji Nozato, Akira Nakasuga, Masanori Nakamura, Naoyuki Nagatani, Keigo Oowashi
  • Patent number: 10647913
    Abstract: A composition comprising a diarylethene photochromic anodic species, a cathodic species and an electrolyte that comprises a supporting electrolyte and a solvent. Electrochromic devices such as optical filters are prepared from such compositions.
    Type: Grant
    Filed: November 17, 2015
    Date of Patent: May 12, 2020
    Assignee: SWITCH MATERIALS INC.
    Inventors: Neil Robin Branda, Glen Ramsay Bremner, Jeremy Graham Finden, Matt Andrew Pilapil, Matthew Neal Roberts, Jonathan Ross Sargent, James Daniel Senior, Veronica Elizabeth Patricia Marshman, Natalie E. Campbell
  • Patent number: 10647914
    Abstract: Scintillating plastics resistant to crazing and fogging, methods of making and using the same are disclosed. The scintillating plastics include: one or more primary polymers present in an amount ranging from about 40 wt % to about 95 wt %; one or more secondary polymers present in an amount ranging from about 1 wt % to about 60 wt %; and one or more fluors present in an amount ranging from about 0.1 wt % to about 50 wt %. Methods of making such plastics include: creating a homogenous mixture of precursor materials including primary polymer, secondary polymer, and fluor in the amounts set forth above; and polymerizing the homogenous mixture. Methods of using such plastics include: exposing the scintillating plastic to one or more extreme environmental conditions for a predetermined amount of time without generating crazing or fogging within the scintillating plastic. Various additional features and specific embodiments of these inventive concepts are also disclosed.
    Type: Grant
    Filed: March 17, 2017
    Date of Patent: May 12, 2020
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Natalia P. Zaitseva, M. Leslie Carman, Andrew M. Glenn, Andrew Neil Mabe, Stephen A. Payne
  • Patent number: 10647915
    Abstract: A converter assembly for converting a primary light into a secondary light includes at least one element which has a light-converting structure with open pores and which is laterally held by a frame. The surfaces of both the light-converting structure as well as of the inner face of the frame are covered with a transparent layer such that each of the afore-mentioned elements forms a region in which a property of the incident light and preferably of the wavelength thereof is changed. In specific embodiments, the converter assembly can be part of display assemblies or of miniaturized components for example. There is also described a method for producing the converter assembly.
    Type: Grant
    Filed: December 13, 2016
    Date of Patent: May 12, 2020
    Assignee: Fraunhofer-Gesellschaft zur Foerderung der angewandten Forschung e.V.
    Inventors: Ulrich Hofmann, Hans-Joachim Quenzer, Thomas Lisec, Thomas Von Wantoch
  • Patent number: 10647916
    Abstract: A scintillation compound can include a rare earth element that is in a divalent (RE2+) or a tetravalent state (RE4+). The scintillation compound can include another element to allow for better change balance. The other element may be a principal constituent of the scintillation compound or may be a dopant or a co-dopant. In an embodiment, a metal element in a trivalent state (M3+) may be replaced by RE4+ and a metal element in a divalent state (M2+). In another embodiment, M3+ may be replaced by RE2+ and M4+. In a further embodiment, M2+ may be replaced by a RE3+ and a metal element in a monovalent state (M1+). The metal element used for electronic charge balance may have a single valance state, rather than a plurality of valence states, to help reduce the likelihood that the valance state would change during formation of the scintillation compound.
    Type: Grant
    Filed: August 17, 2017
    Date of Patent: May 12, 2020
    Assignee: SAINT-GOBAIN CRISTAUX ET DETECTEURS
    Inventors: Samuel Blahuta, Vladimir Ouspenski
  • Patent number: 10647917
    Abstract: A method of producing a quantum dot comprising zinc selenide, the method comprising: providing an organic ligand mixture comprising a carboxylic acid compound, a primary amine compound, a secondary amide compound represented by Chemical Formula 1, and a first organic solvent: RCONHR??Chemical Formula 1 wherein each R is as defined herein; heating the organic ligand mixture in an inert atmosphere at a first temperature to obtain a heated organic ligand mixture; adding a zinc precursor, a selenium precursor, and optionally a tellurium precursor to the heated organic ligand mixture to obtain a reaction mixture, wherein the zinc precursor does not comprise oxygen; and heating the reaction mixture at a first reaction temperature to synthesize a first semiconductor nanocrystal particle.
    Type: Grant
    Filed: October 25, 2018
    Date of Patent: May 12, 2020
    Assignee: SAMSUNG ELECTRONICS CO., LTD.
    Inventors: Jeong Hee Lee, Hyun A Kang, Sung Woo Kim, Jin A Kim, Tae Hyung Kim, Yuho Won, Eun Joo Jang
  • Patent number: 10647918
    Abstract: A liquid crystal composition includes: at least one liquid crystal compound selected from the group consisting of Chemical Formulas 1-1 to 1-8; at least one self-aligned compound selected from the group consisting of Chemical Formulas 2-1 and 2-2; and at least one reactive mesogen selected from the group consisting of Chemical Formulas 3-1 to 3-5. Compositions and devices constructed therewith are capable of ameliorating liquid crystal drip spots that typically occur in a manufacturing process. In addition, the display devices using the composition do not require an additional alignment layer, which simplifies manufacturing.
    Type: Grant
    Filed: August 23, 2018
    Date of Patent: May 12, 2020
    Assignee: Samsung Display Co., Ltd.
    Inventors: Ji Eun Jang, Sun Young Kwon, Min-Hee Kim, Jong Ho Son, Keun Chan Oh, Chang-Hun Lee
  • Patent number: 10647919
    Abstract: Provided are a liquid crystal composition satisfying at least one of characteristics such as high maximum temperature, low minimum temperature, small viscosity, suitable optical anisotropy, large negative dielectric anisotropy, large specific resistance, high stability to ultraviolet light and high stability to heat, or the liquid crystal composition having a suitable balance regarding at least two of the characteristics; and an AM device having characteristics such as a short response time, a large voltage holding ratio, low threshold voltage, a large contrast ratio and a long service life.
    Type: Grant
    Filed: January 14, 2016
    Date of Patent: May 12, 2020
    Assignees: JNC CORPORATION, JNC PETROCHEMICAL CORPORATION
    Inventors: Masayuki Saito, Yoshimasa Furusato
  • Patent number: 10647920
    Abstract: A liquid crystal composition including: a polymerizable liquid crystal compound capable of expressing birefringence with inverse wavelength dispersion; and a (meth)acrylate compound containing two or more (meth)acryloyl groups per one molecule, wherein: an amount of the (meth)acrylate compound is 8 parts by weight or less, the amount being relative to 100 parts by weight of a sum total of the polymerizable liquid crystal compound and the (meth)acrylate compound.
    Type: Grant
    Filed: December 14, 2016
    Date of Patent: May 12, 2020
    Assignee: ZEON CORPORATION
    Inventors: Shunpei Nakajima, Akira Ikeda, Masakazu Saito, Manabu Ito
  • Patent number: 10647921
    Abstract: A liquid crystal composition includes a polymerizable compound (or polymer) and a polar compound, where the homeotropic alignment of liquid crystal molecules can be achieved by the action of these compounds, and a liquid crystal display device includes such a composition. A nematic liquid crystal composition has positive dielectric anisotropy and includes a polymerizable compound as a first additive and a polar compound as a second additive, and the composition may include a specific liquid crystal compound having a large positive dielectric anisotropy and a specific liquid crystal compound having a high maximum temperature or a small viscosity, and a liquid crystal display device includes such a composition.
    Type: Grant
    Filed: February 18, 2016
    Date of Patent: May 12, 2020
    Assignees: JNC CORPORATION, JNC PETROCHEMICAL CORPORATION
    Inventors: Naoko Matsuda, Masayuki Saito
  • Patent number: 10647922
    Abstract: Use of a catalyst composition comprising A) a first component containing oxidic compounds comprising aluminum and silicon with a molar ratio of silicon to aluminum of more than 1) B) a second component containing an oxidic compound of silicon wherein the ratio of the number of acidic sites of component A, determined by temperature programmed desorption with ammonia as a base, to the number of acidic sites of component B, determined under the same conditions, is at least 3: in a process for the catalytic depolymerization of plastics waste.
    Type: Grant
    Filed: December 15, 2016
    Date of Patent: May 12, 2020
    Assignee: SOLVAY SA
    Inventors: Stéphane Streiff, Marco Piccinini, Avelino Corma, Miriam Cerro-Alarcón, Jesús Mengual
  • Patent number: 10647923
    Abstract: A system and method produce hydrocarbons from biomass by fluid catalytic cracking. In one embodiment, the system is a fluid catalytic cracking system. The system includes a riser. The riser contains a catalyst. The system also includes a biological feed comprising biomass-derived liquid for the riser. In addition, the system includes a hydrocarbon feed comprising hydrocarbons for the riser. The biological feed and the hydrocarbons react in the riser in the presence of the catalyst to convert at least a portion of the biological feed and the hydrocarbons to hydrocarbon products. The hydrocarbon products comprise a concentration of oxygen from about 0.005 wt. % to about 6 wt. %.
    Type: Grant
    Filed: February 28, 2018
    Date of Patent: May 12, 2020
    Assignee: Phillips 66 Company
    Inventors: Kristi A. Fjare, TiePan Shi, Constantino Badra, Terry S. Cantu, Milena Vasic, Ruben van Duren, Marty Pronk, Leen Gerritsen
  • Patent number: 10647924
    Abstract: The present invention provides a process for producing liquid hydrocarbon products from a feedstock comprising at least one of a solid biomass-containing feedstock and a solid biomass-derived feedstock and in the range of from 50 to 15000 ppmw of chlorides, said process comprising the steps of: a) incorporating a chloride trap material into said feedstock to provide a combined feedstock/chloride trap material; b) densifying the combined feedstock/chloride trap material to form densified feed in the form of pellets or briquettes; c) contacting said densified feed with a hydropyrolysis catalyst composition and molecular hydrogen in a hydropyrolysis reactor vessel at a temperature in the range of from 350 to 600° C. and a pressure in the range of from 0.50 to 7.50 MPa to produce a product stream comprising a deoxygenated hydrocarbon product, H2O, H2, CO2, CO, C1—C3 gases, char and catalyst fines; and d) removing all or a portion of said char and catalyst fines from said product stream.
    Type: Grant
    Filed: August 2, 2017
    Date of Patent: May 12, 2020
    Assignee: SHELL OIL COMPANY
    Inventors: Vikrant Nanasaheb Urade, Laxmi Narasimhan Chilkoor Soundararajan, Alan Anthony Del Paggio, Srikant Gopal, Prakhar Arora