Abstract: A process for processing a leach solution of black mass of spent alkaline batteries which leach solution comprises metals dissolved to an acidic solution. The process comprises removing of one or more elements from the leach solution by a cementation operation by applying at least one non-noble metal in a metal form as a cementation agent and one or more additional cementation agents from both sulphate and nitrate groups to process the leach solution into a product of at least manganese- and zinc-containing sulphate solution which is suitable for use as micronutrients alone, in fertilizers and/or together with a plant protective agent to aid growth and health of plants. In addition, the invention also relates to a process for processing a black mass of spent alkaline batteries.

Abstract: A process for extracting, recovering and recycling metals and materials from spent lithium ion batteries (LIB) that comprises the contacting battery waste products with a deep eutectic solvent, and leaching the metal from the battery waste product and extracting the metal into the deep eutectic solvent with heat and agitation. After the leaching and extracting, the process further includes recovering the dissolved metals ions from the deep eutectic solvent solution, followed by a step of regeneration of cathode materials.

Abstract: Disclosed is a method for clean metallurgy of molybdenum, including steps: 1) roasting molybdenite with calcium to obtain calcified molybdenum calcine, and leaching the calcified molybdenum calcine with an inorganic acid to obtain a molybdenum-containing inorganic acid leachate; 2) extracting molybdenum in the leachate with a cationic extractant to obtain an organic phase loaded with molybdyl cations and a raffinate; 3) using a hydrogen peroxide solution as a stripping agent to obtain a molybdenum stripping liquor; and 4) heating the molybdenum stripping liquor to dissociate peroxymolybdic acid therein so as to form a molybdic acid precipitate, and then calcining to obtain a molybdenum trioxide product. The method solves the problem of ammonia nitrogen wastewater production and can also be used for the enrichment and recovery of rhenium.

Abstract: Some variations provide a metal matrix nanocomposite composition comprising metal-containing microparticles and nanoparticles, wherein the nanoparticles are chemically and/or physically disposed on surfaces of the microparticles, and wherein the nanoparticles are consolidated in a three-dimensional architecture throughout the composition. The composition may serve as an ingot for producing a metal matrix nanocomposite. Other variations provide a functionally graded metal matrix nanocomposite comprising a metal-matrix phase and a reinforcement phase containing nanoparticles, wherein the nanocomposite contains a gradient in concentration of the nanoparticles. This nanocomposite may be or be converted into a master alloy. Other variations provide methods of making a metal matrix nanocomposite, methods of making a functionally graded metal matrix nanocomposite, and methods of making a master alloy metal matrix nanocomposite. The metal matrix nanocomposite may have a cast microstructure.

Abstract: A high-performance metal alloy is disclosed being suitable for additive manufacturing of machine components, in particular machine components which are subjected to high gas temperature stress. Exemplary machine components are statoric components of gas turbines, such as nozzles.

Abstract: The present disclosure provides a magnesium alloy and a preparation method thereof. The magnesium alloy comprises: Al: 7.01-9.98 wt %; Zn: 0.1-1.2 wt %; Mn: 0.05-0.2 wt %; Sn: 0.3-2.5 wt %; Sm: 0.1-0.5 wt %; and a balance of Mg.

Abstract: The invention relates to biodegradable, metal alloys, methods for their preparation and applications for their use. The alloys include magnesium and other components, such as, yttrium, calcium, zirconium, and zinc. These elements are alloyed together in specific combinations and amounts in order to achieve an alloy having desired properties and characteristics. In certain embodiments, strontium or cerium may be included as an additive. The resulting alloys are particularly suitable for forming various medical devices for implantation into the body of a patient.

Abstract: The invention relates to composite materials based on tungsten carbide and comprising gold, palladium and/or platinum and to a method for producing said composite materials by sintering. By means of the FAST method, hard and biocompatible WC/(Au, Pd, Pt) composite materials can be produced, inter alia for use as coatings on tools and prostheses and as solid bodies in, for example, blood pumps.

Abstract: An additive manufacturing powdered composite material includes metal particles coated with a coating of ceramic particles. The metal particles may include a ternary NiCoCr alloy, with select additions of minor amounts of other elements. The ceramic particles may include yttrium oxide or other oxides. The composite material is suitable for additive manufacturing (AM) into a component for high temperature (>1000° C.) applications. The AM component includes a metal matrix formed from the alloy, with the ceramic particles dispersed in the matrix.

Abstract: Provided are a single layer zinc alloy plated steel material and a fabrication method therefor, the single layer zinc alloy plated steel material comprising a base iron and a zinc alloy plating layer formed on the base iron, wherein the zinc alloy plating layer contains 13-24 wt % of Mg, and the adhesion amount of the zinc alloy plating layer is at most 40 g/m2 (excluding 0 g/m2).

Abstract: Provided is a hot-rolled coated steel sheet having a yield point elongation of less than 4% and a manufacturing method for the same. The hot-rolled steel sheet comprises, by weight, 0.03 to 0.06% of carbon (C), 0.5 to 1.5% of manganese (Mn), 0.01 to 0.25% of silicon (Si), 0.01 to 0.05% of aluminum (Al), 0.001 to 0.02% of phosphorus (P), 0.006% or less of sulfur (S), 0.0001 to 0.02% of titanium (Ti), 0.0001 to 0.03% of niobium (Nb), 0.001 to 0.005% of nitrogen (N), and a balance of iron (Fe) and inevitable impurities, wherein the Ti, Al and N satisfy the following relationship 1, and the Nb, C and N satisfy the following relationship 2: 0.03?(wt % Ti)×(wt % Al)×(wt % N)×106?0.20 (1), and 22?(mol % Nb)/{(mol % C)×(mol % N)}?1826 (2).

Abstract: Provided are a laminate shaped article made of a maraging steel and having excellent toughness, a method for manufacturing the same, and a metal powder for laminate shaping. The laminate shaped article is made of a maraging steel comprising 0.1-5.0 mass % of Ti. When sis is performed on concentration distribution of Ti in a cross section parallel to a lamination direction of the above laminate shaped article, a length of a linear Ti-rich portion having a Ti concentration B of (1.5×A) or more with respect to an average Ti concentration A in the cross section is 15 ?m or less. In addition, the method for manufacturing the laminate shaped article uses a metal powder made of a maraging steel comprising 0.1-5.0 mass % of Ti, and a heat source output is set to 50-330 W and a scanning speed is set to 480-3000 mm/sec during the laminate shaping.

Abstract: A metal matrix composite comprising nanotubes; a method of producing the same; and a composition, for example a metal alloy, used in such composites and methods, are disclosed. A method for continuously infiltrating nanotube yarns, tapes or other nanotube preforms with metal alloys using a continuous process or a multistep process, which results in a metal matrix composite wire, cable, tape, sheet, tube, or other continuous shape, and the microstructure of these infiltrated yarns or fibers, are disclosed. The nanotube yarns comprise a multiplicity of spun nanotubes of carbon (CNT), boron nitride (BNNT), boron (BNT), or other types of nanotubes. The element that infiltrates the nanotube yarns or fibers can, for example, be alloyed with a concentration of one or more elements chosen such that the resulting alloy, in its molten state, will exhibit improved wetting of the nanotube material.

Abstract: Equipment for the continuous hot dip-coating of a metal strip 9 including an annealing furnace, a tank 2 containing a liquid metal bath 3, a snout connecting the annealing furnace and tank 2, through which the metal strip 9 runs in a protective atmosphere and the lower part of the snout, the sabot 5, is at least partly immersed in the liquid metal bath 3 in order to define with the surface of the bath, and inside this snout, a liquid seal 6, an overflow 7 not connected to the snout, the overflow 7 including at least one tray 8, placed in the vicinity of the strip 9 when entering the liquid metal bath 3 and encompassed by liquid seal 6.

Abstract: Provided is a zinc-based plated steel sheet having a post-treated coating filmed thereon including: a steel sheet; a zinc plated layer formed on the steel sheet; and a post-treated coating formed on the plated layer, wherein the atomic ratio (O/M) of oxygen (O) to metals (M) contained in the post-treated coating is greater than 2 and less than 20, and a method for post-treating a zinc-based plated steel sheet. According to this, the zinc-based plated steel sheet having the post-treated coating formed thereon has the effects excellent in lubricity, weldability, adhesiveness, film-removing property and paintability. As the method of post-treating a zinc-based plated steel sheet of the present invention employs a simple coating method irrespective of the kind of plating layer, the process is simple and economical and the process operation cost is low.

Abstract: A method of case hardening toothed gearing using low (LH) or specified hardness (SH) steel and using through surface hardening (TSH) in order to create a described case hardening pattern which increases the fatigue strength of the gear tooth.

Abstract: A substrate film forming machine table and a usage method. The substrate film forming machine table comprises: a first substrate bearing inlet and outlet chamber; a second substrate bearing inlet and outlet chamber; a film forming chamber; an intermediate chamber; a pump set connected to the first substrate bearing inlet and outlet chamber; a second pump connected to the intermediate chamber; a third pump connected to the film forming chamber and the second substrate bearing inlet and outlet chamber; at least one backup pump, which is provided to connect to the film forming chamber and the second substrate bearing inlet and outlet chamber so as to extract air from the film forming chamber and the second substrate bearing inlet and outlet chamber when the third pump is damaged; or, connecting to the intermediate chamber so as to extract air from the intermediate chamber when the second pump is damaged.

Abstract: The invention relates to a method for producing a metal component coated by a hard-material coating, which method comprises the method steps of preparing an anti-caking agent, adding the prepared anti-caking agent to a powder mixture, providing the powder mixture, providing the substrate made of metal, heating the powder and the substrate in a heating device, depositing a coating on the substrate, the coating having a higher hardness than the substrate, and cooling the substrate.

Abstract: A dry powder MOCVD vapor source system is disclosed that utilizes a gravimetric powder feeder, a feed rate measurement and feeder control system, an evaporator and a load lock system for continuous operation for thin film production, particularly of REBCO type high temperature superconductor (HTS) tapes.

Abstract: Described herein is a technique capable of improving an operation rate of an apparatus using a plurality of detoxification apparatuses by removing by-products adhered thereto. According to one aspect of the technique, a processing apparatus includes a controller configured to perform a process recipe of forming a film on a substrate, The controller performs: (a) when an operation state of the first detoxification apparatus is an operation-in-progress state, checking an operation state of the second detoxification apparatus; (b) when the operation state of the second detoxification apparatus is not a maintenance-in-progress state, starting an operation of the second detoxification apparatus and switching the operation state of the first detoxification apparatus to the maintenance-in-progress state; and (c) when the operation state of the second detoxification apparatus is the maintenance-in-progress state, continuing an operation of the first detoxification apparatus.

Abstract: A method of processing a substrate according to a PECVD process is described. Temperature profile of the substrate is adjusted to change deposition rate profile across the substrate. Plasma density profile is adjusted to change deposition rate profile across the substrate. Chamber surfaces exposed to the plasma are heated to improve plasma density uniformity and reduce formation of low quality deposits on chamber surfaces. In situ metrology may be used to monitor progress of a deposition process and trigger control actions involving substrate temperature profile, plasma density profile, pressure, temperature, and flow of reactants.

Abstract: According to one aspect of the technique, there is provided a substrate processing apparatus including: a process chamber in which a substrate is processed; a first gas supply system configured to supply a first gas onto the substrate in the process chamber and including a plurality of tanks configured to store the first gas, wherein the first gas is heated in the plurality of the tanks; and a controller configured to control the first gas supply system such that the first gas is supplied onto the substrate in the process chamber while switching among the plurality of the tanks.

Abstract: An apparatus for controlling precursor flow. The apparatus may include a processor; and a memory unit coupled to the processor, including a flux control routine. The flux control routine may be operative on the processor to monitor the precursor flow and may include a flux calculation processor to determine a precursor flux value based upon a change in detected signal intensity received from a cell of a gas delivery system to deliver a precursor.

Abstract: There is provided a technique that includes: process chamber processing substrate; gas supply system supplying precursor gas into the process chamber; exhaust pipe connected to vacuum pump and evacuating inside of the process chamber; gas concentration sensor configured to measure concentration of the precursor gas passing through the exhaust pipe at front stage of the vacuum pump; a pressure sensor measuring pressure in the exhaust pipe at rear stage of the vacuum pump; dilution gas supply system supplying dilution gas into the vacuum pump or the exhaust pipe at the front stage; and a controller controlling the dilution gas supply system to supply the dilution gas into the vacuum pump or the exhaust pipe at the front stage at low rate corresponding to the measured concentration of the precursor gas and the measured pressure in the exhaust pipe at the rear stage.

Abstract: A metalizing bath for an electroless plating system includes a metal ion source, a reducing agent, insoluble particulate matter, and stabilizing components, wherein the stabilizing components comprise at least one anionic surfactant and at least one cationic surfactant.

Abstract: A nickel-boron coating deposited on a substrate which comprises nickel, boron and a material selected from bismuth, tin, tellurium, selenium, indium and gallium.

Abstract: Provided is an aluminum alloy fastening member including a chemical conversion coating having a novel composition as a colored coating, and a method for producing the aluminum alloy fastening member. The aluminum alloy fastening member includes a chemical conversion coating containing tellurium as a component element.

Abstract: A method of molding a metalized composite part. The method comprises: introducing particles comprising at least one metal into a gas stream; directing the gas stream toward a surface of a thermoplastic composite part, thereby depositing a metal layer on the composite part to form a metallized composite part; and molding the metallized composite part to introduce a bend without delamination of the metal layer from the metallized composite part.

Abstract: A method of manufacturing a gear shaft including depositing only a first material via directed energy deposition (DED), forming a first portion of the gear shaft via the depositing only the first material via directed energy deposition (DED), forming a transitioning portion of the gear shaft via depositing of a varying ratio of the first material with a second material via DED, and forming a second portion of the gear shaft via the depositing via DED of only the second material.

Abstract: This Sn-plated steel sheet includes: a base plated steel sheet having a steel sheet, and a Sn-plated layer on at least one surface of the steel sheet; and a film layer which contains a zirconium oxide and a tin oxide and is positioned on the base plated steel sheet. An adhesion amount of Sn per surface of the Sn-plated steel sheet is 0.1 g/m2 or more and 15 g/m2 or less, an amount of the zirconium oxide in the film layer is in a range of 1 mg/m2 or more and 30 mg/m2 or less in terms of an amount of metal Zr, a peak position of a binding energy of Sn3d5/2 of the tin oxide by X-ray photoelectron spectroscopy in the film layer is within a range of 1.4 eV or more and less than 1.6 eV from a peak position of a binding energy of metal Sn, and a quantity of electricity required for reduction of the tin oxide is in a range of more than 5.0 mC/cm2 and 20 mC/cm2 or less.

Abstract: An electrolysis system and an electrolysis method wherein the electrolysis system includes a pressure-electrolytic cell and a throttle in the catholyte line, by which the catholyte flow can be divided into a gas and liquid phase. In this way, (by-)products of the electrolysis can be recycled, while the electrolytic cell can be operated effectively at a high pressure.

Abstract: The present invention provides an integrated system comprising: an electrocatalysis device, in which an oxidation reaction is carried out at an anode by an electrocatalysis of glycerol, and at a cathode hydrogen is produced through a reduction reaction; and a chemical catalysis device for producing butene oligomers from lignocellulosic biomass through a hydrogenation process, wherein the hydrogen produced by the electrocatalysis device is used for the production of the butene oligomers by the chemical catalysis device, and a thermal energy of the electrocatalysis device and the chemical catalysis device is exchanged with each other.

Abstract: There is disclosed an improved Kolbe reactor system for converting electrical power into a hydrocarbon fuel and hydrogen. More specifically, the present disclosure provides a Kolbe reactor system comprising an open cavity Kolbe reactor and an initial hydrocarbon chemical formulation comprising from about 3N to about 6N C2-C5 carboxylic acid and from about 2M to about 4M alkali C2-C5 carboxylate, wherein the C2-C5 carboxylate and carboxylic acid have the same carbon alkyl length. The Kolbe reactor system can be continuously fed with C2-C5 carboxylic acid to maintain the initial formulation for a continuous process. Electrical energy is stored by converting the carboxylic acid to hydrocarbon fuel and hydrogen, and is recovered by combustion of the hydrocarbon fuel and hydrogen, and or conversion in a hydrogen fuel cell.

Abstract: An electrolytic method of loading hydrogen into a cathode includes placing the cathode and an anode in an electrochemical reaction vessel filled with a solvent, mixing a DC component and an AC component to produce an electrolytic current, and applying an electrolytic current to the cathode. The DC component includes cycling between: a first voltage applied to the cathode for a first period of time, a second voltage applied to the cathode for a second period of time, wherein the second voltage is higher than the first voltage, and wherein the second period of time is shorter than the first period of time. The peak sum of the voltages supplied by the DC component and AC component is higher than the dissociation voltage of the solvent. The AC component is selected based on a local minimum of a Nyquist plot to minimize energy loss while maintaining hydrogen transport.

Abstract: A vapor deposition metal mask substrate includes a nickel-containing metal sheet including a obverse surface and a reverse surface, which is opposite to the obverse surface. At least one of the obverse surface and the reverse surface is a target surface for placing a resist layer. The target surface has a surface roughness Sa of less than or equal to 0.019 ?m. The target surface has a surface roughness Sz of less than or equal to 0.308 ?m.

Abstract: Provided herein is a method for preparing MXenes, such as Ti2CTx, Cr2CTx, and V2CTx, products prepared therefrom, and compositions and devices including the same.

Abstract: Systems and methods for extracting lithium metal ions from a lithium containing ore such as spodumene or lithium salts are provided. The lithium ore or salt is suspended in a hydroxide salt or eutectic and heated to produce a molten salt suspension that is used to electroplate lithiated transition metal oxides on an electrode. Lithium metal or lithium ions can be isolated from the deposited lithiated transition metal oxides. A second metal ore may be included in the suspension and processed with the lithium ore.

Abstract: A method of forming a wear-resistant coating on an article includes depositing a chromium coating on a substrate of the article, and subsequently heating the coated article to enhance a plurality of through-cracks within the chromium coating.

Abstract: A steel sheet coated with a coating comprising from 10 to 40% of nickel, the balance being zinc, such steel sheet having a microstructure comprising from 1 to 50% of residual austenite, from 1 to 60% of martensite and optionally at least one element chosen from: bainite, ferrite, cementite and pearlite, and the following chemical composition in weight: 0.10<C<0.50%, 1.0<Mn<5.0%, 0.7<Si<3.0%, 0.05<Al<1.0%, 0.75<(Si+Al)<3.0% and on a purely optional basis, one or more elements such as Nb?0.5%, B?0.005%, Cr?1.0%, Mo?0.50%, Ni?1.0%, Ti?0.5%, the remainder of the composition making up of iron and inevitable impurities resulting from the elaboration.

Abstract: An advanced electrodeposited copper foil and a copper clad laminate using the same are provided. The advanced electrodeposited copper foil has an uneven micro-roughened surface. As observed by a scanning electron microscope operated with a +35 degree tilt and under 1,000× magnification, the uneven micro-roughened surface has a plurality of production direction stripes formed by copper crystals.

Abstract: An advanced electrodeposited copper foil having long and island-shaped microstructures and a copper clad laminate using the same are provided. The advanced electrodeposited copper foil includes a micro-roughened surface. The micro-roughened surface has a plurality of copper crystals, a plurality of copper whiskers and a plurality of copper crystal groups which are in a non-uniform distribution and form into a long and island-shaped pattern.

Abstract: A coating method for a cationic electrodeposition coating material includes: a step of immersing a metallic article to be coated in a first solution bath, a step of immersing the article in a second solution bath and a step of immersing the article in a third solution bath; and at least one of the three steps includes a cationic electrodeposition coating in which a current is applied. A coating film formed through the three steps contains at least: a base resin component (A), a reaction component (B) and a catalyst (C). The first solution bath, the second solution bath and the third solution bath contain the base resin component (A), the reaction component (B) and the catalyst (C) in a combination of one or two of the components.

Abstract: An insulated conductor of the present invention is an insulated conductor having a conductor and an insulating film provided on a surface of the conductor, in which the insulating film has a low-concentration fluorine layer disposed on a surface side of the conductor and a high-concentration fluorine layer disposed on at least a part of an outside surface of the low-concentration fluorine layer, the low-concentration fluorine layer includes a cured product of a thermosetting resin and a fluororesin and has a fluorine atom content relatively lower than that of the high-concentration fluorine layer, and the high-concentration fluorine layer includes a cured product of a thermosetting resin and a fluororesin and has a fluorine atom content relatively higher than that of the low-concentration fluorine layer.

Abstract: Methods and apparatus for reducing the formation of insoluble deposits in semiconductor electrochemical plating equipment or a surface thereof during electrochemical plating, including: removing electrochemical plating equipment or a surface thereof from an electroplating solution, wherein residual electroplating solution is disposed atop the electrochemical plating equipment or a surface thereof, and wherein the residual electroplating solution has a first pH; contacting the residual electroplating solution with a rinse agent having a second pH similar to the first pH to form a rinsate; and removing the rinsate from the electrochemical plating equipment or a surface thereof.

Abstract: A convection pattern estimation method of a silicon melt includes: applying a horizontal magnetic field of 0.2 tesla or more to a silicon melt in a rotating quartz crucible with use of a pair of magnetic bodies disposed across the quartz crucible; before a seed crystal is dipped into the silicon melt to which the horizontal magnetic field is applied; measuring temperatures at a first and second measurement points positioned on a first imaginary line that passes through a center of a surface of the silicon melt and is not in parallel with a central magnetic field line of the horizontal magnetic field as viewed vertically from above; and estimating a direction of a convection flow in a plane in the silicon melt orthogonal to the direction in which the horizontal magnetic field is applied on a basis of the measured temperatures of the first and second measurement points.

Abstract: A roller guide assembly for use in lifting a seed coupled to a cable includes a mounting plate, a shaft, and a roller guide. The mounting plate has a throughhole. The shaft is coupled to the mounting plate such that the shaft is movable relative to the mounting plate in a direction that is generally perpendicular to a central axis of the shaft. The roller guide is rotationally coupled about the shaft and generally positioned within the throughhole of the mounting plate such that at least a portion of the roller guide extends out of the throughhole.

Abstract: An apparatus and method for molecular beam epitaxy are described herein. The apparatus comprises an enclosure defining a vacuum chamber. A substrate holder is mounted within the vacuum chamber. At least one molecular beam source is in fluid communication with the vacuum chamber. A cooling shroud having at least one surface is mounted within the vacuum chamber spaced from the substrate holder. A cryocooler having at least a portion extending into the vacuum chamber is operatively coupled to the cooling shroud for extracting heat therefrom, and cooling the at least one surface of the cooling shroud to cryogenic temperatures.

Abstract: A convection pattern control method includes: heating a silicon melt in a quartz crucible using a heating portion; and applying a horizontal magnetic field to the silicon melt in the quartz crucible being rotated. In the heating of the silicon, the silicon melt is heated with the heating portion whose heating capacity differs on both sides across an imaginary line passing through a center axis of the quartz crucible and being in parallel to a central magnetic field line of the horizontal magnetic field when the quartz crucible is viewed from vertically above. In the applying of the horizontal magnetic field, the horizontal magnetic field of 0.2 tesla or more is applied to fix a direction of a convection flow in a single direction in a plane orthogonal to an application direction of the horizontal magnetic field in the silicon melt.

Abstract: Embodiments generally relate to methods for depositing silicon-phosphorous materials, and more specifically, relate to using silicon-phosphorous compounds in vapor deposition processes (e.g., epitaxy, CVD, or ALD) to deposit silicon-phosphorous materials. In one or more embodiments, a method for forming a silicon-phosphorous material on a substrate is provided and includes exposing the substrate to a deposition gas containing one or more silicon-phosphorous compounds during a deposition process and depositing a film containing the silicon-phosphorous material on the substrate. The silicon-phosphorous compound has the chemical formula [(R3-vHvSi)—(R2-wHwSi)n]xPHyR?z, where each instance of R and each instance of R? are independently an alkyl or a halogen, n is 0, 1, or 2; v is 0, 1, 2, or 3; w is 0, 1, or 2; x is 1, 2, or 3; y is 0, 1, or 2; z is 0, 1, or 2, and where x+y+z=3.

Abstract: Provided are compositions and methods for preparing and identifying antibodies having CDR3s that vary in sequence and in length from very short to very long which in certain embodiments may bind to a carbohydrate moiety or the active site of an enzyme. Libraries coding for antibodies with the CDR3s are also provided. The libraries can be provided by modifying a pre-existing nucleic acid library.