Abstract: Lost circulation material (LCM) compositions may include a resin; an emulsifier selected from the group consisting of ethoxylated phenol, sodium salt of modified tall oil fatty amide, carboxylic acid terminated fatty polyamide, modified amidoamine, tall oil fatty acid, oxidized tall oil fatty amidoamine, ether carboxylic acid, and combinations thereof; a crosslinker, a cementitious and/or weighting agent; a retarder; a dispersant; and a silicon-based defoamer. The LCM compositions may have a thickening time of from about 3 hours than about 6 hours by reaching a Bearden consistency of 100 Bc. Methods of eliminating or reducing lost circulation in a lost circulation zone from a well may include introducing these LCM compositions into the well.

Abstract: A method of making a chemical-resistant concrete composition, namely a quartz-based casting composition, is provided. The quartz-based casting composition provides excellent resistance to attack by chemicals, including weak and strong acids. The quartz-based casting composition is useful as concrete in various construction applications where corrosion resistance is needed. The casting composition includes a dry component and a wet component. The dry component includes about 25% to about 100% by weight quartz and the corrosion resistance increases with increasing quartz content.

Abstract: A method for plugging and sealing subsurface formations using alkaline nanosilica dispersion and a delayed activation chemistry includes introducing a mixture with a first pH into the subsurface formation. The mixture comprises an aqueous solution, an alkaline nanosilica dispersion and a water-insoluble hydrolyzable compound. The method further includes allowing the water-insoluble hydrolyzable compound to hydrolyze in the subsurface formation to form an acid at 70° C. or greater, thereby acidizing the mixture to a reduced second pH and causing the alkaline nanosilica dispersion to gel into a solid and seal the subsurface formation. A composition for sealing a subsurface formation includes an aqueous mixture including water, an alkaline nanosilica dispersion, and a water-insoluble hydrolyzable compound.

Abstract: A method for controlling loss circulation in a subterranean formation. The method includes circulating in a wellbore a nanosilica drilling fluid having a pH in a range of from about 8 to about 11 and a gel pH of less than 8, where the nanosilica drilling fluid includes an aqueous-based drilling mud and an alkaline nanosilica dispersion. The method also includes introducing into the nanosilica drilling fluid an amount of a chemical activator sufficient to produce a convertible drilling mud where the chemical activator is an acid and the pH of the convertible drilling mud is less than the gel pH. The method also includes allowing the convertible drilling mud to convert into the solid gel lost circulation material. A convertible drilling mud operable to convert into a solid gel lost circulation material is also provided.

Abstract: A method for controlling loss circulation. The method includes introducing into a wellbore a nanosilica drilling fluid comprising water and an alkaline nanosilica dispersion. The method further includes introducing into the nanosilica drilling fluid an amount of a chemical activator comprising a water soluble hydrolysable polyester to produce a convertible drilling mud where the convertible drilling mud has an initial pH between 8 and 11 upon formation. The method also includes allowing the chemical activator to hydrolyze to produce an acid and reduce the pH of the convertible drilling mud to less than a gel pH, thereby converting the convertible drilling mud into a solid gel lost circulation material. A convertible drilling mud operable to convert into a solid gel lost circulation material is also provided.

Abstract: The embodiments described herein generally relate to methods and chemical compositions for use with cementing processes. In one embodiment, a composition is provided comprising a random tetracopolymer having the formula styrene-butadiene-acrylic-fumaric acid, a polyvinyl acetate, and a nonionic surfactant.

Abstract: Methods are provided of inhibiting subterranean groundwater flow through a window in frozen soil including (i) introducing at least one conductor having at least one discharge aperture in proximity to the window; and (ii) discharging a grout material including C-18 alpha olefin or a combination of C-16 alpha olefin and C-18 alpha olefin in a flowable state from the at least one conductor, wherein the grout material, upon being discharged, permeates into surrounding soil materials generally without displacement thereof and wherein the grout forms a barrier to inhibit subterranean groundwater flow through the window.

Abstract: The present disclosure relates to a bentonite modifier, comprising a water-soluble thiosulfate, a water-soluble alcohol compound, and a water-soluble amine compound, wherein the amounts of thiosulfate, the alcohol compound, and the amine compound are in the ratio of (0.3˜1):(0.3˜1):(0.3˜1). The present disclosure further relates to a bentonite-containing cement additive capable of resisting permeation and salt corrosion, comprising bentonite and said modifier, wherein the content of the bentonite modifier is 0.2˜5% of the bentonite by weight. Meanwhile, the present disclosure also provides use of the modified bentonite.

Abstract: Process for the preparation of cement/mortar/concrete compositions or systems, (for simplicity hereafter “cement” compositions or systems or even “cements”), of a generally known type containing low or medium (standard) “filler(s)”, and/or optionally HP filler(s), as carbonate-based filler(s), namely coarse low or medium calcium carbonate(s), namely coarse marble(s); Product comprising, or consisting of, the pre-blend (A) of coarse, low or medium (or optionally HP) “calcium carbonate-based filler” pre-blended with at least an UF; Aqueous compositions (B) obtained by mixing the above pre-blend (A) of coarse filler(s) with UF(s) with an aqueous system such as mix water, aqueous mix fluid; Product (C) consisting of, or comprising, the pre-blend (A) or the compositions (B), treated or pretreated with at least one superplastifier or aqueous system containing superplastifier(s); Cement and Use of cement.

Abstract: The invention is directed to a construction material and to the use of modified layered inorganic material. The construction material of the invention comprises a layered inorganic material, which layered inorganic material comprises an ionic organic modifier compound and a biocide. The construction material of the invention has increased resistance against microbial fouling.

Abstract: A cementitious composition including at least one cementitious and/or pozzolanic material and at least one desugared molasses. A method of preparing a cementitious composition including forming a mixture of water, at least one cementitious and/or pozzolanic material and at least one desugared molasses. An admixture for cementitious compositions including: (i) at least one desugared molasses; and (ii) at least one alkanolamine and/or at least one polyhydroxyalkylamine.

Abstract: Process for the preparation of cement/mortar/concrete compositions or systems, (for simplicity hereafter “cement” compositions or systems), featuring an improved compressive strength Rc namely at 28 days and 90 days, containing at least a “carbonate-based filler”, comprising at least one step where the said at least one “carbonate-based filler” is mixed or blended with at least one aluminosiliceous material, and the obtained “fillers blend” is treated with an efficient treating amount of at least one treating agent consisting of or comprising superplastifier(s); PRODUCT comprising at least a “carbonate-based “filler”” as defined and at least an aluminosiliceous material, what provides a “fillers blend”; cement compositions, use of the said “fillers(s) blends” and cement composition; cement elements or cement products” obtained from the said “cements compositions”, such as construction or building blocks.

Abstract: Skins and/or adhesive layers are formed on a porous ceramic honeycomb by applying a layer of a cement composition to a surface of the honeycomb and firing the cement composition. The cement composition contains a water-swellable clay, high aspect inorganic filler particles and water, and are nearly or completely devoid of particles smaller than 100 nm and a cellulosic polymer.

Abstract: A pre-mixed mortar, stucco or masonry composition includes from 70 to 80 percent sand and from 20 to 30 percent of a light-weight cement mix composition that comprises either slag cement, Gypsum or a combination of slag cement and gypsum; Portland cement; clay; and polystyrene.

Abstract: The present invention provides a method for making sand compositions wherein manufactured sand particles are pretreated with a clay-mitigating polycation and blended with natural sand particles that have washed to remove fines such that at least 90% of the natural sand particles are retained on a 75 micron sieve. Methods of the invention also involve the use of the blended pretreated sand for making concrete wherein the sand is combined with cement, a polycarboxylate type dispersant, a further amount of clay-mitigating polycation compound, and at least one hydryoxyl or hydroxyl carboxylic acid or salt compound.

Abstract: A lightweight concrete composition is mixed from cement, sand, water, and organic material, and placed on an area of soil, proximal a body of water, to protect the soil from erosion and the like due to water action. Preferably, the organic material comes from the area in which the soil is being stabilized, and may include soil, leafy matter, and ground up wood, forming a particulate organic material. Preferably, the final density of the resulting lightweight concrete composition is greater than the density of the water in the body of water, and less than the density of the soil being stabilized. A representative density range is between 62.43 pounds per cubic foot and 100.00 pounds per cubic foot.

Abstract: A composition used for high-strength impermeable concrete. The composition contains sand, stone, cement, water reducer, water and reinforced impermeable sand. The reinforced impermeable sand includes aeolian sand and binder covering the surface of the aeolian sand. The reinforced impermeable sand can fill the gap between the sand and the stone, and well combine various components in the composition, and suppress the seepage phenomenon of the molded concrete, thereby greatly improving the strength and impermeability of the concrete.

Abstract: The present invention relates to a rheology modifier for ceramic glazes comprising a water-swellable granulated clay, a carboxymethyl cellulose and possibly another natural gum. In another aspect the invention relates to the ceramic glaze and the glaze slip obtained using the above rheology modifier, which can be used for glazing green or fired ceramic bodies such as artware, tableware, tile, heavy clays products and sanitaryware.

Abstract: The present invention provides methods, admixture compositions for treating clay-bearing aggregates used for construction purposes, and aggregate compositions for construction purposes. The clay-bearing aggregates are treated with a cationic copolymer made from two and preferably three different monomer components. Cementitious compositions containing the treated aggregates are also described.

Abstract: The present invention provides a method for making sand compositions wherein manufactured sand particles are pretreated with a clay-mitigating polycation and blended with natural sand particles that have washed to remove fines such that at least 90% of the natural sand particles are retained on a 75 micron sieve. Methods of the invention also involve the use of the blended pretreated sand for making concrete wherein the sand is combined with cement, a polycarboxylate type dispersant, a further amount of clay-mitigating polycation compound, and at least one hydryoxyl or hydroxyl carboxylic acid or salt compound.

Abstract: The present invention provides methods, admixture compositions for treating clay-bearing aggregates used for construction purposes, and aggregate compositions for construction purposes. The clay-bearing aggregates are treated with a cationic copolymer made from two and preferably three different monomer components. Cementitious compositions containing the treated aggregates are also described.

Abstract: A method for inerting clays in a hydraulic composition includes one step of putting a hydraulic composition or a constituent of a hydraulic composition in contact with a compound of the following formula (I): R—COO?, (Mn+)1/n??(I), A hydraulic composition including the compound of formula (I), a method for preparing the hydraulic composition, a pretreated granulate which may be obtained by mixing a granulate with the compound of formula (I), and an additive for inerting clays including a superplasticizer and the compound of formula (I) are also described.

Abstract: A method of controlling release of an admixture in a cement-based composition involves intercalating an admixture (e.g. an accelerator, a set retarder, a superplasticizer) for the cement-based composition into a layered double hydroxide or mixture thereof. A cement-based composition prepared in such a manner and containing a cement-based material (e.g. cement, mortar or concrete) has better workability, especially in respect of slump-loss characteristics.

Abstract: A cementitious composition is formed from a dry mix including a quantity of cement; a quantity of silica and a plurality of fibers. The cementitious composition further includes a quantity of water and a complex admixture of cement additives. The complex admixture includes superplasticizer, shrinkage reduction agent and a non-ionic surfactant in a predetermined quantity per hundred pounds of dry mix.

Abstract: A method of servicing a wellbore in a subterranean formation, comprising preparing a cement composition comprising water and a cementitious material, wherein the cementitious material further comprises blast furnace slag, vitrified shale, calcium sulfate hemi-hydrate or combinations thereof, and placing the cement composition in the wellbore. A cement composition comprising water and a cementitious material, wherein the cementitious material further comprises blast furnace slag, vitrified shale, calcium sulfate hemi-hydrate or combinations thereof. A cement composition comprising water and a cementitious material, wherein the cementitious material further comprises blast furnace slag.

Abstract: This process allows the attainment of cementitious materials and activated artificial pozzolana, developed as from shale oils and/or residues of its processing, hereinafter simply called “shale oil”, mixed among them and/or with clays when placed in the rotation oven, in proportion that vary from 1% to 100% of the shale oils in the mixture. These shale oils or mixtures of shale oil with clays, when burn in temperatures between 600° C. and 900° C., in a horizontal oven, in reducing conditions, generate the so called cementitious materials or activated artificial pozzolana, when in contact with the water, providing to the material agglomerating properties.

Abstract: A method of manufacturing a cementitious composite including: (1) mixing an extrudable cementitious composition by first forming a fibrous mixture comprising fibers, water and a rheology modifying agent and then adding hydraulic cement; (2) extruding the extrudable cementitious composition into a green extrudate, wherein the green extrudate is characterized by being form-stable and retaining substantially a predefined cross-sectional shape; (3) removing a portion of the water by evaporation to reduce density and increase porosity; and (4) heating the green extrudate at a temperature from greater than 65° C. to less than 99° C. is disclosed. Such a process yields a cementitious composite that is suitable for use as a wood substitute. Particularly, by using higher curing temperatures for preparing the cementitious building products, the building products have a lower bulk density and a higher flexural strength as compared to conventional products.

Abstract: A well treatment composition comprises: a water-soluble, organic liquid, wherein the organic liquid: (A) comprises the continuous phase of the well treatment composition; and (B) comprises a polyglycol or a derivative of polyglycol; a fluid loss additive, wherein the fluid loss additive: (A) is insoluble in the organic liquid; and (B) comprises a high molecular weight, water-swellable polymer; and a suspending agent, wherein the suspending agent comprises an organophilic clay, wherein the well treatment composition has an activity of at least 15%. A method of cementing in a subterranean formation comprises: introducing a cement composition into the subterranean formation, the cement composition comprising: (i) cement; (ii) water; and (iii) the well treatment composition; and allowing the cement composition to set after introduction into the subterranean formation.

Abstract: A process for the preparation of the healing agent in cement-based materials and structures, wherein said healing agent comprises organic compounds and/or bacteria-loaded porous particles, which porous particles comprise expanded clay- or sintered fly-ash. Furthermore, said porous particles are intact spheres, broken or crushed particles derived from said intact spheres, having a specific density between 0.4 and 2 g cm?3.

Abstract: A method of making a pigment comprising a dye and a clay having pores. The method includes mixing a first reaction component with first and second dye components to form a reaction mixture, wherein the first reaction component comprises the clay and a catalyst associated with the clay, wherein the first and second dye components are adapted to react with each other in the presence of the catalyst to form the dye, and whereupon the catalyst catalyzes the reaction of the first and second dye components, and at least some of the first and second dye components react within the pores.

Abstract: A method of making a stable, sulfur binding composite containing elemental sulfur, a solid aggregate, and an organic modifier is claimed. The resulting sulfur composite compositions are also claimed.

Abstract: This invention relates to a powder comprising a carrier material which is in powdery form and selected from the group consisting of a water-soluble polymer, a water-insoluble polymer, and an inert inorganic material, and a mixture containing at least about 5 wt. % of a compound having the formula (1-a) and at least about 5 wt. % of a compound having the formula (1-b), HO—(R2O)m—H (1-a), R1aO—(R2aO)n—H (1-b). Claimed also are a process to make the powder, its use, as well as a dry mortar formulation containing the same.

Abstract: The present invention relates to the use of polycationic compound in combination with a hydroxycarboxylic acid or salt thereof to enhance slump retention in cements and concretes having clay-bearing aggregates, wherein the clay otherwise absorbs or diminishes the dosage efficiency of polycarboxylate superplasticizers.

Abstract: A controlled release formulation for a cement-based composition can be produced by intercalating an admixture (e.g. an accelerator, a set retarder, a superplasticizer) for the cement-based composition into a layered inorganic material (e.g. a layered double hydroxide (LDH)). A cement-based composition containing a cement-based material (e.g. cement, mortar or concrete) and such a controlled release formulation has better workability, especially in respect of slump-loss characteristics. With such a formulation release of an admixture in a cement-based composition may be controlled.

Abstract: Disclosed herein are defoamers comprising ethylene glycol, a defoaming hydrocarbon base fluid, and a non-ionic surfactant wherein the hydrocarbon base fluid comprises an internal olefin or a straight-chain n-alcohol, and wherein the non-ionic surfactant is present in the defoamer in an amount in the range of from about 1% to about 10% by weight of the defoamer. Also disclosed herein are cement compositions comprising water, hydraulic cement, and a defoamer, wherein the defoamer comprises ethylene glycol, a non-ionic surfactant, and a defoaming hydrocarbon base fluid wherein the hydrocarbon base fluid comprises an internal olefin or a straight-chain n-alcohol, and wherein the non-ionic surfactant is present in the defoamer in an amount in the range of from about 1% to about 10% by weight of the defoamer.

Abstract: Geopolymer composite materials having low coefficient of thermal expansion are disclosed. The materials are useful in high temperature applications due to their low coefficient of thermal expansion and high strength. Also disclosed is a boron modified water glass geopolymer composition that is compatible with ceramic particulate material such as cordierite and fused silica. The geopolymer composite may be extruded to form structures such as honeycomb monoliths, flow filters or used as a plugging or skinning cement and may be fired at temperatures at or below 1100° C. Both the structures and the cement have high green and fired strength, a low coefficient of thermal expansion, and good acid durability. The cost of manufacturing objects using the material of the present invention is substantially reduced, in comparison with typically production methods of cordierite based bodies, due to the substantially shortened firing times.

Abstract: Lightweight composite or “mineral foam” composite materials can be made from reactive materials such as metal oxides. The materials can be prepared from a reaction of metal oxide(s), phosphate(s) and residual materials to which may be added a reactive foaming agent and/or latex polymer to provide enhanced physical properties. The composite materials can have a density of between about 0.35 to 2.25 g/cc, and may be used for many applications including pre-cast structures, in-situ structures, insulating blocks, slabs and composite wall sections, light weight spheres, mixes and coatings.

Abstract: Methods and compositions that comprise sub-micron alumina for accelerating setting of a cement composition. An embodiment includes a method of cementing in a subterranean formation. The method may comprise introducing a cement composition into the subterranean formation, wherein the cement composition comprises hydraulic cement, sub-micron alumina, and water. The method further may comprise allowing the cement composition to set in the subterranean formation. Another embodiment includes a cement composition that may comprise hydraulic cement, sub-micron alumina, and water.

Abstract: A clay plaster formulation and application. The clay plaster is a mixture of various clays, and aggregate. This plaster is both functional and decorative and is for use on new and existing construction.

Abstract: The present invention relates to a material composition using mainly yellow soil for molding structures for construction, such as a brick for construction, a heated floor plate, a block for construction, and the like. More particularly, the material composition for construction using mainly yellow soil, includes yellow soil, decomposed granite soil, a small amount of cement serving as a water-curing material, a solidifying agent serving as a material for solidification, acrylic monomers for improving the compactness of tissue to impart waterproofness and strength, and functional powder.

Abstract: Disclosed herein is a composition for solidifying soil and industrial waste. The solidifying composition contains 16-24 wt % of straight asphalt, 0.06-0.10 wt % of an emulsifier for asphalt, 0.8-1.2 wt % of light oil, heavy oil or a mixture thereof, 0.01-0.03 wt % of calcium chloride, 0.8-1.2 wt % of lignin, 0.7-1.3 wt % of an acrylic emulsion-based asphalt modifier, 0.13-0.21 wt % of sodium hydroxide, 0.22-0.34 wt % of oleic acid, and the balance of water. A solidified material formed using this solidifying composition has increased density, strength and elasticity, improved durability and a short curing time. Furthermore, the solidifying composition enables soil and industrial waste to be recycled as a substitute for stone materials, such that it allows material sources to be readily secured in public or construction work fields, leading to a reduction in construction cost, and can also contribute to the preservation of the natural environment.

Abstract: There are provided a method for manufacturing various products needed in an actual life which may be implemented in combination with a refiner for refining plants by a mechanical method, a method for refining plants, a molding mixture which is made by mixing refined fiber, clay and water and molds and dries as an interior decorative material for architecture, a heat keeping, adiabatic, sound proof, fireproof board, brick and block, a decorative design (cement mortar) mixture, a fiber having an enhanced tensional force, a cement board which has an architecture interior and exterior heat keeping, adiabatic, soundproof, fireproof functions manufactured by mixing cement and water, a cement material, a fiber board manufactured by mixing fiber and adhesive material, paper made of fiber, thread woven with fiber, and a fiber heat keeping material made of fiber.

Abstract: A novel cement slurry composed of cement and water that can be used in cement stabilization applications. The cement slurry compound itself is chemically treated, by means of a cellulosic or other thixotropic thickening agent(s) to create a thixotropic system wherein the wetted cement remains in suspension and does not settle out prior to use even without further mixing. A chemical retarder/stabilizer is also used to prevent the slurry from prematurely setting during shipping. A novel apparatus and method for mixing the novel cement slurry is disclosed to insure the exact proportioning of all ingredients and the proper wetting of the cement.

Abstract: A downhole servicing composition comprising from about 15 percent to about 80 percent by weight of a clay, and from about 10 percent to about 75 percent by weight of a carbon source is disclosed. The invention includes a downhole servicing composition comprising from about 15 percent to about 45 percent by weight of a first clay, from about 15 percent to about 45 percent by weight of a second clay, from about 10 percent to about 35 percent by weight of a filler, and from about 10 percent to about 75 percent by weight of a carbon source. The invention also includes a downhole servicing composition comprising an aqueous base and from about 10 percent to about 75 percent by weight of flaked graphite, wherein the downhole servicing composition has a thermal conductivity not less than about 0.8 BTU/hr-ft-° F.

Abstract: Disclosed herein are a method for solidifying soil and industrial waste and a solidified material prepared thereby. The solidified material of soil and industrial waste is prepared by adding 2-6 parts by weight of a 3-5-fold dilution of a solidifying agent and 3-15 parts by weight of cement to 100 parts by weight of soil, industrial waste or a mixture of two or more thereof. The solidified material prepared according to this method has excellent density, strength, elasticity and durability, and thus can be used as a substitute for stone material. Also, it can be advantageously used in high-temperature and high-humidity areas, because external impact or pressure is relieved because it is absorbed by asphalt.

Abstract: Methods and cement compositions are provided for sealing a subterranean zone penetrated by a wellbore, wherein the cement composition comprises zeolite, cementitious material, and a mixing fluid.

Abstract: The present invention provides a novel method to produce grade road base material using recycled oilfield waste, called “oil and gas waste,” more specifically, drilling waste and aggregate and a novel road base material. Hydration and mixing of the waste materials along with a binder, will achieve an irreversible pozzolanic chemical reaction necessary for stabilization into a road base. An asphalt emulsifier may be included in the binder to manufacture asphalt stabilized road base. The entire method is a cold batch process.

Abstract: The present invention relates to a thickened aqueous solution, or gel solution, for use in providing fiber to a cement composition. Additionally, the present invention relates to a method for adding fibers to cement.

Abstract: The present invention provides a novel method to produce grade road base material using recycled oilfield waste, called “oil and gas waste,” more specifically, drilling waste and aggregate and a novel road base material. Hydration and mixing of the waste materials along with a binder, will achieve an irreversible pozzolanic chemical reaction necessary for stabilization into a road base. An asphalt emulsifier may be included in the binder to manufacture asphalt stabilized road base. The entire method is a cold batch process.

Abstract: Grout slurries are provided that have high thermal conductivities of greater than about 1.4 Btu/hr-ft-° F. and low hydraulic conductivities ranging from about 5×10?9 cm/s to about 1×10?8 cm/s. Such grout slurries comprise water and a grout composition that is available as a one-sack product. The grout composition includes calcium bentonite present in an amount of from about 15% to about 45%, sodium bentonite present in an amount of from about 15% to about 45%, silica flour present in an amount of from about 10% to about 35%, and flaked graphite present in an amount of from about 10% to about 75%, all by weight of the grout composition. Further, methods of installing a conduit such as a heat transfer loop in a hole in the earth include placing the conduit in the hole, forming the foregoing grout slurry, and placing the grout slurry in the hole adjacent to the conduit.