Abstract: A flexible grout composition and method of disposing the composition in position, in contact with an earthen formation, such as a coating on a trench wall, or within a bore hole, for example to cement a conduit within the bore hole to prevent fluid loss, for sealing and grouting well casings, plugging abandoned wells, and waterproofing earthen structures, particularly in environments where the grout composition is in contact with contaminated water. The flexible grout composition includes a water-swellable clay, such as sodium bentonite; an optional solid particulate filler, such as an essentially nonswellable bentonite clay, such as calcium bentonite, herein defined as a bentonite clay having calcium as the predominant exchangeable cation; a water-soluble polymer; and an optional dispersing agent, such as sodium acid pyrophosphate (SAPP).

Abstract: Improved set retarded cement compositions for cementing subterranean zones in wells at low temperatures having excellent short term compressive strength development and methods of using such compositions are provided. The compositions are basically comprised of a hydraulic cement, water and a copolymer containing 2-acrylamido-2-methylpropane sulfonic acid in an amount in the range of from about 65 to about 85 mole percent and acrylic acid in an amount in the range of from about 15 to about 35 mole percent having an average molecular weight below about 5000.

Abstract: Vibration damping thick-film coating composition comprising a coating composition comprising 100 parts by weight of a binder, from 20 to 200 parts by weight of a hydraulic inorganic filler, from 10 to 150 parts by weight of a filler other than the hydraulic inorganic filler, and from 10 to 7 parts by weight of (a) a cored filler or (b) a cored filler and a synthetic resin powder, and a method of forming the same.

Abstract: Lightweight concrete roof tiles are produced by extruding a latex/cement/lightweight aggregates/water mix in a prescribed sequence. The composition comprises:(a) 45-65 parts by weight of an acrylic latex emulsion;(b) 130-180 parts by weight of a cement;(c) 360-400 parts by weight of expanded shale lightweight aggregates; and(d) 50-75 parts by weight of additional water.This lightweight concrete roof tile of the present invention is about half the weight and about the same strength, and absorbs the same amount of water of conventional roof tiles.

Abstract: A thin protective coating for foam surfaced objects achieving high compression and impact strengths without the need of water curing.

Abstract: A fire resistant and high temperature insulating composition is provided. The composition generally comprises a carbonate material in an amount from about 20% to about 80% by weight, an aluminosilicate in amount from about 0.5% to about 15% by weight, talc in amount from about 0.5% to about 10% by weight, cellulose in amount from about 1% to about 30% by weight, a binder in an amount from about 1% to about 45% by weight, and a gelling agent in an amount from about 1% to about 45% by weight. The binder is preferably a mixture of an organic adhesive such as a polymeric resin, and a non-organic adhesive such as cement, but other adhesives can be used alone or in combination therewith. The gelling agent is preferably a polymeric substance that swells in the presence of a liquid such as superabsorbent polymers. The components are combined and water may be added in an amount from about 1 to about 50% by weight to obtain a composition of the desired consistency.

Abstract: Improved set retarded cement compositions and methods of using such compositions which are substantially non-thinning at high temperatures and which can include fresh or salt water are provided. The compositions are comprised of hydraulic cement, sufficient water to form a pumpable slurry, a set retarder and a delayed viscosifying agent which yields viscosity at high temperatures comprised of a treated depolymerized galactomannan gum.

Abstract: Process for making a cement mixture containing fibers wherein a paste is formed by mixing cement and, per 100 parts by weight of cement, approximately 5 to 20 parts by weight of a first pulverized material of which the grains have an average diameter of between 1/5 and 1/10 of the average diameter of the grains of the cement and approximately 20 to 35 parts by weight of water. The paste is then mixed with reinforcing fibers. The paste may also include a second pulverized material the average grain diameter of which is between 1/5 and 1/10 of the average diameter of the first pulverized material. The invention further includes products made from a cement mixture manufactured according to one of the foregoing processes.

Abstract: Oil field cement liquid fluid loss control additives and methods of field preparing such additives prior to preparing a cement composition containing the additive are provided. The method of field preparing the liquid fluid loss control additive comprises admixing an organophilic clay suspending agent with a liquid hydrocarbon, combining a surfactant with the mixture and then combining at least one hydrophilic polymer with the mixture to form the additive.

Abstract: A grouting composition for sealing a borehole or other cavity contains 90-99.9% finely divided water swellable clay and 0.1-10% polyacrylate thinner having a molecular weight of about 5,000 to 95,000. The grouting composition is mixed with fresh water to provide a completely reswellable, unflocculated, easily placed, low permeability sealing composition. The thinner allows a very high concentration of water-swellable clay in the composition. A preferred grouting composition contains 98-99.9% sodium bentonite and 0.1-2% polyacrylate thinner of molecular weight of about 2,000 to 50,000. In use, 50lb. of the preferred grouting composition is mixed with 11-14 gallons of fresh water, to provide a grouting mixture which includes about 25-40% reswellable solids.

Abstract: What is disclosed is a method of accelerating the set of a retarded cement. The cement may range from a drilling fluid containing dispersants or retarders that will slow down the set of the drilling fluid when cementitious fluid is added thereto, through overwashing, or treating a retarded primary or remedial cement that may have been injected into fractures or areas within a well to overwashing a plug or any volume of retarded cement that needs to be set in a well.The specific uses are discussed.

Abstract: A grouting composition for sealing a borehole or other cavity comprising 90-99.9% finely divided water swellable clay and 0.1-10% thinner. The grouting composition is mixed with fresh water to provide a completely reswellable, unflocculated, easily placed, low permeability sealing composition. The thinner allows a very high concentration of water-swellable clay in the composition. A preferred grouting composition comprises 98-99.9% sodium bentonite and 0.1-2% polyacrylate thinner. In use, 50 lb. of the preferred grouting composition is mixed with 11-14 gallons fresh water, to provide a grouting mixture which comprises about 30-35% reswellable solids.

Abstract: What is disclosed is a method of accelerating the set of a retarded cement. The cement may range from a drilling fluid containing dispersants or retarders that will slow down the set of the drilling fluid when cementitious fluid is added thereto, through overwashing, or treating a retarded primary or remedial cement that may have been injected into fractures or areas within a well to overwashing a plug or any volume of retarded cement that needs to be set in a well.The specific uses are discussed.

Abstract: Set retarded cement compositions for cementing across a zone or zones in a well having enhanced compressive strength and rapid gel strength development after placement. The cement compositions are comprised of hydraulic cement, sufficient fresh water to form a pumpable slurry, a set retarder comprising a copolymer of 2-acrylamido, 2-methylpropane sulfonic acid and acrylic acid having an average molecular weight below about 5000 and any other desired additives. Methods of cementing utilizing the cement composition also are provided.

Abstract: A vinyl grafted lignite fluid loss additive comprising a lignite grafted with at least one vinyl monomer selected from the group consisting of: dimethylaminopropyl methacrylamide, methacrylamido propyltrimethyl ammonium chloride, N-vinylformamide, N-vinylacetamide, diallyl dimethyl ammonium chloride, and diallylamine. The vinyl monomer may also be blended with at least one co-monomer. Preferred co-monomers are: 2-acrylamido-2-methylpropanesulfonic acid, dimethylacrylamide, acrylamide, vinylpyrrolidone, vinylacetate, acrylonitrile, dimethylaminoethyl methacrylate, styrenesulfonate, vinylsulfonate, dimethylaminoethyl methacrylate methyl chloride quaternary, acrylic acid and its salts.

Abstract: The cement slurry of the present invention is gas tight, very low strength retrogression at high temperature, and substantially no tendency to settle or segregate. The cement slurry is made with a hydraulic cement, 5-85% microsilica based on the weight of the cement, 5-250% of a high density filler material based on the weight of the cement, 0-5% of a retarder (dry weight) based on the weight of the cement, 0-12% of a thinner (dry weight) based on the weight of the cement, 0-8% of a fluid loss additive (dry weight) based on the weight of the cement, 0-30% silica flour and/or silica sand based on the weight of the cement and water in such an amount that the cement slurry has a density between 1.95 and 2.40 g/cm.sup.3.

Abstract: A particulate solid activator comprising a porous material containing absorbed ammonium phosphate can be prepared by a process which comprises: heating a slurry of the porous material and an ammonium phosphate solution; and then spray drying the slurry to obtain the particulate solid activator. The porous material can be diatomaceous earth. The resulting particulate solid activator can be dry blended with a magnesium-containing compound, e.g. MgO, and an optional aggregate to form a magnesium phosphate fast-setting cement mixture. This mixture reacts in the presence of an aqueous component at ambient temperature to form a monolithic solid.