With Separator Patents (Class 202/197)
  • Patent number: 5409576
    Abstract: A rotating evaporator device is disclosed for the distillation or concentration of liquids. The rotating evaporator device of the present invention utilizes a multiplicity of pairs of disks wherein each disk pair forms a cavity within which heating vapor condenses on the interior surfaces of the disk pair and evaporation occurs from a thin film of distilland deposited on the outside surfaces of the disk pair by means of flexible wipers pressing on the outside surfaces of the disk pair. The centrifugal force created by the rotation of the disks causes the distillate and distilland films to be very thin resulting in very high heat transfer coefficient. The pairs of disks are joined together at the inside peripheries and are rotated about a stationary hollow shaft wherein heating vapor is introduced into the cavities through ports in the shaft and stationary scoops are connected to the shaft to withdraw the condensate from the circumferential peripheries of the cavities.
    Type: Grant
    Filed: July 16, 1993
    Date of Patent: April 25, 1995
    Inventor: Badawi Tleimat
  • Patent number: 5372680
    Abstract: A plant for processing vegetal stock includes a container mounted on a twheel trailer, and provided with bubblers for live steam which are arranged under a net for accommodation of the vegetal stock, and a detachable cover communicating through a steam pipe with a cooler which communicates with a separator through a distillate admission pipe provided with a splitter for preventing plug-shaped formation of oil therein. The bubblers for live steam are arranged in two planes perpendicular to the axis of the container and mounted in the cover is an additional bubbler.
    Type: Grant
    Filed: March 9, 1993
    Date of Patent: December 13, 1994
    Assignee: Aktsionernoe obschestvo "Sistemy novykh tekhnology" (SINTO Ltd)
    Inventors: Nikolai I. Bezdolny, Vladimir P. Kostylev
  • Patent number: 5354428
    Abstract: Method and apparatus for the distillation of liquids which is particularly suited for the removal of soluble impurities and insoluble and non-volatile particles of 10 microns to 0.2 micron or less in size. A substantially elongated distillation chamber having walls equipped with axially disposed concentric boiling rings spaced from the walls near the bottom, and a packing stop, packing redirector rings for condensed vapor, and a reflux condenser in the upper part of the distillation chamber provide, during distillation, a smooth convective upward flow of distilling liquid and vapor proximate the walls and boiling rings and a smooth convective downward flow of distilling liquid and vapor substantially centrally of the distillation chamber.
    Type: Grant
    Filed: July 25, 1989
    Date of Patent: October 11, 1994
    Assignee: Athens Corp.
    Inventors: R. Scot Clark, Joe G. Hoffman, John B. Davison, David W. Persichini, Wallace I. Yuan, Bruce A. Lipisko, Alan H. Jones, Alan W. Jones
  • Patent number: 5346592
    Abstract: A combined water purification and power generating plant is disclosed having special features designed to maximize the cycle thermal efficiency and salt recovery, with little or no concentrated brine produced therefrom. Using the plant, a volume of salt water is delivered to a plurality of indirect and direct contact feed heaters. Within the direct contact heaters, the salt water is heated and diluted by condensation therein by super-heated steam delivered thereto. Any alkaline salts having reverse solubility characteristics particulate and are filtered therefrom. From the last direct contact feed heater, the diluted salt water is delivered to a plurality of high pressure, high temperature evaporators arranged in a series which are used to further heat, evaporate and filter the salt water in multiple stages thereby improving the plant's efficiency. A steam heater is used to super-heat a steam which delivered to various areas of the plant to heat and evaporate the salt water.
    Type: Grant
    Filed: August 11, 1993
    Date of Patent: September 13, 1994
    Inventor: Anas A. Madani
  • Patent number: 5326436
    Abstract: A method of feeding to a fractionator a feed mixture having a wide-boiling range vapor-liquid mixture is provided. Also, provided is a fractionator feed section adapted to receive a two phase feed mixture and has operational stability when fed a feed mixture which generates significant volume of vapor in the feed section.
    Type: Grant
    Filed: November 19, 1992
    Date of Patent: July 5, 1994
    Assignee: Atlantic Richfield Company
    Inventors: Vijay R. Sampath, David E. Bachmann
  • Patent number: 5259928
    Abstract: Apparatus and method for evaporating a liquid includes a casing; a plurality of vertically extending plate-type heating elements within the casing, each heat element having an outer surface and an inner surface and a vertical edge, the heat elements being spaced and forming an open channel along the vertical edge between adjacent elements; a distributor above the heating elements for distributing the liquid over the elements; an inlet connected to the heating elements for introducing a heating medium and for generating vapor from the liquid; and a wall-like device mounted within the casing facing the spaces between the heating elements for collecting and guiding the vapor generated in the evaporator. Preferably, the wall-like element includes a droplet separating device formed by vertically elongated spaced elements having a substantially U-shaped cross-section with inwardly pointing vertical edges.
    Type: Grant
    Filed: May 14, 1991
    Date of Patent: November 9, 1993
    Assignee: A. Ahlstrom Corporation
    Inventor: Rolf Ryham
  • Patent number: 5248394
    Abstract: A distillation purifying system including a section which creates a vacuum pressure that is transmitted throughout the system, a distillation/purification zone in which fluids to be distilled/purified are treated, and a collection zone in which the distilled/purified liquids are transferred. The system is effective for use with liquids, solutions, fluids and the like and can be used for water treatment as well as bodily fluid treatment.
    Type: Grant
    Filed: March 23, 1992
    Date of Patent: September 28, 1993
    Assignee: FSR Patented Technologies, Ltd.
    Inventors: Barry Schlesinger, Harold Rapp
  • Patent number: 5246541
    Abstract: A falling film evaporator includes a chamber having a top and bottom tube plate; a plurality of vertical tubes each having an interior and exterior surface and extending through the chamber and being supported by the top and bottom tube plates; an inlet at the chamber for feeding heating medium into the chamber; a distributor above the tubes for feeding liquid to be evaporated into the tubes and for causing the liquid to be distributed as a falling film along the interior surface of the tubes so as to evaporate the liquid and generate vapor as the liquid passes in heat exchanging relationship with a heating medium present at the exterior surface of the tubes; a vapor space defined by a circumferential wall below the tubes; a plurality of vertically elongated spaced elements having a substantially U-shaped cross-section with inwardly pointing vertical edges for receiving the evaporated liquid and the vapor, the elements being arranged in a circumferential wall below the tubes within the vapor space spaced from
    Type: Grant
    Filed: May 14, 1991
    Date of Patent: September 21, 1993
    Assignee: A. Ahlstrom Corporation
    Inventor: Rolf Ryham
  • Patent number: 5232085
    Abstract: A distillation system has a degassing tank, a distiller for generating vapor of raw water taken from the degassing tank, a heater for heating the vapor from the distiller to convert the vapor into a high temperature and pressure vapor, a hydrophobic porous membrane through which the vapor from the heater flows, and a heat transfer unit provided in the distiller for effecting heat exchange between the vapor from the membrane member and the raw water from the degassing tank. The structural elements such as the heat exchange unit, piping, etc., with which the vapor from the membrane or the condensate thereof is brought into contact are made of titanium or titanium alloy.
    Type: Grant
    Filed: July 25, 1991
    Date of Patent: August 3, 1993
    Assignee: Hitachi, Ltd.
    Inventors: Nobuatsu Hayashi, Susumu Horiuchi, Hiroaki Yoda
  • Patent number: 5227027
    Abstract: A water distillation system and process capable of high efficiency operation used in combination with a heat pump system wherein the water distillation apparatus includes a water pre-heating device positioned within the feed water to heat the feed water to approximately 150 degrees Fahrenheit to facilitate operation of a water evaporator device which vaporizes the water by boiling thereof. Contaminants are removed from this pure water vapor which is at approximately 215 degrees Fahrenheit. The water vapor is passed to a water condenser to provide high purity water at approximately 180 degrees Fahrenheit. The heat pump system provides for refrigerant condensing at approximately 225 degrees Fahrenheit to facilitate boiling of the water in the adjacent water evaporator and includes refrigerant vaporization adjacent the water condenser to facilitate absorbing and reclaiming of the latent heat of the distillate.
    Type: Grant
    Filed: November 7, 1991
    Date of Patent: July 13, 1993
    Inventor: Robert T. Topper
  • Patent number: 5211816
    Abstract: A low temperature vacuum distillation apparatus. The distillation apparatus includes an evaporation section and a condensation section. Fluid flow throughout the system is assisted by an appropriate pump, and heat exchangers, one in each of the evaporation and condensation sections, are interconnected by employment of a heat pump.The condensation section includes a condensation chamber downward from which bubble tubes extend into a collection chamber. Collection chamber is provided with a pump to effect transfer of distillate having volatile impurities entrained therein to a final collection vessel. A pump communicates with vessel to create a partial vacuum therein to ensure venting of the impurities.
    Type: Grant
    Filed: October 7, 1991
    Date of Patent: May 18, 1993
    Assignee: Eco Pure, Inc.
    Inventor: Daniel W. Youngner
  • Patent number: 5200039
    Abstract: A steam chamber has a bottom portion that defines a tray for holding water to be distilled and a top portion for collecting steam created in the chamber by heating the water in the tray. An outlet conducts steam from the top portion of the steam chamber to a condenser. A check valve occupies the outlet for opening communication between the steam chamber and the condenser in response to steam pressure above atmospheric pressure in the steam chamber and for closing communication between the steam chamber and the condenser in the absence of the steam pressure in the steam chamber. In a preferred arrangement, a baffle member extends between the tray and the top portion of the steam chamber for allowing steam to enter the top portion of the steam chamber while preventing water globules carried in the steam from entering the top portion of the steam chamber.
    Type: Grant
    Filed: January 18, 1991
    Date of Patent: April 6, 1993
    Assignee: Emerson Electric Co.
    Inventors: Thomas J. Weber, Dale L. Garrison, Richard E. Forrest
  • Patent number: 5196093
    Abstract: A water distiller has a housing having an open interior area and a door that can be opened and closed to permit and block access into the interior area. A steam chamber is located in the interior area. The steam chamber includes a movable tray for holding water to be distilled. The tray seats against a fixed top where steam created in the chamber by heating the water in the tray is collected. By opening the door to the distiller, the tray can be unseated and removed for cleaning. After cleaning, the tray can be returned to the distiller and reseated against the top steam collecting portion by closing the door. In a preferred arrangement, the tray includes a chamber for holding a water soluble disinfectant for release during the distillation process.
    Type: Grant
    Filed: January 18, 1991
    Date of Patent: March 23, 1993
    Assignee: Emerson Electric Co.
    Inventors: Thomas J. Weber, Dale L. Garrison, Richard E. Forrest
  • Patent number: 5176798
    Abstract: A system is disclosed for recovering and disposing of volatile organic contaminants, from water contaminated with organics, which system includes a pump to feed water from the body of contaminated water to the system, with indirect heat exchange and direct steam addition to raise the temperature of the water, a stripping vessel to strip the heated water with gas to strip the volatile contaminants from the water, gas supply to provide stripping gas to the vessel conduits to pass the removed volatile contaminants to a vessel containing a bed of adsorbent selective for the removal organics and regenerating the near-saturated bed by stripping with ambient air heated by heat exchange with the exhaust gas from a fuel-fired heater, passing the contaminant-containing regenerating gas from the regenerating bed to said fuel-fired heater, and combusting the contaminants in said fuel-fired heater.
    Type: Grant
    Filed: May 17, 1991
    Date of Patent: January 5, 1993
    Assignee: Shell Oil Company
    Inventor: John B. Rodden
  • Patent number: 5171407
    Abstract: A distillation plant is constructed with an evaporator, separator and distillation column integrated together on a common vertical axis so as to eliminate bends and reduced cross sections in the product flow. The distillation column employs a regular packing to further reduce the pressure drop and operating temperatures over the height of the column. The overall pressure drop in the distillation plant is held to a range of less than 20 mbar.
    Type: Grant
    Filed: August 21, 1990
    Date of Patent: December 15, 1992
    Assignee: Sulzer Brothers Limited
    Inventor: Albert Meili
  • Patent number: 5164049
    Abstract: Method for the production of ultrapure sulfuric acid including distillation of sulfuric acid material for the removal of soluble impurities and insoluble and non-volatile particles of 10 microns to 0.2 micron or less in size. Reprocessing is also provided. Distillation takes place in a distillation chamber having walls which are provided with means within the chamber to provide smooth convective upward flow of distilling liquid and vapor proximate the walls and means for smooth convective downward flow substantially centrally of the distillation chamber. Redirection means and packing together with reflux means insure the washing of rising vapor and direct the condensing vapor substantially centrally of the distillation chamber. Ultrapure sulfuric acid is also provided having 5 or less particles per cubic centimeter of a size of 0.5 micron and larger and less than 10 ppb of any specific trace impurity such as cations.
    Type: Grant
    Filed: August 22, 1990
    Date of Patent: November 17, 1992
    Assignee: Athens Corporation
    Inventors: R. Scot Clark, John B. Davison, David W. Persichini, Wallace I. Yuan, Bruce A. Lipisko, Alan W. Jones, Allen H. Jones, Jr., Joe G. Hoffman
  • Patent number: 5160413
    Abstract: Micro-distillation apparatus is provided for analyzing acidic anions in which the acidic anion sample is placed in a lower elongated member in water containing an acidifying material, upon heating the acidic anion leaves the lower member as a gas, passing through a permeable membrane into an upper elongated member containing a material which converts the acidic anion to a salt and the salt is recovered for analysis. The micro-distillation apparatus is sized so that a number of samples can be heated in a small heating member, such as a hot block heater.
    Type: Grant
    Filed: August 16, 1990
    Date of Patent: November 3, 1992
    Assignee: Conoco Inc.
    Inventor: Joe D. Allison
  • Patent number: 5160580
    Abstract: An evaporating process that alternate between different modes of operation, according to the characteristics of the product handled; the product is either force fed into the tube nest, or cascaded through it in a free-falling film.
    Type: Grant
    Filed: January 3, 1990
    Date of Patent: November 3, 1992
    Assignee: Fenco S.p.A.
    Inventor: Carlo Sassi
  • Patent number: 5156747
    Abstract: Small quantities of one or more liquids having a high boiling point dispersed with a large quantity of one or more immiscible liquids having a lower boiling point are separated in a rapid and efficient manner. A non-reactive compressed gas is heated by recycled energy and make-up energy to a temperature above the boiling point of at least one liquid but below that of at least one other liquid. The heated gas is combined with the unheated liquid mixture to be separated, and the liquid-gas blend is mixed, heated and distributed by an improved nebulizer, forming a mist inside a vessel containing a pool liquid of at least one liquid having a boiling point higher than that of at least one other liquid, which pool liquid has been heated to a temperature above the boiling point of at least one liquid but below its own boiling point. The liquid having high-boiling-point in the mist settles by gravity and merges with the pool liquid.
    Type: Grant
    Filed: October 18, 1991
    Date of Patent: October 20, 1992
    Assignee: International Environmental Systems, Inc.
    Inventors: Roland E. Weber, Lawrence K. Wang, John J. Pavlovich
  • Patent number: 5156173
    Abstract: A cleaning apparatus that provides for immersion cleaning in one or two solvents. Using a source of inert gas and a recycling loop, the apparatus provides a drying zone above the solvents and prevents escape of solvent vapor into the surrounding atmosphere. The recycling loop maintains nonequilibrium vapor conditions and includes a centrifugal separator, which facilitates separation and recovery of the solvent vapors and the inert gas during normal operation of the system.
    Type: Grant
    Filed: May 14, 1991
    Date of Patent: October 20, 1992
    Assignee: Envirosolv
    Inventors: Gene E. Keyser, Robert L. Klopfenstein
  • Patent number: 5154061
    Abstract: Liquefaction apparatus and method for removing liquid molecules from a vaporous or gaseous medium, use being made of an annular porous layer (5) of van der Waals-type material through which the medium is radially outwardly directed, the layer being rotatably driven to discharge by centrifugal force the liquid modules that are bound by van der Waals forces in the layer. The layer is mounted concentrically on the inner periphery of a rotatably driven cylindrical separator member (4) having an annular wall portion provided with a passage system at least the outlet portion of which terminates in a plurality of radial passages (17) through which the liquid molecules are centrifugally discharged. In one embodiment, the separator member is cooled by a cooling bath (18) the liquid of which is recirculated through a refrigeration-type heat exchanger (12).
    Type: Grant
    Filed: July 24, 1991
    Date of Patent: October 13, 1992
    Inventor: Peter Weisshaar
  • Patent number: 5139620
    Abstract: Evaporation of saline water in a desalinization process, or evaporation of other types of liquid such as black liquor from paper pulp processing, is accomplished utilizing a multiple effect evaporator. Each effect includes one or more (e.g. first and second) sets of horizontally elongated dimpled plate evaporator elements. Horizontally flowing heating fluid, such as steam, is introduced to the internal passage of at least the second set in all the effects, and a head of circulation liquid is provided to cause liquid being evaporated to flow downwardly from the head over the external surfaces of the sets of dimpled plates in a thin film. The vapor evaporated is drawn through a demistor and is used as the heating fluid for the next effect. Recirculating liquid that has not evaporated and liquid separated by the demisting process are recirculated to the head associated with each effect. Clean condensate--such as distilled water--is withdrawn from the last effect.
    Type: Grant
    Filed: August 13, 1990
    Date of Patent: August 18, 1992
    Assignee: Kamyr, Inc.
    Inventors: Carl E. Elmore, Kyle Infante
  • Patent number: 5135611
    Abstract: A combined spray dryer and gas filter vessel in which a solution containing sulphuric acid and solids, and a hot drying gas, are introduced vertically through the top of the vessel into a spray zone. Solids are removed at a single point at the bottom of the vessel. Filters located above the spray zone clean gas leaving the vessel, and the cleaned gas exits at the top of the vessel. The compact design reduces insulation requirements while avoiding condensation which would create corrosion and yet it provides good separation of solids from gases.
    Type: Grant
    Filed: May 25, 1990
    Date of Patent: August 4, 1992
    Inventor: Gordon M. Cameron
  • Patent number: 5133837
    Abstract: A multi-stage flash evaporator is constructed so that the evaporator elements are dimpled plates mounted so that they extend horizontally. One, two, or more sets of plates may be mounted in each evaporator stage, the sets stacked upon one another in a tier arrangement. Each stage may be formed by a circular cross-section vessel, with I-beams--or like supports--extending horizontally at about the horizontal diameter of the vessel, and supporting the dimpled plates on them. A condensate collection trough is mounted below the dimpled plates and at the I-beams, the I-beams having openings in them through which condensate collected by the trough passes from one end of the vessel to the other. The hot liquid --such as sea water to be desalinated--to be evaporated is passed into a bottom chamber of each stage vessel, with vapor flowing upwardly through demistors and channels, into contact with the dimpled plates, and the condensate falling as a thin film down the plates and collecting in the condensate trough.
    Type: Grant
    Filed: September 10, 1990
    Date of Patent: July 28, 1992
    Assignee: Kamyr, Inc.
    Inventors: Carl L. Elmore, Kyle D. Infante
  • Patent number: 5096543
    Abstract: The waste heat from a steam turbine is condensed and used to desalinate sea water at the same time. The waste steam from a turbine is fed to a condenser through which cold sea water passes. As the cold sea water condenses the waste steam, it is warmed. It is then introduced into a first chamber which includes a number of spray heads disposed over fill (packing) that acts as an evaporator. Any water not evaporated is collected in a sump at the bottom of the first chamber, and the evaporated vapor is passed upwardly under the influence of a fan and ultimately to a second chamber. The second chamber may either be stacked above the first chamber, or in side-by-side relationship with it. A condenser, such as a number of dimpled metal plates, or plastic membranes defining a closed loop, or another set of spray heads and fill, are provided in the second chamber. Air typically recirculates from the bottom of the second chamber back into the first chamber.
    Type: Grant
    Filed: September 27, 1990
    Date of Patent: March 17, 1992
    Assignee: Kamyr, Inc.
    Inventor: Carl L. Elmore
  • Patent number: 5061348
    Abstract: An apparatus and method for reprocessing waste piranha containing contaminated H.sub.2 SO.sub.4 from, for example, a semiconductor processing operation is described. The apparatus and method include a first distillation flask which is maintained under a substantial vacuum. The first distillation flask includes a first column packed with a column packing material and an input pipe for refluxing to retard loss of H.sub.2 SO.sub.4 in the first distillation. The second distillation flask boils off substantially pure H.sub.2 SO.sub.4 and provides for a continuous automatic purge of the contaminants from the second distillation flask thus improving the purity of the H.sub.2 SO.sub.4. The substantially pure H.sub.2 SO.sub.4 flows through a column which is coupled to a condenser which condenses substantially pure H.sub.2 SO.sub.4.
    Type: Grant
    Filed: February 15, 1990
    Date of Patent: October 29, 1991
    Assignee: Alameda Instruments
    Inventors: Marshall W. McCormick, Jesse C. Dobson
  • Patent number: 5034103
    Abstract: A draw-off device is disclosed for a vacuum distillation column in which device a layer of gutters is provided. A secondary wall is arranged in the gutters creating a heat-insulating layer to reduce the condensation of vapor passing along the outer walls of the gutters.
    Type: Grant
    Filed: February 9, 1990
    Date of Patent: July 23, 1991
    Assignee: Shell Oil Company
    Inventors: Johannes A. Hamer, Pieter van der Heijden, Pieter J. Hoek
  • Patent number: 5028298
    Abstract: The present invention relates to a technique of concentrating waste water whereby the water content of the waste water is removed with a high decontamination factor, employs a porous membrane having a property allowing gas such as steam to permeate but not allowing a liquid such as water to do, as a membrane for concentrating the waste water, and adopts a method wherein the waste water is turned into a vapor flow and this vapor flow is made to contact the porous membrane so as for the waste water to be concentrated on the occasion when the waste water is to be concentrated by means of this porous membrane. By turning the waste water into the vapor flow, most of various metal ions, a surfactant, etc. existing in the waste water are separated from the vapor flow. Mist, metal ions in the mist and others contained in the vapor flow are removed by the aforesaid porous membrane from the steam while permeating the same.
    Type: Grant
    Filed: November 4, 1988
    Date of Patent: July 2, 1991
    Assignee: Hitachi, Ltd.
    Inventors: Tsutomu Baba, Koichi Chino, Shunsuke Uchida, Toshio Sawa, Makoto Kikuchi
  • Patent number: 5022967
    Abstract: A microdistillation column for the quantitative steam distillation of cyanide, phenolic compounds, hydrogen fluoride, ammonia, sulfites and other volatile analyte compounds from samples of environmental waters and sludge for their subsequent analysis involves volatilizing the water in the sample tube of the microdistillation column. The pressure which develops due to the water vapor forces all volatile compounds from the water sample, including the water itself, through a hydrophobic membrane and into the collector tube of the microdistillation column. The volatile compounds and the water vapor condense in the cooler collector tube and are quantitatively trapped and retained over the membrane. Relatively small samples may be distilled in the column.
    Type: Grant
    Filed: September 18, 1989
    Date of Patent: June 11, 1991
    Assignee: Lachat Instruments
    Inventor: Scott Stieg
  • Patent number: 4980032
    Abstract: An apparatus and method for reprocessing waste piranha containing contaminated H.sub.2 SO.sub.4 from, for example, a semiconductor processing operation is described. The apparatus and method include a first distillation flask which are maintained under a substantial vacuum. The first distillation flask includes a first column with a column packing means and a reflux means to retard loss of H.sub.2 SO.sub.4 in the first distillation. The second distillation flask boils off substantially pure H.sub.2 SO.sub.4 through a column which is coupled to a condenser which condenses substantially pure H.sub.2 SO.sub.4.
    Type: Grant
    Filed: August 12, 1988
    Date of Patent: December 25, 1990
    Assignee: Alameda Instruments, Inc.
    Inventors: Jesse C. Dobson, Marshall McCormick
  • Patent number: 4978429
    Abstract: An apparatus especially suitable for distilling water is disclosed. This apparatus, as disclosed, includes first and second separate and distinct groups of adjacent, confronting plate members, each of which alternatively defines a series of boiling and condensing chambers and a compressor. The apparatus also includes a device for fluid connecting the various boiling and condensing chambers and compressor to one another so that feed water can first be converted to steam in the boiling chambers, then compressed in the compressor, and finally condensed into pure water in the condensing chambers. The two groups of plate members are connected to and supported by a combination manifold/support assembly which serves both as part of the fluid connecting device and as a device for supporting the confronting plate members.
    Type: Grant
    Filed: January 18, 1989
    Date of Patent: December 18, 1990
    Inventors: Stephan B. Sears, Dan M. Pomeroy, Richard O. Rhodes
  • Patent number: 4957200
    Abstract: A water distillation apparatus has an outer chamber and an inner chamber suspended within the outer chamber by support arms. The inner chamber suspends a heating element to create steam. Heat is transferred from the inner chamber to the outer chamber, wherein the heated water in the outer chamber is allowed to degassify. Degassification removes unpleasant tasting chemicals from the water before distillation. Openings are provided for air circulation to remove the gasses. A condenser is also suspended by the support arms. The stem exits the inner chamber and goes into the condenser. A fan provides air circulation through the condenser. The outer chamber is not penetrated by any openings, thereby precluding the possibility of any leaks. The support arms bear on the outer chamber walls; the inner chamber is removed from the outer chamber for cleaning simply by lifting up. In one embodiment the outer and inner chambers are made of a ceramic material to better regulate heat transfer.
    Type: Grant
    Filed: December 28, 1989
    Date of Patent: September 18, 1990
    Inventors: William F. Turner, James K. Dews
  • Patent number: 4953694
    Abstract: A distilling apparatus includes an evaporation section which heats raw water and causes the generation of vapor from said raw water, and a hydrophobic porous film through which the thus generated vapor is filtered. Because vapor separated from the raw water is supplied to one surface of the hydrophobic porous film, the proportion of the vapor relative to the fluid supplied to that surface of the film can be increased, thereby enabling the efficient filtering of a large amount of vapor through the film. In addition, because the temperature of condensed water obtained by cooling the vapor can be kept in the vicinity of the boiling point thereof, any gases and volatile substances contained in the raw water are prevented from dissolving in the distilled water, thereby enabling the production of extremely pure distilled water.
    Type: Grant
    Filed: June 17, 1988
    Date of Patent: September 4, 1990
    Assignee: Hitachi, Ltd.
    Inventors: Nobuatsu Hayashi, Sankichi Takahashi, Katsuya Ebara, Hideaki Kurokawa, Akira Yamada, Yasuo Koseki, Harumi Matsuzaki, Hiroaki Yoda
  • Patent number: 4950363
    Abstract: A flashing feed inlet device is used in a vapor/liquid contacting column, such as a distillation column, to decrease the amount of liquid entrainment and maldistribution of vapor occurring when the liquid feed stream is introduced into the column at a temperature and/or pressure conditions higher than those existing in the column. The entrainment of the liquid and the maldistribution of the vapor are decreased by substantially decreasing the linear velocity of the vapor produced by the flashing of the liquid feed stream.
    Type: Grant
    Filed: July 19, 1989
    Date of Patent: August 21, 1990
    Assignee: Mobil Oil Corporation
    Inventor: Frank C. Silvey
  • Patent number: 4946559
    Abstract: A method and device for removing, from liquid such as water, dissolved volatile substances and gases when water is being distilled or evaporated. Feed water of a distilling apparatus or evaporator is heated to a sufficiently high temperature, whereby part of the feed water changes into vapor, and is then conducted to a purifying device. The feed water is discharged in the purifying device in the form of a thin film. The gaseous substances present in the feed water or liquid are separated by a separator device provided in the purifying device, and then conducted away through a connector provided on the purifying device.
    Type: Grant
    Filed: November 3, 1988
    Date of Patent: August 7, 1990
    Assignee: Oy Santasalo-Sohlberg AB
    Inventors: Rolf Kroneld, Markku Reunanen, Esko Huhta-Koivisto
  • Patent number: 4938868
    Abstract: The vacuum column system distills liquid under partial vacuum conditions. The system rigorously splashes and boils liquid in a boiler chamber so as to form vapor and a rising mist from the splashing liquid. The vapor and mist rise in a circularly converging path through a mist collector. The heavier mist strikes the surfaces of the mist collector and deposits on those surfaces, thereby separating itself from the vapor. The vapor is then drawn to a condensor chamber where droplets of treated liquid are sprayed through it and fall into a shallow pool of treated liquid. The droplets seed condensation of the vapor directly onto the droplets. Also, the droplets assist in encapsulating bubbles of vapor in the pool as the droplets fall into the pool. The bubbles are then entrained with other treated liquid of the pool as the treated liquid is drawn from the pool down an entrainment conduit.
    Type: Grant
    Filed: May 2, 1988
    Date of Patent: July 3, 1990
    Inventor: Thomas R. Nelson
  • Patent number: 4936955
    Abstract: A two-step distillation process provides semiconductor purity, concentrated hydrofluoric acid. Further, the distillation process, occurring under reduced pressures eliminates essentially pure water after the first distillation step. The product output of the second distillation process provides an acid of weight percent greater than 27 weight percent. The product acid is carefully diluted to the required concentrations during the dilution step.
    Type: Grant
    Filed: August 12, 1988
    Date of Patent: June 26, 1990
    Assignee: Alameda Instruments, Inc.
    Inventors: Jesse Dobson, Marshall McCormick
  • Patent number: 4933047
    Abstract: The invention therefore relates to a chimney tray hat apparatus for de-entraining droplets of liquid entrained in a stream containing vapor and liquid droplets flowing upwardly through a tray chimney in a vapor/liquid processing device, the chimney tray hat apparatus comprising a top cover or hat having an upper side and an underside which intercepts entrained liquid droplets flowing upwardly through the tray chimney, supports for supporting the chimney tray hat directly above the tray chimney, and a catcher ring and gutter for collecting the liquid impinging on the underside of the top cover and draining the liquid onto the supports and through the tray chimney.
    Type: Grant
    Filed: March 22, 1989
    Date of Patent: June 12, 1990
    Assignee: Shell Oil Company
    Inventor: Robert P. Bannon
  • Patent number: 4919257
    Abstract: In a gas dehydration system utilizing glycol a condensate skimming reflux column separates and skims natural gas condensate off glycol by a settling tank-type reservoir having a syphon-type glycol outlet to a reflux section spaced a predetermined distance below a condensate outlet pipe.
    Type: Grant
    Filed: July 12, 1989
    Date of Patent: April 24, 1990
    Inventors: Leslie E. Brigham, Sr., Leslie E. Brigham, Jr.
  • Patent number: 4917771
    Abstract: A column construction or boiling space in a distilling apparatus, having a pure vapor input connector, an input connector for water to be distilled, numerous heat exchange tubes within the column construction, a pure vapor removal connector, a condensate removal connector, and a connector for removing water to be distilled that has not vaporized. Pure steam is disposed to flow through heat exchange tubes, while impure water to be distilled is disposed to flow through an intermediate space between the heat exchange tubes. The heat exchange tubes are, at both ends, joined to flanges.
    Type: Grant
    Filed: February 25, 1988
    Date of Patent: April 17, 1990
    Assignee: Oy Santasalo-Sohlberg Oy
    Inventors: Lauri Santasalo, Esko Huhta-Koivisto, Jouko Ruokonen
  • Patent number: 4917769
    Abstract: A process for removing volatile acids from aqueous solutions which involves steam stripping a volatile acid from an aqueous solution and contacting the vaporized acid with a reactable cation to form a salt of the acid. A preferred embodiment of apparatus comprises an elongated distillation column having therein a plurality of zones or stages wherein the volatile acid in the aqueous feed stream is vaporized by steam and then the vaporized acid is carried by the steam into a salt formation zone or stage to react with a reactable cation to form a salt of the acid.
    Type: Grant
    Filed: May 24, 1989
    Date of Patent: April 17, 1990
    Assignee: OO Chemicals, Inc.
    Inventor: Wendell E. Van Horn
  • Patent number: 4895989
    Abstract: A process is described for the production of alcoholates from alkali metal hydroxides and aliphatic alcohol which in their molecule contain 1 to 6 carbon atoms. The alcoholates are produced in that alkali metal hydroxide is mixed with an alcohol and is reacted with said alcohol at a temperature from 80.degree. to 110.degree. C., preferably from 80.degree. to 100.degree. C., and under a pressure from 0.3 to 1.2 bars, the alcohol water mixture which evaporates during the reaction is separated into its components by at least one membrane, the alcohol vapor and the water vapor are condensed and the condensed alcohol is recycled to the reaction.
    Type: Grant
    Filed: July 11, 1988
    Date of Patent: January 23, 1990
    Assignee: Metallgesellschaft Aktiengesellschaft
    Inventors: Ulrich Sander, Pavel Soukup, Harald Helmrich, Wilfried Weiss
  • Patent number: 4882012
    Abstract: A water distiller includes an inner vessel in which source water is heated, an outer dome or housing on the inner surface of which the vapor from the inner vessel is condensed and a reservoir for receiving the condensate. The inner vessel includes a closure which directs vapor radially of the inner vessel to the dome or housing and which may include a vapor filtration element. A variety of domes or housings are shown including those of double wall construction with ports or vents to direct heat transfer fluid or air between the walls thereof, and those having lower portions which downwardly converge to direct the condensate to a central mouth of a reservoir.
    Type: Grant
    Filed: December 10, 1987
    Date of Patent: November 21, 1989
    Inventor: Kurt Wasserman
  • Patent number: 4882009
    Abstract: A brine concentrator utilizing two separate concentrating devices in combination wherein a first concentrating device comprises a plurality of serpentine pipes interposed within a concentrator tank containing a dilute brine solution and a second concentrating device, including a venturi, is attached to the upper end of the concentrator tank and connected to receive exhaust gases from an exterior source. The brine solution which has been concentrated by the first concentrating device exit the tank through an output opening and is introduced into the venturi via a plurality of nozzles where it is mixed with the exhaust gases.A venting stack is also attached to the upper end of the tank for venting the exhaust gases emitted from the venturi and pre-heating dilute brine solution, which is introduced into the tank through the venting stack. As the solution travels down the stack and into the tank, it comes into contact with the exhaust gases exiting the tank from the venturi.
    Type: Grant
    Filed: July 13, 1987
    Date of Patent: November 21, 1989
    Assignee: Four Nines, Inc.
    Inventors: Joseph J. Santoleri, Richard D. Ross
  • Patent number: 4877489
    Abstract: An electronic control and dosing system for desalinators (10) has a baffle, disposed between the evaporation and condensation chambers, fitted with probes (70, 71) which detect the presence of liquid created by entrained bubbles, that pass through the holes in the baffle. A control circuit (72), connected to the probes (70,71), closes a solenoid valve (62) to shut off the supply of feed water to the desalinator (10) until the threat of entrainment has passed. A foaming and/or scale inhibiting polymer, contained in a tank (64), is periodically introduced to the feed water inlet line (63) by a solenoid valve (65) controlled by a timer circuit (66).
    Type: Grant
    Filed: July 21, 1987
    Date of Patent: October 31, 1989
    Assignee: Nautical Services Pty. Ltd.
    Inventor: Ian Lloyd
  • Patent number: 4865697
    Abstract: A flashing feed inlet device is used in a vapor/liquid contacting column, such as a distillation column, to decrease the amount of liquid entrainment and maldistribution of vapor occurring when the liquid feed stream is introduced into the column at a temperature and/or pressure conditions higher than those existing in the column. The entrainment of the liquid and the maldistribution of the vapor are decreased by substantially decreasing the linear velocity of the vapor produced by the flashing of the liquid feed stream.
    Type: Grant
    Filed: October 15, 1987
    Date of Patent: September 12, 1989
    Assignee: Mobil Oil Corp.
    Inventor: Frank C. Silvey
  • Patent number: 4863567
    Abstract: The invention is a fluid distillation apparatus (10) which, in its preferred embodiment, includes a cylindrical portion (12) which mates with an end wall (14) and a bell portion (16) to form an enclosed volume (18) within which evaporization and condensation of a selected fluid may take place. A heat exchange rotor assembly (20) is formed of head conductive material and includes intertwined evaporization and condensation channels (52, 54) in spiral array. A central tunnel (58) provides access for vapor from an evaporization volume (24) to a condensation volume (26) with a pressure gradient provided by an impeller (100) urging such passage. A drum motor (68) rotates the drum (40) to facilitate liquid flow in the heat exchange rotor (20). An impure fluid input port (32) and output ports are provided for purified fluid (34), concentrated brine (36) and degassing purposes (38).
    Type: Grant
    Filed: May 25, 1988
    Date of Patent: September 5, 1989
    Inventor: Jay F. Raley
  • Patent number: 4818346
    Abstract: A vertical distillation column for vacuum distillation having a feed inlet, a gas outlet and a de-entrainment device which comprises a downstream chamber and an upstream chamber separated from each other by an inclined permeable wall comprising coalescence means and flow controlling means restricting fluid flow through the upper part of the coalescence means.
    Type: Grant
    Filed: May 7, 1987
    Date of Patent: April 4, 1989
    Assignee: Shell Oil Company
    Inventors: Jeremy B. Bentham, Johan J. B. Pek
  • Patent number: 4790904
    Abstract: An atmospheric evaporator for reducing the water content of various chemical solutions, more particularly useful in the electroplating industry, wherein the evaporator includes a solution-secure molded tank in which a removable blower sleeve is mounted having a blower inlet duct and support strut members formed at the opposite end thereof to support a multiplicity of finned evaporator members over which the solution is sprayed. When a large-volume, low RPM blower is mounted to the inlet duct, a straight-line downdraft of both air and solution is created, allowing the air and evaporated water to exhaust through an up-facing outlet duct, thus defining a substantially "U" shaped duct arrangement from the inlet side to the exhaust side of the tank with the heavy chemical particles returning to the process tank from the bottom of the evaporator tank.
    Type: Grant
    Filed: May 19, 1987
    Date of Patent: December 13, 1988
    Inventor: William Yates
  • Patent number: 4778605
    Abstract: An apparatus and method are provided wherein liquid is removed from a liquid-solids mixture by employing both filtration and low pressures to achieve vaporization of liquid. The mixture is introduced to a vessel in which the mixture is filtered so that a substantial portion of the liquid is withdrawn from the vessel. The vessel is then depressurized to an extent necessary to vaporize a substantial portion of the remaining liquid. Such vapor is withdrawn from the vessel. During vaporization, the contents of the vessel are agitated and heated.
    Type: Grant
    Filed: April 29, 1987
    Date of Patent: October 18, 1988
    Assignee: Phillips Petroleum Company
    Inventors: William R. Anthoney, Richard K. Young, Brian H. Limoges