Abstract: A water vapor distillation system.

Abstract: A water vapor distillation system.

Abstract: A distilling device having a vapor compression distiller. The vapor compression distiller can include a reservoir for receiving liquid for distillation. Evaporation surfaces can receive the liquid and evaporate the liquid into evaporated vapor for subsequent condensing. Condensing surfaces can receive the vapor and condense the vapor into distillate. A compressor can deliver the vapor to the condensing surfaces. The distilling device can also include an engine that produces heat. A boiler can be heated by the heat from the engine for producing a working vapor. A vapor turbine can be driven by the working vapor. The vapor turbine can be mechanically coupled to the compressor for mechanically driving the compressor, thereby reducing electrical power needs of the vapor compression distiller.

Abstract: A distiller including an evaporator having at least one evaporation surface for evaporating liquid into vapor. At least one movable liquid applicator assembly has a wiper applicator which can move over the at least one evaporation surface, for wiping and applying a thin even film of the liquid on the at least one evaporation surface for evaporation.

Abstract: A reservoir evaporation system for evaporating fluid from an open reservoir of effluent containing a contaminant includes a fluid evaporator, an air pump, and an air supply conduit functionally connecting the fluid evaporator with the air pump. The fluid evaporator includes a vessel adapted to be positioned in an operative position partially submerged on the top surface of the effluent in the reservoir with a lower chamber submerged in the effluent and an upper chamber extending above the top surface of the effluent. In operation, air from the air pump mixes with the effluent inside the fluid evaporator and subsequently is discharged through exhaust openings. A fluid discharge pipe can also simultaneously discharge aerated effluent back down into the reservoir. Fluid is thereby separated from the effluent in the lower chamber by evaporation in a controlled manner that minimizes spread of contaminants to surrounding environments by wind.

Abstract: A liquid concentrator having an evaporator assembly and a cyclonic separator includes features designed to improve the performance of the liquid concentrator. A settling chamber is separated from a sump of the cyclonic separator. A liquid inlet opening into a mixing chamber of the evaporator injects wastewater at low pressures. Features to aid in the cleaning of the liquid concentrator include easy open doors and clean water injection ports for cleaning interior portions of the liquid concentrator.

Abstract: A liquid concentrator having an evaporator assembly and a cyclonic separator includes features designed to improve the performance of the liquid concentrator. A settling chamber is separated from a sump of the cyclonic separator. A liquid inlet opening into a mixing chamber of the evaporator injects wastewater at low pressures. Features to aid in the cleaning of the liquid concentrator include easy open doors and clean water injection ports for cleaning interior portions of the liquid concentrator. In one feature a settling tank is disposed below the cyclonic separator and has a width that is larger than the width of the cyclonic separator. In another variation, the cyclonic separator has a tubular body with an interior that is substantially unobstructed between an inlet from the evaporator assembly and an exhaust outlet. In yet another variation, the cyclonic separator has an upper chamber that is separated from a lower chamber.

Abstract: A feed gas conditioner.

Abstract: Disclosed are examples of apparatuses for evaporative purification of a contaminated liquid. In each example, there is a first vessel for storing the contaminated fluid. The first vessel includes a surface coated with a layer of superhydrophobic material and the surface is at least partially in contact with the contaminated liquid. The contaminants do not adhere to the surface as the purified liquid evaporates, thus simplifying maintenance of the apparatus.

Abstract: A method of distilling a chemical mixture, the method including receiving, in a vessel comprising a complex, the chemical mixture comprising a plurality of fluid elements, applying electromagnetic (EM) radiation to the complex, wherein the complex absorbs the EM radiation to generate heat at a first temperature, transforming, using the heat generated by the complex, a first fluid element of the plurality of fluid elements of the chemical mixture to a first vapor element, and extracting the first vapor element from the vessel, where the complex is at least one selected from a group consisting of copper nanoparticles, copper oxide nanoparticles, nanoshells, nanorods, carbon moieties, encapsulated nanoshells, encapsulated nanoparticles, and branched nanostructures.

Abstract: A steam generation apparatus 1 including a high-temperature pipe 10 disposed extending horizontally and through which a high-temperature fluid passes; low-temperature pipes 20 disposed on both sides of the high-temperature pipe 10 in a horizontal direction and through which a low-temperature fluid having a temperature lower than that of the high-temperature fluid passes; and a thermoelectric module 30 interposed between the high-temperature pipe 10 and each of the low-temperature pipes 20 for generating electrical power using a temperature difference between the high-temperature pipe 10 and the low-temperature pipes 20, the low-temperature pipes 20 being configured such that the supplied low-temperature fluid in a liquid form is turned into steam due to heat exchange with the high-temperature fluid and is discharged from an upper portion of the low-temperature pipes 20.

Abstract: Accumulation of polymer on equipment, which is in contact with polymerizable material during normal process operation, is minimized by the method and apparatus of the present invention. The method involves positioning and affixing the equipment, such as a pressure relief device, to process apparatus, such as a distillation column, proximate to a wetted region formed by liquid phase fluid in the process apparatus, such that the moving liquid phase fluid is at least intermittently in contact with the equipment and one or more of accumulated polymerizable material, condensate including same, and polymer, is washed off of the equipment. The apparatus of the present invention is effective for maintaining the service-readiness of the equipment, which provides for safe long-term operation of the process apparatus.

Abstract: Disclosed are wastewater treatment systems and methods of treating wastewater. In particular, this disclosure provides a method of lowering the biological oxygen demand, total nitrogen, total suspended solids, and phosphorous within wastewater containing human excrements. In addition to improving the quality of the wastewater on a per Liter basis, this disclosure also provides methods and systems that reduce the absolute quantity of total nitrogen, total suspended solids, and phosphorous released into the environment through effluent. The disclosed methods and systems also provide ways of reintroducing water into the environment.

Abstract: A method of operating an assembly for recycling a solvent from a contaminated solvent solution including a source for the contaminated solvent solution at a level and a recycling assembly including a reservoir module and a recycler module. The reservoir module includes a reservoir and the recycler module includes a controller and a distillation assembly including a distiller having a conduit and a pressure relief valve. The pressure relief valve includes a tube. The method includes connecting the conduit to the source below the level; connecting the pressure relief valve tube to the source; pumping solvent into the reservoir, distiller and conduit to an operational level; and selecting a duty cycle of the controller to regulate a rest period after the controller operation of a distillation cycle.

Abstract: Methods and systems are disclosed which provide for the purification of effluent from a septic system or natural water from rainwater or stormwater collection devices for the storage and reuse of water. The purified water may be supplied to water applications, such as a return conduit to a home for potable or graywater usage. The distillation unit may be powered by a local power independent of a municipal power grid and which may employ sustainable energy mechanisms. The distiller residue may undergo a volume reduction process, such as evaporation, coagulation, electrocoagulation or microfiltration. The purified water may be stored in a holding tank with sensors to monitor the water quality and water level within the tank. Alarms, release valves or relief valves may be activated in response to such monitoring.

Abstract: An accelerated vapor recompression apparatus 10 converts incoming flow 35a to a concentrate 35c by developing a concentration profile 146 within a tank 30 holding a liquid 23 containing dissolved solids. The resulting curve 160 of saturation temperature of the stratified liquid 23 (such as a brine 23 or other material 23) moves away from the curve 162 corresponding to fully mixed conditions. The shift 174, 180 in saturation temperature results in increased boiling without increased energy from a heater 70 or compressor 50. A method 90, 200 of control of the system provides interventions 203, 204, 205, 206 at different levels 92, 94, 96, 98 of control, ranging from mass flows 35 to work of a compressor 50, heat from a heater 70, and a predictive processing 215 of feedback 217 for controlling commands 216 algorithmically.

Abstract: The invention concerns the control of solvent systems in processes and apparatus for the separation of aromatic hydrocarbons from non-aromatic hydrocarbons in liquid-liquid extraction, extractive distillation, and the combination thereof.

Abstract: A method for preparing a suspension from a separation process, wherein the suspension is made of a particulate abrasive and a liquid slurrying agent. The method includes the steps of: a) thinning the suspension in a tank with an additional slurrying agent (PEG) without adding additional water, producing a constant volume ratio between the particulate abrasive and the liquid slurrying agent; b) separating the thinned suspension into a liquid and a solid fraction in a centrifugal separator, and c) subsequent refinement or reuse of the separated liquid and solid fractions.

Abstract: The present invention provides a method for preparing DMF for sucralose production, including, e.g., isolating DMF from a composition comprising DMF, water, and methanol, using a single-tower rectification system. In various embodiments of the present invention, the composition, after the removal of water and methanol, may be further dried/dehydrated, such as, by using a dehydration agent and/or filtration. The resulting substantially pure DMF may comprise at least about 98-99% DMF. The present invention further provides a method of preparing a composition comprising anhydrous sucrose for sucralose production, which may comprise mixing regular sucrose with a water-containing DMF composition, and drying the resulting sucrose-DMF composition. Also provided is a single-tower separation system for isolating DMF from a composition comprising DMF, water, and methanol.

Abstract: The present invention provides a novel tritium distillation device, which includes a container, a radiator covered on top of the container with a protrusion at the bottom, a conduit penetrating the container with an inlet and an outlet, the inlet being arranged in correspondence with the protrusion, and a heating device fixed below the container. The method of operating the tritiated water distillation includes the steps of adding environmental tritiated water in the container, covering the radiator on top of the container closely, heating environmental tritiated water to cause tritiated water steam to be condensed to the bottom of the radiator, and collecting the tritiated water condensation dropped from the protrusion with conduit. The present invention uses a simple structure to ease assembly and reduce the cost of cooling water source.

Abstract: The present invention provides composite membranes for membrane distillation and related methods of manufacture. In particular, there is provided a composite hydrophilic/hydrophobic membrane comprising a hydrophilic polymer layer and a hydrophobic polymer layer comprising fluorinated surface-modifying macromolecules, wherein said composite membrane has a high vapour flux. Also provided herein are methods of manufacturing and optimizing the composite membranes and a membrane distillation system comprising the composite membranes.

Abstract: A method for purifying water and generating ammonia liquor is disclosed. Hydrogen, oxygen, organic matter contaminated water vapor, and ambient air, containing nitrogen, are provided to a combustion chamber. The hydrogen is combusted in the oxygen in the combustion chamber with the contaminated water vapor and nitrogen. The nitrogen is fixated. Water vapor is produced. The contaminated water vapor is heated to decontaminate the contaminated water vapor. The produced water vapor, fixated nitrogen, and organic matter decontaminated water vapor are exhausted from the combustion chamber. The generated water vapor, fixated nitrogen, and decontaminated water vapor are condensed to obtain ammonia liquor. Water is evaporated from the ammonia liquor to form purified water vapor and concentrate the ammonia liquor.

Abstract: A fluid recycling system includes a separator for physically separating glycol from at least a portion of other substances mixed with the glycol to produce a first effluent stream having separated glycol and a second effluent stream having the other substances and residual glycol. A catalytic reactor receives the second effluent stream and chemically reacts the other substances and residual glycol to produce a hydrogen stream and a remainder stream.

Abstract: A system for treating feedwater includes a fluidized bed heat exchanger unit connected to receive feedwater and a flash concentrator column connected to receive feedwater discharged from the fluidized bed heat exchanger unit. A spray dryer is provided to receive a solids/liquid slurry discharged from the flash concentrator column. Feedwater can be treated by converting dissolved solids in the feedwater to suspended solids, vaporizing a portion of the feedwater to produce a solids/liquid slurry, and separating solids from the solids/liquid slurry.

Abstract: A top temperature T1 of a distillation tower 1 is held below a liquefying temperature of a light fraction by returning a part of an exhaust gas W, which is cooled by a condenser 5, to the upper zone of the distillation tower 1. A bottom temperature T2 is raised up to 300° C. at highest by returning a part of a liquid product P from a re-boiler 3 to a lower zone of the distillation tower 1. When a liquid hydrocarbon L comes in countercurrent contact with a stripping gas G inside the distillation tower 1 with the temperature profile that an inner temperature gradually falls down along an upward direction, mercury is efficiently transferred from the liquid L to a vapor phase without effusion of the light fraction in accompaniment with the exhaust gas W.

Abstract: A process is disclosed for recovering 1-butene from a feed steam comprising n-butane, isobutane and butene isomers using a single, divided wall distillation column. The disclosed process includes introducing the feed steam into an inlet of a first side of a distillation column, wherein the distillation column comprises a top, a bottom and a center dividing wall extending between the bottom and the top of the column and dividing the column into the first side and a second side. The process includes taking off an isobutane stream from the top of the second side of column, taking off a 1-butene stream as a bottoms stream from the second side of the column, and taking off a combination 2-butene and n-butane stream as a bottom stream from the first side of column.

Abstract: The object of this invention to provide an improved arrangement that enables to prevent adhesion of polymer on or around the inner wall of a purification apparatus directly equipped on the outer wall thereof with an attachment such as a support by suppressing local temperature lowering inside the apparatus due to the existence of the attachment. The present invention provides a purification apparatus comprising an attachment directly mounted on an outer wall of the apparatus; and a covering material made of a low heat conductive material which partly or entirely covers the outer wall of the apparatus, and which partly or entirely covers the attachment.

Abstract: The present invention provides an apparatus for producing (meth)acrylic acid and a process for producing (meth)acrylic acid with this apparatus wherein the apparatus enables the production of (meth)acrylic acid stably for a long period of time by effectively inhibiting the polymerization of (meth)acrylic acid in its production process (for example, in a reboiler). At least a part of the apparatus is made of a nickel-chromium-iron alloy with a molybdenum content of 3 to 20 mass %, but not including 3 mass %, or with a molybdenum content of 1 to 4 mass % and a copper content of 0.5 to 7 mass %.

Abstract: An apparatus for and method of distillation uses a high temperature thermoelectric device to heat a liquid, such as water to vapor (steam) and cool the vapor to a purified, distilled liquid. Distillation system has no moving parts, thereby increasing reliability while reducing noise and maintenance. Liquid in a container has a heating section on the container extending into it to boil it into a vapor that is fed to a condenser section disposed on the container adjacent to the heating section. A thermoelectric section provided with a Peltier effect device is interposed between the heating section and condenser section. The Peltier effect device has one side in contiguous contact with the condenser to transfer heat from it and another side is in contiguous contact with the heating section to transfer heat to it to boil the liquid into the vapor and feed the vapor through the condenser that condenses it into distilled liquid.

Abstract: The object of this invention to provide an improved arrangement that enables to prevent adhesion of polymer on or around the inner wall of a purification apparatus directly equipped on the outer wall thereof with an attachment such as a support by suppressing local temperature lowering inside the apparatus due to the existence of the attachment. The present invention provides a purification apparatus comprising an attachment directly mounted on an outer wall of the apparatus; and a covering material made of a low heat conductive material which partly or entirely covers the outer wall of the apparatus, and which partly or entirely covers the attachment.

Abstract: A method of in-service cleaning an operating column by inserting into the column a lance through which a compatible liquid is dispensed at a pressure of at least about 5000 psig. Also disclosed is apparatus which comprises a column through which a fluid can pass, nozzles mounted on the outside of the column, where each nozzle comprises a flange welded to the column and a valve bolted to the flange, a lance which can be inserted through the nozzles into the column and means for dispensing a liquid through the lance at a pressure of at least about 5000 psig.

Abstract: The sea water to be desalted is fine-sprayed through nozzles (3) against an underside (1b) of a plate-shaped element (1). The element (1) may, for example, be an aluminum plate forming a heat transfer medium and is exposed to solar radiation through glass cover plates (15). The water sprayed on the underside (1b) is distributed over the surface of the element (1) and is evaporated by the heat stored in this element. The water vapor passes through an outlet (27) to a condenser (10) in which it is condensed and finally through an outlet (12) in the form of fresh water which then is available, for example, for irrigating green spaces. The sea water to be desalted is preferably sprayed against the underside of the element (1) for only a few seconds at predetermined intervals. To clean the element (1), sea-water may be sprayed every hour for, for example, 1 to 1.5 minutes against the underside of the element (1) in order thus to rinse away deposited salt and impurities.

Abstract: This invention discloses a method of in-service cleaning an operating column by inserting into the column a lance through which a compatible liquid is dispensed at a pressure of at least about 5000 psig. Also disclosed is apparatus which comprises a column through which a fluid can pass, nozzles mounted on the outside of the column, where each nozzle comprises a flange welded to the column and a valve bolted to the flange, a lance which can be inserted through the nozzles into the column and means for dispensing a liquid through the lance at a pressure of at least about 5000 psig.

Abstract: Method and apparatus for the distillation of liquids which is particularly suited for the removal of soluble impurities and insoluble and non-volatile particles of 10 microns to 0.2 micron or less in size. A substantially elongated distillation chamber having walls equipped with axially disposed concentric boiling rings spaced from the walls near the bottom, and a packing stop, packing redirector rings for condensed vapor, and a reflux condenser in the upper part of the distillation chamber provide, during distillation, a smooth convective upward flow of distilling liquid and vapor proximate the walls and boiling rings and a smooth convective downward flow of distilling liquid and vapor substantially centrally of the distillation chamber.

Abstract: A distillation apparatus includes a heating device, an inlet for medium to be distilled, a vapor outlet, a distillation space between the distillation medium inlet and the vapor outlet and a drain for the separate components of the solvent, arranged in the bottom part of the distilling space and extending from same. In a heating vessel, which is able to be filled with a heating medium to be heated by the heating device, there is a downwardly extending down tube joined with the inlet and an up tube extending upwards to the vapor inlet. During operation the two tubes are surrounded by heating medium and form the distillation space. The drain is arranged under the junction between the up and down tubes and is provided with a U-trap.

Abstract: A distillation apparatus intended for distilling liquid, primarily water, comprising a distillation unit which includes a porous, hydrophobic membrane (2) which is pervious to steam, or vapor, but impervious to liquid, and a condensation surface (3) located at a distance from the membrane, such as to present an air gap (4) between the membrane and the condensation surface, the distillation apparatus further comprising units for conducting the liquid (20) to be distilled on the membrane surface remote from the air gap (4), and a unit for conducting a liquid (22) which is colder than the first mentioned liquid (20) on the side of the condensation surface (3) remote from the air gap (4). According to the invention the distance (L) between the membrane (2) and the condensation (3) lies in the range of about 0.2 mm-about 1 mm, and the thickness (b) of the membrane (2) is less than about 0.5 mm.

Abstract: Disclosed herein is a process and apparatus for safely distilling relatively small batches of organic compounds such as paint solvents by directly and safely heating the compounds in a vessel having a relatively thick bottom with electrical heating units cast in it and a relatively thick side wall integrally attached to the bottom. The side wall may be integrally attached to the bottom by a weld that penetrates the joint between the side wall and bottom preferably by 100% in order to provide a complete heat transfer from the bottom to the side wall. The vessel is so designed so as to provide a relatively uniform temperature throughout the inner periphery of the vessel thereby avoiding hot spots and insuring that the hottest spot of the inner periphery of the vessel does not exceed the auto ignition temperature of the compound being processed.

Abstract: Apparatus is provided for converting sea or other undrinkable waters to drinkable water without the use of driven or moving parts. Reliance upon gradient effects is made to effect the vaporization of, for example, sea water, followed by the condensation of the vapor to form distilled water. Gradient effects are achieved through the provision of differentials in the thermal conductivity, capillary activity, adsorptive, absorptive and/or pressure characteristics of particulate materials, or combinations of such physicals. For example, a column is packed with material graded as to its conductivity, the least thermally conductive material being nearest the cold or ambient water that is to be purified. In packing the column each successive layer of material has a greater thermal conductivity than the layer beneath it with the most conductive being at the top near the outlet arm of the column.

Abstract: Disclosed is a novel apparatus for use in the rapid refluxing of low boiling liquids. The apparatus comprises a central chamber for the reception of hot gases from a reaction vessel, the chamber being surrounded by a cooling jacket. The central chamber comprises a lower primary condenser of 2 or more bulbous portions connected to and in fluid communication with each other and with a curvilinear column serving as a secondary condenser.

Abstract: A composite membrane separates a distilland and a distillate, such as salt water and fresh water. The composite membrane comprises a thin lyophobic microporous layer or membrane and a thin lyophilic layer or membrane on both sides of the lyophobic membrane or on the distillate side. Evaporation and condensation takes place within the micropores of the lyophobic membrane. The lyophilic layer on the distilland side prevents intrusion of distilland into the pores of the lyophobic layer. The lyophilic layer on the distillate side changes the surface curvature of the liquid/vapor interface in a manner which enhances the distillation rate through the membrane.

Abstract: A process, apparatus and control system for the fractionation of a hydrocarbon feed stream containing relatively nonvolatile impurities. A sidecut liquid stream which is substantially free of the impurities is withdrawn below the feed point. The liquid derived from the feed stream is confined to a first lateral half of the fractionation column to prevent the transfer of the nonvolatile impurities to the second lateral half from which the sidecut is removed. Liquid descending from above the feed point is collected and distributed between the two lateral halves of the column in response to temperature measurements taken in the two halves to thereby equalize liquid flow rates in the two halves. The flow of vapor between the two halves is not obstructed.