Abstract: A steam distillation apparatus is provided which has a column body, a head connected to one end of the column body which has a diameter larger than the column body, a sump connected to the other end of the column body and contact elements disposed within the column body which are positioned and arranged to avoid formation of preferential pathways for the steam passing through the column body while providing for ready flow of the material being steam distilled through the column body. The connection of the head and column body may be frustoconical in shape such that its diameter diminishes from a diameter corresponding with that of the head at its connection with the head to a diameter corresponding with that of the column body at its connection with the column body. A collar is positioned at the connection of the neck and column body and extends into the head to define an annular space between the neck and collar.

Abstract: A method for concentrating salt water. Salt water is separated from oil-water mixture which has been produced from a well. Salt water is introduced into a recirculating weir and mixed with more concentrated brine. Brine is recirculated through a thermal syphon apparatus. Recirculation includes passing brine, including some salt water, from weir into boiler vessel. Brine is heated within boiler vessel to a boiling temperature whereby brine, while boiling, generates steam which passes up out of weir. All of foregoing steps are performed at atmospheric pressure. The density of brine is sensed at a location in the lower vicinity of weir. Concentrated brine is released from lower vicinity when density at sensed temperature is at a level corresponding to a brine concentration near the precipitation of salt from solution. Salt water and brine is passed through a magnetic water treating unit. The concentrated brine, as released, is passed into a holding vessel.

Abstract: A portable water distiller comprising a vaporization chamber containing an electric coil heating element, a finned tube condenser coil, and an electric fan motor for cooling the condenser coil's outer surface. In a preferred embodiment, the vaporization chamber includes an upper vertical tube having an open bottom and closed top communication with the condenser, and a raw water receptacle with its rim surrounding the tube at a distance and with its bottom near the bottom end of the tube. The receptacle of the portable water distiller is automatically kept full with water up to a predetermined level, and is readily removable from the distiller for cleaning of residue, the lower portion of the tube is similarly removable for access to the heating element. The condenser coil is designed to offer low flow resistance resulting in only a small over-pressure in the vaporization chamber thus affecting only a small depression of the water level therein.

Abstract: A method and apparatus of controlling a rotating vacuum evaporation system is disclosed. The rotating flask, containing the medium to be evaporated, is buoyantly supported in a liquid bath and the relative elevation between the flask and the liquid level in the bath is measured. The relative elevation is utilized as the control signal to control the addition of fluid medium to the flask, and to shut off the system when desired.

Abstract: Method and apparatus for disposing of waste rinse water used in photographic processes in which the waste rinse water is heated in a dissolution tank to be reduced to a slurry which is accumulated and stored in drums for later processing. The apparatus is compact consisting of separate tanks for the different rinse water, a holding tank to collect the contaminated rinse water and a separate dissolution tank. There is no discharge of any liquid waste products into the environment.

Abstract: An improved distillation process and apparatus are provided whereby liquid product recovery other than bottom product is maximized and feed stream heating is minimized. Inert gas streams combined with the feed stream and introduced into the distillation tower are controlled whereby feed stream heater residence time and partial pressures of feed stream components are minimized. The temperature of the combined inert gas-feed stream exiting the feed stream heater is controlled at a minimum temperature by establishing signals representative of overflash, bottom product specification and other conditions and comparing such signals whereby the signal which represents the lowest heater outlet temperature is utilized for controlling the heater operation.

Abstract: A water distiller assembly which provides for an efficient distillation process wherein steam generated in a boiling chamber is delivered to a steam condensing chamber where steam condensation is carried out by the combined effect of water cooling and air cooling. The resulting distilled water is stored in the steam condensing chamber where it is kept hot by the incoming steam for hot serving while at the same time helps in condensing the steam it comes into contact with. Water vapor emanating from the surface of the hot coolant water is also condensed and collected. Operating temperature of the coolant water may be adjusted to suit room temperature demands. The distillation process is made automatic, continuous and self-limiting by the use of two simple float controls and a thermostatic water outlet valve.

Abstract: Apparatus for the continuous vacuum cleaning of oil operating on the principle of continuous alteration of a compression, and of a separating cycle, by utilizing a combined action of quasistationary processes instigated by reduced pressure and of non stationary processes generated by a hydrodynamic cavitator. Due to a repeated circulation of the oil filling through a non-stationary and a quasistationary separating process, a high purity of oil, which is subsequently forced back into the container of the oil system, or of an electric transformer, respectively, is achieved and simultaneously a safe removal of contaminations.

Abstract: The invention provides a compact automatically operating distillation apparatus comprising a baseplate that will free-stand, but is more usually located on a reservoir to receive the distillate, which usually is water. A boiler container having an electric heater is removably mounted on a support, which is movably mounted on the baseplate with the weight of the container and the water opposed by a spring. The support operates electric switches that open a solenoid-operated valve to supply water to the boiler when its weight decreases a predetermined amount, and that will switch off the heater if the boiler has insufficient water. The output of the boiler goes to a condenser coil which is supplied with cooling air by a fan. A float in the reservoir controls another switch that will stop operation when the reservoir is full.

Abstract: A process for controlling a distillation column in which feed liquid supplied thereto is heated by heating steam comprises the steps of: controlling the steam flow rate so that the steam flow rate is increased in response to the difference between the temperature measured at the bottom of a calculated column and the temperature of boiling point of the feed liquid until the former temperature exceeds the latter temperature when the former is not higher than the latter; controlling the steam flow rate so that the temperature around an intermediate tray falls within a first predetermined temperature range when the temperature measured at the bottom of the column exceeds the calculated temperature of the boiling point of the feed liquid; controlling the steam flow rate so that a reflux ratio is adjusted to within a predetermined reflux ratio range when the temperature around the intermediate tray falls in the predetermined temperature range; and controlling the steam flow rate so that the reflux ratio is maintain

Abstract: The present invention provides a process for distillation of styrenes which can be stably operated without loss of energy saving effect, by leading a part or all of low boiling point component vapor from the top to a compressor to use as a heat source for a reboiler and returning the low boiling point components condensed in the reboiler or a mixture of the condensate and a part of the uncondensed vapor to a recycling line of a distillation column.

Abstract: The temperature of a crude oil provided from a crude oil preheat furnace to a crude tower is substantially minimized by controlling such temperature so as to maintain a desired minimum overflash flow in the crude tower. Also, the temperature of each of the individual coils in the preheat furnace are balanced with respect to each other. Such minimization and balancing results in substantially optimal utilization of the fuel provided to the preheat furnace which results in considerable economic savings with respect to the operation of the preheat furnace.

Abstract: A water purification and hot water supply apparatus is provided including a feed water intake providing water in excess of the distilled water output, a heater controlling the quantity of water boiled, a waste water exit port to remove accumulated water above a certain level, a distilled water exit port in the vapor space, a condensing device to transfer the heat of condensation to a hot water tank and a waste water heat exchange device to transfer heat from the waste water to the hot water tank. A volatile organic compound removing tank to heat and vent off the contaminants is positioned to receive heat from the water in the still section of the apparatus which then feeds water to the feed water intake.

Abstract: Heated distillation still for separating ethanol-water mixtures divided into an upper solar absorbent vaporization section and a lower pre-heating section by a vaporization floor, float means to automatically control the ethanol-water feed to the lower portion of the preheating section when distillation is taking place, means to evenly distribute the ethanol-water mixture on the vaporization floor, means to heat the ethanol-water mixture in the distillation chamber, and means to remove or recycle residual aqueous liquid from the lower end of the vaporization section.

Abstract: The Reid Vapor Pressure of a hydrocarbon mixture consisting essentially of hydrocarbons selected from the same series is determined based on the actual temperature and vapor pressure of the hydrocarbon mixture. The thus determined Reid Vapor Pressure may be compared to a set point for the Reid Vapor Pressure with the results of the comparison being utilized to maintain the actual Reid Vapor Pressure substantially equal to the desired Reid Vapor Pressure.

Abstract: A pure water tank for distillation equipment comprises a casing on a water tank proper and a communicating pipe via which interiors of the casing and tank proper communicate each other. Water in the casing prevents air from entering into the pure water tank through a condenser when generation of steam is halted.

Abstract: A desired separation between sidedraw product streams withdrawn from a fractional distillation column is maintained by controlling the flow rate of the external reflux associated with a particular sidedraw product stream in response to the output signal from a temperature controller which is reset by an internal reflux controller. Such cascade control improves the stability of a fractionation process and provides for good control of the separation between sidedraw product streams.

Abstract: A vapor generating and recovering apparatus for vaporizing a liquid and condensing a vapor, the apparatus including a container having a liquid therein with heating and cooling systems in heat transfer relation with the liquid and vapor in the container. The heating and cooling systems include means to vaporize the liquid and means to condense the vaporized liquid disposed within the container. Temperature or pressure sensing means in the cooling system is utilized to shut down the heating system when a preselected vapor level is exceeded.

Abstract: In a fractional distillation process in which it is desired to maintain a desired overhead product composition and bottoms product composition, a set point for the flow rate of the external reflux to the fractional distillation column is increased or decreased by an incremental amount or is left constant based on whether the concentration by the heavy key component in the overhead product stream and the concentration of the light key component in the bottoms product stream are above a high limit, below a low limit, between the high limit and low limit or some combination thereof and also based on the relationship between a set point for the flow rate of the external reflux and a high limit for the flow rate of the external reflux. At the same time, a temperature set point for the fractional distillation column is increased or decreased by an incremental amount or is left constant depending on the same factors.

Abstract: A vapor compression distillation system for distillation of any two-component liquid mixture where separation of the more volatile from the less volatile component is required. This system achieves a very high efficiency through the use of vapor compression in conjunction with three heat exchangers: a reboiler which condenses the hot vapors compressed by a vapor pump and uses the heat given up by the condensing vapor to boil bottoms liquid to produce vapor within the stripper, a distillate heat exchanger which recovers heat from the distillate stream, and a bottoms heat exchanger which recovers heat from the outgoing bottoms effluent. This particular component configuration and process results in an exceptionally stable and reliable operation requiring the continuous control of only one parameter, reboiler temperature, while fixing all other process variables.

Abstract: A vapor generating and recovering apparatus for vaporizing a liquid and condensing a vapor, the apparatus including a container having a liquid therein with a heating and cooling system in heat transfer relation with the liquid and vapor in the container. The heating and cooling system includes means to vaporize the liquid; means to condense the vaporized liquid; and, means to compress a refrigerant. The means to compress the refrigerant is in fluid communication on its high pressure side with the means to vaporize a liquid or heat a liquid and on its low pressure side with the means to condense or cool a liquid. The heating and cooling system further includes a complementary condenser system on the high pressure side of the means to compress a refrigerant, discharging its heat external to said apparatus and pump down valve means selectively closeable so that refrigerant can be pumped out of the means to compress a refrigerant.

Abstract: An evaporator apparatus (10) and method for converting a contaminated fluid including mostly water and water soluble substances into a vapor and a residue. Apparatus (10) includes a container (11) for retaining the fluid. A heat source (17) is utilized for supplying heat to evaporate the fluid. A flue assembly (18) positioned in the fluid conveys the heat from the heat source (17) through the fluid. A draft mechanism (20) draws off the resulting vapors as they are formed.

Abstract: In a fractional distillation process in which it is desired to maintain a desired overhead product composition and bottoms product composition, a set point for the flow rate of the external reflux to the fractional distillation column is increased or decreased by an incremental amount or is left constant based on whether the concentration of the heavy key component in the overhead product stream and the concentration of the light key component in the bottoms product stream are above a high limit, below a low limit, between the high limit and low limit or some combination thereof. At the same time, a temperature set point for the fractional distillation column is increased or decreased by an incremental amount or is left constant depending on the same factors. Use of these set points for process control provides control of the overhead product composition and bottoms product composition without the use of analysis controllers.

Abstract: A vapor generating and recovery apparatus for generating a vapor from a liquid solution and recovering the vapor in a liquid form in at least one chamber of the apparatus, the vapor generating portion of the chamber being in heat emitting relation with a heat emitting means and the vapor recovering portion of the chamber being in heat absorbing relationship with a heat absorbing means. A preferred system for providing heat to the vapor generating portion of the chamber and removing heat from the vapor recovering portion of the chamber is a variable heat system which includes a main heat emitting means and a main heat absorbing means in heat transfer relation with the vapor generating and recovery chamber. The variable heat system further includes a complementary heat emitting means outside the chamber between the main heat emitting means and main heat absorbing means for removing excess heat from the heat transfer fluid leaving the vaporizing portion of the chamber.

Abstract: Control of multiple distillation columns for producing anhydrous alcohol suitable for blending with gasoline to produce gasohol. The distillation process involves production of a first-stage distillate containing a predetermined amount of water, followed by azeotropic distillation in the presence of a hydrocarbon entrainer to strip the distillate of its water content, leaving anhydrous alcohol as a bottom product. Tight controls are present during first-stage distillate production to hold its proof at an optimum value derived at through material balance calculations to minimize energy consumption for the overall system. Control over the dehydrating stage is accomplished by a combination of ratio control to regulate and maintain the proper proportion of the entrainer and temperature control to regulate within the column the actual inventory of entrainer.

Abstract: A still comprising, in one aspect, a housing, a heating coil located inside the housing, a condensing coil located inside the housing and above the heating coil with vapor flow space inside turns of the coil, and having a diameter smaller than the housing which defines a vapor flow space outside turns of the coil, and means to remove condensate from the housing.

Abstract: A process and apparatus are provided controlling the heat input of an extractive distillation column. The bottom of the column is heated with a major stream of thermal energy which is either slowly varying in time or controlled by the amount of starting material mixture and with a minor stream of thermal energy which is controlled by sensing the thermodynamic state in the upper half of the column during the process. The major stream can provide about 90 percent and the minor stream about 10 percent of the heat fed to the column. The minor stream can be controlled by the temperature at one point in the upper half of the column, by the temperature difference at two points in the upper half of the column or by gas chromatographic analysis of the extract material concentration near the top of the column. The process allows one to keep a low concentration of the extract material in the raffinate.

Abstract: In an alkylation process in which an acid regenerator is utilized to separate an acid catalyst from acid soluble oil contained in a spent acid catalyst stream, the heat input to the acid regenerator is manipulated based on the feed flow rate of the spent acid catalyst stream so as to maintain a substantially constant heat input per pound of feed flowing to the acid regenerator and the liquid level in the acid regenerator is manipulated so as to maintain the acid catalyst and acid soluble oil interface in the acid regenerator at a desired level. Such manipulation of the heat input to and the liquid level in the acid regenerator results in a substantially optimum separation of acid catalyst from acid soluble oil.

Abstract: In a batch process in which reaction effluent is dumped from the reactor to a flash tank through a dump line which contains both a dump valve and a control valve, the control valve is manipulated in response to a signal which opens the control valve at a desired rate as a function of time or in response to a signal which is representative of the maximum opening of the control valve which can be maintained without exceeding a pressure limit in the flash tank whichever signal is representative of the lower opening of the control valve. In this manner, reaction effluent is withdrawn from the reactor at a substantially maximum rate without causing flashing across the dump valve and without exceeding a pressure limitation for the flash tank.

Abstract: A continuous trickle-down distillation unit for producing hydrated alcohol having a compact, elongated distillation tube through which a fluid mixture including alcohol as one of its constituents passes. Within the distillation tube only the alcohol-predominant portion of the fluid mixture is vaporized while the remaining constituents of the fluid mixture are removed. The vaporized alcohol-predominant portion is condensed within a chamber which communicates with the distillation tube and is removed therefrom by a collection plate which extends partially into the chamber.

Abstract: In a fractional distillation process in which a heating fluid and waste heat stream are utilized to supply heat to a fractional distillation column and in which the heat supplied from the waste heat stream is not controllable, control of the liquid level in the fractional distillation column is accomplished by manipulating the flow rate of the heating fluid so as to maintain a desired liquid level until such time as the flow rate of the heating fluid becomes zero at which time the flow rate of the external reflux to the fractional distillation column is manipulated to maintain a desired liquid level in the fractional distillation column. A switching of control of the liquid level provides a means by which an uncontrollable heat input may be provided to the fractional distillation column without losing control of the liquid level in the fractional distillation column.

Abstract: A vapor generating and recovering apparatus for vaporizing a liquid and condensing a vapor, the apparatus including a container having a liquid therein with heating and cooling systems in heat transfer relation with the liquid and vapor in the container. The heating and cooling systems include means to vaporize the liquid and means to condense the vaporized liquid disposed within the container. Temperature or pressure sensing means in the cooling system is utilized to shut down the heating system when a preselected vapor level is exceeded.

Abstract: In a fractional distillation column in which at least a first component and a second component are at least partially separated with the first component being removed principally as an overhead product and the second component being removed principally as a bottoms product and in which the heat supplied to the fractional distillation column is used as the primary control for the overhead product composition with the flow rate of external reflux to the fractional distillation column being used to control the bottoms product composition, a comparison of the actual concentration of the second component in the overhead product to the desired concentration is utilized to bias the control signal which is utilized to manipulate the flow rate of the external reflux to the fractional distillation column.

Abstract: An electrically and/or solar heated distillation and fractionation system for separating ethanol-water mixtures comprised with an insulated inclined vaporization chamber divided into an upper solar absorbent vaporization section and a lower pre-heating section by a vaporization floor, float means to automatically control the ethanol-water feed to the lower portion of the preheating section when distillation is taking place, means to evenly distribute the ethanol-water mixture on the vaporization floor, means to heat the ethanol-water mixture in the distillation chamber, a packed fractionation column through which the vapors from the distillation chamber must pass, means to control the temperature at the top of the fractionation column-condensing means to recover and/or recycle distillate exiting to the upper portion of the distillation column and means to remove or recycle residual aqueous liquid from the lower end of the vaporization section.

Abstract: Control of multiple distillation columns for producing anhydrous alcohol suitable for blending with gasoline to produce gasohol. The distillation process involves production of a first-stage distillate containing a predetermined amount of water, followed by azeotropic distillation in the presence of a hydrocarbon entrainer to strip the distillate of its water content, leaving anhydrous alcohol as a bottom product. Tight controls are present during first-stage distillate production to hold its proof at an optimum value derived at through material balance calculations to minimize energy consumption for the overall system. Control over the dehydrating stage is accomplished by a combination of ratio control to regulate and maintain the proper proportion of the entrainer and temperature control to regulate within the column the actual inventory of entrainer.

Abstract: The present invention provides a novel apparatus and process for vaporizing a liquid and condensing the vapors thereof. The apparatus and process utilize heat of compression for vaporizing the liquid. The apparatus includes a still (10), a closed refrigeration system (12), an auxiliary condensing coil (24) separate from refrigeration system (12), and a valve (28) for controlling heat extraction by auxiliary coil (24). In a particularly useful embodiment, the apparatus further includes a trough (41) for collecting the condensed vapors. The trough is located within still (10). Auxiliary coil (24) extracts from the vapors, heat in excess of that necessary to maintain thermal balance in the apparatus.

Abstract: A control system for distillation column with a sidedraw line is provided wherein a prediction on the influence by changes in the feed stream with respect to the sidedraw composition is made.

Abstract: A portable water distiller having an insulated container for raw water and a removable cover for the container with a low pressure seal which engages the container wall. A condenser coil is provided in the cover along with a motor-driven fan, and inlet and outlet ports are provided about the periphery of the cover to allow cooling air to be drawn into the cover over the condenser coils and motor. An inlet tube connected to the condenser coil receives steam from the container generated by a heater connected to the container bottom.

Abstract: The apparatus includes a housing enclosing a boiler in the lower portion and a water-filled condenser in the upper portion with an insulated partition between them. The entry of boiler feed water is controlled by a float valve in the boiler, and steam from the boiler is conveyed through the partition and thus through a condenser coil substantially immersed in the water in the condenser.

Abstract: A spent solvent purification apparatus for treating spent acetone includes an evaporation unit, a condensing unit, and a housing for the units which has upper and lower sections and a panel section that divides the housing interior into separate compartments for the respective units. The evaporating unit is housed by the upper section and it includes a container with an interior wall that divides the interior into upper and lower chambers. The lower chamber has a heater for heating a heat exchange fluid that is contained therein and the upper chamber is for containing the spent solvent during the batch distillation procedure to which it is subjected. Both chambers have temperature sensors which are designed to break the control circuit when the temperature in either chamber exceeds a temperature that is predetermined and set for each sensor.

Abstract: A vapor degreaser continually vaporizes and condenses a solvent bath and comprises two closed water loops associated with a refrigeration system. The water loops provide thermal storage for the degreaser and conduct heat to the solvent bath for heating the solvent and from the solvent vapors for condensing the vapors. The degreaser includes auxiliary heating and cooling coils which may be rendered totally inoperative when their operation is not energy efficient.

Abstract: A vapor generating device including a housing having an open top and closed bottom with a cleaning solvent therein. The housing is provided with first heat means in the bottom thereof to boil the solvent and cooling means in the top thereof to condense the solvent and prevent the solvent from escaping from the housing. A second heat means is provided in the bottom of the housing operable whenever a change in energy requirement within the housing is necessary. The vapor generating device is particularly useful as a cleaning device.

Abstract: In a fractionation distillation process in which a pump around stream and an external reflux are utilized to control heat removal from an upper portion of the fractional distillation column and in which the pump around stream is utilized to preheat the feed stream flowing to the fractional distillation, the flow rate of the pump around stream is manipulated so as to substantially maximize the flow rate of the pump around stream while maintaining a desired heat removal from the fractional distillation column. Priority control of the pump around stream and external reflux result in a maximum preheating of the feed stream flowing to the fractional distillation column which improves the energy efficiency of the fractional distillation process.

Abstract: A dirty or otherwise contaminated volatile solvent or other treatment fluid including relatively more volatile non-flammable and relatively less volatile flammable constituents is recovered or reclaimed by boiling it off from its impurities. As the remainder is concentrated, the evaporated vapor becomes increasingly flammable. In a work process, a treatment tank is used for chemically treating work pieces in a volatile treatment fluid which has a liquid phase and a relatively non-flammable heavier-than-air vapor phase. In this process, heat energy is added to the fluid to maintain the upper vapor phase surface at a substantial distance above the upper liquid phase surface in the tank. When the treatment fluid becomes sufficiently contaminated with dirt introduced by the work pieces or otherwise, it must be removed from the tank and replaced with clean treatment fluid.

Abstract: A mixture of xylenol, water, alcohol and other substances is put into an evaporator tank which is adjusted to a pressure and temperature to evaporate the water and alcohol. The water and alcohol vapors flow through an expansion chamber into a condenser and the condensate flows back through a distributor and a control valve into a collector tank. Through a two-stage control dial a second temperature and pressure is imposed upon the evaporator tank to evaporate the xylenol which is similarly condensed and the condensate flows back through the distributor which control valve has been actuated to direct the xylenol into a second collector tank. A second evaporator is connected through a selectively operable shut-off valve to the expansion chamber. The second evaporator tank is provided with an inlet funnel which can be heated to melt solid paraffin therein. A filter is within this funnel to filter out solid foreign matter.

Abstract: Apparatus for purifying liquid including a container for the liquid, means for heating the liquid when in the container to vaporize the liquid, means for cooling the vapor to form a condensate and a collector for collecting the condensate, the heating means comprising a condenser of a refrigerant circulatory systems and the cooling means comprising an evaporator of the system so that refrigerant liquified in the condenser gives off heat to heat the said liquid and evaporation of the liquid in the evaporator causes heat to be absorbed from the vapor thereby cooling the vapor to for the condensate.

Abstract: The portable water distiller is constructed to distill water placed within a housing and to dispense it directly into a separate storage vessel or to a distilled water space in the housing. In the latter case, the distillers are provided with a flexible impermeable partition which may be in the form of a bag and which divides the interior of the housing into a raw water space and a distilled water space. A boiler is disposed within the raw water space in order to vaporize the water and a compact radiator and fan assembly is mounted on top of the housing in order to condense the vapor into distilled water for delivery to the distilled water space within the housing. A heater-thermostat shut-off means is also provided for turning off the heater when the supply of water is too low.

Abstract: A batch operation water distiller is provided with a venting valve between the boiling chamber and the condenser. Operation of the venting valve during the heating phase prior to boiling allows entrained gases such as chlorine to be vented to the atmosphere rather than into the condenser and hence into the purified water. The valve may also be used as a humidification device for the area in which the distiller is operated. A screen-like shield is provided about the condenser inlet so as to prevent bubbles of unpurified water from entering the condenser passage. Also, a flexible fill tube is provided which allows the distilling chamber to be filled prior to use and then drained after use so as to remove mineral laden water from the chamber.

Abstract: An azeotropic column has staged processing, separate dehydration load control, and integral flash desolventizing for greater capacity, efficiency, and control of conditions in a plural stacked fluidized bed column.

Abstract: A control system for a multiple feed fractional distillation column is disclosed in which the flow rate signals of the multiple feed streams are delayed and combined for use in feedforward predictive control of the upper reflux flow, intermediate reflux flow and/or reboiler fluid flow to the fractional distillation column. Temperature measurements of the upper vapor stream, the upper reflux stream, the intermediate vapor stream and the intermediate reflux stream as well as analysis of a product stream can be utilized to provide feedback control of the fractional distillation column.