Forming Nonmetal Coating Using Specified Waveform Other Than Pure Dc Or 60 Hz Sine Wave Ac (e.g., Anodic Oxide Coating, Etc.) Patents (Class 205/106)
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Patent number: 10879010Abstract: Provided is an improved capacitor formed by a process comprising: providing an anode comprising a dielectric thereon wherein the anode comprises a sintered powder wherein the powder has a powder charge of at least 45,000 ?FV/g; and forming a first conductive polymer layer encasing at least a portion of the dielectric by applying a first slurry wherein the first slurry comprises a polyanion and a conductive polymer and wherein the polyanion and conductive polymer are in a weight ratio of greater than 3 wherein the conductive polymer and polyanion forms conductive particles with an average particle size of no more than 20 nm.Type: GrantFiled: July 26, 2018Date of Patent: December 29, 2020Assignee: KEMET Electronics CorporationInventors: Yaru Shi, Antony P. Chacko, Ajaykumar Bunha, Qingping Chen, Elisabeth Crittendon Key
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Patent number: 10858746Abstract: The present inventive concept provides a method of manufacturing graphene using electrochemistry, the method including dipping a cathode including metal and an anode including graphite into an electrolyte and applying a DC power supply between the cathode and the anode, wherein the DC power supply is a DC switching power supply applying a positive (+) voltage and a negative (?) voltage alternately and repetitively. The method according to the present inventive concept can simply mass-produce high purity graphene by applying the DC switching power supply, thereby efficiently controlling the ions to peel the graphite.Type: GrantFiled: December 10, 2018Date of Patent: December 8, 2020Inventors: Wonoh Lee, Sungmook Lim, Jong Hun Han
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Patent number: 10760175Abstract: Anodic films that have a white color, and methods for forming the same, are described. According to some embodiments, the anodic films have multiple metal oxide layers. A first layer can provide scratch and chemical resistance and a second layer can provide a light diffusing pore structure that diffusely reflects incoming light and provides a white appearance to the anodic film. According to some embodiments, the anodic films also include a smoothed barrier layer that specularly reflects incoming light so as to brighten the appearance and enhance the white color of the anodic film. The resulting anodic films have an opaque white appearance not achievable using conventional techniques. The anodic films are well suited for providing cosmetically appealing coatings for consumer products, such as housings for electronic products.Type: GrantFiled: October 24, 2016Date of Patent: September 1, 2020Assignee: APPLE INC.Inventors: Masashige Tatebe, Takahiro Oshima, Jody R. Akana, Yutaka Nakagishi, Junichi Katayama, Kenji Hara, Yasuhiro Ito, Ayumi Hongou
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Patent number: 10683581Abstract: Disclosed is a method for the plasma-electrolytic deposition of a titanium-based non-metallic protective coating on an aluminum-containing material that exhibits excellent resistance to corrosion and high resistance against wear; a coated aluminum-containing metallic article, wherein the coating comprised of oxides and hydroxides of the elements titanium and aluminum has a thickness of at least 15 microns and a cross-section hardness (HV) of at least 800; and a device comprising an arrangement of two adjacent parts at least one being selected from an aluminum-containing metallic material that is coated according to the method and in frictional connection with the other part wherein under operation the frictionally connected parts move relatively to each other, such as, pistons moving in the cylinder within the powertrain of a vehicle.Type: GrantFiled: June 11, 2018Date of Patent: June 16, 2020Assignee: Henkel AG & Co. KGaAInventors: James P. Golding, Jacques Beauvir, Christian Rosenkranz
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Patent number: 10392560Abstract: Compositions useful for the selective removal of titanium nitride and/or photoresist etch residue materials relative to metal conducting, e.g., tungsten, and insulating materials from a microelectronic device having same thereon. The removal compositions contain at least one oxidant and one etchant, may contain various corrosion inhibitors to ensure selectivity.Type: GrantFiled: January 17, 2017Date of Patent: August 27, 2019Assignee: ENTEGRIS, INC.Inventors: Jeffrey A. Barnes, Emanuel I. Cooper, Li-Min Chen, Steven Lippy, Rekha Rajaram, Sheng-Hung Tu
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Patent number: 10233558Abstract: A method of fabricating a part coated with a protective coating, the method including using micro-arc oxidation treatment to form a protective coating on the outside surface of a part, the part including a niobium matrix having metallic silicide inclusions present therein, the current passing through the part being controlled during the micro-arc oxidation treatment in order to subject the part to a succession of current cycles, the ratio of (quantity of positive charge applied to the part)/(quantity of negative charge applied to the part) lying in the range 0.80 to 1.6 for each current cycle.Type: GrantFiled: December 8, 2014Date of Patent: March 19, 2019Assignee: SAFRAN AIRCRAFT ENGINESInventor: Stéphane Knittel
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Patent number: 9809894Abstract: In a process for anodizing a metal object (12), the metal object (12) is contacted with an anodizing electrolyte (32), and is first pre-anodized so as to grow a thin oxide film on the surface. The microscopic surface area is then deduced from electrical measurements either during pre-anodizing or on the pre-anodized surface. The metal object (12) can then be anodized. This is applicable when treating an implant to provide a surface that has the ability to incorporate biocidal material such as silver ions. The pre-anodizing uses a low voltage, for example no more than 2. V, and may take less than 120 seconds.Type: GrantFiled: January 13, 2012Date of Patent: November 7, 2017Assignee: Accentus Medical LimitedInventor: Andrew Derek Turner
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Patent number: 9487877Abstract: In one embodiment, SWNTs are synthesized from an embedded catalyst in a modified porous anodic alumina (PAA) template. Pd is electrodeposited into the template to form nanowires that grow from an underlying conductive layer beneath the PAA and extend to the initiation sites of the SWNTs within each pore. Individual vertical channels of SWNTs are created, each with a vertical Pd nanowire back contact. Further Pd deposition results in annular Pd nanoparticles that form on portions of SWNTs extending onto the PAA surface. Two-terminal electrical characteristics produce linear I-V relationships, indicating ohmic contact in the devices.Type: GrantFiled: February 1, 2008Date of Patent: November 8, 2016Assignee: PURDUE RESEARCH FOUNDATIONInventors: Aaron D. Franklin, Matthew R. Maschmann, Timothy S. Fisher, Timothy D. Sands
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Patent number: 9096943Abstract: Metal objects are treated by anodising (P, SE) the metal object in contact with an acidic solution, and then subjecting the anodised metal object to a reversed voltage (VR). The anodising is performed in two stages, firstly to passivate (P) with the formation of a surface layer, and secondly to form pits in this surface layer (SE). The second stage (SE) of anodising is performed at a lower voltage than the first stage (P). After the reversed voltage step (VR) the metal object is then contacted with a biocidal metal-containing solution. Biocidal metal is absorbed into the surface of the metal object, resulting in improved biocidal properties. The lower voltage of the second stage anodising (SE) results in reduced processing time.Type: GrantFiled: March 29, 2010Date of Patent: August 4, 2015Assignee: Accentus Medical LimitedInventors: James Timothy Shawcross, David Richard Lewis, Andrew Derek Turner
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Patent number: 9047957Abstract: A bit cell of the PROM-device comprises a carbon nanotube having a tilted portion comprising a free end and a fixed portion which is to the reference node. The carbon nanotube comprises a structural defect between the fixed and the tilted portion which causes the carbon nanotube to tilt such that the free end is electrically connected to either the storage electrode or an opposite release electrode.Type: GrantFiled: July 24, 2012Date of Patent: June 2, 2015Assignee: Thomson LicensingInventors: Holger Kropp, Meinolf Blawat
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Publication number: 20150114840Abstract: An antibacterial coating that is composed of silver is disclosed, as well as medical tools and implants comprising such a coating, and a method and an apparatus for the production of such a coating. The medical tools or the dental or orthopaedic implant comprises a metal or metal alloy having a treated surface wherein the treated surface is at least partially converted to an oxide film by plasma electrolytic oxidation using a colloid-dispersed system and wherein the converted surface is partially covered by islands formed by colloid-dispersed silver-particles of the colloid-dispersed system. An Ag—TiO2 coating shows excellent properties in terms of antibacterial efficacy (even against multi-resistant strains), adhesion and biocompatibility. The life-time of an implant in a human body is increased. The antibacterial coating can be used in the field of traumatology, orthopaedic, osteosynthesis and/or endoprothesis, especially where high infection risk exists.Type: ApplicationFiled: January 6, 2014Publication date: April 30, 2015Inventors: Elvira Dingeldein, Cyrille Gasqueres, Frank Witte, Amir Eliezer
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Patent number: 9005765Abstract: Provided is an anodic oxide processing method in which the generation of cracks is suppressed in an anodic oxide film formed on an aluminum alloy substrate surface, such as an inner wall of a vacuum chamber of a plasma processing device, and an anodic oxide film having low heat reflectivity and a high withstand voltage is formed with high efficiency. The method for forming an anodic oxide film involves forming the anodic oxide film on the surface of a JIS 6061 aluminum alloy substrate in a sulfuric acid solution or a mixed acid solution of sulfuric acid and oxalic acid.Type: GrantFiled: September 16, 2009Date of Patent: April 14, 2015Assignee: Kobe Steel, Ltd.Inventors: Koji Wada, Jun Hisamoto
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Publication number: 20150093594Abstract: The present invention provides an aqueous treatment solution containing sulfate ions SO42? in a concentration greater than or equal to 0.01 mol/l, to treat sheet metal including a steel substrate coated on at least one face with a coating including at least zinc and magnesium to reduce blackening or tarnishing of the sheet metal during storage. The present invention also provides a sheet metal treated with a solution of this type.Type: ApplicationFiled: January 1, 2012Publication date: April 2, 2015Applicant: ARCELORMITTAL INVESTIGACIÓN Y DESARROLLO, S.L.Inventors: Daniel Chaleix, Christian Allely, Maxime Monnoyer, Pascale Feltin
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Patent number: 8951402Abstract: A method of ultra-fast boriding of a metal surface. The method includes the step of providing a metal component, providing a molten electrolyte having boron components therein, providing an electrochemical boriding system including an induction furnace, operating the induction furnace to establish a high temperature for the molten electrolyte, and boriding the metal surface to achieve a boride layer on the metal surface.Type: GrantFiled: November 1, 2012Date of Patent: February 10, 2015Assignee: UChicago Argonne, LLCInventors: Servet Timur, Guldem Kartal, Osman L. Eryilmaz, Ali Erdemir
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Patent number: 8890409Abstract: An array of microcavity plasma devices is formed in a unitary sheet of oxide with embedded microcavities or microchannels and encapsulated metal driving electrodes isolated by oxide from the microcavities or microchannels and arranged so as to generate sustain a plasma in the embedded microcavities or microchannels upon application of time-varying voltage when a plasma medium is contained in the microcavities or microchannels.Type: GrantFiled: May 14, 2009Date of Patent: November 18, 2014Assignee: The Board of Trustees of the University of IllnoisInventors: J. Gary Eden, Sung-Jin Park, Taek-Lim Kim, Kwang-Soo Kim
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Publication number: 20140332394Abstract: An antibacterial coating that is composed of silver is disclosed, as well as medical tools and implants comprising such a coating, and a method and an apparatus for the production of such a coating. The medical tools or the dental or orthopaedic implant comprises a metal or metal alloy having a treated surface wherein the treated surface is at least partially converted to an oxide film by plasma electrolytic oxidation using a colloid-dispersed system and wherein the converted surface is partially covered by islands formed by colloid-dispersed silver-particles of the colloid-dispersed system. An Ag—TiO2 coating shows excellent properties in terms of antibacterial efficacy (even against multi-resistant strains), adhesion and biocompatibility. The life-time of an implant in a human body is increased. The antibacterial coating can be used in the field of traumatology, orthopaedic, osteosynthesis and/or endoprothesis, especially where high infection risk exists.Type: ApplicationFiled: January 6, 2014Publication date: November 13, 2014Inventors: Elvira Dingeldein, Cyrille Gasqueres, Frank Witte, Amir Eliezer
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Publication number: 20140268283Abstract: Variable-emittance, electrochromic devices utilizing IR-active conducting polymers and methods of preparing the same are disclosed.Type: ApplicationFiled: March 15, 2013Publication date: September 18, 2014Applicant: ASHWIN-USHAS CORPORATION, INC.Inventor: Prasanna Chandrasekhar
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Patent number: 8819930Abstract: The invention addresses the problem of improving the adhesion between silver surfaces and resin materials, such as epoxy resins and mold materials, used in the production of electronic devices. The invention provides a method for improving the adhesion between a silver surface and a resin material comprising a step of electrolytically treating the silver surface with a solution containing a hydroxide selected from alkali metal hydroxides, alkaline earth metal hydroxides, ammonium hydroxides and mixtures thereof, wherein the silver surface is the cathode.Type: GrantFiled: September 10, 2009Date of Patent: September 2, 2014Assignee: Atotech Deutschland GmbHInventors: Christian Wunderlich, Robert Rüther, Jürgen Barthelmes, Sia-Wing Kok, Nadine Menzel
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Patent number: 8784635Abstract: The invention relates to a method for grafting an organic film onto an electrically conductive or semiconductive surface by electro-reduction of a solution, wherein the solution comprises one diazonium salt and one monomer bearing at least one chain polymerizable functional group. During the electrolyzing process, at least one protocol consisting of an electrical polarization of the surface by applying a variable potential over at least a range of values which are more cathodic that the reduction or peak potential of all diazonium salts in said solution is applied. The invention also relates to an electrically conducting or semiconducting surface obtained by implementing this method. The invention further relates to electrolytic compositions.Type: GrantFiled: February 28, 2007Date of Patent: July 22, 2014Assignees: Alchimer, Alchimedics, Inc.Inventor: Christophe Bureau
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Publication number: 20140166493Abstract: An antibacterial coating that is composed of silver is disclosed, as well as medical tools and implants comprising such a coating, and a method and an apparatus for the production of such a coating. The medical tools or the dental or orthopaedic implant comprises a metal or metal alloy having a treated surface wherein the treated surface is at least partially converted to an oxide film by plasma electrolytic oxidation using a colloid-dispersed system and wherein the converted surface is partially covered by islands formed by colloid-dispersed silver-particles of the colloid-dispersed system. An Ag—TiO2 coating shows excellent properties in terms of antibacterial efficacy (even against multi-resistant strains), adhesion and biocompatibility. The life-time of an implant in a human body is increased. The antibacterial coating can be used in the field of traumatology, orthopaedic, osteosynthesis and/or endoprothesis, especially where high infection risk exists.Type: ApplicationFiled: January 6, 2014Publication date: June 19, 2014Applicant: aap Biomaterials GmbHInventors: Elvira Dingeldein, Cyrille Gasqueres, Frank Witte, Amir Eliezer
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Patent number: 8702954Abstract: The object of the present invention is to provide a process for producing a metal substrate of superior corrosion resistance and finish, and a surface-treated metal substrate obtained by the process; and a surface treatment process that is capable of providing a metal substrate of superior corrosion resistance and finish, and a surface-treated metal substrate obtained by the process. Specifically, the present invention provides a process for producing a surface-treated metal substrate, comprising the steps of immersing a metal substrate for use as a cathode in a treatment composition (I) comprising water and metal component (A), and applying electric current thereto for 10 to 600 seconds by superposing an AC voltage (Va) with a frequency of 0.1 to 1,000 Hz and a peak-to-peak voltage of 1 to 40 V onto a 1 to 50 V DC voltage (Vd).Type: GrantFiled: December 17, 2008Date of Patent: April 22, 2014Assignee: Kansai Paint Co., Ltd.Inventor: Kentaro Kubota
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Publication number: 20140008231Abstract: Disclosed articles as results of a microarc oxidation process, or plurality thereof, which are not limited by size, specifically by certain dimensions of their size, such as their length. Different sections or surfaces of articles of the invention may be subjected to a microarc oxidation process at any given time, such as by gradually subjecting a surface of an article to a microarc oxidation process, or such as by sequentially subjecting different sections of an articles to a microarc oxidation process. Furthermore, disclosed are methods for manufacturing of articles of the invention, or otherwise for subjecting articles of the invention to a microarc oxidation process, or plurality thereof. In some examples, tubes of above 6 meter in length may be coated according to methods of the invention. The coating of said tubes may be beneficial for desalination applications. In other examples, only grooves of pulleys are coated.Type: ApplicationFiled: July 6, 2011Publication date: January 9, 2014Applicant: PCT PROTECTIVE COATING TECHNOLOGIES LIMITEDInventor: David Amit
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Patent number: 8608869Abstract: A method is disclosed for improving the corrosion behavior of cast magnesium alloy articles in which the magnesium alloy comprises an average composition of more than about 5 per cent by weight of aluminum. A microstructure with regions of varying aluminum content is developed during solidification. The microstructure comprises magnesium-rich grains generally surrounded by an aluminum-enriched phase on the boundaries between adjacent grains. The magnesium-rich grain interiors are then selectively chemically or electrochemically attacked to leave a more corrosion resistant aluminum-enriched surface on the articles. The corrosion resistance of the articles may be further enhanced by one or more of anodizing, aluminizing or painting the corrosion-resistant aluminum-enriched surface.Type: GrantFiled: December 16, 2010Date of Patent: December 17, 2013Assignee: GM Global Technology Operations LLCInventors: Deepika Sachdeva, Arun M. Kumar, Guangling Song
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Patent number: 8603317Abstract: A housing having a coating is disclosed. The housing comprises a base substrate made of metallic material; a micro-arc oxide layer formed on the base substrate; and a protection outer film formed on the micro-arc oxide layer and comprising a coating layer and a metallic layer, wherein the metallic layer is formed on the micro-arc oxide layer and covers a portion of the micro-arc oxide layer; and the coating layer is formed on a remaining portion of the micro-arc oxide layer so that the micro-arc oxide layer is covered by the metallic layer and the coating layer.Type: GrantFiled: December 6, 2011Date of Patent: December 10, 2013Assignees: Fu Zhun Precision Industry (Shen Zhen) Co., Ltd., Foxconn Technology Co., Ltd.Inventors: Zhe-Xuan Zhang, Shih-Pin Wang, Yan Xiong, Che-Chao Chu
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Patent number: 8591717Abstract: This is a process to generate alternating current without an external source for cell-houses in electrowinning or electrorefining of copper or other products in which the electric source consists of a conventional rectifier-transformer group that supplies continuous electrical current to the cell-house, which is connected in parallel to a device characterized by having the capacity to extract an electrical current from the cell-house for a period of time and then return it in another period of time, whether periodically or semiperiodically and without changing the average value of the electrical current, supplied to the cell-house by the rectifier-transformer. This results in a electrical current in the cell-house that is the superimposition of a continuous and alternating current. This process is designed to overcome the barrier of electric potential produced by the presence of the pure continuous electric field in cell-houses through the electric agitation of an ion-rich electrolyte.Type: GrantFiled: March 28, 2008Date of Patent: November 26, 2013Assignee: Hecker Electronica de Potencia y Procesos S.A.Inventor: Juan Pablo Bustos Robledo
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Publication number: 20130116696Abstract: The present disclosure is directed, at least in part, to a method of producing ceramic layers on magnesium and its alloys, a magnesium implant with a ceramic layer made by the method, and a magnesium implant having a biocompatible ceramic layer substantially free of material which impairs the biocompatibility of said biocompatible ceramic layer.Type: ApplicationFiled: November 7, 2012Publication date: May 9, 2013Applicant: Synthes USA, LLCInventor: Synthes USA, LLC
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Patent number: 8404096Abstract: The invention relates to methods of preparation of highly sensitive potentiometric sensors with an electroconductive polymer film as a sensing element.Type: GrantFiled: August 23, 2002Date of Patent: March 26, 2013Assignee: Sensortec LimitedInventors: Duncan Ross Purvis, Olga Leonardova, Dmitri Alexandrovich Farmakovski, Vladimir Rurikovich Tcherkassov
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Publication number: 20130026042Abstract: A titanium dioxide coating method is disclosed. An electrolyte containing Ti3+, an oxidant, and at least one of NO3? and NO2? is provided for an electrodeposition device, wherein the oxidant is configured for essentially oxidizing Ti3+ into Ti4+. A substrate is immersed into the electrolyte and electrically connected to the electrodeposition device. A cathodic current is applied to the substrate via the electrodeposition device for reduction of NO2? or NO3?. A titanium dioxide film is thus formed on the surface of the substrate. The thickness, porosity, and morphology of the titanium dioxide film can be controlled by varying the electroplating parameters, and relatively uniform deposits on various substrates of complex shapes can be obtained by use of low cost instruments. The resultant structure of Ti4+ species oxidized from Ti3+ by the oxidant can be used to control the deposition rate of TiO2.Type: ApplicationFiled: September 28, 2012Publication date: January 31, 2013Applicant: NATIONAL TSING HUA UNIVERSITYInventor: NATIONAL TSING HUA UNIVERSITY
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Publication number: 20130001089Abstract: A method of preparing graphene sheets. The method includes: immersing a portion of a first electrode and a portion of a second electrode in a solution containing an acid, an anionic surfactant, a salt, an oxidizing agent, or any combination thereof as an electrolyte, the immersed portion of the first electrode including a first carbon material and the immersed portion of the second electrode including a second carbon material or a metal; causing a potential to exist between the first and second electrodes; and recovering, from the solution, graphene sheets exfoliated from the carbon material(s). Also disclosed is a method of preparing a graphene film electrode. The method includes: dissolving graphene sheets in an organic solvent to form a solution, applying the solution on a substrate, adding deionized water to the solution on the substrate so that a graphene film is formed, and drying the graphene film.Type: ApplicationFiled: June 28, 2011Publication date: January 3, 2013Applicant: Academia SinicaInventors: Lain-Jong Li, Ching-Yuan Su
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Patent number: 8337689Abstract: Disclosed herein is a composition for plasma electrolytic oxidation (PEO) treatment of magnesium alloy products, which contains a sodium hydroxide (NaOH) solution as a main component, the composition comprising, based on the weight of sodium hydroxide contained in the sodium hydroxide solution: 1-20 wt % of sodium fluoride (NaF); 1-15 wt % of trisodium phosphate (Na3PO4); 1-10 wt % of sodium pyrophosphate (Na4P2O7); 1-20 wt % of aluminum hydroxide (Al(OH)3); 1-20 wt % of sodium fluorosilicate (Na2SiF6); 1-10 wt % of potassium hydroxide (KOH); 1-15 wt % of potassium acetate (C2H3O2K); and 1-10 wt % of rare earth metal powder. The disclosed composition can form a firm, dense and uniform oxide film on the surface of a magnesium alloy product.Type: GrantFiled: August 13, 2010Date of Patent: December 25, 2012Assignee: Wiscohitec Co., Ltd.Inventors: Gi Yeol Yun, Jae In You, Jae Yong You, Jae Gon Yun, Jin Hie Kim, Chang Hun Park, Duck Hee Kim, Mi Kyeong Lee
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Patent number: 8172561Abstract: A metal part in which a base material of silicon-aluminum alloy having 1 to 25% by mass of silicon as an anode is immersed in an electrolyte together with a cathode, and at least a portion of a surface of the base material is anodized and coated with an anodic oxide film. A current density provided to both the anode and the cathode is increased from an initial current density of 0 A/dm2 at a rate between 0.15 and 0.35 A/dm2 per minute, wherein once the current density reaches a prescribed current density of between 0.8 A/dm2 and 1.2 A/dm2, the current density provided to the anode and the cathode is maintained at the prescribed current density.Type: GrantFiled: June 5, 2009Date of Patent: May 8, 2012Assignee: JTEKT CorporationInventors: Toshiyuki Saito, Takumi Mio, Koji Nishi, Hajime Fukami, Atsushi Eto, Hiroyuki Yao
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Publication number: 20120031765Abstract: A process for the corrosion protection of metals such as magnesium, aluminium or titanium, where at least two steps are used, including both plasma electrolytic oxidation and chemical passivation. The combination of these two processing steps enhances the corrosion resistance performance of the surface beyond the capability of either of the steps in isolation, providing a more robust protection system. This process may be used as a corrosion protective coating in its own right, or as a protection-enhancing pre-treatment for top-coats such as powder coat or e-coat. When used without an additional top-coat, the treated parts can still retain electrical continuity with and adjoining metal parts. Advantages include reduced cost and higher productivity than traditional plasma-electrolytic oxidation systems, improved corrosion protection, greater coating robustness and electrical continuity.Type: ApplicationFiled: March 30, 2010Publication date: February 9, 2012Applicant: KERONITE INTERNATIONAL LTDInventors: James Curran, Stephen Hutchins, Suman Shrestha
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Publication number: 20110297549Abstract: An aluminum alloy-and-resin composite includes an aluminum alloy substrate, an anodic oxide film formed on the substrate, and resin composition bonded with the anodic oxide film. The anodic oxide film has nano-pores with an average diameter of about 30-60 nm. The resin composition fills the nano-pores and coatings surfaces of the anodic oxide film. The resin composition contains crystalline thermoplastic synthetic resins.Type: ApplicationFiled: April 15, 2011Publication date: December 8, 2011Applicants: HON HAI PRECISION INDUSTRY CO., LTD., HONG FU JIN PRECISION INDUSTRY (ShenZhen) CO., LTD.Inventors: WEN-RONG CHEN, HUANN-WU CHIANG, CHENG-SHI CHEN, DAI-YU SUN, YUAN-YUAN FENG, KE HUANG, CHI LAI, LI-MING SHEN
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Publication number: 20110223390Abstract: Disclosed is a polymer brush composite including a substrate, a solid layer disposed on the substrate and containing at least one of a metal or a metal oxide, and a plurality of polymer chains penetrating the solid layer in such a manner that one end of each of the polymer chains is disposed on the upper side of the substrate and the other end of each the polymer chains is exposed at a surface of the solid layer on an opposite side of the solid layer to the substrate. The polymer brush composite exhibits good adhesion between an organic polymer compound and an inorganic material and has the surface the organic polymer compound and the inorganic material uniformly coexist.Type: ApplicationFiled: September 25, 2009Publication date: September 15, 2011Inventors: Takao Hanawa, Yusuke Tsutsumi, Kwangwoo Nam, Akio Kishida, Hisatoshi Kobayashi, Chiaki Yoshikawa
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Publication number: 20110222189Abstract: A patterned magnetic recording medium, accessible by a magnetic recording head, including a plurality of tracks, a width direction of each track and that of the magnetic recording head being of a skew angle. The patterned magnetic recording medium includes a plurality of magnetic dots, each corresponding to a recording bit, formed on a non-magnetic material. The plurality of magnetic dots are arranged in a plurality of arrays, each array corresponding to one of the tracks. Every N adjacent magnetic dots of the array define a polygon, one side thereof being parallel to the corresponding track, and another side thereof being parallel to a direction corresponding to the skew angle of the corresponding track.Type: ApplicationFiled: November 15, 2010Publication date: September 15, 2011Applicant: Fuji Electric Device Technology Co., Ltd.Inventor: Shinji Uchida
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Publication number: 20110220289Abstract: A member for a plasma treatment apparatus is provided, which has excellent anti-sticking properties, is suitable, for example, as a lower electrode in CVD apparatuses, has a stable shape as the lower electrode, and can suppress abnormal discharge during plasma treatment. The member for a plasma treatment apparatus comprises a base material formed of an aluminum alloy having a smoothly machined surface and a treated anodic oxide coating provided on the surface of the base material and formed by hydrating an anodic oxide coating formed on the surface of the base material to form microcracks therein. The anodic oxide coating has a leak current density of more than 0.9×10?5 A/cm2 at an applied voltage of 100 V, a thickness of not less than 3 ?m, an arithmetic average surface roughness of less than 1 ?m, and a dissolution rate of less than 100 mg/dm2/15 min in a phosphoric and chromic acid immersion test. The flatness of the surface on which the anodic oxide coating has been formed is not more than 50 ?m.Type: ApplicationFiled: December 2, 2008Publication date: September 15, 2011Applicant: Kabushiki Kaisha Kobe Seiko Sho (Kobe Steel, Ltd.)Inventors: Toshiyuki Tanaka, Jun Hisamoto, Hiroto Sugano
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Patent number: 8002960Abstract: A method for manufacturing a nano-particulate electrode for Dye Solar Cells including the steps of providing an electrically conductive substrate, formation of a nanoparticulate layer on the substrate, application of dye to the nanoparticulate layer and an additional step of electrolytic treatment of the nanoparticulate layer in an electrolyte.Type: GrantFiled: December 17, 2004Date of Patent: August 23, 2011Assignee: Dyesol Ltd.Inventors: Igor Lvovich Skryabin, Graeme Leslie Evans
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Publication number: 20110181169Abstract: An array of microcavity plasma devices is formed in a unitary sheet of oxide with embedded microcavities or microchannels and embedded metal driving electrodes isolated by oxide from the microcavities or microchannels and arranged so as to generate sustain a plasma in the embedded microcavities or microchannels upon application of time-varying voltage when a plasma medium is contained in the microcavities or microchannels.Type: ApplicationFiled: May 14, 2009Publication date: July 28, 2011Applicant: The Board of Trustees of the University of IllinoiInventors: J. Gary Eden, Sung-Jin Park, Taek-Lim Kim, Kwang-Soo Kim
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Publication number: 20110174627Abstract: Provided is an anodic oxide processing method in which the generation of cracks is suppressed in an anodic oxide film formed on an aluminum alloy substrate surface, such as an inner wall of a vacuum chamber of a plasma processing device, and an anodic oxide film having low heat reflectivity and a high withstand voltage is formed with high efficiency. The method for forming an anodic oxide film involves forming the anodic oxide film on the surface of a JIS 6061 aluminum alloy substrate in a sulfuric acid solution or a mixed acid solution of sulfuric acid and oxalic acid. The total voltage in the direction of the film thickness is at least 1650 V·?m for the entire film thickness of the anodic oxide film formed.Type: ApplicationFiled: September 16, 2009Publication date: July 21, 2011Applicant: Kabushiki Kaisha Kobe Seiko Sho (Kobe Steel, Ltd.)Inventors: Koji Wada, Jun Hisamoto
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Publication number: 20110174628Abstract: A cathodic member for electrochemical cells used in hypochlorite production comprises a zirconium plate coated with a zirconium oxide layer, which is particularly suitable for minimising the decomposition of the hypochlorite product while ensuring a prolonged lifetime. The coated zirconium plate can be used as the cathodic plate in a monopolar cell, or can be welded to a titanium plate for use in a bipolar configuration.Type: ApplicationFiled: March 28, 2011Publication date: July 21, 2011Applicant: Industrie De Nora S.p.A.Inventors: Carl W. Brown, JR., Richard C. Carlson, Kenneth L. Hardee
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Publication number: 20110160047Abstract: “It has been demanded to produce titanium dioxide having an excellent photocatalytic activity and an excellent super-hydrophilic property by a simple procedure suitable for the production on an industrial scale. Rutile-type titanium dioxide having an excellent photocatalytic activity can be produced by carrying out the anodic oxidization of the surface of a base material comprising titanium or a titanium alloy by applying a voltage (e.g., a high voltage) or carrying out the anodic oxidation of the surface of the base material under high current density conditions. Further, a film is produced on the surface of the base material by the anodic oxidation technique by applying a voltage or the anodic oxidization technique under high current density conditions, and the film is subjected to heat treatment, thereby producing rutile-type titanium dioxide having excellent crystallinity.Type: ApplicationFiled: May 26, 2009Publication date: June 30, 2011Inventors: Naoya Masahasshi, Yoshiteru Mizukoshi, Naofumi Ootsu, Yu Matsuda, Satoshi Senboshi
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Publication number: 20110123141Abstract: A manufacturing method of a bearing according to the present invention includes a bearing forming member preparing step S10 for preparing a bearing forming member W made of AlSi alloy containing 5 weight% to 40 weight % of Si, a pressure sizing step S20 which decreases a maximum crest height Rp of a bearing surface 132 by performing pressure sizing of the bearing surface 132 of the bearing forming member W, and an aluminum oxide film forming step S30 for forming an aluminum oxide film 36 on the bearing surface 132 of the bearing forming member W by anodizing the bearing surface 132 of the bearing forming member W in this order. According to the manufacturing method of a bearing of the present invention, it is possible to manufacture a bearing which can maintain the bearing performance over a long period.Type: ApplicationFiled: November 5, 2007Publication date: May 26, 2011Applicant: GAST JAPAN CO., LTDInventor: Yoshinari Yokoo
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Publication number: 20110114494Abstract: The invention relates to a method for compressing a device component of aluminum and/or an aluminum alloy, comprising an oxide layer on the surface that is produced in a uniform manner by anodizing. The compression method comprises a hot water compression of the component in a bath of completely desalinated water while using positive pressure for a period of at least one minute. Due to the pressure application in a closed compression chamber, the compression process is accelerated and the capacity of the anodizing unit is increased.Type: ApplicationFiled: May 5, 2009Publication date: May 19, 2011Inventor: Dierk Warburg
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Publication number: 20110022162Abstract: An endoprosthesis includes an endoprosthesis wall that includes a ceramic coating and a polymer coating containing a therapeutic agent. A ceramic coating can be formed on the wall by electrochemical deposition. Cyclic voltammetry can be conducted to modify the density of the hydroxyl groups on the surface of the ceramic coating.Type: ApplicationFiled: July 23, 2009Publication date: January 27, 2011Applicant: BOSTON SCIENTIFIC SCIMED, INC.Inventors: Rajesh Radhakishnan, Liliana Atanasoska, Daniel VanCamp
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Publication number: 20100270164Abstract: The object of the present invention is to provide a process for producing a metal substrate of superior corrosion resistance and finish, and a surface-treated metal substrate obtained by the process; and a surface treatment process that is capable of providing a metal substrate of superior corrosion resistance and finish, and a surface-treated metal substrate obtained by the process. Specifically, the present invention provides a process for producing a surface-treated metal substrate, comprising the steps of immersing a metal substrate for use as a cathode in a treatment composition (I) comprising water and metal component (A), and applying electric current thereto for 10 to 600 seconds by superposing an AC voltage (Va) with a frequency of 0.1 to 1,000 Hz and a peak-to-peak voltage of 1 to 40 V onto a 1 to 50 V DC voltage (Vd).Type: ApplicationFiled: December 17, 2008Publication date: October 28, 2010Inventor: Kentaro Kubota
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Patent number: 7780835Abstract: A capacitor comprising an aluminum anode and a dielectric layer comprising phosphate doped aluminum oxide and process for making the capacitor. The capacitor has a CV Product of at least 9 ?F?V/cm2 at 250 volts. Furthermore, the capacitor is formed by the process of: forming an aluminum plate; contacting the plate with an anodizing solution comprising glycerine, 0.1 to 1.0%, by weight, water and 0.01 to 0.5%, by weight, orthophosphate; applying a voltage to the aluminum plate and determining an initial current; maintaining the first voltage until a first measured current is no more than 50% of the initial current; increasing the voltage and redetermining the initial current; maintaining the increased voltage until a second measured current is no more than 50% of the redetermined initial current, and continuing the increasing of the voltage and maintaining the increased voltage until a final voltage is achieved.Type: GrantFiled: April 22, 2009Date of Patent: August 24, 2010Assignee: Kemet Electronics CorporationInventors: John Tony Kinard, Brian John Melody, David Alexander Wheeler, Duane Earl Stenzinger, Albert Kennedy Harrington
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Patent number: 7727372Abstract: A method for anodizing valve metal structures to a target formation voltage is described. The valve metal structures are placed in an anodizing electrolyte and connected to a power supply that generates a source voltage to at least one current limiting device. If at least two current limiting devices are used, they are in series with the valve metal structures with the one current limiting device connected to at least one structure. The valve metal structures are then subjected to a current that decreases over time, a formation voltage that increases over time to a level below the voltage from the power supply and a power level that is self-adjusted to a level that decreases excessive heating in the structure. The invention also includes the components for the method.Type: GrantFiled: December 5, 2005Date of Patent: June 1, 2010Assignee: Greatbatch Ltd.Inventors: Yanming Liu, Neal Nesselbeck, David Goad, Barry Muffoletto
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Patent number: 7651736Abstract: The present invention provides a method of producing a structure, which is capable of easily obtaining a structure of the nanometer scale by using an anodic oxidation method. A method of producing a structure with a hole includes: forming first projected structures regularly arranged on a substrate; forming a first anodic oxidating layer on the substrate having the first projected structures, thereby forming first recessed structures at center portions of cells formed by the projected structures on the anodic oxidating layer; removing the first projected structures to form holes; and subjecting the first anodic oxidating layer to anodic oxidation to form holes at positions of the first recessed structures.Type: GrantFiled: June 22, 2007Date of Patent: January 26, 2010Assignee: Canon Kabushiki KaishaInventors: Aya Imada, Toru Den
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Publication number: 20090258188Abstract: Disclosed herein is a composition for forming an inorganic pattern, comprising an inorganic precursor, at least one stabilizer selected from ?-diketone and ?-ketoester, and a solvent. Use of the composition enables efficient and inexpensive formation of an inorganic micropattern.Type: ApplicationFiled: August 28, 2008Publication date: October 15, 2009Applicant: SAMSUNG ELECTRONICS CO., LTD.Inventors: Seung Nam CHA, Dae Joon KANG, Byong Gwon SONG
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Patent number: 7578921Abstract: An article of manufacture and a process for making the article by generating corrosion-, heat- and abrasion-resistant ceramic coatings comprising titanium and/or zirconium dioxide using direct and alternating current on anodes comprising aluminum and/or titanium. Optionally, the article is coated with additional layers, such as paint, after deposition of the ceramic coating.Type: GrantFiled: October 25, 2004Date of Patent: August 25, 2009Assignee: Henkel KGaAInventor: Shawn E. Dolan