Plural Separate Currents Or Voltages Applied Patents (Class 205/659)
  • Patent number: 11702759
    Abstract: A method of and system for surface finishing an additive manufactured part. A part having a surface roughness with macroasperities is placed in a chamber with an electrolyte and an electrode. A pulse/pulse reverse power supply is connected to the part rendering it anodic and connected to the electrode rendering it cathodic.
    Type: Grant
    Filed: August 11, 2021
    Date of Patent: July 18, 2023
    Assignee: Faraday Technology, Inc.
    Inventors: Timothy D. Hall, Holly M. Garich, Heather McCrabb, Earl Jennings Taylor
  • Patent number: 9365947
    Abstract: A mask is formed over a first conductive portion of a conductive layer to expose a second conductive portion of the conductive layer. An electrolytic process is performed to remove conductive material from a first region and a second region of the second conductive portion. The second region is aligned with the mask relative to an electric field applied by the electrolytic process. The second region separates the first region of the second conductive portion from the first conductive portion. The electrolytic process is concentrated relative to the second region such that removal occurs at a relatively higher rate in the second region than in the first region.
    Type: Grant
    Filed: October 4, 2013
    Date of Patent: June 14, 2016
    Assignee: Invensas Corporation
    Inventors: Cyprian Emeka Uzoh, Sitaram Arkalgud
  • Patent number: 8974656
    Abstract: A method for surface roughening a metal work piece includes disposing a region of the workpiece to be roughened proximate to a counter electrode. The region of the workpiece to be roughened and the counter electrode are subsequently disposed together in an electrolyte. An electric potential with current flow is applied between the work piece and the counter electrode to roughen the metal surface to a desired roughness.
    Type: Grant
    Filed: June 30, 2011
    Date of Patent: March 10, 2015
    Assignee: General Electric Company
    Inventors: Andrew Lee Trimmer, Bin Wei, Joshua Leigh Miller, Nicholas Joseph Kray, Michael Scott Lamphere
  • Publication number: 20140277392
    Abstract: Radiopaque cobalt-based alloys having a smooth electropolished surface with rounded edges and methods for electropolishing such alloys. A cobalt-based alloy includes cobalt, chromium, and one or more radiopaque elements. In one embodiment, examples of radiopaque elements include so-called platinum group metals (i.e., platinum, palladium, ruthenium, rhodium, osmium, or iridium). Group 10 elements (i.e., platinum or palladium) are particularly preferred. Because of the presence of the platinum group metal(s), such alloys are generally difficult to electropolish. Electrolyte formulations and methods for electropolishing such alloys are also disclosed.
    Type: Application
    Filed: March 14, 2013
    Publication date: September 18, 2014
    Applicant: ABBOTT CARDIOVASCULAR SYSTEMS, INC.
    Inventor: William E. Webler, JR.
  • Patent number: 8673405
    Abstract: In a method for producing a starting material (M, N, N?) for the production of a wear layer (420), a coating (40) with a composition which corresponds to that of the wear layer (420) which is to be produced is chemically undissolved from its substrate (30) and is detached as a solid body, and that the starting material (M, N, N?) is formed by the layer material (60) of the detached coating (40).
    Type: Grant
    Filed: July 9, 2007
    Date of Patent: March 18, 2014
    Assignee: Siemens Aktiengesellschaft
    Inventors: Rene Jabado, Jens Dahl Jensen, Ursus Krüger, Daniel Körtvelyessy, Volkmar Lüthen, Ralph Reiche, Michael Rindler, Raymond Ullrich
  • Patent number: 8591717
    Abstract: This is a process to generate alternating current without an external source for cell-houses in electrowinning or electrorefining of copper or other products in which the electric source consists of a conventional rectifier-transformer group that supplies continuous electrical current to the cell-house, which is connected in parallel to a device characterized by having the capacity to extract an electrical current from the cell-house for a period of time and then return it in another period of time, whether periodically or semiperiodically and without changing the average value of the electrical current, supplied to the cell-house by the rectifier-transformer. This results in a electrical current in the cell-house that is the superimposition of a continuous and alternating current. This process is designed to overcome the barrier of electric potential produced by the presence of the pure continuous electric field in cell-houses through the electric agitation of an ion-rich electrolyte.
    Type: Grant
    Filed: March 28, 2008
    Date of Patent: November 26, 2013
    Assignee: Hecker Electronica de Potencia y Procesos S.A.
    Inventor: Juan Pablo Bustos Robledo
  • Publication number: 20130026047
    Abstract: An aluminum support is manufactured at lower cost by efficiently performing a surface roughening treatment with dispersed pits formed on the aluminum support. In an electrolytic surface roughening treatment method for performing an electrolytic surface roughening treatment on a strip-shaped metal as being conveyed in an acidic electrolytic solution by applying an alternating waveform voltage, the method includes a step of applying a negative voltage to the metal plate at least once while the alternating waveform voltage is being applied so that the metal plate assumes a negative polarity.
    Type: Application
    Filed: July 27, 2012
    Publication date: January 31, 2013
    Applicant: FUJIFILM CORPORATION
    Inventors: Hiroshi KOMATSU, Hisashi HOTTA
  • Publication number: 20120061244
    Abstract: An electric contact in the outer edge thereof, is used for electroplating substrates, e.g. as a wafer in a cup plater. In order to obtain an even electroplating result, at least two electrolytic partial cells are formed which are supplied with current by respective electroplating current sources (9?) and (9?) that can be individually adjusted. The partial cathode (12?) and the associated partial anode (7?) are supplied in the region of the diametrically remote partial cathode (12?). Conversely, the partial cathode (12?) is supplied via the base layer of the partial cathode (12?). The required levelling of the layer thickness distribution is inter alia carried out by alternate different adjustments of the quantity of the electroplating current of the two partial cells and by the electrodes (7,12) that rotate relative to each other.
    Type: Application
    Filed: May 18, 2010
    Publication date: March 15, 2012
    Applicant: SOMONT GMBH
    Inventor: Egon Engmark Hübel
  • Publication number: 20110303553
    Abstract: An electrochemical machining system for metals and alloys having a strongly passivating character including an electrolyte solution that is free of hydrofluoric acid, an electrode in contact with the electrolyte solution, a workpiece spaced apart from the electrode and in contact with the electrolyte solution and a power source including a first electrical lead electrically coupled to the electrode and a second electrical lead electrically coupled to the workpiece, the power source being configured to pass an electric current between the electrode and the workpiece, wherein the electric current includes anodic pulses and cathodic pulses, and wherein the cathodic pulses are interposed between at least some of the anodic pulses.
    Type: Application
    Filed: June 6, 2011
    Publication date: December 15, 2011
    Inventors: Maria E. Inman, E. Jennings Taylor, Alonso Lozano-Morales, Holly Garich, Timothy Hall
  • Patent number: 7153410
    Abstract: Methods and apparatuses for electrochemical-mechanical processing of microelectronic workpieces. One embodiment of an electrochemical processing apparatus in accordance with the invention comprises a workpiece holder configured to receive a microelectronic workpiece, a workpiece electrode, a first remote electrode, and a second remote electrode. The workpiece electrode is configured to contact a processing side of the workpiece when the workpiece is received in the workpiece holder. The first and second remote electrodes are spaced apart from the workpiece holder. The apparatus can also include an AC power supply, a DC power supply, and a switching assembly. The switching assembly is coupled to the workpiece electrode, the first remote electrode, the second remote electrode, the AC power supply, and the DC power supply.
    Type: Grant
    Filed: March 4, 2002
    Date of Patent: December 26, 2006
    Assignee: Micron Technology, Inc.
    Inventors: Scott E. Moore, Whonchee Lee, Scott G. Meikle, Trung T. Doan
  • Patent number: 7063780
    Abstract: The present invention provides a method for indirect-electrification-type continuous electrolytic etching of a metal strip suitable for producing a low-core-loss, grain-oriented silicon steel sheet not susceptible to the deterioration of core loss after stress-relief annealing, and an apparatus for the indirect-electrification-type continuous electrolytic etching.
    Type: Grant
    Filed: March 3, 2003
    Date of Patent: June 20, 2006
    Assignee: Nippon Steel Corporation
    Inventors: Hisashi Mogi, Naruhiko Nomura, Shigenobu Koga, Masahiro Fujikura, Shuichi Yamazaki
  • Patent number: 7022216
    Abstract: A method for selectively removing a layer of electrolytically dissoluble metal such as copper overplate from a substrate such as a low-k dielectric comprising: providing a substrate bearing on a major surface thereof a layer of electrolytically dissoluble metal, the metal layer serving as a dissoluble electrode and having a central region and an adjacent peripheral region; providing at least a first counterelectrode and a second counterelectrode; positioning the counterelectrodes opposite the metal layer and spaced from the metal layer and spaced from each other; in a first electrolytic step, passing an electric current between the first counterelectrode and the central region of the metal layer, wherein the first counterelectrode is cathodic with respect to the metal layer, and the first electrolytic step includes a first phase, a second phase, and a third phase and during the first phase the electric current is a low amperage current, during the second phase the electric current includes a train of anodi
    Type: Grant
    Filed: June 11, 2003
    Date of Patent: April 4, 2006
    Assignee: Faraday Technology Marketing Group, LLC
    Inventors: E. Jennings Taylor, Heather Dyar
  • Patent number: 6939457
    Abstract: A contact-discharge truing/dressing method and a device therefor, capable of very simply conducting truing/dressing of a superabrasive grindstone, especially a superabrasive grindstone having a metal binder. The contact-discharge truing/dressing method brings a rotated conductive grindstone into contact with a pair of electrodes to which a DC voltage or pulse voltage is applied, and subjecting the conductive grindstone to an intermittent truing/dressing by contact discharge produced when opening/closing a circuit of a positive electrode, electrode chips, a grindstone binder, electrode chips, a negative electrode, and parts of the side surfaces of dual-ring rotary electrodes insulated by an insulation layer being used as a pair of electrodes.
    Type: Grant
    Filed: July 12, 2001
    Date of Patent: September 6, 2005
    Assignee: Japan Science and Technology Corporation
    Inventor: Masahiro Mizuno
  • Patent number: 6902659
    Abstract: The present invention deposits a conductive material from an electrolyte solution to a predetermined area of a wafer. The steps that are used when making this application include applying the conductive material to the predetermined area of the wafer using an electrolyte solution disposed on a surface of the wafer, when the wafer is disposed between a cathode and an anode, and preventing accumulation of the conductive material to areas other than the predetermine area by mechanically polishing the other areas while the conductive material is being applied.
    Type: Grant
    Filed: September 9, 2002
    Date of Patent: June 7, 2005
    Assignee: ASM Nutool, Inc.
    Inventor: Homayoun Talieh
  • Patent number: 6837984
    Abstract: An apparatus for electropolishing a wafer includes a wafer chuck and a stationary jet. The wafer chuck is configured to rotate and translate the wafer. The stationary jet is configured to apply an electrolyte to the wafer when the wafer is translated and rotated by the wafer chuck.
    Type: Grant
    Filed: April 10, 2002
    Date of Patent: January 4, 2005
    Assignee: ACM Research, Inc.
    Inventor: Hui Wang
  • Publication number: 20040256245
    Abstract: A metal layer formed on a surface of a wafer is electropolished using a wafer chuck and a moveable nozzle. The surface on which the metal layer is formed is the same surface on which features of devices are formed. The wafer chuck is configured to rotate the wafer when the wafer is placed on top of the wafer chuck. The moveable nozzle is disposed vertically above the wafer when the wafer is placed on top of the wafer chuck. The moveable nozzle is configured to move from a first position to apply a stream of electrolyte to a first portion of the metal layer to a second position to apply the stream of electrolyte to a second portion of the metal layer when the wafer is rotated by the wafer chuck, where the first and second portions of the metal layer are located at different radial positions on the wafer.
    Type: Application
    Filed: July 21, 2004
    Publication date: December 23, 2004
    Applicant: ACM Research, Inc.
    Inventor: Hui Wang
  • Publication number: 20040217013
    Abstract: The present invention relates to an apparatus and method for electropolishing a metal wire layer on a semiconductor device. To electropolish the metal wiring layer, a wafer is dipped into an electrolyte solution, and positive and negative voltages are applied to the wafer and electrodes, respectively. The electrodes include a main electrode and a plurality of auxiliary electrodes disposed above the main electrode. In a preferred embodiment, the plurality of auxiliary electrodes are mesh-type electrodes and are annular in shape and concentrically disposed, and thus the electrolyte solution can readily flow between them. Further, the metal wiring layer is preferably sequentially electropolished outwardly from the center of the wafer by sequentially applying negative voltages to the plurality of annular auxiliary electrodes. In this manner, a uniform electropolishing process is performed.
    Type: Application
    Filed: March 31, 2004
    Publication date: November 4, 2004
    Applicant: Samsung Electronics Co., Ltd.
    Inventors: Sun-jung Lee, Ki-chul Park
  • Patent number: 6706166
    Abstract: A method for improving an electrodeposited metal film uniformity and preventing metal deposition and peeling of deposited metal from an electrode during an electrodeposition and electropolishing process including providing a first anode electrode assembly and a semiconductor wafer plating surface disposed in an electrolyte bath including a plating metal for deposition onto the semiconductor wafer plating surface; providing at least one additional anode electrode assembly including the plating metal disposed peripheral to the first anode electrode assembly for selectively applying the cathodic electrical potential during an electropolishing process; and, periodically alternating between an electrodeposition process and electropolishing process with respect to the semiconductor wafer plating surface such that the plating metal is preferentially plated onto the at least one additional electrode assembly.
    Type: Grant
    Filed: May 6, 2002
    Date of Patent: March 16, 2004
    Assignee: Taiwan Semiconductor Manufacturing Co. Ltd.
    Inventors: Shih-Wei Chou, Ming-Hsing Tsai
  • Patent number: 6682645
    Abstract: In a process for producing an aluminum support of a lithographic printing plate, the desired aluminum support is produced by imparting fine asperities to an aluminum plate and then roughening it electrochemically in an acidic aqueous solution. The roughened aluminum plate may be electropolished or chemically etched.
    Type: Grant
    Filed: June 5, 2001
    Date of Patent: January 27, 2004
    Assignee: Fuji Photo Film Co., Ltd.
    Inventors: Atsuo Nishino, Yoshitaka Masuda, Hirokazu Sawada, Akio Uesugi
  • Publication number: 20040004006
    Abstract: A method for selectively removing a layer of electrolytically dissoluble metal such as copper overplate from a substrate such as a low-k dielectric comprising:
    Type: Application
    Filed: June 11, 2003
    Publication date: January 8, 2004
    Inventors: E. Jennings Taylor, Heather Dyar
  • Patent number: 6558231
    Abstract: A surface of an electrolytically dissolvable material, e.g., an electrolytically dissolvable metal, is smoothed by a two-step electrochemical process wherein a the surface to be smoothed and a counterelectrode are contacted with an electrolyte and an electric current is passed between the substrate and counterelectrode, with the substrate as the anode. In a first step relatively large asperities on the substrate are reduced in height by maintaining a macroprofile regime by using a pulsed electric current with short pulses. In a second step, small asperities and the remainder of the large asperities are reduced or removed by maintaining a microprofile regime by using a pulsed current having longer pulses or a direct current.
    Type: Grant
    Filed: October 17, 2000
    Date of Patent: May 6, 2003
    Assignee: Faraday Technology Marketing Goup, LLC
    Inventor: E. Jennings Taylor
  • Patent number: 6423206
    Abstract: To avoid or minimize the occurrence of cross streaks or current streaks on a substrate that is transported through an electrolytic bath and roughened electrochemically in it, the current density is regulated in the electrolyte between a first alternating or three-phase current electrode and the substrate in such a way that at the beginning of a roughening zone, the current density has a lesser value than within the roughening zone, in the transport direction of the substrate. Downstream of the first alternating or three-phase current electrode, either a further alternating current electrode or a further three-phase current electrode acts on the substrate. In a preferred embodiment, the first alternating or three-phase current electrode has a rounded outline, which is composed of a curved portion and adjoining it a straight portion.
    Type: Grant
    Filed: March 1, 2000
    Date of Patent: July 23, 2002
    Assignee: Agfa-Gevaert N.V.
    Inventors: Georg Haby, Raimund Haas, Uwe Gartmann, Günter Hultzsch, Klaus Joerg, Jörg Kaden, Hermann Idstein
  • Patent number: 6416650
    Abstract: An apparatus and method of electrochemical polishing a workpiece with ring-form electrode is provided. A mechanism with a tool electrode, a DC power supply and electrolysis-supply tank of the present invention can be installed on the traditional production equipment. The tool electrode is connected with the negative pole of the DC power supply, while the workpiece is connected with the positive pole of the DC power supply and kept a fixed distance from the tool electrode. The electrode or the workpiece advances at a predetermined feeding speed while the workpiece is electrochemically polished. The present invention uses the centrifugal force of rotational tool electrode to discharge electrolytic byproducts, making electrochemical polishing more effective.
    Type: Grant
    Filed: July 27, 2000
    Date of Patent: July 9, 2002
    Assignee: National Science Council
    Inventor: Cheng-Hong Ho
  • Patent number: 6402931
    Abstract: Electrochemical machining of metals and alloys is accomplished by using a pulsed electric current incorporating modulated reverse electric current. Reverse (cathodic) pulses are interposed between forward (anodic) pulses. The process is useful for electrochemical shaping of metals, electrochemically polishing metal surfaces, and electrochemical deburring of metal articles. The process is especially useful for electrochemical processing of metals and alloys that readily form passive surface layers.
    Type: Grant
    Filed: May 18, 1998
    Date of Patent: June 11, 2002
    Assignee: Faraday Technology Marketing Group, LLC
    Inventors: Chengdong Zhou, E. Jennings Taylor, Jenny J. Sun, Lawrence E. Gebhart, Robert P. Renz
  • Patent number: 6261438
    Abstract: A method and apparatus for electrochemically roughening a support is disclosed to minimize the occurrence of surface discharges or electrical discharges on the support. A DC voltage acts on the support at the start of the movement of the support through the electrolyte bath. Subsequently, a three-phase or single-phase current acts on the support in the roughening zone. Three-phase electrodes are arranged in the electrolyte bath and are connected to the secondary of a three-phase transformer. The primary of the three-phase transformer is connected, via control transformers to a three-phase power transformer. A DC electrode is located upstream of the three-phase electrodes in the direction in which the support is transported through the bath. The DC electrode may be connected to the positive pole of a DC source while the negative pole of this DC source makes contact with the support.
    Type: Grant
    Filed: December 20, 1999
    Date of Patent: July 17, 2001
    Assignee: Agfa-Gevaert NV
    Inventors: Georg Haby, Günter Hultzsch, Klaus Joerg, Uwe Gartmann, Jörg Kaden, Hermann Idstein
  • Patent number: 6231748
    Abstract: A method of electrochemically machining an electrically conductive workpiece in an electrolyte by applying electrical pulses between the workpiece and an electrically conductive electrode, one or more machining pulses alternating with passivation voltage pulses for depositing passivation layers on the workpiece. The amplitude of the passivation voltage pulses is adjusted during an adjustment procedure in which the amplitude of the passivation voltage pulses is increased gradually from zero to the voltage at which the workpiece starts to dissolve in the electrolyte. After each voltage increase the resistance of the gap between the electrode and the workpiece is measured. The voltage value for the highest gap resistance is stored in a memory and used during further machining. The time span of the passivation voltage pulses may be divided into time slices and for each time slice the voltage is adjusted for maximum gap resistance during that time slice.
    Type: Grant
    Filed: April 5, 1999
    Date of Patent: May 15, 2001
    Assignee: U.S. Philips Corporation
    Inventors: Igor L. Agafonov, Rinat A. Alimbekov, Aleksandr L. Belogorskij, Nasich Z. Gimaev, Aleksandr N. Zajcev, Viktor N. Kucenko, Rafail R. Muchutdinov
  • Patent number: 6221236
    Abstract: This invention provides an apparatus for electrolytic treatment capable of removing the ununiformity according to the frequency and can achieve high treating speed and high current density treatment, which comprises etching a metal web electrolytically using alternating waveform current continuously, wherein a frequency-variable means having an ability to vary frequency of an electric power supply of said alternating waveform current arbitrarily is provided, and a method therefor.
    Type: Grant
    Filed: June 24, 1999
    Date of Patent: April 24, 2001
    Assignee: Fuji Photo Film Co., Ltd.
    Inventors: Tsuyoshi Hirokawa, Toru Yamazaki, Atsushi Matsuura
  • Patent number: 6139715
    Abstract: A method and apparatus for deburring or radiusing articles made of TZM alloys by electrochemical machining uses a pulsating current and a binary salt electrolyte solution simultaneously applied across a gap between a tool electrode and a TZM workpiece. The pulse duration is typically in the range between about 0.5 milliseconds to about 100 milliseconds and the pulse interval is between 5 milliseconds and 150 milliseconds. The pulse voltage amplitude is typically in the range between about 8 volts to about 30 volts. The binary salt electrolyte solution is an aqueous salt solution with a total concentration typically in the range between about 14% to about 20% by weight of sodium chloride and sodium nitrate. The ratio of sodium chloride to sodium nitrate is typically in the range of between about 1:1 to about 1.5:1. The standoff distance, or gap, between the tool electrode and the TZM workpiece is typically in the range between 0.015 mm to about 3.0 mm.
    Type: Grant
    Filed: November 2, 1998
    Date of Patent: October 31, 2000
    Assignee: General Electric Company
    Inventor: Bin Wei
  • Patent number: 5993637
    Abstract: An electrode structure is constituted by a first electrode, and at least one second electrode providing a pair of opposite portions with a prescribed spacing therebetween at which the first electrode is disposed. The electrode structure is suitably used for electrolytic etching and is effective in providing an accurate etching pattern without damaging the surface of an etching object.
    Type: Grant
    Filed: December 3, 1997
    Date of Patent: November 30, 1999
    Assignee: Canon Kabushiki Kaisha
    Inventors: Masaya Hisamatsu, Akio Hasebe, Tsutomu Murakami, Hirofumi Ichinose, Satoshi Shinkura, Yukie Ueno
  • Patent number: 5863412
    Abstract: A method for etching an object having a portion to be etched on the surface thereof, comprising a step of immersing said object in an electrolyte solution such that said object serves as a negative electrode; a step of arranging a counter electrode having a pattern corresponding to a desired etching pattern to be formed at said portion to be etched of said object in said electrolyte solution so as to maintain a predetermined interval between said counter electrode and said object, and a step of applying a direct current or a pulse current between said object and said counter electrode to etch said portion to be etched of said object into a pattern corresponding to said pattern of said counter electrode.
    Type: Grant
    Filed: October 17, 1996
    Date of Patent: January 26, 1999
    Assignee: Canon Kabushiki Kaisha
    Inventors: Hirofumi Ichinose, Ippei Sawayama, Akio Hasebe, Tsutomu Murakami, Masaya Hisamatsu, Satoshi Shinkura, Yukie Ueno
  • Patent number: 5823357
    Abstract: The invention provides a method and system for automated sorting or articles such as railroad wheels. After the wheels are inspected and designated as fitting a particular category, the wheels are moved to a transfer car and the wheel and transfer car are moved to a wheel pick up station, where an overhead hoist awaits. As the wheel and transfer car are moved, a hook portion of the hoist is received in the wheel axles hole. The hoist raises the wheel out of the transfer car and then the hoist and wheel move laterally to a wheel drop off station corresponding with the category of the wheel. A shuttle car with an empty wheel receiving slots is below each wheel drop off station. The hoist lowers the wheel into the aligned wheel slot of the appropriate shuttle car for that category of wheel. After the wheel is deposited in the slot, the shuttle car indexes away from the hoist, freeing the wheel and hoist from one another. The hoist is then raised and returned to the wheel pick up station.
    Type: Grant
    Filed: July 11, 1997
    Date of Patent: October 20, 1998
    Assignee: AMSTED Industries Incorporated
    Inventors: Christopher Z. Sieradzki, Jaime F. Pozo
  • Patent number: 5755949
    Abstract: A plate-, foil- or web-shaped workpiece of aluminum or an alloy thereof is subjected, in an electrolyte bath, to an alternating current at a frequency of 0.1 to 25 Hz. During the AC treatment, an anodic potential is imposed on the workpiece, in the range of 0 to 5 Volts. The total charge input is 10 to 60 kC/m.sup.2. Prior to the electrochemical graining, the workpiece is mechanically grained. After the graining steps, an etching treatment as well as an anodical oxidation and, thereafter, a hydrophilization are performed.
    Type: Grant
    Filed: December 22, 1994
    Date of Patent: May 26, 1998
    Assignee: AGFA-Gevaert AG
    Inventor: Martin Philip Amor
  • Patent number: 5667666
    Abstract: A process for roughening a surface of a support for a lithographic printing plate in which an electric current is supplied between a metal web and an electrode facing the metal web in an electrolyte containing metal ions so that the metal web is subjected to electrochemical processing continuously, 1-20 pause sections are provided in the electrochemical processing and the time taken for passage through once processing pause section in the electrochemical processing is set to 1-30 seconds. With the process, the grain shape can be controlled with no troublesome condition setting to improve a scumming resistance without deteriorating a printing durability and a fill-in reduction so that the plate has superior performance.
    Type: Grant
    Filed: July 30, 1996
    Date of Patent: September 16, 1997
    Assignee: Fuji Photo Film Co., Ltd.
    Inventors: Atsushi Matsuura, Akio Uesugi
  • Patent number: 5630932
    Abstract: A tip and substrate preparation system for use with scanning probe microscopes (SPMs) includes a scanning tunneling microscope (STM) tip maker, STM tip coater, a substrate treatment method for producing clean, flat gold substrates for STM use and methods for preparing chemically activated substrates for use with an atomic force microscope (AFM). The tip maker includes a coater and an etcher which are preferably controlled by electronic controllers. The etcher provides fully automatic tip etching in a two-stage process in sodium hydroxide (NaOH) solution, permitting platinum alloys to be etched without the use of cyanide-containing chemicals. The coater is used to insulate the tips with soft polymer coatings so as to ensure very low tip leakage current (on the order of about 1 pA typical). The substrate treatment device comprises a quartz plate and a quartz torch for annealing substrates in a hydrogen flame.
    Type: Grant
    Filed: September 6, 1995
    Date of Patent: May 20, 1997
    Assignee: Molecular Imaging Corporation
    Inventors: Stuart M. Lindsay, Tianwei Jing, Yuri L. Lyubchenko, Alexander A. Gall
  • Patent number: 5518589
    Abstract: A method of producing a support for a planographic printing plate which comprises roughening a surface of an aluminum plate electrochemically, etching the surface by 0.01 to 20 g/m.sup.2 with alkali, and roughening the surface electrochemically in an electrolytic solution containing hydrochloric acid and/or a water-soluble hydrochloride salt which forms hydrochloride ion or nitric acid and/or a water-soluble nitrate salt which forms nitrate ion as the principle component.
    Type: Grant
    Filed: August 31, 1994
    Date of Patent: May 21, 1996
    Assignee: Fuji Photo Film Co., Ltd.
    Inventors: Atsushi Matsuura, Akio Uesugi