Uniform Solids Withdrawal Patents (Class 208/171)
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Patent number: 7547387Abstract: A process for contacting a bed of particulate material, usually catalyst, with a transverse flow of fluid is disclosed. The particulate material moves or is prevented from not moving, while the fluid passes through the bed at a rate greater than the stagnant bed pinning flow rate. This invention is applicable to hydrocarbon conversion processes and allows for higher fluid throughput rates compared to prior art processes.Type: GrantFiled: June 6, 2007Date of Patent: June 16, 2009Assignee: UOP LLCInventors: Weikai Gu, Paul A. Sechrist
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Patent number: 7399450Abstract: A fluidized-bed reactor is disclosed. The fluidized-bed reactor steadies the gas flow through the fluidized bed chamber of the reactor. The swirl chamber of the reactor consists of a conical housing in which a conical insert is also situated. This creates an annular gap between the housing and the insert, which acts as the swirl chamber and which, according to the geometry of the two components, causes a velocity of the gas flow which remains the same along the height, which increases or which decreases. Such a reactor can also be called a constant annular-gap reactor.Type: GrantFiled: March 16, 2005Date of Patent: July 15, 2008Inventor: Sebastian Zimmer
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Patent number: 7241376Abstract: A process for contacting a bed of particulate material, usually catalyst, with a transverse flow of fluid is disclosed. The particulate material moves or is prevented from not moving, while the fluid passes through the bed at a rate greater than the stagnant bed pinning flow rate. This invention is applicable to hydrocarbon conversion processes and allows for higher fluid throughput rates compared to prior art processes.Type: GrantFiled: November 8, 2004Date of Patent: July 10, 2007Assignee: UOP LLCInventors: Weikai Gu, Paul A. Sechrist
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Patent number: 6814857Abstract: A process for contacting a bed of particulate material, usually catalyst, with a transverse flow of fluid is disclosed. The particulate material moves or is prevented from not moving, while the fluid passes through the bed at a rate greater than the stagnant bed pinning flow rate. This invention is applicable to hydrocarbon conversion processes and allows for higher fluid throughput rates compared to prior art processes.Type: GrantFiled: January 31, 2002Date of Patent: November 9, 2004Assignee: UOP LLCInventors: Weikai Gu, Paul A. Sechrist
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Patent number: 6576120Abstract: The invention relates to a process for the catalytic dewaxing of a hydrocarbon feed containing waxy molecules by contacting the hydrocarbon feed under catalytic dewaxing conditions with a catalyst composition having metallosilicate crystallites, a binder and a hydrogenation component, wherein the weight ratio of the metallosilicate crystallites and the binder is between 5:95 and 35:65. The invention also relates to a catalyst composition having at least a low acidity refractory oxide binder, which binder is essentially free of aluminum, metallosilicate crystallites and a hydrogenation component, wherein the weight ratio of the metallosilicate crystallites and the binder is between 5:95 and 35:65.Type: GrantFiled: May 16, 2001Date of Patent: June 10, 2003Assignee: Shell Oil CompanyInventors: Carolus Maria Van Ballegoy, Edward Julius Creyghton, Jean-Paul Darnanville, Eric Duprey, Laurent Georges Huve, Carolus Matthias Anna Maria Mesters, Thomas Joris Remans, Maria Barbara Hendrica Crijnen-Van Beers
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Patent number: 5916529Abstract: A method, and a reactor, for hydroprocessing a hydrocarbon feed stream through multistage moving catalyst beds contained within a single onstream reactor vessel, with separate catalyst addition and withdrawal systems for each of the multistages of moving catalyst beds. The reactor contains two or more different and distinct moving catalyst beds for any hydroprocessing application. The method includes serially passing, without leaving the reactor vessel, at least a partially treated hydrocarbon stream from one hydroconversion reaction zone containing a moving catalyst bed with a first set of catalytic characteristics to another hydroconversion reaction zone containing a moving catalyst bed with a second set of catalytic characteristics that differ in catalytic abilities from the first set of catalytic characteristics.Type: GrantFiled: April 24, 1996Date of Patent: June 29, 1999Assignee: Chevron U.S.A. IncInventor: Georgieanna L. Scheuerman
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Patent number: 5840176Abstract: A method for replacing particles in a process that transfers particles is disclosed. This invention employs a seal zone which is in communication with two zones of the process and in which particles that are being added to the process are purged. This invention allows particles to be replaced without reducing the normal rate of particle transfer through the process, which results in a savings in downtime costs. This invention is adaptable to a multitude of processes for the catalytic conversion of hydrocarbons in which deactivated catalyst particles are regenerated.Type: GrantFiled: August 12, 1996Date of Patent: November 24, 1998Assignee: UOP LLCInventors: Roger R. Lawrence, Frank T. Micklich, Charles T. Ressl, Paul A. Sechrist
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Patent number: 5804058Abstract: A process is disclosed for the catalytic dewaxing of a hydrocarbon oil feed comprising waxy molecules, which process comprises:contacting a feed under catalytic dewaxing conditions with a catalyst composition comprising a molecular sieve containing crystallites covalently bound alumina moieties in its framework and having pores with a diameter in the range of from 0.35 to 0.80 nm and recovering a product having a reduced pour point, wherein the molecular sieve has been modified to reduce the mole percentage of alumina by coating the surface of the crystallites with a refractory inorganic oxide which is essentially free of alumina.Type: GrantFiled: June 13, 1996Date of Patent: September 8, 1998Assignee: Shell Oil CompanyInventors: Pierre Grandvallet, Laurent Georges Huve, Theodorus Ludovicus Michael Maesen
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Patent number: 5545312Abstract: A method and apparatus for replacing particles in a process that transfers particles is disclosed. This invention employs a seal zone which is in communication with two zones of the process and in which particles that are being added to the process are purged. This invention allows particles to be replaced without reducing the normal rate of particle transfer through the process, which results in a savings in downtime costs. This invention is adaptable to a multitude of processes for the catalytic conversion of hydrocarbons in which deactivated catalyst particles are regenerated.Type: GrantFiled: May 6, 1994Date of Patent: August 13, 1996Assignee: UOPInventors: Roger R. Lawrence, Frank T. Micklich, Charles T. Ressl, Paul A. Sechrist
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Patent number: 5076908Abstract: This invention makes possible substantially continuous flow of uniformly distributed hydrogen and hydrocarbon liquid across a densely packed catalyst bed to fill substantially the entire volume of a reactor vessel by introducing the fluids as alternate annular rings of gas and liquid at a rate insufficient to levitate the bed and with catalyst selected by a density, shape and size at a design feed rate of liquids and gas to prevent ebulation of the packed bed at the design feed rates. Catalysts are selected by measuring bed expansion in a large pilot plant run with hydrocarbon, hydrogen, and catalyst at the design pressures and flow velocities. The liquid and gas components of the feed flow into the bed in alternate annular rings across the full area of the bed.Type: GrantFiled: July 19, 1989Date of Patent: December 31, 1991Assignee: Chevron Research & Technology CompanyInventors: Bruce E. Stangeland, David C. Kramer, David S. Smith, James T. McCall, Georgieanna L. Scheuerman, Robert W. Bachtel
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Patent number: 4902407Abstract: An improved method of controlling catalyst inventory in the reactor of an ebullated bed process has been discovered. Pressure differentials are measured to calculate a catalyst inventory characterization factor. Aged catalyst is withdrawn and fresh catalyst added in an amount to reestablish the value of the factor.The catalyst to oil ratio is maintained despite changes in bed ebullation, gas and liquid holdups and oil residence time changes.Type: GrantFiled: June 9, 1988Date of Patent: February 20, 1990Assignee: Texaco Inc.Inventors: Ting Y. Chan, John C. Strickland
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Patent number: 4664782Abstract: The particulate solid is maintained in a bed in contact with a liquid within a high pressure vessel. The particulate solid is supported in the vessel in a cone-like configuration. A discharge tube is provided communicating with the particulate solid running from the bottom of the cone externally of said vessel and pressure on the supported particulate is produced to discharge said particulate out of said vessel via the discharge tube.Type: GrantFiled: January 9, 1986Date of Patent: May 12, 1987Assignee: Intevep, S.A.Inventors: Roberto E. Galiasso, Jose I. Belandria, Pasquale L. Caprioli
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Patent number: 4502946Abstract: Process for the complete replacement under operating conditions of particles in a vessel provided with a feed inlet and, if desired, a separate particle inlet, a particle outlet and an effluent outlet, wherein part of the feed passing through the vessel during withdrawal of particles is by-passing the vessel when the particles still present in the vessel do not occupy more than 20% v of the volume initially occupied by particles and the feed is passed through the vessel before or during the addition of fresh particles.The process is particularly suitable for the complete replacement under operating conditions of spent hydrodemetallization catalysts.Type: GrantFiled: March 28, 1984Date of Patent: March 5, 1985Assignee: Shell Oil CompanyInventor: Gerrit J. Pronk
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Patent number: 4478793Abstract: A radial flow reactor design which allows the maintenance of a temperature profile along the height of a catalyst bed which descends through the reactor by gravity flow. Two feed inlet conduits are provided on the inlet side of the annular catalyst bed, with the inlets being divided by a porous flow control and distribution means. The inlet streams have different temperatures and the distribution means produces a changing admixture rate between the two streams along the bed. A preferred form of the distribution means is an open-topped cone located within the centerpipe of the reactor.Type: GrantFiled: September 22, 1982Date of Patent: October 23, 1984Assignee: UOP Inc.Inventor: Anthony G. Vickers
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Patent number: 4444653Abstract: Catalysts solid particles are supplied to a vertical reactor for the catalytic treatment of fluid charges, at the upper part of said reactor and are progressively withdrawn from the lower part thereof either continuously or periodically through a funnel having the shape of an inverted cone or an inverted pyramid. At least a portion of the charge is introduced at the lower part of the reactor through orifices above the walls of the funnel at a distance thereof from 1 to 500 times the average size of a catalyst particle.Type: GrantFiled: February 2, 1983Date of Patent: April 24, 1984Assignee: Institut Francais du PetroleInventors: Jean-Paul Euzen, Yves Jacquin
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Patent number: 4392943Abstract: In a process for the catalytic treatment of hydrocarbon charges in the presence of hydrogen in a vertical reactor where the catalyst is introduced at the top and withdrawn at the bottom, countercurrently with the charge which is introduced at the bottom and discharged from the top. There is provided a flared funnel for the catalyst discharge having small perforations for the upward flow of the charge with the perforations of a size sufficiently small to prevent passage of the catalyst therethrough. These perforations are in association with injection tubes having orifices opening in the vicinity of the funnel wall, wherethrough at least a portion of the fluid charge is injected.Type: GrantFiled: April 29, 1982Date of Patent: July 12, 1983Assignee: Institut Francais du PetroleInventors: Jean-Paul Euzen, Yves Jacquin, Hugo Van Landeghem, deceased
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Patent number: 4277444Abstract: An improved radial reactor for hydrocarbon conversion is provided, having a new catalyst collector whose center is located nearer to the internal wall than to the external wall of the annular enclosure for receiving the moving catalyst bed.Type: GrantFiled: May 29, 1979Date of Patent: July 7, 1981Assignee: Institut Francais du PetroleInventor: Hugo Van Landeghem
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Patent number: 4110081Abstract: An improved radial flow moving bed reactor, or other type of fluid-solid contacting vessel, in which stagnant catalyst volumes are reduced. The improvement results from the placement of a plurality of catalyst collection scoops or a single discoid cover plate just above the catalyst withdrawal conduits in a manner which directs the removal of catalyst through an annular opening adjacent the inner catalyst retention screen.Type: GrantFiled: June 9, 1977Date of Patent: August 29, 1978Assignee: UOP Inc.Inventors: Robert F. Millar, Paul J. Persico, Robert H. Jensen
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Patent number: 3978150Abstract: Continuous operation and a high rate of conversion are obtained in a normal paraffin dehydrogenation process through the use of a moving bed non-fluidized reaction zone operated at a subatmospheric pressure. Quantities of catalyst are periodically removed from the reaction zone, passed through regeneration and reducing zones operated at superatmospheric pressures and returned to the top of a reaction zone.Type: GrantFiled: March 3, 1975Date of Patent: August 31, 1976Assignee: Universal Oil Products CompanyInventor: Frederick G. McWilliams, Jr.