By Calendering Patents (Class 264/175)
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Patent number: 6419858Abstract: This invention is directed to a process for the rapid in-situ curing of polymerizable materials to provide macromolecular networks and articles of manufacture that are “morphology-trapped”; that is, they exhibit a fixed phase morphology and/or molecular orientation that is locked in by the curing step. The process includes the steps of mixing together a dead polymer, a reactive plasticizer and an initiator to give a polymerizable composition; further processing the mixture in order to achieve a desired phase morphology and/or molecular orientation of the polymeric constituents; shaping the polymerizable composition into a desired geometry; and exposing the polymerizable composition to a source of polymerizing energy, without mixing, to give a final product with the desired phase morphology and/or molecular orientation locked in place.Type: GrantFiled: June 13, 2000Date of Patent: July 16, 2002Assignee: ZMS, LLCInventors: Michael R. Houston, Toshiaki Hino, David S. Soane
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Patent number: 6362306Abstract: A reactor grade copolyester composition, as well as a heat-shrinkable film made therefrom, unexpectedly has higher ductility than a multi-component blend of copolyesters with the same monomer concentrations. The reactor grade copolyester composition is made from a diacid component of at least about 90 mole percent and a diol component of (a) about 72 to about 88 mole percent ethylene glycol, about 10 to about 15 mole percent 1,4-cyclohexanedimethanol, and about 2 to about 13 mole percent diethylene glycol, or (b) about 59 to about 77.5 mole percent ethylene glycol, about 15 to about 28 mole percent 1,4-cyclohexane-dimethanol, and about 7.5 to about 13 mole percent diethylene glycol. Further, the heat-shrinkable film may be produced to closely match the shrink characteristics of polyvinyl chloride by varying the amounts of the diol components of the reactor grade copolyester composition. Furthermore, a reactor grade copolyester composition has a b* color value of −1.0 to less than 4.Type: GrantFiled: August 11, 2000Date of Patent: March 26, 2002Assignee: Eastman Chemical CompanyInventors: Marcus David Shelby, Wayne Ken Shih, Rondell Paul Little, Jr., Candace Michele Tanner, William LeRoy Wortman
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Publication number: 20020035401Abstract: An osteogenic osteoimplant in the form of a flexible sheet comprising a coherent mass of bone-derived particles, the osteoimplant having a void volume not greater than about 32% and a method of making an osteogenic osteoimplant having not greater than about 32% void volume, the method comprising: providing a coherent mass of bone-derived particles; and, mechanically shaping the coherent mass of bone-derived particles to form an osteogenic osteoimplant in the form of a flexible sheet.Type: ApplicationFiled: October 9, 2001Publication date: March 21, 2002Applicant: OSTEOTECH, INC.Inventors: Todd M. Boyce, David Kaes, Nelson L. Scarborough
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Patent number: 6352760Abstract: The invention relates to a flexible, waterproof shower pan liner comprised of a water-insoluble thermoplastic sheet. The shower pan liner includes on at least one surface selected indicia such as product information or plumbing codes at regular intervals. The indicia are embossed into the shower pan liner thereby eliminating the need for a protective top coat. In a process for making the invention, the thermoplastic is heated, calendered, and thereafter embossed with the selected indicia while in a heated condition.Type: GrantFiled: October 25, 2000Date of Patent: March 5, 2002Assignee: Omnova Solutions Inc.Inventors: David L. Fishel, Peter F. Payne
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Publication number: 20020013112Abstract: A method of manufacturing a multi-layered web uses contoured honeycomb drums for the manufacture of non-woven webs used to make the multi-layered web. The method can use spunbonded, melt blown, or electro-static spun techniques for depositing solidifying filaments on outer collection surfaces of a multi-drum system. The multi-drum system may be employed to improve multi-layered web uniformity and the overall quality of the multi-layered web by presenting a single optimal collection surface for each independent web layer being produced.Type: ApplicationFiled: June 19, 2001Publication date: January 31, 2002Inventors: George J. Bontaites, George Lee
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Patent number: 6340530Abstract: Book covers and a substantially transparent, coextruded matte, bilayer nylon film which is contact transparent to a paper stock to form a soft book cover having high scratch, abrasion and mar resistance, a soft feel and good moisture curl properties. A substantially transparent, coextruded film which has a first nylon layer attached adjacent to a second nylon layer, the first nylon layer has from about 20 weight percent to about 70 weight percent of a refractory filler based on the weight of the first nylon layer.Type: GrantFiled: April 28, 2000Date of Patent: January 22, 2002Assignee: Honeywell International Inc.Inventors: Simon J. Porter, Jeffrey D. Moulton, Lance R. Altizer
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Patent number: 6325880Abstract: A lenticular lens sheet for use as a rear projection screen, comprises a base lenticular lens sheet having a surface provided with a plurality of lenticular elements, and a surface diffusing part having minute diffusing elements. The surface diffusing part is combined with the base lenticular lens sheet by laminating a plastic film having one surface provided with the minute diffusing elements to the base lenticular lens sheet so that the minute diffusing elements lie on the surfaces of the lenticular elements or by embossing the minute diffusing elements in the surfaces of the lenticular elements of the base lenticular lens sheet with an embossing plastic film having a surface of a shape complementary to the minute diffusing elements.Type: GrantFiled: March 7, 2000Date of Patent: December 4, 2001Assignee: Dai Nippon Printing Co., Ltd.Inventors: Yoshiyuki Yamashita, Hitomu Watanabe
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Patent number: 6312631Abstract: A polyolefin composition having enhanced dyeing capabilities containing: (a) a polyolefin; (b) from 0.01 to 10% by weight, based on the weight of the polyolefin in, of a migratable amphiphile, excluding phenolic and sulfur-containing stabilizers and n-octyl phenyl salicylate; and (c) from 0.01 to 1000 ppm of a transition metal, based on the weight of the polyolefin.Type: GrantFiled: January 13, 2000Date of Patent: November 6, 2001Assignee: Henkel Kommanditgesellschaft auf AktienInventors: Norbert Bialas, Paul Birnbrich, Herbert Fischer, Joerg-Dieter Klamann, Raymond Mathis
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Publication number: 20010030031Abstract: From about 50 to about 90% by weight of fibers, in particular wood fibers, and/or pellets made from cellulose or from wood, are mixed with from about 10 to about 50% by weight of a hot-curing resin, each of the percentages by weight being based on the total weight of the mixture. Instead of a single resin it is also possible to use a mixture made from two or more hot-curing resins. The mixture made from fibers and/or pellets and resin is kneaded and homogenized and then passed on to an extruder which has various heating zones in which the mixture is heated. Care has to be taken here that the maximum temperature, arising at the extruder exit, does not exceed about 120° C., since above this temperature the resin(s) begin(s) to cure.Type: ApplicationFiled: February 20, 2001Publication date: October 18, 2001Applicant: TRESPA INTERNATIONAL B.V.Inventor: Remco Cornelis Willemse
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Patent number: 6299977Abstract: The present invention relates to a nonwoven fabric exhibiting dense, delicate, high quality appearance, and also relates to man made leathers exhibiting dense, delicate, high quality appearance, and bearing a resemblance to high quality natural leathers.Type: GrantFiled: April 27, 1999Date of Patent: October 9, 2001Assignee: Teijin LimitedInventors: Naohiko Takeyama, Masahisa Mimura
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Publication number: 20010026027Abstract: An improved process for producing polybutadiene golf ball cores is disclosed. The golf ball cores are from polybutadiene rubber compositions having a high Mooney viscosity and/or a high molecular weight and a low dispersity is disclosed. An apparatus for producing the polybutadiene golf ball cores is also disclosed. The apparatus includes an internal mixer that compounds a batch of golf ball core stock. A sheeter forms sheets of golf ball core stock and has a sheeter inlet proximate the mixer outlet and a sheeter outlet. A preform shaper forms golf ball core preforms from the sheets of golf ball core stock.Type: ApplicationFiled: April 5, 2001Publication date: October 4, 2001Applicant: SPALDING SPORTS WORLDWIDE, INC.Inventor: R. Dennis Nesbitt
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Patent number: 6294036Abstract: A process for manufacturing composite sheets. The sheets are made of at least one ply of yarn with this ply having at least two materials with different melting points. The ply is introduced continuously into a zone where it is heated to a temperature between the two melting points and below the degradation temperature of the material having the lower melting point. This ply is then passed over at least one rotating bar heated to a temperature lying between the melting points and below the degradation temperature of the material with the lower melting point. The ply is then compressed on leaving the rotating bar and is cooled to form a composite web. The web is collected in the form of one or more composite plies.Type: GrantFiled: September 15, 1999Date of Patent: September 25, 2001Assignee: Vetrotex FranceInventors: Dominique Loubinoux, Jacques Voiron, Jean-Paul Debalme, Charles Saint-John
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Patent number: 6270707Abstract: This invention concerns a method of manufacturing a highly conductive polytetrafluoroethylene sheet; a method of manufacturing a highly conductive unsintered polytetrafluoroethylene sheet: and a method of manufacturing a highly conductive sintered sheet. In the first method, a paste of polytetrafluoroethylene powder admixed with conductive substance and extrusion lubricant is extruded to preform an unsintered tube-like material, and at least one place on the circumference of this extruded material, the material is cut open longitudinally and the resulting sheet is calendered if necessary. The second method includes a sintering process for the sheet. This invention also concerns a highly conductive polytetrafluoroethylene sheet having a wide-width and long-length, which is obtained by the above-mentioned method. This sheet is not less than 170 mm in width and has variance of volume resistivity (conductivity) in the longitudinal direction, 10% or less, preferably 7% or less in the cross direction.Type: GrantFiled: September 2, 1998Date of Patent: August 7, 2001Assignee: Daikin Industries, Ltd.Inventors: Yoshinori Hori, Toshinori Kadowaki, Hiroyuki Yoshimoto, Kyohiro Kang
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Publication number: 20010008910Abstract: This invention provides a flexible polymer modified waterproofing cement material which can be used on a substrate or in concealed areas of construction engineering, water conservancy projects, municipal works, and its making process. The waterproofing material is made by kneading a hydraulic cement, a polymer dispersion, a water-soluble polymer or re-dispersible resin and water at a weight ratio of cement/polymer of about 100:15 to about 100:150 under conditions of about 25° C. to about 120° C., about 20 rpm to about 80 rpm until the water content of the kneaded materials reaches about 5% to about 20%. The kneaded material is mixed with a toughening polymer at a weight ratio of about 100:10 to about 100:50, then is calendered into sheets. These materials can adhere to dry or wet substrates firmly. They can be used in cold or hot and wet climate areas. After application, the waterproofing structure formed can bear retractive stress and deformation of the base or can resist outer impact.Type: ApplicationFiled: January 12, 2001Publication date: July 19, 2001Applicant: Tianjin Building Materials Science Research InstituteInventors: Ji Guang Yu, Dong Xia, Lei Zhu, Yu Qing Guo, Peng Chen
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Patent number: 6261487Abstract: In order to control and optimize, without stopping production, bowing in the outer wall of a calender roll in which bowing is produced by the action of pressure on an incompressible liquid enclosed in the roll, the invention proposes that, based on error signals generated from continuous thickness measurements and from at least one other quality characteristic, the temperature of the liquid is controlled and the nip modified to correct for deviations from the correct thickness.Type: GrantFiled: September 9, 1998Date of Patent: July 17, 2001Assignee: Brunckner Maschinenbau GmbHInventors: Horst Bongaerts, Dietmar Jenke
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Patent number: 6238605Abstract: The invention relates to a process for the production of a low-fibrillation moulded body containing polytetrafluorethylene. The process is characterised in that a pre-moulded body of polytetrafluorethylene is twisted and then pressed flat. The pre-moulded body can be twisted around itself or around another material e.g. a mono- or multifilament or a spun yarn. The invention relates furthermore to a low fibrillation moulded body containing polytetrafluorethylene which can be obtained by means of the process in accordance with the invention and the use of the moulded body in accordance with the invention as dental floss.Type: GrantFiled: April 12, 1999Date of Patent: May 29, 2001Assignee: Lenzing AktiengesellschaftInventor: Adalbert Wimmer
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Patent number: 6228499Abstract: The present invention relates to; resin molded articles having on one side of the resin substrate thereof, such as polycarbonate, a scuff resistant organic hard coat layer and on the other surface of the substrate an antifogging organic hard coat layer; resin shaped articles such as into helmet shields, goggles, and the like, in which the organic hard coat layer will not peel off the substrate when molded into a curve-shaped article having a radius of curvature of 50 mm or less and which will cause no optical distortions; a process for the manufacture thereof; and the covering materials for forming each hard coat layer.Type: GrantFiled: December 9, 1997Date of Patent: May 8, 2001Assignee: Mitsubishi Rayon Co., Ltd.Inventors: Jun Nakauchi, Osamu Kawai
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Publication number: 20010000417Abstract: The invention discloses a method by which a fluid heat reactive resin system is formulated below the melting point of the resin. This permits the application of coatings and the formation of shapes and powders from the fluid heat reactive system. Liquefied gases are used to solvate resins so that curing agents, hardeners, pigments and flow control agents, and especially curing agents which are too reactive to be mixed with the resins above the melting point of the resins may be dispersed in the resins.Type: ApplicationFiled: November 30, 2000Publication date: April 26, 2001Inventor: Douglas S. Richart
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Patent number: 6217982Abstract: A calenderable thermoplastic polymer alloy composition made by blending ethylene/alkyl (meth)acrylate with a blend of polypropylene, ethylene copolymer ionomer resin, ethylene/glycidyl acrylate or methacrylate copolymer, and uncrosslinked ethylene propylene rubber.Type: GrantFiled: October 8, 1998Date of Patent: April 17, 2001Assignee: E. I. du Pont de Nemours and CompanyInventor: Robert Louis Dawson
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Patent number: 6218000Abstract: A membrane of microporous, for example stretched, PTFE is filled with particles having a size in the nanometer range. By filling with, for example, TiO2, the abrasion resistance of the membrane can be increased. Low particle size means that the original structure of the PTFE membrane with its knots and fibrils is retained, as is, consequently, the original desired properties of this material. In addition to these properties, filling of the material achieves additional properties, for example increased abrasion resistance.Type: GrantFiled: September 21, 1998Date of Patent: April 17, 2001Inventors: Christiane Rudolf, Wolfgang Burger, Ralf Tillmanns
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Patent number: 6203741Abstract: An apparatus and methods for forming micro spike thermoplastic liners and micro spike thermoplastic liners formed thereby are provided. A textured thermoplastic liner having at least one roughened surface with a plurality of irregularly shaped projections extending therefrom is disclosed. The thermoplastic liner of the subject invention is formed by using a calendering roll having a generally cylindrically shaped body with a non-smooth outer surface and a plurality of blind apertures, each having an irregularly shaped opening formed coextensively with the non-smooth surface. The liner is formed by having the non-smooth surface of the calendering roll impress a roughened pattern onto the liner and simultaneously form the plurality of irregularly shaped projections. The calendering roll is formed by initially drilling a plurality of blind apertures and, subsequently, roughening the outer surface of the roll such that the openings of each of the apertures are each caused to be irregularly shaped.Type: GrantFiled: April 4, 2000Date of Patent: March 20, 2001Assignee: AGRU Kunststofftechnik GmbHInventor: Heinrich Heinzlreiter
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Patent number: 6200406Abstract: A method of forming a side wall of a cupped cake cup at high speed, including paying off a paper sheet through a plurality of paying off rolls; cutting a blank off the paper sheet with a paper cutter disposed at least one of normal and oblique to a direction in which the paper sheet is fed; immediately before or after the cutting, applying a sealing agent; supplying the blank to a specified roll gap formed between a forming cone roll and a holding cone roll capable of rotating in opposite directions; performing shaping, cutting and sealing works on the blank during one rotation of the forming and holding cone rolls, wherein the blank is made into the side wall of the cupped cake cup; separating the side wall of the cup from the forming cone roll; and guiding the side wall of the cupped cake cup in the axial direction of the forming cone roll.Type: GrantFiled: March 27, 1998Date of Patent: March 13, 2001Inventor: Sadaharu Ito
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Patent number: 6190594Abstract: Tool rolls and methods of using the tool rolls to manufacture articles with one or more structured surfaces are disclosed. The tool rolls include an outer surface that, when used in connection with materials of the proper viscosity or formability, can form a structured surface on an article. Because the tools are manufactured in roll-form, they can be advantageously used in continuous manufacturing processes. Alternatively, discrete articles may be processed using the tool rolls. The tool rolls are constructed of a cylindrical base roll and are wrapped with one or more continuous wires in a helical pattern. The wires are used, in essence, to form a structured surface on the tool roll that is the negative of the structured surface to be formed on the articles processed using the tool roll. One of the wires wound around the base roll may include a plurality of voids formed therein that, when wound in helical coils about the base roll, form a plurality of mold cavities on the outer surface of the tool roll.Type: GrantFiled: March 1, 1999Date of Patent: February 20, 2001Assignee: 3M Innovative Properties CompanyInventors: Michael R. Gorman, Roger D. Pavlis
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Patent number: 6187244Abstract: A method for making a flexible, waterproof shower pan liner comprised of a water-insoluble thermoplastic sheet. The shower pan liner includes on at least one surface selected indicia such as product information or plumbing codes at regular intervals. The indicia are embossed into the shower pan liner thereby eliminating the need for a protective top coat. In the process for making the invention, the thermoplastic is heated, calendered, and thereafter embossed with the selected indicia while in a heated condition.Type: GrantFiled: February 9, 1999Date of Patent: February 13, 2001Assignee: Omnova Services Inc.Inventors: David L. Fishel, Peter F. Payne
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Patent number: 6187238Abstract: A fiber material of PTFE and, optionally, hydrophilizing additives, for use in the production of diaphragms for the electrolysis of alkali chlorides, as well as for filter layers. The fiber material comprises fiber bundles and these, in turn, comprise individual microfibrils, there being irregularly shaped interstices between the microfibrils. The fiber material is produced in that a PTFE dispersion, consisting of a salt solution with PTFE particles and, optionally, hydrophilizing additives, is treated in a hot gas/vapor stream in a fluidized bed apparatus charged with inert solids. The method permits the fiber material to be produced also in larger quantities in an economic manner.Type: GrantFiled: August 19, 1997Date of Patent: February 13, 2001Assignees: Magdeburger Energie-und Umwelttechnik GmbH, De Nora Deutschland GmbHInventors: Bruno Klatt, Manfred Horx, Hartmut Koelling, Karlheinz Berndt, Gerhard Krueger, Hans-Joachim Kuenne, Lothar Moerl, Lothar Backhauss
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Patent number: 6180037Abstract: Compositions and methods for manufacturing sheets having a highly inorganically filled matrix. Suitable inorganically filled mixtures are prepared by mixing together an organic polymer binder, water, one or more inorganic aggregate materials, fibers, and optional admixtures in the correct proportions in order to form a sheet which has the desired performance criteria. The inorganically filled mixtures are formed into sheets by first extruding the mixtures and the passing the extruded materials between a set of rollers. The rolled sheets are dried in an accelerated manner to form a substantially hardened sheet, such as by heated rollers and/or a drying chamber. The inorganically filled sheets may have properties substantially similar to sheets presently made from traditional materials like paper, cardboard, polystyrene, plastic, or metal. Such sheets can be rolled, pressed, scored, perforated, folded, and glued.Type: GrantFiled: June 7, 1995Date of Patent: January 30, 2001Assignee: E. Khashoggi Industries, LLCInventors: Per Just Andersen, Simon K. Hodson
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Patent number: 6159412Abstract: A method for making thermotropic liquid crystalline polymer films with improved transverse direction properties comprises two preferably embossed rollers which oscillate oppositely with respect to each along their respective rotational axes. Film made by passing a liquid crystalline polymer between such rolls has improved transverse direction properties. Such films are useful in multilayer containers and for circuit boards.Type: GrantFiled: August 5, 1997Date of Patent: December 12, 2000Assignee: Dupont Canada Inc.Inventors: Eldon Lawrence Fletcher, Anthony Joseph Cesaroni
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Patent number: 6129539Abstract: A material transfer arrangement having a pair of generally cylindrical adjacent rolls which are counter-rotatable about their respective cylindrical axes and which define therebetween a nip between which material passes is disclosed. There is a corresponding pair of spaced apart doctor blades, each in close proximity to a corresponding one of the rolls so that material may be conveyed between the roll nip and the space between the doctor blades. In one form, the nip passes material to the space between the doctor blades and that space has a downstream restriction which causes the material to compress in an accordion-like way forming a corrugated material web. In another form, the doctor blades function to deliver thermoplastic extrudate to the nip between the rolls to form elongated sheets or webs of plastic material of improved uniformity.Type: GrantFiled: July 23, 1998Date of Patent: October 10, 2000Assignee: Materials Research Innovations CorporationInventor: Rexford H. Bradt
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Patent number: 6099791Abstract: Porous fluoropolymer films, such as PTFE films, formed by a method including the steps of (a) forming a fluoropolymer (e.g., PTFE) paste, (b) extruding, calendaring, or otherwise processing the paste to form a film extrudate, (c) causing the film extrudate to be calendared in a first directional axis, (d) subsequently calendaring the film extrudate in a second directional axis which is different from the first directional axis, (e) subsequently calendaring the film extrudate in at least one additional directional axis which is different from said first and second directional axes, thereby forming a multiaxially calendared film extrudate, (f) drying the multiaxially calendared film extrudate, and (g) radially expanding the multiaxially calendared film extrudate to form a radially oriented fluoropolymer (e.g., PTFE) film. The porous fluoropolymer films formed by this method are multiaxially oriented and exhibit isotropic strength properties.Type: GrantFiled: March 8, 1996Date of Patent: August 8, 2000Assignee: Baxter International Inc.Inventors: Donald Shannon, John McIntyre, Chris Kuo, Chris McCollam, Robert Peterson
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Patent number: 6093354Abstract: A method of continuously manufacturing and curing in-line a sheet of ethylene-propylene diene monomer to form an EPDM roofing membrane. The method includes the steps of forming a continuous sheet material of ethylene-propylene diene monomer and then continuously heating and pressing the sheet material to partially cure the sheet material and remove any voids within the sheet material. The partially cured sheet material is then continuously fed through a curing oven to fully cure the sheet material to form EPDM roofing membrane.Type: GrantFiled: December 1, 1998Date of Patent: July 25, 2000Assignee: Omnova Solutions Inc.Inventors: Michael J. Hubbard, Walter J. Kelly, Anthony Verrocchi, Raymond J. Weinert
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Patent number: 6080471Abstract: The present invention provides a non-woven fabric for an alkali cell separator capable of preventing active materials from transfer, and having distinguished electrolyte solution absorbability and retainability in spite of a small areal weight and also provides a process for producing the same. The non-woven fabric is substantially free from perforations and has a center surface average roughness SRa of not more than 13 .mu.m at streaks of entanglement on at least one side of the non-woven fabric, a maximum pore diameter of not more than 50 .mu.m and a water absorbability under pressure of not less than 20 g/m.sup.2, and a standard deviation of pore diameter distribution of not more than 20 .mu.m, as determined by bubble point method.Type: GrantFiled: August 13, 1997Date of Patent: June 27, 2000Assignee: Mitsubishi Paper Mills LimitedInventors: Toshihiro Shigematsu, Yoshitami Ishikawa, Yasuyuki Oku
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Patent number: 6077373Abstract: A method for making multilayer polymer films with involves the use of preferably embossed rollers which oscillate oppositely with respect to each along their respective rotational axis. Multilayer film is made by passing two or more molten thermoplastic films through the nip of these rollers, thereby laminating the individual films together. The method is particularly useful for improving the adhesion between film layers, and/or when at least one of the layer is a liquid crystalline polymer. Such films are useful in packaging, multilayer containers and for circuit boards.Type: GrantFiled: August 5, 1997Date of Patent: June 20, 2000Assignee: Du Pont Canada Inc.Inventors: Eldon Lawrence Fletcher, Anthony Joseph Cesaroni, Rodney Martin
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Patent number: 6068804Abstract: A process of producing an asphalt-impregnated fiberboard comprises the steps of forming an aqueous slurry of a fibrous material and asphalt, the solids content of the slurry being less than about 8 weight percent, mixing the slurry to uniformly distribute its components, dewatering the slurry to form a wet mat, pressing the wet mat to consolidate it, and drying the consolidated wet mat. Fiberboards made by the process can be employed as durable resilient expansion joints between various types of structural members.Type: GrantFiled: July 2, 1998Date of Patent: May 30, 2000Assignee: Celotex CorporationInventors: William E. Betzner, Fred L. Migliorini
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Process for producing filament and filament assembly composed of thermotropic liquid crystal polymer
Patent number: 6051175Abstract: A process for producing a filament assembly composed of a thermotropic liquid crystal polymer, includes the step of melt extruding a thermotropic liquid crystal polymer through an orifice nozzle into a high-speed fluid to thereby hold filaments spun right under the spinning nozzle at a high temperature, so that the filaments are taken up at a high draft ratio by the frictional force of the high-speed fluid.Type: GrantFiled: May 3, 1995Date of Patent: April 18, 2000Assignee: Polymer Processing Research Inst., Ltd.Inventors: Kazuhiko Kurihara, Hiroshi Yazawa, Toshikazu Oishi, Yoichi Mazawa -
Patent number: 6027680Abstract: A method and apparatus is disclosed for the in-line pre-impregnation of glass or synthetic fibers with a non-aqueous chemical treatment. The apparatus includes a first applicator for applying a curable, non-aqueous chemical treatment agent and a second applicator for applying a curing agent for the chemical treatment agent. The fibers are passed over the first and second applicators which are arranged either in parallel or in series, and are then joined by a gathering device to initiate curing of the chemical treatment agent on the fibers. In an alternative embodiment, the apparatus includes a spray gun in which a mixture of the non-aqueous chemical treatment agent and curing agent are sprayed onto an applicator roll in contact with the fibers.Type: GrantFiled: December 30, 1997Date of Patent: February 22, 2000Assignee: Owens Corning Fiberglas Technology, Inc.Inventors: Andrew Woodside, Margaret Woodside, David Shipp, Frank J. Macdonald
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Patent number: 6025436Abstract: The invention provides a thermoplastic fluorine-containing resin composition intended to be passed between at least two rollers of a calender to be thinned into a sheet or film. This composition includes: 100 parts by weight of a mixture containing 10-90 wt % of a fluorine-containing elastomeric polymer having a glass transition temperature below room temperature and 90-10 wt % of a fluorine-containing crystalline resin having a melting point not higher than 300.degree. C.; and 0.05-2.0 parts by weight of an agent for releasing the composition from the at least two rollers. The composition has a good melt characteristic and a good elasticity for calendering of the composition, and a good releasibility from a calender roller in calendering of the composition.Type: GrantFiled: May 23, 1997Date of Patent: February 15, 2000Assignee: Central Glass Company, LimitedInventors: Chikashi Kawashima, Katunori Kawamura, Seiiti Minegishi
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Patent number: 6025066Abstract: The present invention provides a stencil sheet roll formed by winding up a stencil sheet to form a roll, the sheet including a thermoplastic resin film and a porous support laminated thereto, wherein the compression elastic modulus of the sheet is not less than 32 kg/cm.sup.2. The invention also provides a stencil sheet roll formed by winding up a stencil sheet to form a roll, the sheet including a thermoplastic resin film and a porous support laminated thereto and having been subjected to calender treatment. Also disclosed is a method for manufacturing a stencil sheet roll comprising laminating a thermoplastic resin film to a porous support to form a stencil sheet, subjecting the stencil sheet to calender treatment, and winding up the calender-treated stencil sheet to form a roll.Type: GrantFiled: June 4, 1996Date of Patent: February 15, 2000Assignee: Riso Kagaku CorporationInventors: Hideki Terasawa, Hiroyo Kikuchi, Takayuki Kurosaki, Mitsuru Ujiie
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Patent number: 6015626Abstract: Described is a weather-resistant, plasticizer-free, deep-drawable film based on a semicrystalline ethylene/propylene/diene terpolymer and a homo- and/or copolymer of an alkene plus stabilizers and optional fillers, lubricants, pigments, and other ordinary additives. This film is characterized by the fact that the mixture of the semicrystalline ethylene/propylene/diene terpolymer and the homo- and/or copolymer of the alkene contains:70-30 wt % semicrystalline ethylene/propylene/diene terpolymer (A) with approximately 56-76 wt % ethylene, approximately 15-30 wt % propylene, and approximately 9-14 wt % third component,while the terpolymer (A) has a melt-flow index MFI (230/2, 16) of approximately 5-15.0 g/10 min,and 70-30 wt % homo- and/or copolymer (B) of ethylene and/or propylene,while the homo- and/or copolymer has a melt-flow index MFI (230/2, 16) greater than 2.5 g/10 min. This film is especially suited for the interior covering and fittings of motor vehicles.Type: GrantFiled: February 19, 1998Date of Patent: January 18, 2000Assignee: Benecke-Kaliko AGInventor: Walter Kopytko
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Patent number: 6009690Abstract: A process for the production of divisible tablets by melt calendering in which two molding rolls are combined together, at least one of which has depressions with at least one bar which extends up to the surface line of the molding roll and forms a score.Type: GrantFiled: June 18, 1997Date of Patent: January 4, 2000Assignee: BASF AktiengesellschaftInventors: Joerg Rosenberg, Werner Maier, Helmut Fricke, Jorg Breitenbach
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Patent number: 5998005Abstract: The present invention provides a sheet made of a polyester resin composition, which composition shows no adhesion to calender rolls and can be made into a sheet by calendering. Specifically, the present invention provides a sheet made of a polyester resin composition, wherein the polyester resin composition comprises100 parts by weight of a copolyester resin obtained by replacing, in production of polyethylene terephthalate resin, 10 to 40 mole % of the ethylene glycol component with cyclohexanedimethanol, and0.1 to 2 parts by weight of a fatty acid ester lubricant.Type: GrantFiled: March 29, 1999Date of Patent: December 7, 1999Assignee: Sumitomo Bakelite Company LimitedInventor: Hiroshi Kanno
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Patent number: 5993935Abstract: A composite article is provided having covalently reactive particles incorporated in a continuous, porous matrix. The reactive particles have surfaces of covalently reactive functional groups capable of directly forming covalent chemical bonds with ligands without need for an intermediate activation step. An adduct composite article is also provided comprising a continuous, porous matrix and derivatized particles dispersed therein. The derivatized particles comprise a direct, covalent reaction product of ligand with the covalently reactive particles. Methods of making and using the composite articles and adduct composite articles are also provided. Preferred covalently reactive functional groups are azlactone-functional groups of the formula: ##STR1## wherein: R.sup.1 and R.sup.Type: GrantFiled: October 11, 1991Date of Patent: November 30, 1999Assignee: 3M Innovative Properties CompanyInventors: Jerald K. Rasmussen, Steven M. Heilmann, Larry R. Krepski, Patrick L. Coleman, Dean S. Milbrath, Margaret M. Walker, Donald F. Hagen, Paul E. Hansen, John C. Campbell
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Patent number: 5985194Abstract: The method of making a semiconductor body from a semiconductor polymeric compound containing about 20% by weight lampblack having a porous structure, about 60% by weight of low density polyethylene, about 8.5% by weight ethylene vinyl acetate copolymer, about 4.0% by weight calcium stearate, about 3.0% by weight antioxidant and about 0.5% by weight calcium titanate includes the steps of extruding the semiconductor polymeric compound to form an extruded product and subsequently calendering the extruded product to produce a semiconductor body having an electrical conductivity which is as uniform as possible throughout the entire bulk of the semiconductor body.Type: GrantFiled: May 22, 1998Date of Patent: November 16, 1999Assignee: Metagal Industria E Comercio LTDAInventors: Humberto Takashi Kadooka, Ricardo Proveda Moreno, Olavo Nunes Da Costa
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Patent number: 5952120Abstract: A method of making a trilayer, shutdown battery separator has the following steps: extruding a polyethylene precursor; extruding a polypropylene precursor; forming a trilayer precursor, the trilayer precursor having the polyethylene precursor sandwiched between two polypropylene precursors; bonding the trilayer precursor; annealing the trilayer precursor; stretching the trilayer precursor; and forming thereby the battery separator.Type: GrantFiled: April 15, 1997Date of Patent: September 14, 1999Assignee: Celgard LLCInventors: Wei-Ching Yu, Shawn E. Hux
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Patent number: 5932317Abstract: A method to produce a dust control mat with stronger longitudinal borders by co-calendering the rubber backing thereof with narrow strips of carboxylated nitrile rubber prior to formation of the dust control into a unitary product for use as a dust control mop.Type: GrantFiled: June 27, 1994Date of Patent: August 3, 1999Assignee: Milliken & CompanyInventor: Robert Charles Kerr
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Patent number: 5928679Abstract: An elastomeric extruding apparatus having a head, to which a plurality of extruders are coupled, and a rotatable, driven roller disposed at the front end of the head so as to form an extruding space between the roller and the head. The head is provided with a passage arrangement, through which the elastomeric materials pass, eventually opening into the extruding space. The extruding space has a uniform chamber extending from the opening of the passage arrangement and a finishing chamber communicating with the uniform chamber for shaping the elastomer into its final sectional shape.Type: GrantFiled: July 11, 1996Date of Patent: July 27, 1999Assignee: Sumitomo Rubber Industries, Ltd.Inventors: Masahiko Ohki, Shuichi Yamamori
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Patent number: 5919530Abstract: Disclosed is a method for customizing a thermoplastic resin in which a thermoplastic resin body is at least partially coated with a thermoplastic coating composition comprising an additive component and a polymeric component. The thermoplastic resin body is at a temperature that is above the onset temperature of the melt processing range of the coating composition. After the coating is applied, the resin body is cooled to solidify the coating composition. Customized thermoplastic resins may be produced more efficiently using the present method than by conventional methods. The customized thermoplastic resins produced according to the invention may be heated to above the onset temperature of the melt processing range of the resin body, mixed to form a substantially uniform mixture and formed into an article.Type: GrantFiled: June 30, 1997Date of Patent: July 6, 1999Assignee: BASF CorporationInventors: James M. Hurley, Bernd B. Brian, Mary E. Tuttle, Bill Popovski
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Patent number: 5908528Abstract: A method for preparing an uncured supported elastomer material includes the steps of: providing a fibrous reinforcement material; providing a layer of uncured elastomer material substantially adjacent to the fibrous reinforcement material; exposing the layer and the fibrous reinforcement to a temperature below a curing temperature and above a flow point of the uncured elastomer material, and a pressure sufficient that the uncured elastomer material flows into the fibrous reinforcement material, so as to provide an uncured supported elastomer material.Type: GrantFiled: April 16, 1998Date of Patent: June 1, 1999Assignee: United Technologies CorporationInventors: Lisa A. Walla, Charles R. Watson
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Patent number: 5904955Abstract: An electronic device in a cavity in a mold is encapsulated by a composite plastic having two materials placed, respectively, in sequential locations in a reservoir in the mold. The first material has desirable properties when in contact with the surface of the device, e.g., better adhesion. The second and different material has other desirable properties, e.g., mechanical strength, low moisture permeability, etc. The first location is first in line in a direction through the mold chambers to the cavity. The two-part encapsulant is injected into the cavity without significant turbulence so as to avoid much mixing of the two materials. This creates a boundary layer of the first material which preferentially applies a coating to the device while the second material substantially fills the bulk of the space in the mold cavity. A composite encapsulation is formed having overall superior properties.Type: GrantFiled: September 5, 1997Date of Patent: May 18, 1999Assignee: Motorola, Inc.Inventors: Robert Goldstein, Nikolai Osipenko, George Hawkins
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Patent number: 5882456Abstract: A method for manufacturing a tread strip with shoulder cover strips for a pneumatic vehicle tire includes the step of continuously extruding a shoulder cover strip and calendering the shoulder cover strip to a desired thickness. The thus thickness-reduced cover strip is then applied to the tread strip. The shoulder cover strip is then cut to length in order to match a circumferential length of the tread strip for building a tire.Type: GrantFiled: May 2, 1997Date of Patent: March 16, 1999Assignee: Continental AktiengesellschaftInventor: Stephan Kohne
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Patent number: 5879498Abstract: A barrier liner for sealing reinforced composite vessels at cryogenic temperatures is provided wherein the barrier liner is composed of a polymeric composition containing a curing agent, such as a methyl bis-methyl anthranilate, and an elastomer adhesive, such as a two-part polyether based urethane adhesive. A method of manufacturing and applying the barrier liner is also provided, including the steps of mixing and degassing the polymeric composition and introducing the polymeric composition between two polyethylene carrier sheets. The two carrier sheets and the intermediate polymeric composition layer are then passed between two sizing rollers set apart at a predetermined distance. The encapsulated polymeric composition is then partially cured to a tacky gel state and cooled to arrest polymerization until application of the gel layer. The gel layer and the two carrier sheets can then be cut into any desired shape such as strips, and applied to the inner surface of a vessel.Type: GrantFiled: October 8, 1997Date of Patent: March 9, 1999Assignee: McDonnell Douglas CorporationInventor: Carl R. Lemons