Abstract: The present disclosure includes apparatuses and methods related to freezing a sacrificial material in forming a semiconductor. In an example, a method may include solidifying, via freezing, a sacrificial material in an opening of a structure, wherein the sacrificial material has a freezing point below a boiling point of a solvent used in a wet clean operation and removing the sacrificial material via sublimation by exposing the sacrificial material to a particular temperature range.

Abstract: A low-temperature quick-freezing freeze-drying system provided by the invention includes: a compressor unit, a first heat exchanger, an air cooler, a second heat exchanger, a throttling element, a third heat exchanger, a circulating fan, a drying chamber, a third valve, a fourth valve and connecting pipelines, and the above elements form a refrigeration circulation loop, a quick freezing/freeze-drying circulation loop, and a desorption drying circulation loop, thereby realizing the low-temperature quick-freezing and freeze-drying of materials. The invention adopts the heat exchangers with a cold storage function, so that the refrigeration capacity of the compressor is stored and used intensively to achieve rapid cooling of the materials.

Abstract: The present invention is related to a method of fabricating a film. The method may comprise filling ink droplets containing a solvent and material constituting the film into pixel units of an array substrate; freezing the ink droplets on the array substrate; and sublimating the solvent of the ink droplets on the array substrate. The pixel units of the array substrate may be separated by a pixel define layer and arranged in a matrix.

Abstract: A method of preparing a pharmaceutical product in a single multiple chamber flexible bag. A pharmaceutical product is introduced in a liquid state into a first chamber of the flexible bag through a first port. The pharmaceutical product is lyophilized within the first chamber of the flexible bag to provide a lyophilized pharmaceutical product. The flexible bag has a second chamber and the first chamber and the second chamber are separated by a breakable seal. The second chamber further includes a reconstituting solution for reconstituting the lyophilized pharmaceutical product in the first chamber. A user may apply pressure to the flexible bag to break the seal and mix the lyophilized pharmaceutical product and the reconstituting solution to order to administer the pharmaceutical product to a patient.

Abstract: A method of preparing a pharmaceutical product in a single multiple chamber flexible bag. A pharmaceutical product is introduced in a liquid state into a first chamber of the flexible bag through a first port. The pharmaceutical product is lyophilized within the first chamber of the flexible bag to provide a lyophilized pharmaceutical product. The flexible bag has a second chamber and the first chamber and the second chamber are separated by a breakable seal. The second chamber further includes a reconstituting solution for reconstituting the lyophilized pharmaceutical product in the first chamber. A user may apply pressure to the flexible bag to break the seal and mix the lyophilized pharmaceutical product and the reconstituting solution to order to administer the pharmaceutical product to a patient.

Abstract: A method of preparing a pharmaceutical product in a single multiple chamber flexible bag. A pharmaceutical product is introduced in a liquid state into a first chamber of the flexible bag through a first port. The pharmaceutical product is lyophilized within the first chamber of the flexible bag to provide a lyophilized pharmaceutical product. The flexible bag has a second chamber and the first chamber and the second chamber are separated by a breakable seal. The second chamber further includes a reconstituting solution for reconstituting the lyophilized pharmaceutical product in the first chamber. A user may apply pressure to the flexible bag to break the seal and mix the lyophilized pharmaceutical product and the reconstituting solution to order to administer the pharmaceutical product to a patient.

Abstract: A method of applying RF energy to an object in a cavity is disclosed. In some embodiments, the method may include applying to the object a first amount of RF energy at power increasing from an initial power level to a final power level; and if an electrical discharge occurs, stopping RF energy application for a period sufficient to allow the electrical discharge to decay. The method may further include applying to the object a second amount of RF energy after the period ends. The second amount of RF energy may be applied at intermediate power, higher than the initial power level and lower than the final power level.

Abstract: An equipment rack system includes a plurality of holders at least including a pair of first holders, a pair of second holders, a pair of third holders, a pair of fourth holders, and a pair of fifth holders, a base; a vertical column have a first end and a second end; a valve; and a powerer. Each pair of first holders, the pair of second holders, the pair of third holders, the pair of fourth holders, and the pair of fifth holders comprise fluid apertures about their lengths. The equipment is placed on the pair of first holders, the pair of second holders, the pair of third holders, the pair of fourth holders, and the pair of fifth holders on the equipment rack during an in-use condition to sanitize and air dry equipment to neutralize odors, and eliminate bacteria, and germs.

Abstract: A heating device (124) for heating particles to be freeze-dried in a rotary drum (102) of a freeze-dryer (100) is provided, the device comprising at least one radiation emitter (202) for applying radiation heat to the particles, and a tube-shaped separator (204) for separating the particles from the at least one emitter (202). The separator (202) being integrally closed at one end and separating an emitter volume (206) encompassing the at least one emitter (202) from a drum process volume (126) inside the drum (102), wherein the heating device (124) protrudes into the drum process volume (126) such that said integrally closed end of the separator (204) is arranged inside the drum (102) as a free end.

Abstract: A drying apparatus for drying sports pads or apparel is provided. The drying apparatus may include a first member and a second member. The first member may be aligned substantially perpendicular to the second member and slid into the second member to form the drying apparatus. The drying apparatus may be inserted into the sports pads or a portion of the apparel to permit air to flow throughout the innards of the sports pads or apparel, thereby facilitating the drying of the sports pads or apparel.

Abstract: A method for making a dry pulp comprising the steps of (i) forming a dispersion in water of a pulp comprising polymeric fibers having a tenacity of at least 20 g/dtex, (ii) filtering the dispersion to form a mass of wet pulp having a solids content of from 5 to 60%, (iii) freezing the wet pulp until the mass is at least 95% frozen, (iv) subliming the water from the frozen mass by subjecting the frozen mass to vacuum of less than 4.5 Torr until the final moisture content of the pulp is no greater than 5% and (v) warming the pulp to ambient temperature under vacuum.

Abstract: A vacuum freeze-drying apparatus capable of rapid drying is provided. A cold trap for drying, which is arranged inside a drying chamber, is set to a low temperature of ?70 degrees Celsius or below, and heat is supplied to frozen particles on a conveyor belt to a degree such that the frozen particles do not melt. The amount of the liquid component evaporating from the frozen particles increases, and the amount of the liquid component entering the frozen particles decreases so that the time for drying the frozen particles is shortened.

Abstract: An apparatus for freeze drying a substrate is provided. A chamber for receiving a substrate is provided. An electrostatic chuck (ESC) for supporting and electrostatically clamping the substrate is within the chamber. A temperature controller controls the temperature of the electrostatic chuck. A condenser is connected to the chamber. A vacuum pump is in fluid connection with the chamber.

Abstract: A method of manufacturing heat-sensitive pharmaceutical powder is disclosed. The original pharmaceutical substances are dissolved in a solution or suspended in a suspension, which is sprayed through an atomizing nozzle and frozen in a cold gas phase or liquid nitrogen atomized directly in the spray-freeze chamber or gas jacket at the same time (for cooling purposes). The particles are freeze-dried at roughly atmospheric pressure in a down-stream fluid flow with exit filter thereby to remove moisture entrapped on or inside the frozen particles. The system has applicability for forming other powders.

Abstract: A method for the preparation of fluoropolymer powdered materials is disclosed. A suspension of solid fluoropolymer particles in a liquid carrier, preferably water, is frozen and the frozen carrier is then removed by sublimation at sub-atmospheric pressure to produce a dry powder of fluoropolymers particles.

Abstract: The invention relates to a method and a movable apparatus for utilizing microwave energy to dry materials (optionally with sterilization) by the direct application of bifurcated out-of-phase microwave energy.

Abstract: A process of freeze drying of an essentially aqueous solution comprising at least one first step having a first temperature and pressure level (i.e. primary drying phase) and at least one second step having a second temperature and pressure level (i.e. secondary drying phase) following the first step, wherein in the secondary drying phase limited desorption energy input is applied.

Abstract: A process for producing nanoparticles of paclitaxel and albumin having antitumor properties, by which a mixture obtained by adding paclitaxel in powder form to an aqueous solution of albumin with chloroform is subjected to high pressure homogenization treatment.

Abstract: The electrical hair treatment appliance (1) includes an electrically controlled hair treatment device, preferably including infrared emitter elements (20), and an operator control panel (2) rigidily attached to the hair treatment device. The operator control panel (2) includes a receptacle (5) rigidly attached to the hair treatment device, an operator control and display device (3) mounted in the receptacle (5) so as to rotate in the receptacle and an electrical connection (6) for electrically connecting between the operator control and display device (3) and the receptacle (5). The rotatable operator control and display device (3) preferably includes buttons for setting and adjusting operating parameters of the hair treatment device and has a circular face (4). The electrical connection (6) may include a flat cable (7), such as a stranded flat cable or a flexible electrical conductor track foil.

Abstract: A method and an apparatus for effecting freeze-drying specimens containing solvents or condensing solvents having a shallow pan treatment chamber with little or no obstructions, holes or orifices. The treatment is effected by cooling the base of the chamber by using coolant-containing coils mounted beneath the base of the chamber. The direct thermal conduction of heat through the base of the chamber provides a more effective method of both cooling specimens and condensing solvents, typically water. A source of vacuum is provided to the chamber by a conduit located in the cover, sidewalls or base of the chamber. The method and apparatus may employ a moveable specimen holder positioned in the chamber. The moveable specimen holder may be mounted on a perforated tube which slidably engages a conduit in the base of the chamber. The perforated tube may a conduit to the source of vacuum.

Abstract: Freeze-dried products of high quality produced from materials to be freeze-dried in a freeze-drying apparatus comprising a sealed vessel enclosing a processing chamber provided therein with a rotary cage receiving a gas-permeable container containing one or more frozen products of the said material, prepared by freezing the said material with dry ice, and a heating device for heating the frozen product by radiant heat rays, wherein the freeze-dried product is produced by a process which can attain efficient sublimating removal of large amount of carbon dioxide gas evolved from dry ice and of moisture included in the material, while preventing adhesion of the frozen products to each other and while permitting reduction of the sublimation duration, wherein the frozen product retained in the gas-permeable container placed in the rotary cage is heated uniformly by the heating device under vacuum condition while holding it under rotational movement to thereby facilitate the sublimation of dry ice and of the frozen

Abstract: Freeze-dried products of high quality produced from materials to be freeze-dried in a freeze-drying apparatus comprising a sealed vessel enclosing a processing chamber provided therein with a rotary cage receiving a gas-permeable container containing frozen pieces of the said material, prepared by freezing the said material with a refrigerant, and a heating device for heating the frozen material by radiant heat rays, wherein the freeze-dried product is produced by a process which can attain, even when dry ice is used as the refrigerant, efficient sublimating removal of large amount of carbon dioxide gas evolved from dry ice and of moisture included in the material, while preventing adhesion of the frozen pieces of the said material to each other and while permitting reduction of the sublimation duration, wherein the frozen material retained in the gas-permeable container placed in the rotary cage is heated uniformly by the heating device under vacuum condition while it is being maintained under rotational mov

Abstract: The present invention provides methods and apparatus for freeze drying in which a solution, which can be a radioactive salt dissolved within an acid, is frozen into a solid on vertical plates provided within a freeze drying chamber. The solid is sublimated into vapor and condensed in a cold condenser positioned above the freeze drying chamber and connected thereto by a conduit. The vertical positioning of the cold condenser relative to the freeze dryer helps to help prevent substances such as radioactive materials separated from the solution from contaminating the cold condenser. Additionally, the system can be charged with an inert gas to produce a down rush of gas into the freeze drying chamber to also help prevent such substances from contaminating the cold condenser.

Abstract: A lyophilizer system is adapted for operation in a first mode or a second mode with microwave assisted drying. The system includes a lyophilizing chamber, including shielding from microwaves. The chamber is connected to a pressure controller for controlling vacuum in the lyophilizing chamber and a device for trapping water vapor. One or more microwave generators, direct microwaves into the lyophilizing chamber. Refrigeration units lower the temperature of the lyophilizing chamber and condenser. The chamber environment maintains a temperature and a pressure that facilitates sublimation in the chamber in a first mode, and for creating a chamber environment having vacuum and temperature such that when combined with microwaves directed into the chamber, facilitates sublimation in the chamber in a second mode. The chamber has arc inhibiting surfaces and shielding and a corona discharge detection and control system, including optical, thermal and other detection systems.

Abstract: The present invention provides methods and apparatus for freeze drying in which a solution, which can be a radioactive salt dissolved within an acid, is frozen into a solid on vertical plates provided within a freeze drying chamber. The solid is sublimated into vapor and condensed in a cold condenser positioned above the freeze drying chamber and connected thereto by a conduit. The vertical positioning of the cold condenser relative to the freeze dryer helps to help prevent substances such as radioactive materials separated from the solution from contaminating the cold condenser. Additionally, the system can be charged with an inert gas to produce a down rush of gas into the freeze drying chamber to also help prevent such substances from contaminating the cold condenser.

Abstract: A method of washing and drying of discrete components in bulk, wherein the components are washed with a cleaning liquid and the wet components are dried in a freeze-drying process by bringing the wet components to a temperature below the melting point of the cleaning liquid, so that the cleaning liquid becomes a solid substance, and by evaporating the solid substance through introduction of the components and the solid substance into a space having a pressure lower than the vapour pressure of the solid substance.

Abstract: Fiber reinforced structural components, such as panels with honeycomb cores sandwiched between at least two outer skin layers are dried to remove moisture that may have entered into the interior of the structure. For this purpose the component is cooled in a cooling environment below the freezing point to about -5.degree. to -20.degree. C. and then exposed to a reduced pressure of less than 0.5 mbar. Under these drying conditions moisture is driven out of the component by sublimation so that the moisture does not pass through the liquid phase. The drying time may be reduced by a temperature increase to 80.degree.-100.degree. C. while maintaining the low pressure. The freezing increases the capillary action for the moisture removal. However, for an increased efficiency in the moisture removal small diameter holes, e.g. 0.1 mm bores, may be drilled into the component to facilitate the moisture escape. After drying is complete the holes are closed again e.g. by laminating further cover sheets to the component.

Abstract: The invention relates to a process for the regulation of lyophilization in which the evaporative flux--that is to say, the output of evaporated water transferred on the trap (4)--is measured in a continuous manner, and action is carried out at the temperature of the racks (2) in order to reach, as close as possible, a predetermined optimal flux.

Abstract: The invention relates to a process and apparatus for desiccation in which the exterior walls of the apparatus are heated and cooled in synchronization with the interior of the apparatus to avoid temperature gradients and inconsistent desiccation of material placed within the apparatus. The apparatus wall temperature regulating means also allows for more accurate sterilization of the apparatus after the desiccation process has been completed.