Abstract: Embodiments under the present disclosure include the application of an electric field in a region of liquid undergoing ultra-high shear impact, mixing and or cavitation. The co-location of electrolysis and high shear mixing and or cavitation has demonstrated the ability to cause advanced oxidation reactions and advanced reduction reactions in fluid systems such as water with both dissolved and suspended solids, and hydrocarbon with and without water emulsion.

Abstract: Methods for the production of carbon black using an extender fluid(s) are provided as well as methods to control one or more particle properties of carbon black utilizing extender fluids and other techniques.

Abstract: The present invention relates to an apparatus for metering flowable media or gases, and to the use thereof.

Abstract: A fast and sensitive method and device for protein sequencing are disclosed. The method uses a combination of Edman degradation chemistry and mass spectrometry to sequence proteins and polypeptides. A peptide degradation reaction is performed on a polypeptide or protein ion reactant in the gas phase. The reaction yields a first ion product corresponding to a first amino acid residue of the polypeptide or protein reactant and a polypeptide or protein fragment ion. The mass-to-charge ratio for the first ion product, or the polypeptide or protein fragment ion, or both, is then determined. The first amino acid residue of the polypeptide or protein reactant is then identified from the mass-to-charge ratio so determined.

Abstract: The present invention relates to an apparatus for the continuous production of carbon nanotubes (CNT), as well as the method to carry it out. The apparatus for the CNT synthesis includes: two sets or more of tubes to synthesize in its interior the CNT; a set of nozzles for the same number of tubes that each set has, to feed to the interior of the tubes the precursory chemical compounds of the CNT; a furnace to maintain one of the sets to a suitable temperature to allow the formation of the CNT inside the tubes; a system for the detaching and collection of the CNT formed in the previous stage; and a control system, preferably a PLC (PLC by its abbreviation in English) to program the sequence of activities of the equipment.

Abstract: The invention relates to a method for producing carbon black or other flame aerosols, comprising the following steps: the heat is removed from the flame by dissipation and/or radiation; a thin gas boundary layer is formed; the flow formed by the flame and the gas boundary layer is accelerated or expanded; the obtained aerosol is withdrawn; and the cooling surface is cleaned. The invention further relates to a device for carrying out such a method and a black carbon having a maximum pH value of 6.0, a maximum ignition residue of 0.1 percent, and a maximum 5 ?m screening refuse of 200 ppm. The inventive black carbon can be used in rubber, plastic, printing inks, inks, inkjet inks, toners, lacquers, dyes, paper, bitumen, concrete, and other construction materials.

Abstract: The present invention provides a method and apparatus for the controlled synthesis of nanoparticles using a high temperature process. The reactor chamber includes a high temperature gas heated by means such as a plasma torch, and a reaction chamber. The homogenizer includes a region between the reactant inlets and the plasma (the spacer zone) to ensure that feeds from the reactant inlets are downstream of the recirculation zone induced by the high temperature gas. It also includes a region downstream of the reactant inlets that provides a nearly I dimensional (varying only in the axial direction) flow and concentration profile in the reaction zone to produce nanoparticles with narrow size distribution.

Abstract: The present invention relates to a method for mass preparation of granular polycrystalline silicon in a fluidized bed reactor, comprising (a) a reactor tube, (b) a reactor shell encompassing the reactor tube, (c) an inner zone formed within the reactor tube, where a silicon particle bed is formed and silicon deposition occurs, and an outer zone formed in between the reactor shell and the reactor tube, which is maintained under an inert gas atmosphere, and (d) a controlling means to keep the pressure difference between the inner zone and the outer zone being maintained within the range of 0 to 1 bar, thereby capable of maintaining physical stability of the reactor tube and efficiently preparing granular polycrystalline silicon even at a relatively high reaction pressure.

Abstract: This invention relates to a carbon black reactor comprising; a combustion zone for generating a hot combustion gas by burning a mixture of a hydrocarbon fuel and an oxygen containing gas, a reaction zone for producing a carbon black by contacting the hot combustion gas with a feedstock introduced in a plurality of divided flows to thermally decompose and/or incompletely combust the feedstock, and a quench zone for stopping a carbon black growth reaction by injection a coolant to said carbon black containing flow, and these three zones are arrayed laterally in order, wherein the cross-section shape of the feedstock introduction part in the reaction zone is not a circle nor a polygon. The carbon black reactor can produce the carbon black having same characteristics, especially the distribution of the aggregate size, as one produced by pilot-scale reactor, while its production scale is increased to the level of that of reactor actually operated.

Abstract: A process to prepare a mixture of hydrogen and carbon monoxide from a methane containing gaseous feed by performing the following steps, (a) performing a partial oxidation by contacting the feed with an oxygen containing gas to prepare a gaseous mixture comprising hydrogen, carbon monoxide, steam, carbon dioxide, methane and soot particles said mixture having an elevated temperature, (b) passing the gaseous mixture of step (a) through a filter where the soot particles are retained on the filter and a mixture comprising hydrogen, carbon monoxide, carbon dioxide, methane poor in soot is obtained wherein the filter is a ceramic foam filter or a ceramic wall-flow filter, and (c) converting the retained soot particles at the elevated temperature to carbon oxide.

Abstract: An apparatus for continuous production of aligned carbon nanotubes is disclosed. The apparatus includes a reactor, an injector for delivering a feed solution into the reactor, and a conveyor for passing through the reactor a substrate on which nanotubes may be formed and grown. The apparatus further may include an inert, porous medium through which the feed solution may be passed. The apparatus produces aligned carbon nanotubes of a predetermined external diameter, and is suitable for large scale production of aligned carbon nanotubes in an industrial setting.

Abstract: There is described an apparatus for making metal oxide particles which are substantially free of coarse tail from an oxidizing agent and a metal reactant in a flow reactor. The apparatus can be a concentric tubular flow reactor comprising a substantially funnel-shaped reactant contacting region located adjacent to a reaction zone which is able to direct a flow of a hot oxidizing agent towards a flow of the metal reactant to form a reaction stream which flows downstream into a reaction zone, whereby the hot oxidizing agent of the reaction stream is able to surround the flow of metal reactant sufficient to prevent the metal reactant from contacting the wall of the reactant contacting region and forming scale on the wall.

Abstract: This disclosure relates to process for producing titanium dioxide (TiO2) pigments, comprising the following steps: a) oxidizing a mixture of titanium tetrahalide and a rutile forming agent, such as aluminum halide, present in the vapor phase and in the presence of a nucleant to form a gaseous suspension comprising titanium dioxide particles; b) passing the gaseous suspension to a cooling conduit; c) introducing scouring material into the cooling conduit; wherein the particles of the scouring material have a diameter in the range of about 0.25 mm to about 12.7 mm; d) separating the vapor phase to form a powder comprising the titanium dioxide particles and the scouring material; and e) simultaneously subjecting the powder to substantially uniform heating at a temperature of about 300° C. to about 600° C.

Abstract: A gas re-use system for carbon fiber manufacturing processes based on hydrocarbon thermal decomposition. The system permits re-use of the output gas from the carbon fiber manufacturing process, a process based on the use of an industrial gas as the main raw material. The system can comprise a feedback pipeline provided with force and filtering means to raise the pressure from the reaction furnace output manifold to its input. There are also return and bleed lines operated separately to assure suitable pressure ranges at the same time both in the reaction furnace input area and extraction area.

Abstract: What is disclosed herein deals with low to medium pressure, high temperature, all ceramic, air-to-air, indirect heat exchangers, novel ball joints, high load-bearing ceramic tube sheets, and tube seal extenders for ceramic tubes that are useful in such heat exchangers. Also disclosed are new and novel systems used in new and novel industrial processes such as chemical processing, sludge destruction and the production of particulates such as, for example, carbon black. Systems utilizing several heat exchangers are also disclosed.

Abstract: Disclosed is an apparatus for production of vapor-phase growth carbon fibers. The apparatus can continuously produce these carbon fibers for a long time without blocking a furnace of tubular reactor of the apparatus. Also disclosed is a process for production of carbon fibers by means of the apparatus, a device for preventing deposition of carbon fibers on an inside of a furnace of tubular reactor, and vapor-phase growth carbon fibers produced in the apparatus. The vapor-phase growth carbon fibers include carbon nanofibers and/or carbon nanotubes. The apparatus includes a furnace of tubular reactor, at an end of which a feedstock-supplying nozzle is provided, and a discharge pipe inserted in the furnace of tubular reactor, the top end of which faces the opening of the nozzle and the bottom end discharges the carbon fibers.

Abstract: A method and apparatus for producing fullerenes, in large quantities at an economical cost, from liquid and gaseous hydrocarbons treated by a high energy source in a reactor devoid of oxygen are presented. The liquid hydrocarbons preferably selected from used hazardous materials such as used motor oils, oils, crude petroleum or petroleum cracking by-products, and the gaseous hydrocarbons such as methane and acetylene, are introduced into the oxygen deprived reactor and exposed to a high energy source which may be a plasma jet, a laser beam or a submerged electrical arc. Exposure to the high energy source causes the hydrocarbon atoms to disassociate, thereby converting the liquid and gaseous components into a vapor or cloud of mixed material. The vapor or cloud is then processed to enable the liberated carbon atoms to bind and recombine to form fullerenes. The cloud is then introduced into a condensation zone of said reactor to form a mixture of fullerenes, solid soot and residue gases.

Abstract: A process for producing carbon black comprising reacting a reaction stream formed by a prior carbon black forming process with an oxidant and a carbon black yielding feedstock to produce carbon black and cooling, separating and recovering the carbon black. The process advantageously reduces the amount of fuel needed to produce carbon black. Also disclosed is an apparatus for practicing the process.

Abstract: The present invention provides processes for introducing a fluid stream into a carbon black reactor and for producing carbon black. According to the present invention a fluid stream comprising an oxidant; nitrogen, hydrogen a hydrocarbonaceous material or mixtures thereof is introduced into the effluent flowing through a carbon black reactor in an axial direction.

Abstract: A CO2 fixation system for fixing Co2 gas existing in the atmosphere or in an exhaust gas emitted from factories and other burning sites. The system includes a fermenting tank for anaerobically fermenting organic wastes, whereby methane gas is produced. The methane gas is decomposed and hydrogen gas is produced. The hydrogen gas is reacted with the CO2 gas to produce carbon powder and water, whereby the CO2 gas is fixed to become harmless to the global warming.

Abstract: In a method for the production of carbon black and hydrogen by means of pyrolysis of hydrocarbons with a plasma torch (3) in a reaction chamber the pressure in the reaction chamber (1), the feed rate for the hydrogen plasma gas and hydrocarbons and the angle of the injection nozzles (2) in the reaction chamber (1) are adjusted in order to establish a reaction zone (5) in the chamber's central area with a location which determines the reaction enthalpy for decomposition of the hydrocarbons into hydrogen and carbon black in order to obtain a desired quality for the carbon part. The enthalpy value is adjusted in a range between 1 and 50 kWh/Nm.sup.3 and the temperature in the reaction zone is maintained between 1000.degree. C. and 4000.degree. C.

Abstract: The production of fibers is carried out by allowing a gas mixture containing a gaseous hydrocarbon or an appropriate gas to pass through a substrate (generally a steel sheet) arranged facing the direction of the gas stream and situated in a furnace wherein the gas reaches a temperature of 1.000.degree. C. approximately. The schematized device is comprised of the corresponding gas reservoirs, that is to say the hydrocarbon gas and the carrying and activating gas, a mixing and preheating chamber, the furnace at the outlet of which are collected or burnt the inflammable gases and the grid from the surface of which, duly activated, the carbon fibers may grow. The gist of the invention is that the gas goes through the substrate situated facing the flow, so that said flow of gas is parallel to the direction of the fiber growth. The maximum length of the fibers is set by the distance between the substrate and a substrate or mask situated at the other extremity of the chamber.

Abstract: A new process and apparatus for producing carbon black is provided and unique reactor with separate carbon black forming reaction zones is described. The process utilizes such a reactor is to give unique carbon blacks which give rise to low hysteresis loss and good wear where used in rubber compounds for reinforcement and particularly in rubber tires.

Abstract: Ionene polymers having biologically-active organic and/or inorganic anions are described. Methods to prepare the ionene polymers, compositions containing them and their methods of use are also described.

Abstract: The present invention relates to an insulation system for a high temperature reactor in which chlorosilanes and hydrogen gases are present. The system described comprises an inner graphite radiant heat shield and an outer carbon-based, rigid, felt insulation of high density. The inner radient heat shield provides increased chemical stability at the hot face in a chlorosilane and hydrogen reactor. Also, the inner radient heat shield reduces the temperature at the interface with the carbon-based rigid felt, thereby reducing the reactivity of the chlorosilanes with the carbon-based rigid felt. The high density of the carbon-based rigid belt further reduces radiant heat loss. More importantly, the high density of the carbon-based rigid felt excludes the highly heat conductive hydrogen gas from the voids of the flet. The insulation system, as described, allows reactors containing chlorosilanes and hydrogen gases to be operated at higher and more efficient temperatures for longer periods of time.

Abstract: A carbon black reactor having an extended reaction choke substantially reduces the presence of coke and refractory grit in the carbon black product and erosion of the carbon black reactor due to impingement of particles of forming carbon black within the reactor. The carbon black reactor generally comprises a reaction choke which extends into an exit chamber to an outlet opening within the exit chamber. Hot gas and particles of forming carbon black flow through the reaction choke, through the outlet opening into the exit chamber. The outlet opening of the reaction choke is located within the exit chamber sufficiently distal from the upstream end of the exit chamber to substantially eliminate impingement of the particles of forming carbon black against the upsteam end of the exit chamber.

Abstract: A vertical cylinder reactor which comprises a plurality of vertically coupled cylindrical modules. An upper end of the reactor, a first module, employs a spraying device for subdividing a liquid reactant into a plurality of small droplets and a toroidal ring for introducing a gas reactant around the liquid phase droplets. A second module connected downstream to the first is provided with a gas inlet jacket for introducing a heating and/or drying gas into the reactor. Connected to the second module is a third module which has a tangential gas inlet for introducing a gas tangentially into the reactor. Finally the reactor is provided with a conical bottom and an outlet conduit for removing gas containing fine solid particles.

Abstract: In a preferred embodiment, an apparatus for forming carbon fibers in a continuous gas phase reaction is disclosed wherein a reactor defines a vertical reaction chamber with a close upper end and a lower outlet, with a vertical reactant feed tube which extends generally axially therewithin. Gaseous reactants are injected into the reactor through an opening of the feed tube. The feed tube and chamber are constructed and arranged to define a gas flow path which extends generally axially upward through the feed tube into the chamber and thereafter generally axially downward through the chamber. Preferably, the tube and reactor chamber are radially spaced and concentric. The feed tube may encompasss a capillary tube which supplies a vaporizable liquid reactant. The reactor and feed tube are each elongate and of a material which is relatively resistent to heat and corrosion and are preferably of a mullite material. The feed tube extends more than one-half of the axial length of the reactor.

Abstract: An axial flow carbon black reactor for producing carbon black particles having a relatively narrow particle size distribution. Feedstock oil is introduced into the reactor by a spray nozzle located coaxial with the longitudinal center line of the reactor. The oil spray flows either in the countercurrent or the concurrent direction relative to the flow of hot gas through the reactor and produces an oil spray pattern covering either substantially the entire frontal area of the hot gas flow or substantially less than the frontal area. Countercurrent feedstock flow increases coverage of the gas flow area by the oil spray and narrows the particle size distribution of carbon black produced by the reactor, and concurrent feedstock flow produces the opposite result.

Abstract: A tubular furnace as a reactor for producing carbon black is disclosed having a constriction in at least the area of the spray device for the carbon black starting material which is oriented along the reactor axis. A combustion chamber for generating the gaseous pyrolysis medium for the carbon black raw material is laterally located in front of the constriction. The central axes of the reactor tube and the combustion chamber are in the same plane and are essentially at right angles to one another. In addition, a method for producing furnace carbon blacks is disclosed in which the described reactor can be used.

Abstract: An indicator sheet for an autoclave test pack wherein a pair of porous masses (10) are held in close superimposed relationship by means of a clamp (13) with the indicator sheet (12) sandwiched between them. The indicator sheet (12) has printed thereon a pattern of markings (14) formed from one or more substances which are adapted under steam sterilizing conditions to provide an indication of the presence of air and/or excessive moisture such that each is evident and individually identifiable.

Abstract: A system for increasing the capacity of a process for producing titanium dioxide by reacting titanium tetrachloride vapors with oxygen wherein the process includes an oxygen preheat assembly for preheating oxygen to a predetermined temperature level and a first titanium tetrachloride preheat assembly for preheating titanium tetrachloride to a first, relatively high, temperature level, a portion of the oxygen and the titanium tetrachloride vapors at the first temperature level being reacted in a first reaction zone to produce a mixture of titanium dioxide reaction product, oxygen and unreacted titanium tetrachloride vapors at the first temperature level.

Abstract: High purity magnesium oxide fine particles are produced by introducing a flow of a magnesium vapor-containing gas and a flow of an inert gas separately into a mixing region to provide a flow of a mixture gas; by introducing the flow of the mixture gas into an oxidizing region while a flow of a molecular oxygen-containing gas is introduced into the oxidizing region concurrently with the flow of the mixture gas; to provide a flow of a reaction mixture in which the magnesium vapor is oxidized, by introducing the flow of the reaction mixture containing the resultant magnesium oxide fine particles into a collecting region; and, by collecting the magnesium oxide particles from the reaction mixture by, for example, a filter located in the collecting region.

Abstract: A new reactor for the production of carbon black, a method for the production of carbon black, and a carbon black are disclosed. The carbon blacks are characterized by a surface area preferably in the range of 70 to 150 m.sup.2 /g and "G" values of either less than 1.20 or greater than 1.85, corresponding to very narrow or very broad aggregate size distributions, respectively. The reactor is preferably for axial flow of combustion gases and is characterized by serial arrangement of a cylindrical combustion zone, a frustoconical converging zone, a throat, an abrupt diverging zone and a cylindrical pyrolysis zone. In certain aspects of the invention, the combustion gases are formed by combusting low BTU fuel and forcing these gases through the throat at a velocity approaching Mach 1. In one method of carbon black production, the feedstock is introduced into the converging zone. In another method, it is introduced as a spray.

Abstract: A reactor apparatus (10) adapted for continuously producing molten, solar grade purity elemental silicon by thermal reaction of a suitable precursor gas, such as silane (SiH.sub.4), is disclosed. The reactor apparatus (10) includes an elongated reactor body (32) having graphite or carbon walls which are heated to a temperature exceeding the melting temperature of silicon. The precursor gas enters the reactor body (32) through an efficiently cooled inlet tube assembly (22) and a relatively thin carbon or graphite septum (44). The septum (44), being in contact on one side with the cooled inlet (22) and the heated interior of the reactor (32) on the other side, provides a sharp temperature gradient for the precursor gas entering the reactor (32) and renders the operation of the inlet tube assembly (22) substantially free of clogging. The precursor gas flows in the reactor (32) in a substantially smooth, substantially axial manner.

Abstract: In a heat exchange unit that recovers waste heat from carbon black smoke by preheating oxygen-containing gas such as air being passed to a carbon black producing reactor, a control loop is provided that automatically diverts the oxygen-containing gas being preheated through a by-pass line if the temperature of the effluent smoke being removed from the heat exchange is below a minimum temperature value in order to minimize the deposition of carbon on the heat exchange surfaces in said heat exchange zone.

Abstract: A reactor tube 20 for a high-temperature fluid wall reactor has a generally cylindrical shape and is made of a refractory material which permits the tube to be heated to incandescence. The reactor tube in turn radiates energy inwardly to a reaction zone to sustain the desired high-temperature reaction. At least a length of the tube 20 is perforated to permit an inert gas to pass through the tube to form a protective fluid wall for preventing the radially-inward reactant products from contacting the inner surface 84 of the tube. Perforations 78 are located, shaped and dimensioned such that inert gas jets 86 are formed each having a substantially radially-directed momentum sufficient to repel the reactants. The injection of inert gas is controlled so that gas jets overlap to form the protective fluid wall, but the gas jets do not disturb flow within the radially-inward reaction zone. Sections of the reactor tube may remain unperforated, but are protected by the downstream flow of the injected inert gas.

Abstract: A reactor apparatus (10) adapted for continuously producing molten, solar grade purity elemental silicon by thermal reaction of a suitable precursor gas, such as silane (SiH.sub.4), is disclosed. The reactor apparatus (10) includes an elongated reactor body (32) having graphite or carbon walls which are heated to a temperature exceeding the melting temperature of silicon. The precursor gas enters the reactor body (32) through an efficiently cooled inlet tube assembly (22) and a relatively thin carbon or graphite septum (44). The septum (44), being in contact on one side with the cooled inlet (22) and the heated interior of the reactor (32) on the other side, provides a sharp temperature gradient for the precursor gas entering the reactor (32) and renders the operation of the inlet tube assembly (22) substantially free of clogging. The precursor gas flows in the reactor (32) in a substantially smooth, substantially axial manner.

Abstract: A flue for cooling the flow of reaction product from the high temperature oxidation of a metal halide to the metal oxide in the presence of oxygen, said flue comprising a first section of a given cross-sectional area and a second section wherein the cross-sectional area is decreased thereby increasing the velocity and turbulence of the flow.

Abstract: A reactor tube 20 for a high-temperature fluid wall reactor has a generally cylindrical shape and is made of a refractory material which permits the tube to be heated to incandescence. The reactor tube in turn radiates energy inwardly to a reaction zone to sustain the desired high-temperature reaction. At least a length of the tube 20 is perforated to permit an inert gas to pass through the tube to form a protective fluid wall for preventing the radially-inward reactant products from contacting the inner surface 84 of the tube. Perforations 78 are located, shaped and dimensioned such that inert gas jets 86 are formed each having a substantially radially-directed momentum sufficient to repel the reactants. The injection of inert gas is controlled so that gas jets overlap to form the protective fluid wall, but the gas jets do not disturb flow within the radially-inward reaction zone. Sections of the reactor tube may remain unperforated, but are protected by the downstream flow of the injected inert gas.

Abstract: A method and apparatus is disclosed for producing large particles of material from gas, or gases, containing the material (e.g., silicon from silane) in a free-space reactor comprised of a tube (20) and controlled furnace (25). A hot gas is introduced in the center of the reactant gas through a nozzle (23) to heat a quantity of the reactant gas, or gases, to produce a controlled concentration of seed particles (24) which are entrained in the flow of reactant gas, or gases. The temperature profile (FIG. 4) of the furnace is controlled for such a slow, controlled rate of reaction that virtually all of the material released condenses on seed particles and new particles are not nucleated in the furnace. A separate reactor comprised of a tube (33) and furnace (30) may be used to form a seed aerosol which, after passing through a cooling section (34) is introduced in the main reactor tube (34) which includes a mixer (36) to mix the seed aerosol in a controlled concentration with the reactant gas or gases.

Abstract: An apparatus and method for producing carbon black wherein a refractory reactor lining is effectively cooled. A combustible gaseous mixture is injected into a chamber defined by the refractory lining, oil feedstock also being injected into the chamber. Coolant fluid is passed through a passageway in the refractory material.

Abstract: A sinterable powdery material of minute composite ceramic particles having a dual structure, comprising the core formed of zirconium oxide and the outer shell formed of aluminum oxide,a process for producing thereof, which comprisesintroducing gaseous zirconium chloride into a combustion chamber provided with a constricting section at the center part thereof and a burner at the upper part thereof,introducing gaseous aluminum chloride into the combustion chamber at the constricting section or the lower part thereof, andthermally decomposing both the thus introduced zirconium chloride and aluminum chloride by a flame from said burner under an oxidative atmosphere, andan apparatus for producing thereof.

Abstract: A carbon black reactor having tangential entry of combustion gases is provided with semicircular ramps to smoothly guide the flow of each tangentially introduced stream of combustion gases toward the reactor outlet enough to avoid turbulent impact with other tangentially introduced combustion gas streams.

Abstract: Process for producing low cost, high purity solar grade Si wherein a reduction reaction, preferably the reduction of SiF.sub.4, by an alkali metal (liquid Na preferred) is carried out essentialy continuously by injecting of reactants in substantially stoichiometric proportions into a reaction chamber having a controlled temperature thereby to form a mist or dispersion of reactants. The reactants being supplied at such a rate and temperature that the reaction takes place far enough away from the entry region to avoid plugging of reactants at the entry region, the reaction is completed and whereby essentially all reaction product solidifies and forms a free flowing powder before reaction product hits a reaction chamber wall. Thus, the reaction product does not adhere to the reaction chamber wall or pick up impurities therefrom. Separation of reaction products is easily carried out by either a leach or melt separation process.

Abstract: A process is provided for the production of antimony oxide from antimony sulfide which comprises the steps of comminuting the antimony sulfide to form a plurality of antimony sulfide containing particles, mixing the antimony sulfide containing particles with substantially pure oxygen, reacting the antimony sulfide with oxygen to form a gaseous stream of antimony oxide and sulfur dioxide, cooling the gaseous stream below the boiling point of antimony oxide, separating the condensed antimony oxide from the sulfur dioxide, further cooling the separated sulfur dioxide and utilizing the cooled sulfur dioxide to cool the gaseous stream of antimony oxide and sulfur dioxide. Apparatus for accomplishing this process is also provided.

Abstract: This invention relates to the production of carbon black by means of an incomplete air-acetylene combustion reaction.The apparatus comprises heating means arranged around an acetylene jet and arranged to cause heat cracking of the acetylene molecules prior to the combustion reaction.The invention is applicable in particular for forming linings for facing moulds or the like used in metallurgy or glass-making, for forming insulating facings on conveying elements and for lubricating drawing heads.

Abstract: The disclosed apparatus is of the type in which feed units feed air and hydrocarbon material into a reaction chamber, where they react to form carbon black. A filter then removes the carbon black. Disclosed is the provision of a mixing chamber between the feed units and the reaction chamber. The mixing chambers pass through a demountable hollow reactor cover through which there is circulated a heat transfer fluid for controlling the temperature of the mixing chamber walls. The mixing chamber can be common to a plurality of feed units or be separate for each feed unit.Also disclosed is a feed unit which has a vortex plate, an output nozzle, and a hydrocarbon spray nozzle, all mounted on a hydrocarbon supply tube which in turn is fixed to a demountable cover of the feed unit. This permits these components to be readily removed with the cover for replacement or service. The feed units can also have their temperature controlled by the heat transfer fluid for the mixing chambers.

Abstract: In a carbon black reactor having at least one combustion zone opening into a reaction zone, each combustion zone has opening thereinto, in a generally tangential direction, quench fluid inlet means operably connected to a source of quench fluid. The quench fluid is introduced into the combustion zone to control the temperature of the combustion gases to a desired temperature before the combustion gases are introduced into the reaction zone. Control means is provided for controlling the quench fluid input in response to the temperature of the combustion gases.

Abstract: There is disclosed an improved process and apparatus for the production of finely-divided metal and metalloid oxides by flame hydrolysis of corresponding metal and metalloid halides whereby fouling of burner apparatus is substantially completely avoided.