Means Within Reaction Chamber For Redistributing Reaction Stream As It Passes Between Adjacent Stages Patents (Class 422/648)
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Patent number: 9126168Abstract: A structure and method are provided for adding a catalyst bed platform to an existing reactor without welding to the structural portion of the reactor walls. The structure is constructed from components that can be passed through an existing opening in a reactor. The structure allows a catalyst bed in an existing reactor to be divided into catalyst beds with a reduced length to diameter ratio.Type: GrantFiled: December 14, 2011Date of Patent: September 8, 2015Assignee: ExxonMobil Research and Engineering CompanyInventors: Antonio O. Ramos, Benjamin S. Umansky, William J. Tracy, III, Ramesh X. Gandhi, Hans G. Korsten, Enrique Feliz
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Patent number: 9011790Abstract: A reactor for carrying out a three-phase reaction of a liquid phase, a gaseous phase, and a catalyst over a fixed catalyst bed is disclosed. The liquid and gaseous phases are passed through the reactor via a mixing and distribution device positioned over the fixed catalyst bed. The mixing and distribution device includes a trough distributor for the liquid phase, having trough-shaped channels, outlet tubes in the trough-shaped channels for the liquid phase, a distributor plate below the trough distributor, and vertical nozzles, having one or more openings for the gaseous phase and one or more openings, arranged below the openings for the gaseous phase. For entry of the liquid phase, the nozzles are installed so that, at a predetermined liquid feed rate, the surface of the liquid on the distributor plate is below the openings for the gaseous phase and above the openings for the liquid phase.Type: GrantFiled: June 20, 2008Date of Patent: April 21, 2015Assignee: BASF SEInventors: Stefan Iselborn, Andreas Daiss, Reiner Geier, Marcus Bechtel, Michael Wille, Benjamin Hepfer, John Sauter
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Patent number: 8865086Abstract: A quenching apparatus for a reactor is disclosed. The quenching apparatus includes a quenching unit (31) and a mixing unit (41). The quenching unit includes fluid distribution pipes (33) which branch off from a central portion of the quenching unit in radial directions and eject quenching fluid, and one or more first fluid outlets (35) which are formed through the bottom of the quenching unit. The mixing unit includes inclined baffles (43), one or more partitions (42) and a second fluid outlet (45). The inclined baffles are respectively disposed under the first fluid outlets. The partitions partition a space between inner and outer sidewalls of the mixing unit into a plurality of separated spaces in which the inclined baffles are respectively disposed. Fluid guided by the inclined baffles and the partitions is discharged out of the mixing unit through the second fluid outlet.Type: GrantFiled: December 29, 2009Date of Patent: October 21, 2014Assignee: SK Innovation Co., Ltd.Inventors: Tae Young Jang, Min Ki Ahn, Sun Hyuk Bae, Gyung Rok Kim, Yoon Mang Hwang, Kyoo Sung Park, Sun Choi, Myung Jun Kim
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Patent number: 8691156Abstract: A preferential oxidation reactor for removing carbon monoxide in a hydrogen mixture gas is disclosed. The preferential oxidation reactor may include a housing having a catalytic layer provided therein, a mixture gas supply portion inserted into the interior of the housing and penetrating the catalytic layer, a condensate receiving portion contained within the housing and in fluid communication with a gas outlet port of the mixture gas supply portion and condensate control tubes arranged in the catalytic layer of the housing and in fluid communication with the condensate receiving portion. The condensate control tubes may have a capillary structure. A fuel cell system including the preferential oxidation reactor is also disclosed.Type: GrantFiled: December 1, 2010Date of Patent: April 8, 2014Assignee: Samsung SDI Co., Ltd.Inventors: Jong-Rock Choi, In-Hyuk Son, Jin-Goo Ahn, Woo-Cheol Shin, In-Seob Song
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Patent number: 8691159Abstract: A modular catalyst bed support can be used to increase the number of catalyst beds available in a reactor. The modular catalyst bed support can include a lattice with a plurality of lattice openings and modules inserted into the lattice openings. The modular catalyst bed support can rest on top of an underlying catalyst bed, which can reduce or eliminate the need for attachment of the modular catalyst bed support to the walls of the reactor.Type: GrantFiled: March 15, 2012Date of Patent: April 8, 2014Assignee: Exxonmobil Research and Engineering CompanyInventors: Antonio O. Ramos, Benjamin S. Umansky, William J. Tracy, III, Ramesh X. Gandhi, Hans G. Korsten, John T. Wyatt, Jr., William J. Novak
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Patent number: 8673246Abstract: One exemplary embodiment can be a process for contacting one or more fluids in a vessel. The process may include passing one or more fluids into a chamber from an overhead tray and providing a conduit outside the chamber coupling a respective spillway to a respective hole for increasing contact time inside the conduit. Typically, the chamber forms one or more sidewalls forming at least one hole and the overhead tray forms at least one spillway.Type: GrantFiled: March 23, 2011Date of Patent: March 18, 2014Assignee: UOP LLCInventors: Pengfei Chen, Zhanping Xu
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Patent number: 8603399Abstract: An improved processing system of an oxygenate-containing feedstock for increased production or yield of light olefins. Such processing involves oxygenate conversion to olefins and subsequent cracking of heavier olefins wherein at least a portion of the products from each of the reactors is elevated in pressure, using a common compressor, prior to being routed to a common product fractionation and recovery section. The system further comprises acid gas removal means to remove acid gases from the cracked product gas and that the olefin cracking reactor is a moving bed reactor.Type: GrantFiled: October 1, 2009Date of Patent: December 10, 2013Assignee: UOP LLCInventors: Tom N. Kalnes, Robert B. James, Jr., Daniel H. Wei, Bryan K. Glover
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Patent number: 8568669Abstract: This invention relates to a device for cooling and distributing mixed charges on fixed catalyst beds for use in the cooling zone of descending flow reactors which comprises a flat tray fitted with collector and distributor tubes for liquid superimposed upon and connected to another flat tray of similar design to the upper tray. The device, which is of smaller size in comparison with other commercially available devices, is extremely simple to install industrially and compact, and has as its main characteristic the efficiency with which it promotes reduction of the temperature of the reaction medium when it receives the cooling fluid within the catalytic reactor.Type: GrantFiled: October 29, 2010Date of Patent: October 29, 2013Assignee: Petroleo Brasileiro S.A.—PetrobrasInventors: Wilson Kenzo Huziwara, Donizeti Aurelio Silva Belato, Jorge Roberto Duncan Lima, Rogério Michelan, William Victor Carlos Candido, Angelo Jose Gugelmin, Paulo Sérgio Freire, Nelson Patrício, Jr.
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Patent number: 8357342Abstract: A multiphase multifunctional reactor, system and method is described which has the capacity to effect extractive oxidation of sulfur and nitrogen compounds and unstable unsaturated compounds that are present in raw hydrocarbon streams, in such a way that the reaction conditions are adjusted and avoid losses of yield of the treated hydrocarbon in the stages of the extraction and/or absorption. The objective is achieved by means of the conception of a reactor which comprises a column divided into five sections which can be classified as two reaction sections (1, 2) two decantation sections (3, 4) and an inert gas section (5) under pressure.Type: GrantFiled: September 15, 2009Date of Patent: January 22, 2013Assignee: Petroleo Brasileiro S.A.-PetrobrasInventors: Wladmir Ferraz de Souza, Adriana Moret Borges, Jose Antonio Vidal Vieira
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Patent number: 8333940Abstract: A mass-exchange contact device is proposed, comprising upper and lower flat ring-shaped trays attached to a column, a sleeve having windows with bottom edges in the plane of the lower tray, a barbotage unit having orifices in its sidewalls placed on the top sleeve, a movable double-acting valve including upper and lower plates connected with a rod. The barbotage unit includes an ascending limiter of valve's movement, the sleeve's bottom includes a descending limiter. Alternatively, the barbotage unit is made as a portion of the sleeve. Embodiments comprise a number of rows of the proposed devices situated one above the other, and separated by multi-layer packing fittings. The devices can be used in catalytic distillation columns, wherein the fittings are filled with catalytic material. Alternatively, the fitting is substituted with a grating supporting a catalytic granular layer. The proposed design improves device operation, reliability, durability, reduces its weight and costs.Type: GrantFiled: May 10, 2010Date of Patent: December 18, 2012Inventors: Bogdan Maleta, Olesia Maleta
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Patent number: 8282891Abstract: The instant application provides apparatus and methods for the generation of gas, preferably chlorine dioxide. The methods and apparatus of the invention use a removable reaction chamber for the reaction of precursor chemicals, e.g., chlorite salt and an acid. The methods and compositions of the invention provide gas for a number of personal and commercial applications.Type: GrantFiled: July 1, 2010Date of Patent: October 9, 2012Assignee: TBS Technologies, LLCInventors: Thomas J. Dee, Paul Sabin, Douglas Sabin
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Patent number: 8206659Abstract: Methods and devices for controlled evaporation of solvent from a solution are provided. In one embodiment, the device can control evaporation of different solutions comprising solvents of dissimilar volatilities simultaneously. In another embodiment, control over the flow of solvent vapor out of the device is provided by selecting the pressure at an inlet port and an exhaust port of the device. In yet another embodiment, control over the flow of solvent vapor out of the device is provided by selecting the size of a disk flow control orifice positioned between the wells and a vapor removal outlet of the device. In still another embodiment, control over the flow of solvent vapor out of the device is provided by the opening and closing of the vapor removal outlet of the device. In yet a further embodiment, the rate of evaporation of solvent is controlled by controlling the temperature of the solution.Type: GrantFiled: June 12, 2009Date of Patent: June 26, 2012Assignee: Vertex Pharmaceuticals IncorporatedInventors: Jack Barger, James Sinclair, Michael P. Emery
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Patent number: 8182750Abstract: A carbon monoxide treatment apparatus according to an exemplary embodiment of the present invention includes: a reactor body; a partitioning plate located inside the reactor body for partitioning an internal space of the reactor body into a first section and a second section; a channel member in the first section for transporting an introduced gas including a reformed gas and an oxidant gas to the second section; and a reaction unit around the channel member of the first section for reducing a concentration level of carbon monoxide in the introduced gas moving through the first section by utilizing a preferential oxidation reaction of the carbon monoxide and the oxidant gas of the introduced gas, wherein moisture of the introduced gas that has been partially condensed when passing through the channel member is stored in the second section.Type: GrantFiled: February 20, 2008Date of Patent: May 22, 2012Assignee: Samsung SDI Co., Ltd.Inventors: Man-Seok Han, Seong-Jin An, Ju-Yong Kim, Sung-Chul Lee, Yong-Kul Lee, Chan-Ho Lee, Jun-Sik Kim, Jin-Goo Ahn
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Patent number: 8158074Abstract: Described here is a system (8; 9; 50) of walls for catalytic beds of reactors (1) for the heterogeneous synthesis of chemical compounds characterized in that it comprises a wall (14) of predetermined thickness in direct contact with a catalytic bed (7) for containing it, said wall having a plurality of portions (17) permeable to gases and a plurality of portions (19; 54; 55) impermeable to gases, said portions (17) permeable to gases each being equipped with a plurality of slits (18; 52, 53; 60; 70) of a size such as to allow the free passage of the synthesis gases through them but not the passage of the catalyst.Type: GrantFiled: January 16, 2007Date of Patent: April 17, 2012Assignee: Ammonia Casale S.A.Inventors: Ermanno Filippi, Enrico Rizzi, Mirco Tarozzo
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Patent number: 8147765Abstract: A novel process and apparatus is disclosed for sustainable, continuous production of hydrogen and carbon by catalytic dissociation or decomposition of hydrocarbons at elevated temperatures using in-situ generated carbon particles. Carbon particles are produced by decomposition of carbonaceous materials in response to an energy input. The energy input can be provided by at least one of a non-oxidative and oxidative means. The non-oxidative means of the energy input includes a high temperature source, or different types of plasma, such as, thermal, non-thermal, microwave, corona discharge, glow discharge, dielectric barrier discharge, or radiation sources, such as, electron beam, gamma, ultraviolet (UV). The oxidative means of the energy input includes oxygen, air, ozone, nitrous oxide (NO2) and other oxidizing agents.Type: GrantFiled: October 23, 2008Date of Patent: April 3, 2012Assignee: University of Central Florida Research Foundation, Inc.Inventors: Nazim Z. Muradov, Franklyn Smith, Ali Tabatabaie-Raissi
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Patent number: 8124035Abstract: Continuous processes for monoalkylating aromatic compound with an aliphatic feedstock comprising aliphatic olefin of 8 to 18 carbon atoms per molecule are effected using at least 3 reaction zones in series, each containing solid alkylation catalyst with effluent cooling between reaction zones, each of which reaction zones is supplied a portion of the fresh aliphatic feedstock, such that the Reaction Zone Delta T in each reaction zone is less than about 15° C. The overall aromatic compound to olefin molar ratio is less than about 20:1. The alkylation product has desirable linearity and low amounts of dimers, dealkylated compounds and diaryl compounds even though a low aromatic compound to olefin molar ratio is used.Type: GrantFiled: February 5, 2010Date of Patent: February 28, 2012Assignee: UOP LLCInventor: Mark G. Riley
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Patent number: 8017095Abstract: The present invention provides a novel means to provide more effective mixing of gas and fluids in a height constrained interbed space of a catalytic reactor without increasing pressure drop. In particular, the device improves the effectiveness of an existing mixing volume in mixing the gas phase and liquid phase of two-phase systems. According to the present invention, the mixing device helps create a highly arcuate flow to incoming effluents and a high degree of mixing within a constrained interbed space of a catalytic reactor.Type: GrantFiled: May 29, 2009Date of Patent: September 13, 2011Assignee: Chevron U.S.A. Inc.Inventors: Abdenour Kemoun, Steven X. Song
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Patent number: 7922981Abstract: Apparatus for intensifying heterogeneous chemical reactions is described. For the case of liquid-liquid reactions, with drops of a reactant distributed throughout the second continuous reactant, the physical phenomena of drop dispersion (break up) and drop coalescence are identified as the main physical steps affecting reaction rates. A basic flow cell structure is described in which the respective actions of dispersion and coalescence can be greatly intensified through the creation of enhanced body forces and shear flow zones. The basic cell structure can be arranged into pipe flow reactors to suit any production or process requirements. The basic cell structure is equally applicable to gas-liquid reactions with drops of one reactant being conveyed by a moving gas stream.Type: GrantFiled: April 3, 2009Date of Patent: April 12, 2011Assignee: Anilitics Process Chemistry & Engineering, Inc.Inventor: Edward G. Hauptmann