Abstract: A method of separating a mixture of carbon dioxide and a hydrocarbon gas using a metal-organic framework (MOF) material having a three-dimensional carborane ligand structure.
Type:
Grant
Filed:
December 29, 2008
Date of Patent:
June 29, 2010
Assignee:
Northwestern University
Inventors:
Omar K. Farha, Joseph T. Hupp, Youn-Sang Bae, Randall Q. Snurr, Alexander M. Spokoyny, Chad A. Mirkin
Abstract: A method and apparatus for refining silicon which can remove impurity elements such as phosphorus and antimony as well as impurity elements such as boron and carbon using an electron beam in the same vacuum chamber are provided. Silicon is irradiated and melted with an electron beam in a low vacuum inside a vacuum vessel, a compound-forming substance such as H2O which reacts with boron or the like in the molten silicon and forms a vaporizable oxide is introduced into the vacuum chamber, and impurity elements such as boron having a low vapor pressure in a vacuum are evaporated from the molten silicon as part of the vaporizable compound. Silicon in the vacuum vessel is then irradiated with an electron beam in a high vacuum in the vacuum vessel, and impurity elements contained in the silicon having a high vapor pressure in a vacuum such as phosphorus are removed.
Type:
Grant
Filed:
July 10, 2006
Date of Patent:
April 27, 2010
Inventors:
Norichika Yamauchi, Takehiko Shimada, Minoru Mori
Abstract: An analytical element (typically DNA chip) composed of a solid carrier and a group of nucleotide derivatives or their analogues fixed to the solid carrier via covalent bonding is favorably produced by a method of bringing in a liquid phase a group of nucleotide derivatives or their analogues having a reactive group at one end thereof or its vicinity into contact with a solid carrier having thereon a reactive group in the presence of a transition metal-containing catalyst.
Type:
Grant
Filed:
December 27, 2000
Date of Patent:
April 9, 2002
Assignee:
Fuji Photo Film Co., Ltd.
Inventors:
Tadahisa Sato, Koki Nakamura, Hiroshi Shinoki
Abstract: A method for stabilizing urease in an assay reagent for determination of urea nitrogen in a sample and a method for accurately determining urea nitrogen in a sample are disclosed. After urea nitrogen in the sample is reacted with urease in the presence of an organic boron compound, the amount of ammonia formed by the reaction is determined.
Abstract: Stable, solid acetyl peroxyborate compounds which are active oxygen-containing compounds derived from acetic acid and boron-oxygen compounds. The compounds of the invention have a peracetic acid content which can be liberated instantly and directly in water with only minor formation of hydrogen peroxide The acetyl peroxyborates of the invention are useful in washing, bleaching and cleaning agent and disinfectant applications and as oxidizing agents in organic synthesis.
Type:
Grant
Filed:
December 2, 1991
Date of Patent:
October 31, 1995
Assignee:
Peroxid-Chemie GmbH
Inventors:
Richard Roesler, Siegfried Schelle, Michael Gnann, Werner Zeiss
Abstract: Process for the manufacture of granular monohydrated sodium perborate, endowed with abrasion resistance, starting from the corresponding tetrahydrated perborate, characterized in that a carboxylic acid, containing from 1 to 3 C atoms, or an alkali metal salt thereof, is added to the tetrahydrated perborate, already present in the granular state, whereafter a dehydration of the tetrahydrated perborate is carried out.
Abstract: High-purity sodium tetraborate pentahydrate (Na.sub.2 B.sub.4 O.sub.7.5H.sub.2 O) is produced by:(a) reacting the mineral colemanite (2CaO.3B.sub.2 O.sub.3.5H.sub.2 O) with sodium carbonate (Na.sub.2 CO.sub.3) in an aqueous environment to produce an aqueous solution of sodium tetraborate and sodium hydroxide, with precipitation of solid calcium carbonate;(b) treating the aqueous solution obtained in stage (a), after separating the precipitated calcium carbonate, with boric acid (H.sub.3 BO.sub.3) to neutralize the sodium hydroxide and form a further quantity of sodium tetraborate;(c) separating sodium tetraborate pentahydrate by crystallization from the aqueous solution obtained in stage b.