Ternary Compound Containing Metal Or Ammonium Patents (Class 423/279)
  • Patent number: 12152477
    Abstract: Methods of enhancing productivity of a subterranean wellbore may include introducing a carbonated mixture comprising water and carbonate anions to a target zone of the subterranean wellbore; introducing basaltic particles to the target zone of the subterranean wellbore; contacting the basaltic particles with the carbonated mixture; dissolving at least a part of the basaltic particles with the carbonated mixture to release divalent cations including calcium cations, magnesium cations and ferrous cations; reacting, in the target zone of the subterranean wellbore, the divalent cations with the carbonate anions in the carbonated mixture to produce carbonate minerals; providing stimulus to the basaltic particles and the carbonated mixture to promote the dissolving and the reacting; depositing at least a part of the carbonate minerals to fractures of the target zone; and monitoring the reacting of the divalent cations with the carbonated anions and depositing.
    Type: Grant
    Filed: January 10, 2022
    Date of Patent: November 26, 2024
    Assignee: SAUDI ARABIAN OIL COMPANY
    Inventors: Abdulaziz S. Al-Qasim, Ali A. Al-Yousef
  • Patent number: 11880195
    Abstract: The embodiments are and include at least an apparatus, system and method for forming print material particles for additive manufacturing (AM) printing. The apparatus, system and method include at least a melt chamber comprising a polymer melt; a vertical extruder that fluidically receives the polymer melt; an atomizer that atomizes the polymer melt from the vertical extruder and that distributes the atomized polymer melt; a fall chamber comprising a plurality of zones into which the atomized polymer melt is distributed; and a collector to receive the print material particles formed of the atomized polymer melt after falling through the plurality of zones.
    Type: Grant
    Filed: May 11, 2020
    Date of Patent: January 23, 2024
    Assignee: JABIL INC.
    Inventors: Nicholas J. Dippel, Thomas Gardner, Daryn York
  • Patent number: 11795059
    Abstract: Provided are an atomic layer sheet that contains boron and oxygen as framework elements, is networked by nonequilibrium couplings having boron-boron bonds, and has a molar ratio of oxygen to boron (oxygen/boron) of less than 1.5, a laminated sheet containing a plurality of such atomic layer sheets and metal ions between ones of the sheets, and a thermotropic liquid crystal and a lyotropic liquid crystal containing these. In addition, there is provided a method for manufacturing an atomic layer sheet and/or a laminated sheet containing boron and oxygen, the method including: adding MBH4, where M represents an alkali metal ion, into a solvent containing an organic solvent in an inert gas atmosphere to prepare a solution; and exposing the solution to an atmosphere containing oxygen.
    Type: Grant
    Filed: January 31, 2019
    Date of Patent: October 24, 2023
    Assignee: Tokyo Institute of Technology
    Inventors: Tetsuya Kambe, Shotaro Imaoka, Aiko Watanabe, Kimihisa Yamamoto
  • Patent number: 11230491
    Abstract: A method of forming a dissolvable part of amorphous borate includes: preparing a mixture comprising one or more boron compounds and one or more alkali compounds, at least one of the one or more boron compounds and the one or more alkali compounds being hydrous; heating the mixture to a melting temperature for a predetermined time to melt the mixture and release water from the mixture to form an anhydrous boron compound that is moldable, wherein the amount of alkali compound being selected to achieve an alkali oxide content of between about 10 to 25%; with the anhydrous boron compound at a molding temperature, molding the anhydrous boron compound in a mold; and cooling the anhydrous boron compound to form a solid.
    Type: Grant
    Filed: August 7, 2019
    Date of Patent: January 25, 2022
    Assignee: 1824930 Alberta Ltd.
    Inventors: Wesley James Wall, Adam Wall, Ray Whitaker
  • Patent number: 11162025
    Abstract: A boron nitride fluorescent material, having at least one light emission peak wavelength in a range of 480 nm or more and less than 650 nm as excited with light having a light emission peak wavelength in a range of 250 nm or more and 460 nm or less, and comprising: at least one element A selected from the group consisting of alkaline earth metal elements; nitrogen and boron; and optionally at least one element M1 selected from the group consisting of Tb, Sm, Pr, Ce, Mn, and Yb.
    Type: Grant
    Filed: April 9, 2019
    Date of Patent: November 2, 2021
    Assignee: NICHIA CORPORATION
    Inventor: Yoshinori Murazaki
  • Patent number: 9713805
    Abstract: A catalyst for exhaust gas purification includes a carrier and a platinum group element supported on the carrier. The carrier includes a modified aluminum borate which contains an aluminum borate and at least one of oxides of an element selected from the group consisting of Zr, Si, Fe, and Ti. The modified aluminum borate contains the oxide in a concentration of 0.06% to 18% by mass relative to the mass of the modified aluminum borate.
    Type: Grant
    Filed: November 10, 2014
    Date of Patent: July 25, 2017
    Assignee: MITSUI MINING & SMELTING CO., LTD.
    Inventors: Yuki Nagao, Hironori Iwakura, Michiyo Inoue, Yunosuke Nakahara, Masato Machida
  • Patent number: 9687817
    Abstract: Provided is a carrier for an exhaust gas purification catalyst containing aluminum borate particles having a peak (pore peak) exhibiting the highest intensity in a void volume diameter range of from 20 nm to 100 nm in a logarithmic differential void volume distribution measured using a mercury intrusion porosimeter, in order to provide a new catalyst support capable of effectively suppressing a decrease in catalytic performance caused by sulfur (S) component contained in the exhaust gas, in the case of supporting Pd as a catalytically active component.
    Type: Grant
    Filed: October 17, 2014
    Date of Patent: June 27, 2017
    Assignee: Mitsui Mining & Smelting Co., Ltd.
    Inventors: Akira Abe, Takahiro Sato, Ohki Houshito, Yuki Nagao, Yunosuke Nakahara
  • Patent number: 8685355
    Abstract: A method of forming methanol, formaldehyde, formic acid and ammonium pentaborate tetrahydrate includes the steps of providing ammonium hydroxide and producing air bubbles within the ammonium hydroxide to form a solution. Sodium borohydride is added and dissolved within the solution of air bubbled ammonium hydroxide to form methanol, formaldehyde, formic acid and ammonium pentaborate tetrahydrate. An alternative method of forming methanol, formaldehyde, formic acid and ammonium pentaborate tetrahydrate is also provided which includes the steps of providing ammonium hydroxide and dissolving sodium borohydride therein to form a solution. Sodium bicarbonate is added to the solution of ammonium hydroxide and sodium borohydride to form methanol, formaldehyde, formic acid and ammonium pentaborate tetrahydrate.
    Type: Grant
    Filed: March 27, 2012
    Date of Patent: April 1, 2014
    Assignee: Biologistics LLC
    Inventor: Michael A. Madson
  • Publication number: 20140042477
    Abstract: A luminophore composition comprising amorphous aluminoborate powders is disclosed. The composition is obtainable by preparing an aluminoborate resin by a wet chemical route based on precursors solutions substantially free from monovalent and divalent cations; drying the resin to obtain a solid; grinding the solid to obtain a powder; pyrolyzing the powder at a pyrolysis temperature lower than the crystallization temperature of the composition; and calcinating the powder so pyrolyzed at a calcination temperature lower than the crystallization temperature of the composition. Furthermore, a process for the preparation of said composition is disclosed. The composition is particularly suitable for use in solid-state lighting, and for example for converting UV light into warm white visible light.
    Type: Application
    Filed: December 23, 2011
    Publication date: February 13, 2014
    Applicant: CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE -CNRS
    Inventors: Alain Ibanez, Vinicius Ferraz Guimaraes, Lauro June Queiroz Maia, Antonio Carlos Hernandes
  • Patent number: 8557449
    Abstract: An air cathode for a metal-air battery is disclosed which contains a catalyst chosen to make the metal air battery more easily rechargeable. This catalyst is based on cobalt phosphate, cobalt borate mixed metal cobalt phosphates, mixed metal cobalt borates, or mixed metal cobalt phosphate borates.
    Type: Grant
    Filed: June 24, 2011
    Date of Patent: October 15, 2013
    Inventors: Wilson Hago, Ivan Marc Lorkovic
  • Patent number: 8501138
    Abstract: A production method of high purity silver tetrafluoroborate, capable of producing silver tetrafluoroborate (AgBF4) at purity higher than the conventional, without using an organic solvent. The production method of the present invention is characterized in that the method comprises the step of: reacting silver fluoride with boron trifluoride in the presence of anhydrous hydrofluoric acid. Boron trifluoride is delivered into a solution obtained by dissolving or suspending silver fluoride in an anhydrous hydrofluoric acid solution.
    Type: Grant
    Filed: June 9, 2006
    Date of Patent: August 6, 2013
    Assignee: Stella Chemifa Coporation
    Inventors: Hirohisa Kikuyama, Masayuki Miyashita, Masahide Waki, Tomohiko Satonaga, Kazuhiko Shogami
  • Publication number: 20130156866
    Abstract: Hyperhalogens, a new class of highly electronegative species, are now invented. A hyperhalogen is a superhalogen-containing composition in which the electron affinity (EA) of the hyperhalogen is even larger than that of the superhalogens they are composed of. Novel production methods are provided in which highly electronegative species are produced by surrounding a central metal atom by superhalogen moieties.
    Type: Application
    Filed: September 8, 2011
    Publication date: June 20, 2013
    Applicant: Virginia Commonwealth University
    Inventor: Puru Jena
  • Patent number: 8357344
    Abstract: The gaseous effluent to be treated is contacted in column C1 with an absorbent solution selected for its property of forming two separable phases when it is heated. The regenerated absorbent solution is separated into two phases in drum B1; a fraction rich in water and a fraction rich in reactive compounds. Separation allows to optimize the operations performed on the regenerated absorbent solution. On the one hand, separation allows to carry out vaporization, through reboiler R1, of a fraction of the absorbent solution, preferably containing a limited reactive compound concentration in relation to the absorbent solution, thus limiting their degradation. On the other hand, separation of the phases allows to reduce the amount of solution to be treated in order to remove the non-regeneratable salts and thus to reduce the costs linked with their elimination. Finally, separation allows to eliminate the degradation products by carrying out a specific and suitable purification for each phase.
    Type: Grant
    Filed: March 10, 2010
    Date of Patent: January 22, 2013
    Assignee: IFP
    Inventors: Pierre-Antoine Bouillon, Marc Jacquin
  • Publication number: 20120328715
    Abstract: A method of preventing or treating osteochondrosis comprising administering a therapeutically effective amount of a boron containing compound to a mammal in need of such treatment.
    Type: Application
    Filed: August 16, 2012
    Publication date: December 27, 2012
    Inventor: Edgar W. Johnson
  • Patent number: 8268280
    Abstract: The present invention relates to a method for production of calcium compounds having very low content of phosphorus and boron from an impure calcium chloride, solution containing phosphorus and boron, which method comprises the following steps: a) addition of a FeCl3-solution to the calcium chloride solution, b) adjusting the pH of the solution by addition of a base to between 3 and 9.5 for precipitation of iron hydroxide, iron phosphate and boron compounds, c) removal of the solid precipitate from the solution in step b) obtaining a purified calcium chloride solution, d) precipitation of a calcium compound from the solution from step c), and e) separation of the calcium compound from the solution in step d).
    Type: Grant
    Filed: January 7, 2009
    Date of Patent: September 18, 2012
    Assignee: Elkem Solar AS
    Inventors: Torfinn Buseth, Einar Andersen
  • Publication number: 20120160478
    Abstract: A well tool can include a flow path, and a flow blocking device which selectively prevents flow through the flow path. The device can include an anhydrous boron compound. A method of constructing a downhole well tool can include forming a structure of a solid mass comprising an anhydrous boron compound, and incorporating the structure into the well tool.
    Type: Application
    Filed: February 27, 2012
    Publication date: June 28, 2012
    Applicant: HALLIBURTON ENERGY SERVICES, INC.
    Inventors: Bradley L. TODD, Thomas D. WELTON, Luke W. HOLDERMAN, Ivan SULEIMAN
  • Patent number: 8197780
    Abstract: A method of producing a boron suboxide composite material having improved fracture toughness.
    Type: Grant
    Filed: May 4, 2011
    Date of Patent: June 12, 2012
    Assignee: Element Six (Production) (Pty) Ltd.
    Inventors: Geoffrey John Davies, Iakovos Sigalas, Mathias Herrmann, Thembinkosi Shabalala
  • Publication number: 20110315936
    Abstract: A sputtering target including an oxide sintered body, the oxide sintered body containing indium (In) and at least one element selected from gadolinium (Gd), dysprosium (Dy), holmium (Ho), erbium (Er) and ytterbium (Yb), and the oxide sintered body substantially being of a bixbyite structure.
    Type: Application
    Filed: February 28, 2008
    Publication date: December 29, 2011
    Applicant: IDEMITSU KOSAN CO., LTD.
    Inventors: Kazuyoshi Inoue, Koki Yano, Masashi Kasami
  • Publication number: 20110318656
    Abstract: An air cathode for a metal-air battery is disclosed which contains a catalyst chosen to make the metal air battery more easily rechargeable. This catalyst is based on cobalt phosphate, cobalt borate mixed metal cobalt phosphates, mixed metal cobalt borates, or mixed metal cobalt phosphate borates.
    Type: Application
    Filed: June 24, 2011
    Publication date: December 29, 2011
    Inventors: Wilson Hago, Ivan Marc Lorkovic
  • Patent number: 7993546
    Abstract: An apparatus for forming nano-structures of carbon solids includes a reactor chamber into which extends a plasma torch configured to generate a plasma plume that extends into the interior of the reactor chamber. CO2 from is applied to the plasma plume where the CO2 is dissociated into carbon and oxygen. A plurality of nozzles also extends into the reactor chamber, which sprays liquid water on the plume, cooling at least a portion of the carbon causing it to form solid carbon nano-structures in a mixture of liquid water. The mixture is conveyed to a flocculation tank.
    Type: Grant
    Filed: September 23, 2008
    Date of Patent: August 9, 2011
    Assignee: Plasma Waste Recycling, Inc.
    Inventors: Rodrigo B. Vera, Alexander P. Rutberg
  • Patent number: 7955579
    Abstract: A boron suboxide composite material having improved fracture toughness consists of particulate or granular boron suboxide distributed in a binder phrase, such as AlxByOz, for example.
    Type: Grant
    Filed: September 6, 2006
    Date of Patent: June 7, 2011
    Assignee: Element Six (Production) (Pty) Ltd.
    Inventors: Geoffrey John Davies, Iakovos Sigalas, Mathias Herrmann, Thembinkosi Shabalala
  • Publication number: 20110027158
    Abstract: This invention relates to production of micronized calcined tincal having a high content as a result of a succession of procedures consisting of: hardening of earth minerals due to lose of water during subjecting coarse tincal ore (Na2B4O7-10H2O) to heat treatment in rotary furnace with flights; forming of swollen soft, expanded structure of tincal ore caused by calcination and consequently being calcined followed by purification from impurities in a high rate in a way subjecting calcined tincal to pneumatic separation procedure by means of hot air used for calcination process after autogenic grinding effect of dried and hardened clays on swollen ore and obtaining micronized calcined tincal with high efficiency. The invention also relates to the production of compacted calcined tincal product with increased density in the second step as result of compacting micronized calcined tincal with low density under pressure.
    Type: Application
    Filed: October 17, 2007
    Publication date: February 3, 2011
    Applicant: ETI MADEN ISLETMELERI GENEL MUDURLUGU
    Inventors: Orhan Yilmaz, Yucel Yalcinoglu, Tanzer Ergul, Tumay Uludag, Bilal Senturk, Hasan Akcin, Ibrahim Kayandan, Celal Demirbag
  • Patent number: 7820124
    Abstract: A material comprising a plurality of nanoparticles. Each of the plurality of nanoparticles includes at least one of a metal phosphate, a metal silicate, a metal oxide, a metal borate, a metal aluminate, and combinations thereof. The plurality of nanoparticles is substantially monodisperse. Also disclosed is a method of making a plurality of substantially monodisperse nanoparticles. The method includes providing a slurry of at least one metal precursor, maintaining the pH of the slurry at a predetermined value, mechanically milling the slurry, drying the slurry to form a powder; and calcining the powder at a predetermined temperature to form the plurality of nanoparticles.
    Type: Grant
    Filed: October 5, 2006
    Date of Patent: October 26, 2010
    Assignee: General Electric Company
    Inventors: Kalaga Murali Krishna, Sergio Paulo Martins Loureiro, Mohan Manoharan, Geetha Karavoor, Shweta Saraswat
  • Publication number: 20100267591
    Abstract: The present invention relates to bridging agents for use in subterranean formations, to well drill-in and servicing fluids comprising such bridging agents, and to methods of using such bridging agents and well drill-in and servicing fluids in subterranean drilling operations. An example of a well drill-in and servicing fluid of the present invention comprises a viscosified fluid, a fluid loss control additive, and a bridging agent comprising a degradable material.
    Type: Application
    Filed: May 25, 2010
    Publication date: October 21, 2010
    Applicant: Halliburton Energy Services, Inc.
    Inventors: Bradley L. Todd, Trinidad Munoz, JR.
  • Publication number: 20100254875
    Abstract: A material comprising a plurality of nanoparticles. Each of the plurality of nanoparticles includes at least one of a metal phosphate, a metal silicate, a metal oxide, a metal borate, a metal aluminate, and combinations thereof. The plurality of nanoparticles is substantially monodisperse. Also disclosed is a method of making a plurality of substantially monodisperse nanoparticles. The method includes providing a slurry of at least one metal precursor, maintaining the pH of the slurry at a predetermined value, mechanically milling the slurry, drying the slurry to form a powder; and calcining the powder at a predetermined temperature to form the plurality of nanoparticles.
    Type: Application
    Filed: October 5, 2006
    Publication date: October 7, 2010
    Inventors: Kalaga Murali Krishna, Sergio Paulo Martins Loureiro, Mohan Manoharan, Geetha Karavoor, Shweta Saraswat
  • Patent number: 7704478
    Abstract: A method and apparatus for refining silicon which can remove impurity elements such as phosphorus and antimony as well as impurity elements such as boron and carbon using an electron beam in the same vacuum chamber are provided. Silicon is irradiated and melted with an electron beam in a low vacuum inside a vacuum vessel, a compound-forming substance such as H2O which reacts with boron or the like in the molten silicon and forms a vaporizable oxide is introduced into the vacuum chamber, and impurity elements such as boron having a low vapor pressure in a vacuum are evaporated from the molten silicon as part of the vaporizable compound. Silicon in the vacuum vessel is then irradiated with an electron beam in a high vacuum in the vacuum vessel, and impurity elements contained in the silicon having a high vapor pressure in a vacuum such as phosphorus are removed.
    Type: Grant
    Filed: July 10, 2006
    Date of Patent: April 27, 2010
    Inventors: Norichika Yamauchi, Takehiko Shimada, Minoru Mori
  • Publication number: 20090272948
    Abstract: Disclosed is a method of growing a single crystal from a melt contained in a crucible. The method includes the step of making the temperature of a melt increase gradually to a maximum point and then decrease gradually along the axis parallel to the lengthwise direction of the single crystal from the interface of the single crystal and the melt to the bottom of the crucible. The increasing temperature of the melt is kept to preferably have a greater temperature gradient than the decreasing temperature thereof. Preferably, the axis is set to pass through the center of the single crystal. Preferably, the convection of the inner region of the melt is made smaller than that of the outer region thereof.
    Type: Application
    Filed: July 2, 2008
    Publication date: November 5, 2009
    Applicant: Siltron Inc.
    Inventor: Hyon-Jong CHO
  • Patent number: 7578455
    Abstract: A particulate material is ground more efficiently using a mixture of at least two different sizes of yttrium-stabilized zirconia balls. The method facilitates preparation of photocatalysts with high activity.
    Type: Grant
    Filed: August 9, 2004
    Date of Patent: August 25, 2009
    Assignee: General Motors Corporation
    Inventors: Jin D. Kim, Wei Li, Se H. Oh
  • Patent number: 7534377
    Abstract: Novel nonlinear optical materials are described having the general formula MxM?yScz(BO3)4 where M and M?are metals, typically rare earth metals, and the sum of x, y, and z is about four. One example of such a material is La0.7Y0.3Sc3(BO3)4. Exemplary crystalline materials according to the general formula exhibit useful optical characteristics and desirable physical properties for nonlinear optical applications. Novel compositions and devices using the nonlinear optical materials also are described.
    Type: Grant
    Filed: July 14, 2003
    Date of Patent: May 19, 2009
    Assignee: State of Oregon acting by and through the State Board of Higher Education on behalf of Oregon State University
    Inventors: Douglas A. Keszler, Jennifer L. Stone-Sundberg, Ning Ye, Michael A. Hruschka
  • Publication number: 20090082229
    Abstract: Processes for the rapid and efficient drying of boron-containing compounds, in particular boron-containing minerals and ores, are described, as well as the products which result from such processes. The process comprises the steps of providing a boron-containing material; introducing the boron-containing material into a pre-heated furnace; heating the boron-containing material in the furnace at a temperature between about 800° F. and 1000° F.; retaining the boron-containing material within the furnace for a time ranging from about 5 minutes to about 120 minutes; and removing the boron-containing material from the furnace and allowing it to cool to ambient temperature. Optionally, the process may also comprise one or more steps of grinding and/or sizing the boron-containing material to a specific particle size prior to the introduction of the material to a furnace.
    Type: Application
    Filed: September 24, 2008
    Publication date: March 26, 2009
    Applicant: Texas United Chemical Company, LLC
    Inventors: James W. Dobson, JR., Shauna L. Hayden, Asheley D. Bowles
  • Publication number: 20090068531
    Abstract: The present invention provides a solid electrolyte with high ion-conductivity which is cheap and exhibits high conductivity in an alkaline form, and stably keeps high conductivity because of a small amount of the leak of a compound bearing conductivity even in a wet state. The invention is useful in an electrochemical system using the solid electrolyte, such as a fuel cell. The solid electrolyte with high ion-conductivity comprises a hybrid compound which contains at least polyvinyl alcohol and a zirconic acid compound, and also a nitrogen-containing organic compound having a structure of amine, quaternary ammonium compound and/or imine, obtained by hydrolyzing a zirconium salt or an oxyzirconium salt in a solution including water, polyvinyl alcohol, a zirconium salt or an oxyzirconium salt and a nitrogen-containing organic compound having a structure of amine, quaternary ammonium compound and/or imine coexist, removing a solvent and contacting with alkali.
    Type: Application
    Filed: July 1, 2008
    Publication date: March 12, 2009
    Inventors: Haruo SAWA, Haruyuki Nakanishi, Shinichi Matsumoto
  • Patent number: 7473381
    Abstract: A method of producing hydrogen comprises reacting a hydrogenated compound and water. The hydrogenated compound is in contact with, or may be mixed with an oily substance.
    Type: Grant
    Filed: December 28, 2005
    Date of Patent: January 6, 2009
    Assignee: Commissariat A l'Energie Atomique
    Inventors: Jean Yves Laurent, Frédéric Gaillard, Nathalie Giacometti, Bruno Valon
  • Publication number: 20080317654
    Abstract: A boron suboxide composite material having improved fracture toughness consists of particulate or granular boron suboxide distributed in a binder phrase, such as AlxByOz, for example.
    Type: Application
    Filed: September 6, 2006
    Publication date: December 25, 2008
    Inventors: Geoffrey John Davies, Iakovos Sigalas, Mathias Herrmann, Thembinkosi Shabalala
  • Publication number: 20080233030
    Abstract: Process for manufacturing an electrochemical device including a cathode, an anode and at least one electrolyte membrane disposed between the anode and the cathode, wherein at least one of the cathode, the anode and the electrolyte membrane, contains at least a ceramic material.
    Type: Application
    Filed: March 30, 2004
    Publication date: September 25, 2008
    Applicant: PIRELLI & C.S.P.A.
    Inventors: Agustin Sin Xicola, A. Yuri Dubitsky, Enrico Albizzati, Evgeny Kopnin, Elena Roda
  • Patent number: 7374616
    Abstract: Acentric, tetragonal lithium borate crystals are disclosed along with a hydrothermal method for forming such crystals. The crystals possess unique optical, non-linear optical, and other photonic properties and may be formed of sufficient size to be useful in a wide variety of photonic devices. In addition, the disclosed crystals are very hard and can be used in specialty grinding applications such as for grinding optical components for deep UV applications.
    Type: Grant
    Filed: July 9, 2004
    Date of Patent: May 20, 2008
    Assignee: Clemson University
    Inventor: Joseph W Kolis
  • Patent number: 7354561
    Abstract: A chemical reactor and method for converting a first material into a second material is disclosed and wherein the chemical reactor is provided with a feed stream of a first material which is to be converted into a second material; and wherein the first material is combusted in the chemical reactor to produce a combustion flame, and a resulting gas; and an electrical arc is provided which is passed through or superimposed upon the combustion flame and the resulting gas to facilitate the production of the second material.
    Type: Grant
    Filed: November 17, 2004
    Date of Patent: April 8, 2008
    Assignee: Battelle Energy Alliance, LLC
    Inventor: Peter C. Kong
  • Patent number: 7306780
    Abstract: A compact solid source of hydrogen gas, where the gas is generated by contacting water with micro-disperse particles of sodium borohydride in the presence of a catalyst, such as cobalt or ruthenium. The micro-disperse particles can have a substantially uniform diameter of 1-10 microns, and preferably about 3-5 microns. Ruthenium or cobalt catalytic nanoparticles can be incorporated in the micro-disperse particles of sodium borohydride, which allows a rapid and complete reaction to occur without the problems associated with caking and scaling of the surface by the reactant product sodium metaborate. A closed loop water management system can be used to recycle wastewater from a PEM fuel cell to supply water for reacting with the micro-disperse particles of sodium borohydride in a compact hydrogen gas generator. Capillary forces can wick water from a water reservoir into a packed bed of micro-disperse fuel particles, eliminating the need for using an active pump.
    Type: Grant
    Filed: April 23, 2004
    Date of Patent: December 11, 2007
    Assignee: Sandia Corporation
    Inventors: Stanley H. Kravitz, Andrew M. Hecht, Alan P. Sylwester, Nelson S. Bell
  • Patent number: 7208130
    Abstract: The invention concerns a process for preparing rare earth borates, and the use of these borates in luminescence. The preparation process is characterized in that it comprises the following steps mixing boric acid and a rare earth salt; a reacting the mixture obtained with a carbonate or a bicarbonate; a calcining the precipitate obtained.
    Type: Grant
    Filed: December 14, 2000
    Date of Patent: April 24, 2007
    Assignee: Rhodia Electronics and Catalysis
    Inventors: Jean-Jacques Braconnier, Muriel Goubard
  • Patent number: 7087174
    Abstract: A method of enhancing the recovery of useful coal or potassium chloride or borax from screenbowl centrifuge separation operations comprising adding to the screenbowl centrifuge, from about 0.03 lbs active polymer/ton dry solids in centrifuge to about 0.70 lbs active polymer/ton dry solids in centrifuge, of a cationic terpolymer, wherein said cationic terpolymer is prepared by polymerizing from about 1 to about 99.1 mole percent of one or more cationic monomers, from about 0.1 to about 10 mole percent of one or more hydroxyalkyl(meth)acrylates and from one to about 98.1 mole percent of one or more nonionic monomers.
    Type: Grant
    Filed: April 8, 2004
    Date of Patent: August 8, 2006
    Assignee: Nalco Company
    Inventors: Peter A. Dimas, Kenneth M. McGough, Wesley L. Whipple
  • Patent number: 7029528
    Abstract: There are provided a method of superflattening an oxide crystal that is soluble neither with acid nor with alkaline, a method of making a ReCa4O(BO3)3 family oxide single crystal thin film using the superflattening method, a ReCa4O(BO3)3 family oxide single crystal thin film having a SHG property, a superflattening method for light incident/emitting surfaces, and a defect assessing method for oxide crystals. The surface of an oxide crystal that is soluble neither with acid nor with alkaline is reduced with a reducing agent, the reduced oxide crystal surface is dissolved with an aqueous solution of acid or alkaline, the surface dissolved oxide crystal is heat-treated in the atmosphere, whereby the surface of an oxide crystal that is soluble neither with acid nor with alkaline is superflattened to an atomic level.
    Type: Grant
    Filed: March 15, 2002
    Date of Patent: April 18, 2006
    Assignee: Japan Science and Technology Corporation
    Inventors: Hideomi Koinuma, Yuji Matsumoto, Takatomo Sasaki, Yusuke Mori, Masashi Yoshimura
  • Patent number: 6991773
    Abstract: A hydrogen storage medium is provided, where the medium is comprised of boron oxide and closely related compounds such as orthoboric acid, metaboric acid, hydrated boric acid, and disodium borohydrate. The medium is substantially an amorphous glassy network, albeit with local regions of order, pores, and networks that provide surface area. Hydrogen is adsorbed by the medium with a heat of adsorption of about 9 kJ/mol to about 13 kJ/mol, a value which is higher than that of the heat of adsorption of hydrogen on carbon. The value for the heat of adsorption of hydrogen on the inventive storage medium is provided by computation, and corroborated by experimental observation. The higher heat of adsorption of the medium provides for operation at temperatures higher temperatures higher than those provided by carbon.
    Type: Grant
    Filed: October 8, 2002
    Date of Patent: January 31, 2006
    Assignee: Nanomix, Inc.
    Inventors: Seung-Hoon Jhi, Young-Kyun Kwon, Keith Bradley, Jean-Christophe P. Gabriel
  • Patent number: 6780913
    Abstract: A zinc borate having a particular crystallite size and containing very little sodium components and a method of preparing the same. The zinc borate has a particular chemical composition, has a crystallite size of not smaller than 40 nm as found from diffraction peaks of indexes of planes of (020), (101) and (200) in the X-ray diffraction image (Cu-k&agr;) and contains sodium components in amounts of not larger than 100 ppm as measured by the atomic absorptiometric method.
    Type: Grant
    Filed: September 5, 2001
    Date of Patent: August 24, 2004
    Assignee: Mizusawa Industrial Chemicals, Ltd.
    Inventors: Hiroshi Sawada, Hiroshi Igarashi, Akira Tatebe, Kazunori Sakao
  • Patent number: 6773625
    Abstract: Dry bleach compositions particularly suitable for cleaning of hard surfaces or fabrics which, upon mixing with water, form a mixture that is easily removed from surfaces upon standing.
    Type: Grant
    Filed: August 26, 2002
    Date of Patent: August 10, 2004
    Assignee: Unilever Home & Personal Care USA, division of Conopco, Inc.
    Inventors: Nancy Ann Falk, Pamela Chau Lam
  • Patent number: 6716524
    Abstract: A rare earth borate in the form of substantially spherical, uniform diameter particles having an average particle diameter of 0.5-2 &mgr;m is prepared by mixing substantially spherical rare earth oxide co-precipitates having an average particle diameter of 0.5-2 &mgr;m with boric acid or boron oxide, and heating the mixture at 600-1100° C. for reaction. It is a useful raw material for phosphor manufacture.
    Type: Grant
    Filed: January 29, 2002
    Date of Patent: April 6, 2004
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Kazuhiro Wataya, Miyuki Ohyama
  • Patent number: 6596196
    Abstract: An improved material in the form of rare-earth borate, its precursor(s) and a luminophore made thereof is provided. The material is characterizable as comprising spherical, cubic or parallelepipedal particles having an average particle size not more than 10 &mgr;m, over a narrow particle size distribution (dispersion index not greater than 0.8). The material may comprise a rare earth element having that lacks luminescence in combination with a dopant.
    Type: Grant
    Filed: December 22, 2000
    Date of Patent: July 22, 2003
    Assignee: Rhodia Chimie
    Inventors: Denis Huguenin, Pierre Macaudiere
  • Patent number: 6455461
    Abstract: A composition comprises a hydrogenation catalyst supported on an inorganic support which comprises aluminum, zirconium, and a borate. A process for producing the composition comprises the steps of (1) contacting an aluminum salt, a zirconium salt, and an acidic boron compound under a condition sufficient to effect the production of a solid material comprising aluminum, zirconium, and borate; and (2) combining a hydrogenation catalyst with the inorganic support. Also disclosed is a process for reducing aromatic compounds content in a hydrocarbon-containing fluid which comprises contacting a hydrocarbon-containing fluid, in the presence of a catalyst composition, with hydrogen wherein said catalyst composition comprises a hydrogenation catalyst and an inorganic support wherein said support comprises aluminum, zirconium and a borate.
    Type: Grant
    Filed: September 23, 1999
    Date of Patent: September 24, 2002
    Assignee: Phillips Petroleum Company
    Inventor: Lyle R. Kallenbach
  • Patent number: 6417954
    Abstract: Nonlinear optical materials, methods of crystal growth, and devices employing such materials satisfy the general formula (&Sgr;i=1-3M&agr;i1)(&Sgr;j=1-3M&bgr;j2)(&Sgr;k=1-6M&ggr;k3)B14O25  Formula 1 wherein M1, M2, and M3 are mono-, di, or tri-valent metal ions respectively; wherein (&Sgr;i=1-3&agr;i)=X and ranges from 0 to 2, (&Sgr;j=1-3&bgr;j)=Y and ranges from 0 to 4, and (&Sgr;k=1-6&ggr;k)=Z and ranges from 0 to 2, and wherein X+Y+Z=4.0. Other nonlinear optical compounds according to this invention also generally satisfy Formula 2 through 7 below: (&Sgr;j=1-3M&bgr;j2)B14O25, where (&Sgr;j=1-3&bgr;j)=4  Formula 2 M42B14O25  Formula 3 (&Sgr;i=1-3M&agr;i1)(&Sgr;k=1-6M&ggr;k3)B14O25  Formula 4 where (&Sgr;i=1-3&agr;i)=2, and (&Sgr;k=1-6&ggr;k)=2.
    Type: Grant
    Filed: January 23, 2001
    Date of Patent: July 9, 2002
    Assignee: RejTech Corporation
    Inventors: Thomas A. Reynolds, Theodore Alekel, Douglas A. Keszler
  • Patent number: 6391229
    Abstract: A borate single crystal which can stably perform light wavelength conversion with high efficiency down to the ultraviolet region is represented by the chemical formula (A2O).(B2O3)x, and is an orthorhombic crystal belonging to the P212121 space group, wherein A includes two elements selected from the group consisting of Li, Na, K, Rb, and Cs, and 1.5<x<2.5.
    Type: Grant
    Filed: January 3, 2000
    Date of Patent: May 21, 2002
    Assignee: Mitsubishi Materials Corporation
    Inventors: Noriko Watanabe, Tamotsu Sugawara, Genta Masada, Hiroyuki Shiraishi, Yasuhiro Hanaue, Ryuichi Komatsu, Tsuyoshi Kajitani, Yasuhiro Ono
  • Publication number: 20010030032
    Abstract: The invention comprises a borosilicate retention aid composition and a method for improving the production of paper by addition of the borosilicate. The borosilicate may be utilized in conjunction with a high molecular weight synthetic flocculant and/or starch, with or without the addition of a cationic coagulant. The borosilicate material is preferably a colloidal borosilicate. Methods for the preparation of the borosilicate material are disclosed.
    Type: Application
    Filed: April 22, 2001
    Publication date: October 18, 2001
    Inventors: Bruce A. Keiser, James E. Whitten
  • Publication number: 20010023752
    Abstract: The invention comprises a borosilicate retention aid composition and a method for improving the production of paper by addition of the borosilicate. The borosilicate may be utilized in conjunction with a high molecular weight synthetic flocculant and/or starch, with or without the addition of a cationic coagulant. The borosilicate material is preferably a colloidal borosilicate. Methods for the preparation of the borosilicate material are disclosed.
    Type: Application
    Filed: April 22, 2001
    Publication date: September 27, 2001
    Inventors: Bruce A. Keiser, James E. Whitten