Abstract: This invention relates to a catalyst for alkylating polyalkylene glycol and a method of alkylating polyalkylene glycol using the same, wherein the catalyst enables polyalkylene glycol to be alkylated at a high conversion rate without generating harmful materials and the terminal of polyalkylene glycol can be alkylated using the same. Thereby, the terminal of polyalkylene glycol can be alkylated in an environmentally friendly and economical manner through a simple process.

Abstract: A LCD device comprising the liquid crystal cell and a surface modification method for an IR material are provided. The IR material is obtained via the surface modification method, and a component comprising the IR material is disposed in the liquid crystal cell. As the liquid crystal cell can emit infrared light, it is beneficial for healthy. The surface modified IR material is compatible and has optimal matching property with the structure of the liquid crystal cell, the heat exchange capacity between the IR material and the backlight as well the ambient light can be improved without compromising the performance of the LCD device, and the surface modified IR material will emit far-IR light of specific wavelength with higher emissivity.

Abstract: The invention relates to a coating composition consisting of an oxide compound. The invention also relates to a method for producing a coating composition consisting of an oxide compound and to a method for coating substrates composed of metal, semiconductor, alloy, ceramic, quartz, glass or glass-type materials with coating compositions of this type. The invention further relates to the use of a coating composition according to the invention for coating metal, semiconductor, alloy, ceramic, quartz, glass and/or glass-type substrates.

Abstract: Feed material comprising uniform solution precursor droplets is processed in a uniform melt state using microwave generated plasma. The plasma torch employed is capable of generating laminar gas flows and providing a uniform temperature profile within the plasma. Plasma exhaust products are quenched at high rates to yield amorphous products. Products of this process include spherical, highly porous and amorphous oxide ceramic particles such as magnesia-yttria (MgO—Y2O3). The present invention can also be used to produce amorphous non oxide ceramic particles comprised of Boron, Carbon, and Nitrogen which can be subsequently consolidated into super hard materials.

Abstract: A process for preparing a mesoporous alumina is described, comprising the following steps: a) mixing, in aqueous solution, at least one source of aluminum constituted by an aluminum alkoxide, at least one cationic surfactant and at least one organic solvent selected from methanol and ethanol; b) hydrothermally treating the mixture formed in said step a); c) drying the solid formed in said step b); d) calcining the solid formed in said step c).

Abstract: A precursor sol of aluminum oxide includes particles containing a hydrolysate and/or a condensate of an aluminum compound, a solvent, and an organo aluminum compound. When a pulsed-NMR T2 relaxation curve of nuclide 1H of the precursor sol of aluminum oxide includes two components with different T2 relaxation times and the component with the longer T2 relaxation time has an abundance level of CL (%) and the component with the shorter T2 relaxation time has an abundance level of CS (%), the relative proportion RCS (%) defined by [{CS/(CS+CL)}×100] is in the range of 23.5% to 50.0%, both inclusive.

Abstract: The present invention relates to a method for preparing high-purity aluminum, the method comprising: a mother liquor preparing step for preparing a mother liquor by dissolving and aging ordinary aluminum hydroxide; a refining step for adding pulp to absorb impurities from the prepared mother liquor after the mother liquor preparing step; and an obtaining step for obtaining high-purity alumina by adding a seed into the mother liquor and precipitating a precipitate, and filtering, washing, and recrystallizing the precipitate, and calcining the precipitate. Thus, the present invention enables an environmentally-friendly and low-cost preparation of high-purity alumina.

Abstract: The invention is directed towards methods and compositions for treating slurry to better dewater alumina trihydrate precipitated from the Bayer process. The method comprises using a product comprising the combination of at least two surfactants together with an optional coupling agent to treat the alkaline slurry with certain amount of alumina trihydrate present. Synergistic effects between binary combinations of nonionic and anionic surfactants result in more efficient dewatering aids for alumina trihydrate slurry when combinations of such surfactants are applied. A coupling agent may be used in formulations to reduce viscosity of such surfactant combinations, allowing the practical application of such products.

Abstract: A method of making aluminum oxynitride includes introducing a mixture having aluminum oxide and carbon into a chamber, agitating the mixture within the chamber, and heating the mixture to make aluminum oxynitride.

Abstract: The present invention relates to a process for preparing boehmitic aluminas by hydrolysis of aluminum alcoholates in aqueous, alkaline solution. It further relates to aluminas or alumina hydrates prepared by this process and their uses.

Abstract: A method for manufacturing a cathode active material for a lithium rechargeable battery, including: selecting a first metal compound from a group consisting of a halide, a phosphate, a hydrogen phosphate and a sulfate of Mg or Al; selecting a second metal compound from a group consisting of an oxide, a hydroxide and a carbonate of Mg or Al; combining the first metal compound and the second metal compound to obtain a metal compound, the metal compound containing either Mg or Al atoms; mixing a lithium compound, a transition metal compound and the metal compound to obtain a mixture; and sintering the mixture.

Abstract: Provided is a process for producing a high-purity ?-alumina in which an Si content, an Fe content, a Ca content, and an Na content are simultaneously removed. The high-purity ?-alumina is produced by burning aluminum hydroxide having an Na content of 0.11 mass % or less, an Fe content of 6 ppm or less, a Ca content of 1.5 ppm or less, and an Si content of 10 ppm or less as impurities in terms of alumina respectively, and having an average particle diameter of 55 ?m or less at a burning temperature of 1,100 to 1,500° C. by using a burning vessel containing Al2O3 in a range of 85 to 93 wt % and SiO2 in a range of 7 to 14 wt % and subjecting the obtained ?-alumina to wash treatment.

Abstract: Particular embodiments are directed toward a rubber mixture comprising (i) a rubber; and (ii) a filler component, where the filler component includes a filler selected from the group consisting of amorphous aluminum hydroxycarbonate, amorphous aluminum hydroxyoxycarbonate, and amorphous aluminum oxycarbonate, where said amorphous aluminum hydroxycarbonate, amorphous aluminum hydroxyoxycarbonate, and amorphous aluminum oxycarbonate are characterized by a BET specific surface area of less than 40 m2/g.

Abstract: The invention relates to amphiphilic, nanoscalar particles comprising lipophilic hydrolyzable groups on their surface. The invention also relates to methods for producing amphiphilic, nanoscalar particles and to compositions containing said particles.

Abstract: The invention relates to a coating composition consisting of an oxide compound. The invention also relates to a method for producing a coating composition consisting of an oxide compound and to a method for coating substrates composed of metal, semiconductor, alloy, ceramic, quartz, glass or glass-type materials with coating compositions of this type. The invention further relates to the use of a coating composition according to the invention for coating metal, semiconductor, alloy, ceramic, quartz, glass and/or glass-type substrates.

Abstract: A process of producing a ceramic powder including providing a plurality of precursor materials in solution, wherein each of the plurality of precursor materials in solution further comprises at least one constituent ionic species of a ceramic powder, combining the plurality of precursor materials in solution with an onium dicarboxylate precipitant solution to cause co-precipitation of the ceramic powder precursor in a combined solution; and separating the ceramic powder precursor from the combined solution. The process may further include calcining the ceramic powder precursor.

Abstract: A process comprises (a) combining (1) at least one base and (2) at least one metal carboxylate salt comprising (i) a metal cation selected from metal cations that form amphoteric metal oxides or oxyhydroxides and (ii) a lactate or thiolactate anion, or metal carboxylate salt precursors comprising (i) at least one metal salt comprising the metal cation and a non-interfering anion and (ii) lactic or thiolactic acid, a lactate or thiolactate salt of a non-interfering, non-metal cation, or a mixture thereof; and (b) allowing the base and the metal carboxylate salt or metal carboxylate salt precursors to react.

Abstract: The present invention is a process for the conversion of aluminum oxide hydroxide (AlOOH) to aluminum oxide. About 30 to 70 wt-% of AlOOH, about 30 to 70 wt-% ammonium hydrogencarbonate NH4HCO3 and 0 to 20 wt-% water are combined to produce a mixture. This mixture is then cured at a temperature from about 30° to about 90° C. to convert at least 5% of the AlOOH to a ammonium hydroxycarbonate (dawsonite-type) intermediate and then the dawsonite-type intermediate is decomposed at a temperature from about 130° to 320° C. to produce aluminum oxide. The aluminum oxide can be further calcined at 500° to 800° C. to produce a gamma-theta phase alumina.

Abstract: A method for fabricating a high specific surface area mesoporous alumina is disclosed, which includes the following steps: (a) providing a water solution containing an aluminum salt and a fluoro-surfactant; (b) adding concentrated hydrochloric acid to adjust the PH value of the solution to about 6.0 to 8.0; (c) aging the solution at 70° C. to 110° C. for 12 to 20 hours; (d) washing the precipitate with water; (e) washing the precipitate with an organic solvent; (f) drying the precipitate; and (g) sintering the precipitate in a furnace of 500° C. to 1000° C.

Abstract: A method for making hollow spheres of alumina or aluminate comprises: coating polymeric beads with an aqueous solution of an alumoxane, drying the beads so as to form an alumoxane coating on the beads; heating the beads to a first temperature that is sufficient to convert the alumoxane coating to an amorphous alumina or aluminate coating and is not sufficient to decompose the polymeric beads; dissolving the polymeric bead in a solvent; removing the dissolved polymer from the amorphous alumina or aluminate coating; and heating the amorphous alumina or aluminate coating to a second temperature that is sufficient to form a hollow ceramic sphere of desired porosity and strength. The hollow spheres can be used as proppants or can be incorporated in porous membranes.

Abstract: The present invention provides ?-alumina powders comprising ?-alumina particles of which at least 80% of the ?-alumina particles have a particle size of less than 100 nm. The invention also provides slurries, particularly aqueous slurries, which comprise ?-alumina powders of the invention. The invention further provides methods of manufacturing ?-alumina powders and ?-alumina slurries of the invention and methods of polishing using same.

Abstract: A process for the preparation of a catalyst, which process comprises the steps of: i) mixing an alumina precursor with combustible carbon-containing fibers with a diameter in the range of from 0.5 to 5 ?m and a length of no greater than 100 ?m in an amount in the range of from 20 to 40 wt % based on the total dry mixture; ii) adding nitric acid and water to form an extrudable mass; iii) extruding the mixture to form shaped particles; iv) drying the shaped particles; v) heating the particles in an atmosphere comprising no more than 5 vol % oxygen at a temperature in the range of from 350 to 600° C.; and vi) then heating the particles in a gas mixture comprising at least 12 vol % oxygen at a temperature in the range of from 450 to 600° C.

Abstract: A unique combination of solution stabilization and delivery technologies with special ALD operation is provided. A wide range of low volatility solid ALD precursors dissolved in solvents are used. Unstable solutes may be stabilized in solution and all of the solutions may be delivered at room temperature. After the solutions are vaporized, the vapor phase precursors and solvents are pulsed into a deposition chamber to assure true ALD film growth.

Abstract: A process for producing plate-like alumina particles with a high aspect ratio is described. Nano-sized particles of an aluminium precursor compound, optionally formed by milling, are mixed with a sufficient volume fraction of a diluent and heat treated to form substantially discrete plate-like alpha alumina particles dispersed in the diluent. A mineraliser may be added to lower the effective melting point of the system. Substantially discrete plate-like particles may be formed without agitation when the heat treatment is conducted below the melting point of the diluent.

Abstract: It is an object to provide a method for producing stable alkaline metal oxide sols having a uniform particle size distribution. The method comprises the steps of: heating a metal compound at a temperature of 60° C. to 110° C. in an aqueous medium that contains a carbonate of quaternary ammonium; and carrying out hydrothermal processing at a temperature of 110° C. to 250° C. The carbonate of quaternary ammonium is (NR4)2CO3 or NR4HCO3 in which R represents a hydrocarbon group, or a mixture thereof. The metal compound is one, or two or more metal compounds selected from a group of compounds based on a metal having a valence that is bivalent, trivalent, or tetravalent.

Abstract: A method for preparing metal oxide particles having a primary particle size on the order of nanometers is provided. The method comprises subjecting a metal ion present in an aqueous solution and an amino alcohol to an initial stage of reaction with each other at normal temperatures under normal pressures for a given time, and adding at least once either of a metal ion or an amino alcohol or both thereof to the resulting reaction system for carrying out a subsequent stage of reaction for a given time wherein total amounts of the metal ion and the amino alcohol are such that the amino alcohol is used in the range of not less than a molar equivalent to the metal ion.

Abstract: A method capable of easily producing a nanostructured material having regular nanoscale arrangement. The method comprises a raw material solution preparation step of preparing a raw material solution by dissolving, in a solvent, a block copolymer comprising a polymer block component “A” and a polymer block component “B” which are immiscible to each other, and an inorganic precursor which coordinates with the polymer block component “A” but does not coordinate with the polymer block component “B”; and a nanostructure-forming step of forming a nanophase-separated structure “10” in which a polymer phase “1A” comprising the polymer block component “A” with which the inorganic precursor is coordinated, and a polymer phase “1B” comprising the polymer block component “B” are regularly arranged by self-assembly. A nanostructured material can be obtained by this method.

Abstract: Multi-step metal compound oxidation process to produce compounds and enhanced metal oxides from various source materials, e.g. metal sulfides, carbides, nitrides and other metal containing materials with metal oxides from secondary reaction steps being utilized as an oxidation agent in the first reactions.

Abstract: The present invention provides ?-alumina powders comprising ?-alumina particles of which at least 80% of the ?-alumina particles have a particle size of less than 100 nm. The invention also provides slurries, particularly aqueous slurries, which comprise ?-alumina powders of the invention. The invention further provides methods of manufacturing ?-alumina powders and ?-alumina slurries of the invention and methods of polishing using same.

Abstract: It is an object to provide a method for producing stable alkaline metal oxide sols having a uniform particle size distribution. The method comprises the steps of: heating a metal compound at a temperature of 60° C. to 110° C. in an aqueous medium that contains a carbonate of quaternary ammonium; and carrying out hydrothermal processing at a temperature of 110° C. to 250° C. The carbonate of quaternary ammonium is (NR4)2CO3 or NR4HCO3 in which R represents a hydrocarbon group, or a mixture thereof. The metal compound is one, or two or more metal compounds selected from a group of compounds based on a metal having a valence that is bivalent, trivalent, or tetravalent.

Abstract: A method for producing an ?-alumina powder is described. The method for producing an ?-alumina powder comprises a step of calcining an aluminum salt in the presence of a seed crystal at 600-890° C.

Abstract: A method of producing hollow alumina particles capable of controlling the grain size of hollow alumina particles and providing high formation ratio of hollow particles while suppressing the formation of solid particles, the method comprising irradiating supersonic waves to an aqueous solution containing aluminum nitrate or aluminum acetate, and a surfactant or an organic acid to generate micro-liquid droplets in an atomized state, introducing the generated micro-liquid droplets only for the portion of minute liquid droplets having a certain grain size or less by an air stream and burning them in air.

Abstract: Mesoporous aluminum oxides with high surface areas have been synthesized using inexpensive, small organic templating agents instead of surfactants. Optionally, some of the aluminum can be framework-substituted by one or more other elements. The material has high thermal stability and possesses a three-dimensionally randomly connected mesopore network with continuously tunable pore sizes. This material can be used as catalysts for dehydration, hydrotreating, hydrogenation, catalytic reforming, steam reforming, amination, Fischer-Tropsch synthesis and Diels-Alder synthesis, etc.

Abstract: A two-step method for producing monolithic alumina aerogels having porosities of greater than 80 percent. Very strong, very low density alumina aerogel monoliths are prepared using the two-step sol-gel process. The method of preparing pure alumina aerogel modifies the prior known sol method by combining the use of substoichiometric water for hydrolysis, the use of acetic acid to control hydrolysis/condensation, and high temperature supercritical drying, all of which contribute to the formation of a polycrystalline aerogel microstructure. This structure provides exceptional mechanical properties of the alumina aerogel, as well as enhanced thermal resistance and high temperature stability.

Abstract: A catalyst for hydrofining fraction oils, comprises an alumina carrier and at least one metal and/or thereof oxide of Group VIB and at least one metal and/or thereof oxide of Group VIII supported on said alumina carrier. The pore volume of said alumina carrier is not less than 0.35 ml/g, in which the pore volume of the pores having a diameter of 40-100 angstrom accounts for more than 80% of the total pore volume, the alumina carrier is prepared by a special process. The catalyst possesses relatively high hydrogenation activity.

Abstract: The present invention pertains to an improved process for the preparation of quasi-crystalline boehmite. In this improved process a quasi-crystalline boehmite precursor is aged at a pH below 7, prefereably under hydrothermal conditions. It was found that when conducting the preparation processes for quasi-crystalline aluminas described in the prior art at a pH below 7 and under hydrothermal conditions instead of the high pH and thermal aging used in the prior art, QCBs with higher crystallinity are obtained. In the process according to the invention additives may be added to the quasi-crystalline boehmite precursor. This results in a high quality QCB with additives in a homogeneously dispersed state. Suitable additives are compounds containing elements selected from the group of rare earth metals alkaline earth metals, transition metals, actinides, silicon, gallium, boron, and phosphorus.

Abstract: Metal oxide microspheres, particularly zirconia microspheres, produced by a method of hydrolysis of metal alkoxides in alcohol solutions in the presence of an organic acid or salt thereof with washing step or addition of a surfactant.

Abstract: A process for the production of an aluminum oxide composition which includes subjecting an aluminoxane with a basic structural element of —Al—O—Al— or a basic oligomeric structural element of —Al—O—Al—O—Al—O—Al— to mild hydrolysis with at least one inert gas moistened below its dew point to produce a composition and subjecting the composition to thermolysis at temperatures from about 300 to about 900° C.

Abstract: The invention concerns a process for synthesising aluminas with a controlled porosity in which the pore diameter is in the range 0.6 nm to 80 nm. This process is carried out in a plurality of steps including at least one step a) in which an alumina precursor is prepared by hydrolysis of at least one anionic inorganic source of aluminium in the presence of at least one surfactant. Step a) of the process is carried out in an essentially aqueous medium the pH of which is generally higher than the isoelectric point of the alumina. The process of the invention also comprises at least one step b) in which the precipitate obtained is dried in air at a temperature of about 40° C. to 110° C. for a period of about 2 to 30 hours, and at least one step c) in which the dried precipitate is calcined at a temperature which is sufficient to eliminate the molecules of surfactant present in the precursor.

Abstract: A catalyst for hydrodemetalization of heavy oil, especially residuum oil, and a process for preparing the same, wherein said catalyst comprises the metal elements of Groups VIII and/or VIB as active components supported on an alumina carrier having large pores. The total pore volume of said carrier is in the range of 0.80˜1.20 ml/g (by mercury porosimetry method), the specific surface area in the range of 110˜200 m2/g, the peak pore diameter in the range of 15˜20 nm, and the bulk density in the range of 0.50˜0.60 g/ml. In the process of the invention, a physical pore-enlarging agent and a chemical pore-enlarging agent are added simultaneously during the mixing of the pseudoboehmite to a plastic mass, then extruding, drying, calcining, the carrier is obtained, then impregnating with active components by spraying onto the carrier, after drying and calcining, the catalyst is obtained.

Abstract: Hydrated aluminium compounds of the present invention are represented by the general formula nS, mM, Al2O3, xH2O where S is a surfactant or a group of surfactants, n is the number of moles of S, M is an alkaline cation, preferably selected from the group formed by Na+, K+, NH4+, m is the number of moles of M and x is the number of moles of water. The hydrated compounds are obtained from inorganic aluminium sources which are in the form of cation-monomers and/or cation-oligomers. The surfactants are anionic and/or non-ionic surfactants. When the group of surfactants comprises at least one anionic surfactant, at least one cationic surfactant can optionally be added.

Abstract: A process for producing alumina and other aluminia products where the formation of a Schiff base imine by reaction of a orgaonaluminum amide or imide oligomer with a carbonyl compound is promoted by the Lewis acid character of the oligomer. The water byproduct of the Schiff base serves as an in situ reagent for subsequent hydrolysis and sol-gel condensation of the aluminum species with concomitant production of alkane. The imine then is washed from the alumina with a suitable solvent. Any of a number of primary amines and aldehydes or ketones may be reagents. Calcining of the sol-gels yields high surface area alumina as characterized by scanning electron microscopy, and gas physisorption measurements. Microporous and/or mesoporous alumina is obtained depending on synthesis conditions. Alumina microspheres are obtained under certain conditions.

Abstract: A process for providing elemental metals or metal oxides distributed on a carbon substrate or self-supported utilizing graphite oxide as a precursor. The graphite oxide is exposed to one or more metal chlorides to form an intermediary product comprising carbon, metal, chloride, and oxygen This intermediary product can be flier processed by direct exposure to carbonate solutions to form a second intermediary product comprising carbon, metal carbonate, and oxygen. Either intermediary product may be further processed: a) in air to produce metal oxide; b) in an inert environment to produce metal oxide on carbon substrate; c) in a reducing environment to produce elemental metal distributed on carbon substrate. The product generally takes the shape of the carbon precursor.

Abstract: Semi-crystalline alumina compositions with framework mesopores are disclosed. The compositions are assembled from inorganic aluminum precursors and nonionic polyethylene oxide surfactants. The new assembly pathway introduces several new concepts to alumina mesostructure synthesis. The application of low-cost, non-toxic and biodegradable surfactants and low cost aluminum reagents as alumina precursors which are inorganic and low solution reaction temperatures, introduces efficient and environmentally clean synthetic techniques to the formation of mesostructures. Recovery of the surfactant can be achieved through solvent extraction where the solvent may be water or ethanol or by calcination.

Abstract: Transparent, monolithic metal oxide aerogels of varying densities are produced using a method in which a metal alkoxide solution and a catalyst solution are prepared separately and reacted. The resulting hydrolyzed-condensed colloidal solution is gelled, and the wet gel is contained within a sealed, but gas permeable, containment vessel during supercritical extraction of the solvent. The containment vessel is enclosed within an aqueous atmosphere that is above the supercritical temperature and pressure of the solvent of the metal alkoxide solution.

Abstract: A process and an apparatus for the production of iron oxides having low chloride ion content comprising charging of a free HCl containing iron chloride solution into a spray roaster with a feeding device and a spray boom for charging the iron chloride containing solution into a reaction chamber heated by combustion gases thermally decomposing the solution into iron oxide, HCl gas and reaction gases a discharging device for the iron oxide and a cooling zone between the burner's focal plane and the discharging device cooling of iron oxide granules to temperatures at less than 450.degree. C. reducing the concentration of HCl gas to less than 10 volume percent charging the layer of iron oxide granules onto a conveyor plate charged with hot steam and feeding the exhaust gases into the central combustion duct of the spray roaster. The resulting iron oxide has a residual chloride ion content of less than 500 ppm Cl.sup.- and a specific surface area in excess of 3.5 m.sup.3 /g.

Abstract: The present invention relates to catalyst supports and improvements thereof for use with supported activators and supported transition metal catalyst systems. The invention specifically involves reacting a carrier containing reactive functionalities, e.g., hydroxyl containing silica, with halogenated organic compounds, e.g., fluorosubstituted phenols. The reaction is preferably carried out in the presence of a base. The reaction consumes undesired functionalities on the support to provide a halogenated support which is suitable for activators and catalytic precursors which are adversely affected by functionalities typically found on supports. The supported activators or catalytic precursors are prepared by contacting the precursors or activators with the halogenated support.

Abstract: A process for providing elemental metals or metal oxides distributed on a carbon substrate or self-supported utilizing graphite oxide as a precursor. The graphite oxide is exposed to one or more metal chlorides to form an intermediary product comprising carbon, metal, chloride, and oxygen. This intermediary product can be further processed by direct exposure to carbonate solutions to form a second intermediary product comprising carbon, metal carbonate, and oxygen. Either intermediary product may be further processed: a) in air to produce metal oxide; b) in an inert environment to produce metal oxide on carbon substrate; c) in a reducing environment to produce elemental metal distributed on carbon substrate. The product generally takes the shape of the carbon precursor.

Abstract: Mesoporous, alumina compositions having an average pore diameter substantially ranging from about 15 .ANG. to about 40 .ANG. and an average surface area of no less than about 500 meter square/gram are disclosed. These materials can be formed by treating an aluminum source that is derived from an aluminum alkoxide in an organic-aqueous solution with an organic structured directing agent to form meso-sized micelles followed by calcination of the resulting composition. Appropriate organic structural directing agents are alkyl carboxylic acids.

Abstract: A proces for preparing a spherical support for the polymerization of alpha-olefins from an ammonium dawsonite which is spray-dryed and formed into spherical particles which are then calcined and impregnated with titanium to produce a spherical catalyst of good mechanical strength is described. Also described is the polymerization process which, in the presence of the spherical catalyst, yields polyolefin particles which preserve the spherical characteristics of the support, with low flow angle and good bulk density, as well as the product polyethylene obtained from the process.