Metal Containing Patents (Class 423/592.1)
  • Patent number: 11845673
    Abstract: A novel material and a transistor using a novel material are provided. A composite oxide includes at least two regions, one of which includes In, Zn and an element M1 (the element M1 is one or more of Al, Ga, Si, B, Y, Ti, Fe, Ni, Ge, Zr, Mo, La, Ce, Nd, Hf, Ta, W, Mg, V, Be, and Cu), and the other of which includes In, Zn, and an element M2 (the element M2 is one or more of Al, Ga, Si, B, Y, Ti, Fe, Ni, Ge, Zr, Mo, La, Ce, Nd, Hf, Ta, W, Mg, V, Be, and Cu). The proportion of the element M1 to In, Zn, and the element M1 in the region including the element M1 is less than that of the element M2 to In, Zn, and the element M2 in the region including the element M2. In an analysis of the composite oxide by X-ray diffraction, the diffraction pattern result in the X-ray diffraction is asymmetric with the angle at which the peak intensity of X-ray diffraction is detected as the symmetry axis.
    Type: Grant
    Filed: November 10, 2022
    Date of Patent: December 19, 2023
    Assignee: Semiconductor Energy Laboratory Co., Ltd.
    Inventor: Shunpei Yamazaki
  • Patent number: 11814715
    Abstract: A method of depositing a metal-containing material is disclosed. The method can include use of cyclic deposition techniques, such as cyclic chemical vapor deposition and atomic layer deposition. The metal-containing material can include intermetallic compounds. A structure including the metal-containing material and a system for forming the material are also disclosed.
    Type: Grant
    Filed: August 19, 2022
    Date of Patent: November 14, 2023
    Assignee: ASM IP Holding B.V.
    Inventors: Katja Väyrynen, Timo Hatanpää, Anton Vihervaara, Mikko Ritala, Markku Leskelä
  • Patent number: 11697094
    Abstract: A method of purifying air polluted by smoke and fumes, such as from wildfires and other hazard, may deploy a series of fluid filled vessels that act as filters to trap and/or neutralize components that would foul an aqueous suspension of gold nanoparticles that is effective in converting toxic carbon monoxide to carbon dioxide. Non-toxic fluids may be used. As the gold nanoparticles are effective in a basic solution, the solution may contain a visible pH indicator or an apparatus that deploys the method may continuously monitor the pH thereof.
    Type: Grant
    Filed: May 13, 2022
    Date of Patent: July 11, 2023
    Inventors: John Jerome Chambless, Robert Paul French
  • Patent number: 11545608
    Abstract: A device includes: a substrate including a superconductor quantum device, the superconductor quantum device including a superconductor material that exhibits superconducting properties at or below a corresponding critical temperature; a cap layer bonded to the substrate; and a sealed cavity between the cap layer and the substrate.
    Type: Grant
    Filed: September 14, 2016
    Date of Patent: January 3, 2023
    Assignee: Google LLC
    Inventor: Anthony Edward Megrant
  • Patent number: 11532800
    Abstract: A light emitting device including a first electrode, a second electrode, a quantum dot layer disposed between the first electrode and the second electrode and a first auxiliary layer disposed between the quantum dot layer and the first electrode, wherein the first auxiliary layer includes nickel oxide nanoparticles having an average particle diameter of less than or equal to about 10 nanometers (nm) and an organic ligand, a method of manufacturing the light emitting device, and a display device including the same.
    Type: Grant
    Filed: September 1, 2020
    Date of Patent: December 20, 2022
    Assignee: SAMSUNG ELECTRONICS CO., LTD.
    Inventors: Chan Su Kim, Kun Su Park, Tae Ho Kim, Eun Joo Jang, Dae Young Chung
  • Patent number: 11508895
    Abstract: A device includes: a substrate including a superconductor quantum device, the superconductor quantum device including a superconductor material that exhibits superconducting properties at or below a corresponding critical temperature; a cap layer bonded to the substrate; and a sealed cavity between the cap layer and the substrate.
    Type: Grant
    Filed: September 14, 2016
    Date of Patent: November 22, 2022
    Assignee: Google LLC
    Inventor: Anthony Edward Megrant
  • Patent number: 11094463
    Abstract: Spherical ceramic-glass nanocomposite dielectrics made from ceramics and glasses that are separately pre-milled by mechanical ball milling using selected ball-to-powder weight ratios and combined to form a mixture that is ball milled. A stable liquid suspension of the milled mixture including an added dispersant such as polyacrylic acid to improve uniformity is spray dried through a nozzle and recovered product is annealed. The novel dielectrics have a microstructure where ceramic primary particles are uniformly distributed and fully embedded in a glass matrix. The dielectrics have a mean particle size of about 1-20 um and a sphericity of about 0.8 or higher which are suitable for fabricating multilayer ceramic capacitors for high temperature applications. The novel dielectrics afford decreased sintering temperature, enhanced breakdown strength, lower dielectric lose tangent, and lower costs.
    Type: Grant
    Filed: February 27, 2019
    Date of Patent: August 17, 2021
    Assignee: Aegis Technology Inc.
    Inventors: Zhigang Lin, Chunhu Tan
  • Patent number: 11046869
    Abstract: A polishing liquid comprising a liquid medium, an abrasive grain and a polymer, wherein the polymer includes a first molecular chain having a functional group directly bonded thereto, and a second molecular chain branched from the first molecular chain, and the functional group is at least one selected from the group consisting of a carboxyl group, a carboxylic acid salt group, a hydroxyl group, a sulfo group and a sulfonic acid salt group.
    Type: Grant
    Filed: June 13, 2016
    Date of Patent: June 29, 2021
    Assignee: SHOWA DENKO MATERIALS CO., LTD.
    Inventors: Toshiaki Akutsu, Hisataka Minami, Tomohiro Iwano, Tetsuro Yamashita, Masako Aoki, Masato Fukasawa
  • Patent number: 11028026
    Abstract: The present invention relates to a reactor for non-oxidative direct conversion of methane and a method of manufacturing ethylene and an aromatic compound using the same. More particularly, the present invention relates to a reactor for non-oxidative direct conversion of methane in which a catalytic reaction velocity is maximized, the production of coke is minimized, and a high conversion rate of methane and a high yield of ethylene and an aromatic compound are ensured when ethylene and the aromatic compound are manufactured from methane, and a method of manufacturing ethylene and an aromatic compound using the same.
    Type: Grant
    Filed: October 30, 2019
    Date of Patent: June 8, 2021
    Assignee: KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY
    Inventors: Yong Tae Kim, Sung Woo Lee, Seung Ju Han, Seok Ki Kim, Hyun Woo Kim
  • Patent number: 11014817
    Abstract: The present disclosure relates to a method of preparing a graphene metal nanoparticle-composite, including: preparing graphene by applying a shearing force to a first solution containing a graphite-based material and thus exfoliating the graphite-based material; preparing metal nanoparticles by applying a shearing force to a second solution containing a metal precursor, a capping agent, and a reducing agent; and physically combining the metal nanoparticles on the graphene by applying a shearing force to a third solution containing the graphene and the metal nanoparticles, and a graphene metal nanoparticle-composite prepared according to the method.
    Type: Grant
    Filed: May 31, 2017
    Date of Patent: May 25, 2021
    Assignee: GACHON UNIVERSITY OF INDUSTRY-ACADEMIC COOPERATION FOUNDATION
    Inventors: Tae Young Kim, Jong Pal Hong
  • Patent number: 10899631
    Abstract: A ferrous modified selenium sol for inhibiting accumulation of cadmium and arsenic in rice and the preparation method and application thereof are disclosed. The method includes: dissolving an iron-containing compound and a selenium-containing compound into water; adding a reductant to the solution, and stirring until no more precipitation is generated, then adding carbonate, continuing to stir until no more precipitation is generated, and then filtering, taking the precipitation, and washing to obtain the precipitation of the selenium element and ferrous carbonate; adding an emulsifier to a citric acid buffer solution to obtain an emulsified citric acid buffer solution; adding the precipitation of the selenium element and ferrous carbonate to the emulsified citric acid buffer solution to obtain a sol system; and evaporating to concentrate the sol system, and adjusting the pH to 4.5-8.5 to obtain a ferrous modified selenium sol for inhibiting the accumulation of cadmium and arsenic in rice.
    Type: Grant
    Filed: April 30, 2020
    Date of Patent: January 26, 2021
    Inventors: Fangbai Li, Chuanping Liu, Jianghu Cui
  • Patent number: 10894906
    Abstract: Composite particles with lower mean particle size and smaller size distribution are obtained through refining treatments. The refined composite particles, such as ceria coated silica particles are used in Chemical Mechanical Planarization (CMP) compositions to offer higher removal rate; very low within wafer (WWNU) for removal rate, low dishing and low defects for polishing oxide films.
    Type: Grant
    Filed: August 6, 2019
    Date of Patent: January 19, 2021
    Assignee: Versum Materials US, LLC
    Inventors: Hongjun Zhou, John Edward Quincy Hughes, Krishna P. Murella, Reinaldo Mario Machado, Mark Leonard O'Neill, Dnyanesh Chandrakant Tamboli
  • Patent number: 10507456
    Abstract: A metal oxide catalyst involved in a hydrogenation reaction in which a ketone is converted into an alcohol, a method of preparing the metal oxide catalyst, and a method of preparing an alcohol using the same are provided. The metal oxide catalyst has a spinel structure represented by the following Formula 1: XAl2O4,??<Formula 1> wherein X represents nickel or copper.
    Type: Grant
    Filed: March 27, 2018
    Date of Patent: December 17, 2019
    Assignee: KOREA KUMHO PETROCHEMICAL CO., LTD.
    Inventors: Ji Won Park, Yong Hee Yun, Kyoung Ho Row
  • Patent number: 9993804
    Abstract: A catalyst for exhaust gas purification is described which includes a substrate and a catalyst coating layer provided on the substrate. The catalyst coating layer includes first and second metal oxide particles. The first metal oxide particles have a catalyst metal supported thereon, and the second metal oxide particles do not have a catalyst metal supported thereon. The first and second metal oxide particles have a specific particle size. This is because, when the sizes of the particles supporting the catalyst metal remain relatively large but the sizes of the particles not supporting a catalyst metal are minimized, it is possible to decrease the thickness of the catalyst coating layer while maintaining durability and improving gas diffusibility of the coating layer. Therefore, a thickness of the catalyst coating is decreased without decreasing durability, and the catalyst can exhibit high exhaust gas purification performance even under high load conditions.
    Type: Grant
    Filed: April 7, 2017
    Date of Patent: June 12, 2018
    Assignees: TOYOTA JIDOSHA KABUSHIKI KAISHA, CATALER CORPORATION
    Inventors: Yoshinori Saito, Masahide Miura, Tetsuhiro Hirao, Masanao Sato, Hirotaka Ori
  • Patent number: 9951240
    Abstract: The invention relates to nanoparticle-based ink compositions. In particular, this invention relates to semi-conductive nanoparticle-based ink compositions suitable for different printing methods.
    Type: Grant
    Filed: June 26, 2014
    Date of Patent: April 24, 2018
    Assignee: GENES' INK SA
    Inventors: Emmanuelle Pietri, Virginie El Qacemi, Louis Dominique Kauffman, Corinne Versini, Yahia Didane
  • Patent number: 9537149
    Abstract: Disclosed is a method for manufacturing a lithium transition metal phosphate. The disclosed method for manufacturing a lithium transition metal phosphate comprises the steps of: injecting reaction materials containing lithium, a transition metal, and a phosphate, into a reactor, and mixing the raw materials at the molecular level in the reactor; and allowing the reaction materials to chemically react in the reactor so as to cause nucleation.
    Type: Grant
    Filed: April 20, 2011
    Date of Patent: January 3, 2017
    Assignee: SAMSUNG SDI CO., LTD.
    Inventors: Chun Joong Kim, Yun Jung Park, Dong Gyu Chang, Ji Ho Park, Woo Young Yang
  • Patent number: 9464038
    Abstract: Method for preparing certain oximes and oxime O-methyl ethers by reacting poorly water-soluble carbonyl compounds with salts of hydroxylamine or hydroxylamine O-methyl ether or the free base of hydroxylamine in the presence of certain phosphoric esters or salts thereof of the formula (I) wherein R1, R2 and X are defined as specified in the description.
    Type: Grant
    Filed: May 20, 2014
    Date of Patent: October 11, 2016
    Assignee: BAYER CROPSCIENCE AKTIENGESELLSCHAFT
    Inventors: Albert Schnatterer, Dieter Heinz, Martin Littmann, Ulrich Philipp, Juergen Ludwig, Constantin Frerick, Michael Barz
  • Patent number: 9450239
    Abstract: A method for fabricating intercalated lithium batteries in open air deposits a thin dense layer of amorphous solid-state lithium boride electrolyte directly onto a negative electrode via flame spray pyrolysis. In one embodiment, the negative electrode is attached to a prefabricated positive electrode via hot pressing (embossing), thus forming an intercalated lithium battery. The method significantly improves upon current methods of fabricating thin film solid state batteries by permitting fabrication without the aid of a controlled environment, thereby allowing for significantly cheaper fabrication than prior batch methods.
    Type: Grant
    Filed: February 26, 2013
    Date of Patent: September 20, 2016
    Inventor: Erik K. Koep
  • Patent number: 9416013
    Abstract: The invention relates to a method to produce a type II silicon clathrate, a method to produce a type I clathrate, and a method to decrease sodium in silicon clathrates.
    Type: Grant
    Filed: February 2, 2015
    Date of Patent: August 16, 2016
    Assignee: Colorado School of Mines
    Inventors: Lakshmi Krishna, Eric Toberer, Adele Tamboli
  • Patent number: 9397366
    Abstract: A method for preparing an ionic liquid nanoscale ionic material, the ionic liquid nanoscale ionic material and a battery that includes a battery electrolyte that comprises the ionic liquid nanoscale ionic material each provide superior performance. The superior performance may be manifested within the context of inhibited lithium dendrite formation.
    Type: Grant
    Filed: July 10, 2012
    Date of Patent: July 19, 2016
    Assignee: CORNELL UNIVERSITY
    Inventors: Lynden A. Archer, Surya S. Moganty, Yingying Lu
  • Patent number: 9050776
    Abstract: The present disclosure relates to a method of synthesis of Lithium Titanate Oxide used for a cathode of Lithium ion battery, the method comprising: (A) diluting TiCl4 with TiOCl2; (B) adding YCl3 or NbCl5 at the rate of 0.1˜2 mol % to Ti(mol); (C) forming a complex salt by dissolving to put at least one selected from a group consisting of Hydroxy propyl cellulose or Polyethylene glycol in a solvent, the Hydroxy propyl cellulose being a complexing agent and being a dispersing agent as well, whereas the Polyethylene glycol being a dispersing agent; (D) synthesizing a titanium precursor by adding an aqueous ammonia solution; (E) preparing Y or Nb doped titanium dioxide(TiO2) powder by heat-treating the synthetic product in a temperature of 500˜700° C.; and (F) mixing the Y or Nb doped TiO2 powder with LiOH.H2O and heat-treating the mixture in a temperature of 800˜900° C.
    Type: Grant
    Filed: August 31, 2012
    Date of Patent: June 9, 2015
    Assignee: KOREA INSTITUTE OF CERAMIC ENGINEERING AND TECHNOLOGY
    Inventors: Byung Hyun Choi, Mi Jung Ji, Eun Kyung Kim, Young Jin Kwon, Sung Hun Jung, Yong Tae An
  • Publication number: 20150140331
    Abstract: Embodiments of the present disclosure include metal boride nanoparticles, methods of making metal boride nanoparticles, methods of using metal boride nanoparticle, metal oxide nanoparticles, methods of making metal oxide nanoparticles, methods of using metal oxide nanoparticle, and the like.
    Type: Application
    Filed: October 17, 2012
    Publication date: May 21, 2015
    Applicant: UNIVERSITY OF GEORGIA RESEARCH FOUNDATION, INC.
    Inventor: University of Georgia Research Foundation, Inc.
  • Publication number: 20150139893
    Abstract: A method of making unit cell sized oxide particulates comprising preparing a water solution of a metal or ceramic salt or methanol solution of Pt, adding a 2-fold molar excess of KO2 to the water solution and forming a reaction solution, spinning down the reaction solution, and creating oxide nanoparticles.
    Type: Application
    Filed: October 29, 2014
    Publication date: May 21, 2015
    Applicant: The Government of the United States of America, as represented by the Secretary of the Navy
    Inventor: Thomas E. Sutto
  • Patent number: 9028726
    Abstract: The present invention provides a sputtering target suitable for producing an amorphous transparent conductive film which can be formed without heating a substrate and without feeding water during the sputtering; which is easily crystallized by low-temperature annealing; and which has low resistivity after the crystallization. An oxide sintered compact containing an indium oxide as a main component, while containing tin as a first additive element, and one or more elements selected from germanium, nickel, manganese, and aluminum as a second additive element, with the content of tin which is the first additive element being 2-15 atom % relative to the total content of indium and tin, and the total content of the second additive element being 0.1-2 atom % relative to the total content of indium, tin and the second additive element.
    Type: Grant
    Filed: September 18, 2009
    Date of Patent: May 12, 2015
    Assignee: JX Nippon Mining & Metals Corporation
    Inventors: Masakatsu Ikisawa, Masataka Yahagi
  • Publication number: 20150126355
    Abstract: Feed material comprising uniform solution precursor droplets is processed in a uniform melt state using microwave generated plasma. The plasma torch employed is capable of generating laminar gas flows and providing a uniform temperature profile within the plasma. Plasma exhaust products are quenched at high rates to yield amorphous products. Products of this process include spherical, highly porous and amorphous oxide ceramic particles such as magnesia-yttria (MgO—Y2O3). The present invention can also be used to produce amorphous non oxide ceramic particles comprised of Boron, Carbon, and Nitrogen which can be subsequently consolidated into super hard materials.
    Type: Application
    Filed: January 15, 2015
    Publication date: May 7, 2015
    Applicant: AMASTAN TECHNOLOGIES LLC
    Inventors: Kamal Hadidi, Makhlouf Redjdal
  • Patent number: 9005568
    Abstract: The invention provides a process for production of powder of perovskite compound which comprises: the first step for obtaining an aggregate of perovskite compound which comprises at least one A group element selected from the group consisting of Mg, Ca, Sr, Ba and Pb and at least one B group element selected from the group consisting of Ti, Zr, Hf and Sn, and which is represented by the general formula ABO3 wherein A is at least one A group element and B is at least one B group element; and the second step for heating the aggregate of perovskite compound obtained in the first step in a solvent at a temperature in a range from 30° C. to 500° C. whereby disintegrating the aggregate.
    Type: Grant
    Filed: February 9, 2005
    Date of Patent: April 14, 2015
    Assignee: Sakai Chemical Industry Co., Ltd.
    Inventors: Takashi Shikida, Shinji Ogama, Yoshiaki Ikeda, Kazuhisa Hidaka
  • Patent number: 9005567
    Abstract: A method for producing isolatable oxide microparticles or hydroxide microparticles using an apparatus that processes a fluid between processing surfaces of processing members that are arranged opposite each other so as to be able to approach to or separate from each other and such that at least one can rotate relative to the other. At least two fluids are mixed and oxide microparticles or hydroxide microparticles are separated, said two fluids including: a fluid containing a microparticle raw material solution comprising a microparticle raw material mixed into a solvent, and a fluid containing a microparticle-separation solution.
    Type: Grant
    Filed: August 26, 2011
    Date of Patent: April 14, 2015
    Assignee: M. Technique Co., Ltd.
    Inventors: Jun Kuraki, Kaeko Araki, Masaki Maekawa, Daisuke Honda, Masakazu Enomura
  • Patent number: 8986648
    Abstract: The present invention relates to a method for continuously preparing mineral particles by means of the thermolysis of mineral precursors in an aqueous medium, comprising contacting: a reactive flow, including mineral precursors at a temperature lower than the conversion temperature thereof; and a heat transfer flow that is countercurrent to said reactive flow and contains water at a temperature that is sufficient to bring the precursors to a temperature higher than the conversion temperature thereof, the mixture flow that results from said reactive flow and said heat transfer flow then being conveyed into a tubular reactor, inside of which particles are formed by gradually converting the precursors, and where the reactive flow and the heat transfer flow are placed in contact with each other inside a mixing chamber, inside of which the reactive flow and the heat transfer flow are fed by supply pipes having outlet cross-sections that are smaller than the maximum cross-section of said mixing chamber.
    Type: Grant
    Filed: July 20, 2010
    Date of Patent: March 24, 2015
    Assignees: Centre National de la Recherche Scientifique (C.N.R.S.), Universite de Bourgogne
    Inventors: Daniel Aymes, Moustapha Ariane, Frédéric Bernard, Hervé Muhr, Frédéric Demoisson
  • Publication number: 20150075603
    Abstract: A coating is described. The coating includes a metal oxide layer, which in turn includes a surface having a water contact angle greater than 90 degrees. A metal-oxide coating composition is also described. The composition includes effective amounts of a first type and a second of metals and an effective amount of oxygen to react with the first type and the second type of metals to produce a first type and a second type of metal oxides, both of which produce a structure that is greater than about 50% (by volume) amorphous.
    Type: Application
    Filed: March 21, 2013
    Publication date: March 19, 2015
    Inventors: Mark Allen George, Ching-Lin Chang, Ravi Prasad
  • Publication number: 20150075065
    Abstract: The invention provides a processing method for upgrading an organic phase substance by removing heavy element species from the organic phase substance originating from a resource substance in mild environmental conditions, and further provides a method for collecting removed heavy element species and a method for collecting other substances.
    Type: Application
    Filed: October 24, 2014
    Publication date: March 19, 2015
    Applicant: NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY
    Inventors: Tooru Nakamura, Yutaka Hayashi, Akira Suzuki, Richard Brommeland, Andrew Myles
  • Publication number: 20150069307
    Abstract: Compositions and methods of making are provided for treated mesoporous metal oxide microspheres electrodes. The compositions include microspheres with an average diameter between about 200 nanometers and about 10 micrometers and mesopores on the surface and interior of the microspheres. The methods of making include forming a mesoporous metal oxide microsphere composition and treating the mesoporous metal oxide microspheres by at least annealing in a reducing atmosphere, doping with an aliovalent element, and coating with a coating composition.
    Type: Application
    Filed: November 12, 2014
    Publication date: March 12, 2015
    Applicant: UT-BATTELLE, LLC
    Inventors: Mariappan Parans Paranthaman, Zhonghe Bi, Craig A. Bridges, Gilbert M. Brown
  • Patent number: 8969264
    Abstract: A treatment fluid comprises: a metal oxide, wherein the metal oxide is capable of forming a chelate complex or coordination complex with a ligand, wherein the chelate complex or coordination complex has a setting time of less than 90 minutes at a temperature of 71° F. and a pressure of 1 atmosphere. A method of treating a portion of a subterranean formation comprises: introducing the treatment fluid into the subterranean formation; allowing or causing a chelate complex or coordination complex to form between the metal oxide and a ligand; and allowing or causing the chelate complex or coordination complex to set.
    Type: Grant
    Filed: April 4, 2013
    Date of Patent: March 3, 2015
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Dale E. Jamison, Donald L. Whitfill, Matthew L. Miller, Kay A. Morris
  • Publication number: 20150056798
    Abstract: Some embodiments include methods of forming memory cells. Metal oxide may be deposited over a first electrode, with the deposited metal oxide having a relatively low degree of crystallinity. The degree of crystallinity within the metal oxide may be increased after the deposition of the metal oxide. A dielectric material may be formed over the metal oxide, and a second electrode may be formed over the dielectric material. The degree of crystallinity may be increased with a thermal treatment. The thermal treatment may be conducted before, during, and/or after formation of the dielectric material.
    Type: Application
    Filed: October 3, 2014
    Publication date: February 26, 2015
    Inventors: Noel Rocklein, Durai Ramaswamy, Dale W. Collins, Swapnil Lengade, Srividya Krishnamurthy, Mark S. Korber
  • Publication number: 20150044128
    Abstract: A deacidification apparatus and a deacidification process using the apparatus are disclosed. The deacidification apparatus includes a deacidification furnace, of which a furnace upper section, a furnace middle section and a furnace lower section are provided in upper, middle and lower portions respectively, wherein a gas-solid mixture inlet (1), a exhaust outlet (3) and a filtered air port (2) are provided on the furnace upper section, a product outlet (13) is provided on the furnace lower section, the upper portion of the deacidification is mounted with a filter (5) to which the gas-solid mixture inlet (1), the exhaust outlet (2) and the filtered air port (3) are connected, the filtered air port (2) is connected with a gas pulse device and a vacuum device by a three-way connecting device, and the exhaust outlet (3) is connected with atmosphere or connected with the vacuum device.
    Type: Application
    Filed: March 23, 2012
    Publication date: February 12, 2015
    Applicant: GUANGZHOU GBS HIGH-TECH & INDUSTRY CO., LTD.
    Inventors: Chunlei Wu, Xianjian Duan, Chengkun Long, Yuelin Wang
  • Patent number: 8951496
    Abstract: Feed material comprising uniform solution precursor droplets is processed in a uniform melt state using microwave generated plasma. The plasma torch employed is capable of generating laminar gas flows and providing a uniform temperature profile within the plasma. Plasma exhaust products are quenched at high rates to yield amorphous products. Products of this process include spherical, highly porous and amorphous oxide ceramic particles such as magnesia-yttria (MgO—Y2O3). The present invention can also be used to produce amorphous non oxide ceramic particles comprised of Boron, Carbon, and Nitrogen which can be subsequently consolidated into super hard materials.
    Type: Grant
    Filed: December 4, 2012
    Date of Patent: February 10, 2015
    Assignee: Amastan Technologies LLC
    Inventors: Kamal Hadidi, Makhlouf Redjdal
  • Patent number: 8945504
    Abstract: The present invention relates to nano structures of metal oxides having a nanostructured shell (or wall), and an internal space or void. Nanostructures may be nanoparticles, nanorod/belts/arrays, nanotubes, nanodisks, nanoboxes, hollow nanospheres, and mesoporous structures, among other nanostructures. The nanostructures are composed of polycrystalline metal, oxides such as SnO2. The nanostructures may have concentric walls which surround the internal space of cavity. There may be two or more concentric shells or walls. The internal space may contain a core such ferric oxides or other materials which have functional properties. The invention also provides for a novel, inexpensive, high-yield method for mass production of hollow metal oxide nanostructures. The method may be template free or contain a template such as silica. The nanostructures prepared by the methods of the invention provide for improved cycling performance when tested using rechargeable lithium-ion batteries.
    Type: Grant
    Filed: December 20, 2012
    Date of Patent: February 3, 2015
    Assignee: Cornell Research Foundation, Inc.
    Inventors: Lynden A. Archer, Xiong Wen Lou
  • Publication number: 20150023866
    Abstract: A process and system may be employed to produce large, defect-free oxide crystals with high melting points which may utilize a water-cooled horizontal furnace with a hot zone design comprising multiple independently controllable heaters surrounded by a vapor shield and various layers of thermal insulation of varying thickness and composition. Raw materials such as sapphire crystals or alumina powder may be placed in a crucible or boat that may be positioned to ride on rollers. The crucible may be pulled (or pushed) through a furnace environment surrounded by a vapor shield and insulation at a controlled rate to melt and then crystallize the raw material into a sapphire crystal. The vacuum level may be controlled by a vacuum system attached to the furnace. Process parameters such as power, temperature, pulling speed (i.e.
    Type: Application
    Filed: July 22, 2013
    Publication date: January 22, 2015
    Applicant: Rubicon Technology, Inc.
    Inventors: Matthew Montgomery, Timothy D. Burks, Sergey Podlozhenov, Jonathan Levine
  • Publication number: 20150017084
    Abstract: A method of forming a metal oxide composite, the method comprising mixing a metal oxide, at least two monomers and a dispersant to produce a slurry; gel casting the slurry to produce a green metal oxide composite; and sintering the green metal oxide composite to produce the metal oxide composite. A metal oxide composite formed according to the method. Use of the metal oxide composite, for catalysing hydrolysis of metal borohydride to produce hydrogen.
    Type: Application
    Filed: February 18, 2013
    Publication date: January 15, 2015
    Inventors: Lan Zhang, Siew Hwa Chan, Hongquan He
  • Patent number: 8926937
    Abstract: The present invention relates to a novel method for preparing a new type of catalyst for the oxidation of CO in a reactant gas or air. The method provides the preparation of a catalyst having nano-sized metal particles and a capping agent deposited on a solid support. The size and distribution of the metal particles can be easily controlled by adjusting reaction condition and the capping agent used. The catalyst prepared has high activity at low temperature toward selective oxidation of CO and is stable over an extended period of time. The catalyst can be used in air filter devices, hydrogen purification processes, automotive emission control devices (decomposition of NOx, x is the integer 1 or 2), F-T synthesis, preparation of fuel-cell electrode, photocatalysis and sensors.
    Type: Grant
    Filed: November 13, 2006
    Date of Patent: January 6, 2015
    Assignee: Agency for Science, Technology and Research
    Inventors: Ziyi Zhong, Jianyi Lin
  • Patent number: 8911904
    Abstract: Compositions and methods of making are provided for treated mesoporous metal oxide microspheres electrodes. The compositions comprise (a) microspheres with an average diameter between 200 nanometers (nm) and 10 micrometers (?m); (b) mesopores on the surface and interior of the microspheres, wherein the mesopores have an average diameter between 1 nm and 50 nm and the microspheres have a surface area between 50 m2/g and 500 m2/g, and wherein the composition has an electrical conductivity of at least 1×10?7 S/cm at 25° C. and 60 MPa. The methods of making comprise forming a mesoporous metal oxide microsphere composition and treating the mesoporous metal oxide microspheres by at least one method selected from the group consisting of: (i) annealing in a reducing atmosphere, (ii) doping with an aliovalent element, and (iii) coating with a coating composition.
    Type: Grant
    Filed: October 5, 2012
    Date of Patent: December 16, 2014
    Assignee: UT-Battelle, LLC
    Inventors: Mariappan Parans Paranthaman, Zhonghe Bi, Craig A. Bridges, Gilbert M. Brown
  • Patent number: 8906501
    Abstract: Disclosed herein is an article having: a substrate and a RuO2 coating having nanoparticles of RuO2. Also disclosed herein is an article having: a substrate and a RuO2 coating. The coating is made by: immersing the substrate in a solution of RuO4 and a nonpolar solvent at a temperature that is below the temperature at which RuO4 decomposes to RuO2 and warming the substrate and solution to ambient temperature under ambient conditions to cause the formation of the coating.
    Type: Grant
    Filed: November 26, 2010
    Date of Patent: December 9, 2014
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Jeffrey W Long, Jeffrey C Owrutsky, Christopher N. Chervin, Debra R Rolison, Joseph S. Melinger
  • Patent number: 8901027
    Abstract: A method of forming a Fischer-Tropsch catalyst by providing at least one metal nitrate solution, combining each of the at least one metal nitrate solutions with a precipitating agent whereby at least one catalyst precipitate is formed, and incorporating a strong base during precipitation, subsequent precipitation, or both during and subsequent precipitation. Catalysts produced via the disclosed method are also provided.
    Type: Grant
    Filed: November 15, 2011
    Date of Patent: December 2, 2014
    Assignee: Res USA, LLC
    Inventors: Deena Ferdous, Belma Demirel
  • Patent number: 8889095
    Abstract: Provided is a method for stabilizing a size of a platinum hydroxide polymer capable of maintaining solution stability of a platinum hydroxide polymer in a solution. The method may include adding Zr ions to a solution containing a platinum hydroxide polymer at a Zr/Pt ratio of 1.0 to 40 in terms of molar concentration ratio.
    Type: Grant
    Filed: May 7, 2012
    Date of Patent: November 18, 2014
    Assignee: Suzuki Motor Corporation
    Inventors: Toyofumi Tsuda, Fumikazu Kimata, Kazuya Miura
  • Publication number: 20140326918
    Abstract: A system and method thereof are provided for multi-stage processing of one more precursor compounds into a battery material. The system includes a mist generator, a drying chamber, one or more gas-solid separators, and one or more in-line reaction modules comprised of one or more gas-solid feeders, one or more gas-solid separators, and one or more reactors. Various gas-solid mixtures are formed within the internal plenums of the drying chamber, the gas-solid feeders, and the reactors. In addition, heated air or gas is served as the energy source within the processing system and as the gas source for forming the gas-solid mixtures to facilitate reaction rate and uniformity of the reactions therein. Precursor compounds are continuously delivered into the processing system and processed in-line through the internal plenums of the drying chamber and the reaction modules into final reaction particles useful as a battery material.
    Type: Application
    Filed: May 23, 2013
    Publication date: November 6, 2014
    Inventor: LIang-Yuh Chen
  • Publication number: 20140311913
    Abstract: A method for synthesis of nanostructured metal oxide powders. The method comprises converting the metallic material into a precipitate of metal hydroxide by an electrochemical reaction and calcinating the metal hydroxide to form the metal oxides. The method of the invention is also used for the development of cermet particulates and topological insulator particles.
    Type: Application
    Filed: April 15, 2014
    Publication date: October 23, 2014
    Applicant: UNIVERSITI BRUNEI DARUSSALAM
    Inventors: Peter Hing, Lim Chee Ming, Jung Sang Cheol, Low Siaw Huei
  • Patent number: 8864045
    Abstract: Exemplary embodiments provide materials and methods for forming monodisperse particles. In one embodiment, the monodisperse particles can be formed by first spraying a nanoparticle-containing dispersion into aerosol droplets and then heating the aerosol droplets in the presence of a shell precursor to form core-shell particles. By removing either the shell layer or the nanoparticle core of the core-shell particles, monodisperse nanoparticles can be formed.
    Type: Grant
    Filed: November 18, 2011
    Date of Patent: October 21, 2014
    Assignee: STC.UNM
    Inventors: Xingmao Jiang, C. Jeffrey Brinker
  • Patent number: 8853116
    Abstract: A method of forming composition-modified barium titanate ceramic particulate includes mixing a plurality of precursor materials and a precipitant solution to form an aqueous suspension. The plurality of precursors include barium nitrate, titanium chelate, and a metal or oxometal chelate. The precipitant solution includes tetraalkylammonium hydroxide and tetraalkylammonium oxalate. The method further includes treating the aqueous suspension at a temperature of at least 150° C. and a pressure of at least 200 psi, and separating particulate from the aqueous suspension after treating.
    Type: Grant
    Filed: May 10, 2010
    Date of Patent: October 7, 2014
    Assignee: EEStor, Inc.
    Inventors: Richard D. Weir, Carl W. Nelson
  • Publication number: 20140296062
    Abstract: A process for preparing a mesoporous metal oxide, i.e., transition metal oxide, Lanthanide metal oxide, a post-transition metal oxide and metalloid oxide. The process comprises providing an acidic mixture comprising a metal precursor, an interface modifier, a hydrotropic ion precursor, and a surfactant; and heating the acidic mixture at a temperature and for a period of time sufficient to form the mesoporous metal oxide. A mesoporous metal oxide prepared by the above process. A method of controlling nano-sized wall crystallinity and mesoporosity in mesoporous metal oxides. The method comprises providing an acidic mixture comprising a metal precursor, an interface modifier, a hydrotropic ion precursor, and a surfactant; and heating the acidic mixture at a temperature and for a period of time sufficient to control nano-sized wall crystallinity and mesoporosity in the mesoporous metal oxides. Mesoporous metal oxides and a method of tuning structural properties of mesoporous metal oxides.
    Type: Application
    Filed: September 25, 2013
    Publication date: October 2, 2014
    Applicant: UNIVERSITY OF CONNECTICUT
    Inventors: Steven L. Suib, Altug Suleyman Poyraz
  • Publication number: 20140286846
    Abstract: A process for preparing a mesoporous metal oxide, i.e., transition metal oxide, Lanthanide metal oxide, a post-transition metal oxide and metalloid oxide. The process comprises providing a micellar solution comprising a metal precursor, an interface modifier, a hydrotropic ion precursor, and a surfactant; and heating the micellar solution at a temperature and for a period of time sufficient to form the mesoporous metal oxide. A mesoporous metal oxide prepared by the above process. A method of controlling nano-sized wall crystallinity and mesoporosity in mesoporous metal oxides. The method comprises providing a micellar solution comprising a metal precursor, an interface modifier, a hydrotropic ion precursor, and a surfactant; and heating the micellar solution at a temperature and for a period of time sufficient to control nano-sized wall crystallinity and mesoporosity in the mesoporous metal oxides. Mesoporous metal oxides and a method of tuning structural properties of mesoporous metal oxides.
    Type: Application
    Filed: September 25, 2013
    Publication date: September 25, 2014
    Applicant: UNIVERSITY OF CONNECTICUT
    Inventors: Steven L. Suib, Altug Suleyman Poyraz
  • Patent number: 8840863
    Abstract: A method for the synthesis of nano-products, such as atomic titanium oxide wires. The method allows wires of anatase titanium oxide wires to be formed in a range of tunable diameters and aspect ratios in the nanometer and subnanometer size scales. The method also allows the titanium wires to be capped by oleic acid to enhance dispersing and solubility. The method allows the titanium wires to be surface doped with nitrogen species to enhance stability and functionality such as enhanced absorption in the visible wavelength region, which is useful for photodegradation of organic wastes in water by sunlight.
    Type: Grant
    Filed: August 28, 2009
    Date of Patent: September 23, 2014
    Assignee: The Hong Kong University of Science and Technology
    Inventors: Shihe Yang, Chenmin Liu