Metal Particles Patents (Class 427/191)
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Publication number: 20100003530Abstract: Provided is a magnetic graphite nanoplatelet, and a method of manufacturing nanocomposites by introducing the magnetic nanoplatelets into a composite matrix. Expanded crystalline graphite, in the form of graphite nanoplatelets, is mixed with magnetic particles to adhere the particles to the nanoplatelets. The magnetic graphite nanoplatelets are combined with a composite matrix, typically a polymer, to form a nanocomposite.Type: ApplicationFiled: July 1, 2008Publication date: January 7, 2010Inventors: Rahul Ganguli, Julia J. Mack, Vivek Mehrotra
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Patent number: 7628840Abstract: Each of the metal nano-particles present in a dispersion, which comprises at least one metal selected from the group consisting of precious metals and transition metals or an alloy of at least two metals selected from the foregoing metals, comprises a metal particle in which an organic metal compound of a fatty acid and/or an amine-metal complex is adhered to the periphery of the metal particle. This organic metal compound and the amine-metal complex are admixed together in a solvent and then the resulting mixture is subjected to a reducing treatment to thus form a dispersion containing metal nano-particles in a concentration of not less than 5% by mass and not more than 90% by mass. The resulting dispersion is applied onto the surface of a base material, followed by drying the applied layer of the dispersion and then firing the dried layer of the dispersion at a low temperature to thus form a thin metallic wire or a metal film having conductivity.Type: GrantFiled: September 7, 2004Date of Patent: December 8, 2009Assignees: ULVAC, Inc., JEMCO, Inc.Inventors: Tsutomu Atsuki, Masaaki Oda, Toshiharu Hayashi, Reiko Kiyoshima
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Publication number: 20090297704Abstract: There is provided a method for applying an improved chromium diffusion coating on an industrial item such as a turbine blade of a gas turbine engine. Chromium and other active metals are combined to form an alloy coating. Active elements include silicon, hafnium, zirconium, yttrium, tantalum, and rhenium. For producing the modified coatings through pack cementation chromium and a master alloy are mixed into a packing along with inert material and a halide activator. The packing surrounds a target in a diffusion box. The metals are then deposited by diffusion onto a target surface by pack cementation methods. The diffusion of the desired metals takes place during a coating thermal cycle. Alternatively, the diffusion can take place using an out-of-pack arrangement. Such modified coatings are utilized as improved performance coatings for environmental resistance applications over the current chromium diffusion coatings.Type: ApplicationFiled: April 30, 2004Publication date: December 3, 2009Inventor: Murali Madhava
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Patent number: 7608296Abstract: A friction stir welding anvil and method of producing a friction stir welding anvil that precludes diffusion or mechanical bonding of the anvil to the work pieces are provided. The alternatives for producing such an anvil comprise coating the anvil with diffusion barriers such as oxides, nitrides, intermetallics, and/or refractory metals; manufacturing an anvil either completely or partially from the same; or placing a coating of such materials in the form of a thin sheet or a powder between the anvil and the work pieces. The anvil disclosed herein exhibits high strength and hardness even at elevated temperatures, such as those greater than 800° C., so as to prevent the anvil from mechanically or diffusion bonding to the work pieces and so as to minimize, or eliminate altogether, anvil deformation.Type: GrantFiled: March 13, 2006Date of Patent: October 27, 2009Assignees: Brigham Young University, SII MegaDiamond, Inc., Advanced Metal ProductsInventors: Scott M. Packer, Tracy W. Nelson, Carl D. Sorensen
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Patent number: 7601389Abstract: A metal material comprises a Zn—Al—Sn based alloy (ZAS alloy) and Cu diffused in the alloy, wherein Cu is diffused into the inside of the alloy to a depth from the surface of 0.5 mm or more, the concentration of Cu decreases from the surface of the ZAS alloy towards the inside thereof, and there is present no specific interface between Cu and the ZAS alloy; and a method for producing the metal material involves applying, to the surface of the ZAS alloy, an agent comprising a solvent and, dispersed therein, a material containing Cu such as a Cu powder and a Cu—Mn alloy powder and preferably, dispersed or dissolved therein, a reducing agent capable of reducing an oxide film present on the surface of the ZAS alloy, and heating the ZAS alloy having the agent applied thereon, to thereby diffuse Cu into the alloy.Type: GrantFiled: July 31, 2003Date of Patent: October 13, 2009Assignee: Honda Giken Kogyo Kabushiki KaishaInventors: Mitsuo Kuwabara, Tadashi Okada, Naoji Yamamoto, Masahito Hasuike, Hideo Yoshikawa, Michiharu Hasegawa, Tetsuaki Aoki, Masanori Kogawa, Kazunori Sakamoto, Keizou Tanoue
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Patent number: 7592039Abstract: There are provided a method capable of mass-producing a nanotube material easily with low costs, and a nanotube material. The method of the present invention for producing a nanotube material has at least forming a metal oxide thin film or an organic/metal oxide composite thin film on an inner wall of a porous substrate and removing the porous substrate. The nanotube material of the invention has a structure provided from a body comprising a metal oxide thin film or an organic/metal oxide composite thin film formed on an inner wall of the porous substrate, from which a portion corresponding to the porous substrate is removed.Type: GrantFiled: March 17, 2004Date of Patent: September 22, 2009Assignee: RikenInventors: Jian-guo Huang, Toyoki Kunitake
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Publication number: 20090232431Abstract: In the case of a plain bearing having at least one support part (25), which is composed of an iron-containing base material, of a bearing sleeve (24) which is provided at the raceway side with a coating (8, 26) which is composed of a coating material, is formed as a melted-on layer and is metallurgically connected to the base material by means of an FeSn2-containing connecting zone (9), it is possible to obtain a long service life in that the thickness of the FeSn2-containing connecting zone (9) is at most 10 ?m.Type: ApplicationFiled: April 25, 2007Publication date: September 17, 2009Applicant: SMS DEMAG AGInventors: Konrad Roeingh, Karl Keller
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Publication number: 20090233120Abstract: A laminate comprising: an insulated substrate, an insulating resin layer having an imide bond and/or amide bond superimposed on the insulated substrate, and a metal thin film layer involving a structure having metal particles fusion bonded to each other, superimposed on the insulating resin layer, wherein the insulating resin layer sticks fast to the metal thin film layer in such a fashion that some of the fusion bonded metal particles are buried in the insulating resin layer, and wherein a metal oxide is present at a contact interface of the insulating resin layer with the metal thin film layer.Type: ApplicationFiled: February 23, 2006Publication date: September 17, 2009Inventors: Mutsuhiro Maruyama, Toshinori Kashiwagi
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Patent number: 7556720Abstract: Container for the storage and/or transportation of liquids or powders, in particular inflammables, suitable for preventing the formation of electrostatic charge, comprising a tank supported by a pallet, housed in a metallic cage and having an outer surface in contact with said metallic cage. The tank comprises a base layer of plastic material, a layer modified through plasma and a layer of metallic material deposited with vacuum PVD (Physical Vapor Deposition )technique. The metallic layer is in contact with the cage. The metallization of a plastic tank is carried out by generating in a chamber a plasma which activates the outer surface of said tank so as to form a surface layer and carrying out, with vacuum PVD technique, the deposition of a layer of conductive metallic material superposing said surface layer to obtain a tank metallized on the outside.Type: GrantFiled: June 28, 2006Date of Patent: July 7, 2009Assignee: Daviplast-Servicos de Consultoria, Sociedade Unipessoal Lda.Inventor: Virginio Cassina
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Patent number: 7553563Abstract: The invention concerns a composite material consisting of intermetallic phases and ceramic, in particular in the form of a coating on metallic substrates, as well as an arc wire spraying process for production of the composite material in which the intermetallic phases and the ceramics to be deposited are newly formed during the deposit process from the components of the supplied wires by chemical reaction. The invention further concerns wear resistant layers formed by the composites, tribologic layers and plating or hard-facing materials.Type: GrantFiled: February 9, 2004Date of Patent: June 30, 2009Assignee: Daimler AGInventors: Stefan Grau, Michael Scheydecker, Karl Weisskopf
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Publication number: 20090092823Abstract: In one embodiment, a carbide-containing article includes a carbide body with an attached optional superabrasive layer. A braze metal coating is attached to a surface the carbide substrate. The coating primarily is made of particles of a metal having a melting point of less than 1200° C., the particles having a size of less than 0.1 mm. In another embodiment, a process for applying a braze metal coating to a carbide body of a superabrasive or other article includes depositing finely divided particles of a low melting point metal onto the carbide body by spraying the particles and gas onto the body at a velocity that is between 500 km/sec and 2 km/sec, with volumetric delivery of the particles being less than 50 grams per minute.Type: ApplicationFiled: October 6, 2008Publication date: April 9, 2009Applicant: Diamond Innovations, Inc.Inventors: Steven W. Webb, Gaurav Aggarwal
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Patent number: 7507447Abstract: Disclosed is a method for producing a transparent conductive film comprising a coating step for coating a coating solution containing metal nanoparticles on a substrate to form a coated layer, a drying step for drying the coated layer and a baking step for baking the coated layer to obtain a transparent conductive film, wherein a metal in the metal nanoparticles is oxidized to a metal oxide during at least one of the coating step, the drying step and the baking step. According to this method, a transparent conductive film having a low specific resistance and a high light transmittance can be produced by coating.Type: GrantFiled: February 26, 2003Date of Patent: March 24, 2009Assignee: Fujifilm CorporationInventors: Hiroyuki Hirai, Yasushi Araki, Yoshio Tadakuma
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Patent number: 7501149Abstract: An electrode and a method for forming the electrode. The electrode comprises: a substrate; and a plurality of metal particles adhering to the substrate. The method comprises steps of: providing a substrate; providing a solution including a solvent and a plurality of metal particles on the substrate; removing the solvent; and making the plurality of metal particles adhere to the substrate.Type: GrantFiled: January 4, 2006Date of Patent: March 10, 2009Assignee: Industrial Technology Research InstituteInventors: Ying-Chiang Hu, Yii-Tay Chiou, Chun-Hsun Chu, Bor-Chen Tsai
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Publication number: 20090041935Abstract: A method is for causing, within a decompression device, a particulate base material to carry an alloy particle having a particle size smaller than that of the particulate base material, the alloy particle containing at least two elements, the method including: forming the particulate base material by a chemical deposition; causing, in the decompression device, the particulate base material to carry a microparticle element; and forming the alloy particle by alloying the particulate base material and the microparticle element.Type: ApplicationFiled: August 7, 2008Publication date: February 12, 2009Inventors: Mutsuki Yamazaki, Kohei Nakayama, Yoshihiko Nakano, Wu Mei
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Patent number: 7479299Abstract: The present invention thus provides an improved method for coating turbine engine components. The method utilizes a cold high velocity gas spray technique to coat turbine blades, compressor blades, impellers, blisks, and other turbine engine components. These methods can be used to coat a variety of surfaces thereon, thus improving the overall durability, reliability and performance of the turbine engine itself. The method includes the deposition of powders of alloys of nickel and aluminum wherein the powders are formed so as to have an amorphous microstructure. Layers of the alloys may be deposited and built up by cold high velocity gas spraying. The coated items displayed improved characteristics such as hardness, strength, and corrosion resistance.Type: GrantFiled: January 26, 2005Date of Patent: January 20, 2009Assignee: Honeywell International Inc.Inventors: Derek Raybould, Murali N. Madhava
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Patent number: 7455881Abstract: The present invention provides methods and materials for use in applying a coating on a surface of a magnesium component. The method includes the steps of: accelerating a coating powder to a velocity of between about 500 to about 1200 meters/second, wherein the coating powder comprises a material selected from the group consisting of aluminum, aluminum alloys, titanium, titanium alloys, and composites; directing the coating powder through a convergent-divergent nozzle onto the surface of the magnesium component; and forming a coating on the surface of the magnesium component so as to substantially cover the surface of the magnesium component. The coating thickness may be between approximately 0.1 to approximately 1.0 mm.Type: GrantFiled: April 25, 2005Date of Patent: November 25, 2008Assignee: Honeywell International Inc.Inventors: Derek Raybould, Murali N. Madhava, Vincent Chung, Timothy R. Duffy, Margaret Floyd
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Patent number: 7442408Abstract: The present invention is drawn toward a method of forming conductive paths on a substrate using ink-jet technology. An ink-jettable suspension or solution can be formed containing a conductive particulate having certain desired conductive properties. The suspension can then be ink-jetted onto a substrate such as ceramic, epoxy glass, or other materials in a given pattern using various ink-jet printing technologies and methods. Depending on the chosen conductive particulates, suspension components, and substrate, the printed pattern of conductive particulates may then be heated to further enhance the conductive properties of the particulates through bonding and/or sintering.Type: GrantFiled: March 26, 2002Date of Patent: October 28, 2008Assignee: Hewlett-Packard Development Company, L.P.Inventors: Thomas A. Saksa, John M. Da Cunha
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Patent number: 7437817Abstract: A process for fabricating a ceramic electroactive transducer of a predetermined shape is disclosed. The process comprises the steps of providing a suitably shaped core having an outer surface, attaching a first conductor to the outer surface of the core, coating an inner conductive electrode on the outer surface of the core such that the inner conductive electrode is in electrical communication with the first conductor, coating a ceramic layer onto the inner electrode, thereafter sintering the ceramic layer, coating an outer electrode onto the sintered ceramic layer to produce an outer electrode that is not in electrical communication with the first conductor, and then poling the sintered ceramic layer across the inner electrode and the outer electrode to produce the ceramic electrode.Type: GrantFiled: January 11, 2006Date of Patent: October 21, 2008Assignee: The Penn State Research FoundationInventors: Jindong Zhang, Robert E. Newnham
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Patent number: 7431964Abstract: A method is provided for forming a porous metal catalyst (44) on a substrate (42) for nanotube (84) growth in an emissive display. The method comprises depositing a metal (44) onto a surface of a substrate (12) at an angle (?) to the surface, depositing a metal catalyst (72) onto the metal (44), and forming nanotubes (84) on the metal catalyst (72).Type: GrantFiled: December 17, 2004Date of Patent: October 7, 2008Assignee: Motorola, Inc.Inventors: Yi Wei, Jeffrey H. Baker, Bernard F. Coll, Steven M. Smith
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Publication number: 20080220269Abstract: A camouflage material for use in a snowy environment includes a laminated, extruded polyethylene sheet; an aluminum coating on one surface of the sheet and a layer of nylon on the other surface of the sheet. The resulting white material is reflective to radar and to thermal properties which are very similar to the infrared characteristics of background snow.Type: ApplicationFiled: March 6, 2007Publication date: September 11, 2008Inventor: Jean Dumas
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Patent number: 7422769Abstract: A refractory, oxidation-resistant, and corrosion-resistant protective coating for application to a substrate, in particular for application to parts of turbines or aircraft propulsion engines, is described, including a spray coating made of a thermally sprayed, primarily metallic material, the coating being at least partially subjected to a thermochemical aluminum (Cr, Si) deposition process having a specifically high aluminum deposition activity after the application of the protective coating to the substrate, in such a way that the protective coating has alloy gradients of Al (Cr, Si) which increase from the substrate surface to the coating surface and isolated globulitic metal oxide particles. Furthermore, a method for manufacturing this protective coating and its use are described.Type: GrantFiled: July 14, 2005Date of Patent: September 9, 2008Assignee: Mtu Aero Engines GmbHInventors: Stefan Kassner, Markus Niedermeier, Horst Pillhoefer
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Publication number: 20080206460Abstract: Methods are disclosed for forming a metal substructure that will subsequently be overcoated with ceramic layers to create a dental restoration. The methods involve the steps of providing a metal powder and applying the metal powder to a die and sintering the metal powder to form a solid structure that may be used as a coping. The application of the metal powder is done in a controlled fashion while minimizing the amount of necessary handwork. These application methods include: (a) alternatingly applying an adhesive and a metal powder to the selected portion of the die surface; and (b) forming the metal powder into a viscous slurry or slip and then dipping the die therein or spraying or pouring the slurry or slip onto the selected portion of the die surface.Type: ApplicationFiled: February 14, 2008Publication date: August 28, 2008Inventors: Lawrence J. Rhoades, John Y.P. Rhoades
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Patent number: 7402277Abstract: The present invention relates to a method of forming metallic foams using cold spray processing. The method allows for the formation of metallic foams on existing substrates as a layer. The method includes the steps of providing a substrate for coating of a metallic foam; cold spraying a mixture of metal particles and a foaming agent onto the substrate to form a substrate coated with an unexpanded metallic layer; foam heat treating the substrate coated with an unexpanded metallic layer at a temperature above the decomposition temperature of the foaming agent for a time sufficient to form a heated substrate coated with an expanded metal foam layer; and cooling the heated substrate coated with an expanded metal foam layer to about ambient temperature to form a cooled substrate coated with an expanded metal foam layer. The method of forming metallic foams on substrates finds application in the oil, gas, and chemical industry by being an integral part of casings, pipelines, transfer lines, and other flow lines.Type: GrantFiled: February 7, 2006Date of Patent: July 22, 2008Assignee: ExxonMobil Research and Engineering CompanyInventors: Raghavan Ayer, Norman Pokutylowicz
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Patent number: 7393559Abstract: Methods for the production of functionally graded material (FGM) are provided. FGM is processed by powder cold spraying ceramic-metal layers, the final shape is pre-pressed by cold isostatic pressing and is then sintered using field activated sintering technique (FAST). The FGM materials can be used for medical applications.Type: GrantFiled: February 1, 2005Date of Patent: July 1, 2008Assignee: The Regents of the University of CaliforniaInventors: Joanna R Groza, Vladimir Kodash
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Patent number: 7378132Abstract: There is provided a method for depositing a modified MCrAlY coating on a surface of a gas turbine engine component. The method includes cold gas dynamic spraying techniques to provide a metallurgical bond between a substrate, such as a superalloy substrate, and the modified MCrAlY composition. The method further includes post deposition heat treatments including hot isostatic pressing. The modified MCrAlY composition includes one or more elements of Pt, Hf, Si, Zr, Ta, Re, Ru, Nb, B, and C, which improves the corrosion and environmental resistance of the coated component.Type: GrantFiled: December 14, 2004Date of Patent: May 27, 2008Assignee: Honeywell International, Inc.Inventors: Federico Renteria, Murali N. Madhava, Yiping Hu, Derek Raybould, Huu-Duc Trinh-Le
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Patent number: 7335341Abstract: A new kinetic spray process is disclosed that enables one to secure a plurality of ceramic elements together quickly without the need for glues or other adhesives. The process finds special utilization in the formation of non-thermal plasma reactors wherein the kinetic spray process can be used to simultaneously secure the ceramic elements together and to form electrical connections between like electrodes in the non-thermal plasma reactor.Type: GrantFiled: October 30, 2003Date of Patent: February 26, 2008Assignee: Delphi Technologies, Inc.Inventors: Thomas Hubert Van Steenkiste, Joseph V. Mantese, Bob Xiaobin Li, Pertrice Auguste Wethey, Robert Paul Johnston, David Emil Nelson
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Publication number: 20080038575Abstract: There is provided a method for depositing a modified MCrAlY coating on a surface of a gas turbine engine component. The method includes cold gas dynamic spraying techniques to provide a metallurgical bond between a substrate, such as a superalloy substrate, and the modified MCrAlY composition. The method further includes post deposition heat treatments including hot isostatic pressing.Type: ApplicationFiled: December 14, 2004Publication date: February 14, 2008Inventors: Federico Renteria, Murali N. Madhava, Yiping Hu, Derek Raybould, Huu-Duc Trinh-Le
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Patent number: 7267869Abstract: A conductive, corrosion-resistant coating includes a mixture of corrosion-resistant binder and highly conductive corrosion-resistant particles. The size of the particles is equal to or greater than the final thickness of the coating. After the coating is applied and cured, the surface of the coating is machined to remove the top surface layer of the binder as well as the top parts of the particles embedded in the binder, thus opening multiple direct conductive paths to the underlying substrate through the conductive particles.Type: GrantFiled: July 28, 2004Date of Patent: September 11, 2007Inventor: Leo Kriksunov
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Patent number: 7250192Abstract: A method of applying a heat-rejection coating directly on a substrate of a metallic component is disclosed. The steps include supplying a metallic component, such as of a gas turbine engine, before applying a reflective-coating mixture onto the component, wherein the reflective-coating mixture comprises a metallic pigment and a reflective-coating-mixture carrier, and wherein the step of applying is accomplished by a method selected from the group consisting of air-assisted spraying, airless spraying, brushing, and decal transfer. The component having the reflective-coating mixture thereon is fired to form a reflective coating on the component.Type: GrantFiled: December 3, 2003Date of Patent: July 31, 2007Assignee: General Electric CompanyInventors: Andrew Jay Skoog, Jane Ann Murphy, Bryan Thomas Bojanowski
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Patent number: 7244466Abstract: An improved nozzle for use in kinetic spray systems is disclosed. The nozzle includes a supersonic portion comprising a tubular section and a flow regulator. A portion of the flow regulator is received in the tubular portion. The flow regulator includes a biconical flow concentrator that allows one to create very small dimension coatings on substrates. Using the present nozzle enables one to create spot coatings and very narrow width line coatings that find use in electrical components.Type: GrantFiled: March 24, 2004Date of Patent: July 17, 2007Assignee: Delphi Technologies, Inc.Inventor: Thomas Hubert Van Steenkiste
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Patent number: 7220456Abstract: A process for the patterning of a desired substance on a surface includes: (i) charging a particle formation vessel with a compressed fluid; (ii) introducing into the particle formation vessel a first feed stream comprising a solvent and the desired substance dissolved therein and a second feed stream comprising the compressed fluid, wherein the desired substance is less soluble in the compressed fluid relative to its solubility in the solvent and the solvent is soluble in the compressed fluid, and wherein the first feed stream is dispersed in the compressed fluid, allowing extraction of the solvent into the compressed fluid and precipitation of particles of the desired substance; (iii) exhausting compressed fluid, solvent and the desired substance from the particle formation vessel at a rate substantially equal to a rate of addition of such components to the vessel in step (ii) through a restrictive passage to a lower pressure whereby the compressed fluid is transformed to a gaseous state, and wherein the reType: GrantFiled: March 31, 2004Date of Patent: May 22, 2007Assignee: Eastman Kodak CompanyInventors: Rajesh V. Mehta, Ramesh Jagannathan, Seshadri Jagannathan, David J. Nelson
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Patent number: 7208193Abstract: A method for direct writing an electrically conductive metallic feature on an insulating substrate comprises creating a gas jet comprising metallic particles (301), ejecting the gas jet comprising metallic particles through a straight bore tube (302), and impacting the gas jet comprising metallic particles onto a substrate to impinge the metallic particles on the substrate to form the electrically conductive metallic feature (303).Type: GrantFiled: September 26, 2003Date of Patent: April 24, 2007Assignee: Research Foundation of the State University of New YorkInventors: Richard Gambino, Robert Greenlaw, Shaun Kubik, Jon Longtin, Joshua Margolies, Sanjay Sampath
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Patent number: 7201940Abstract: The invention relates to devices for the treatment of heart disease and particularly to endo-arterial prostheses, which are commonly called stents. More particularly, the invention relates to methods of manufacturing and coating stents utilizing thermal spray processing (TSP). In one aspect the invention involves the use of TSP for the manufacture of fine grained tubing for subsequent use as a stent or other tubular or ring-based implant, or the manufacture of intermediate sized tubing that may then be drawn to final size tubing and for the coating of a stent. An average grain size of less than 64 microns is achieved by the invention resulting in a stent having an annular wall average thickness of about eight or more grains.Type: GrantFiled: June 12, 2001Date of Patent: April 10, 2007Assignee: Advanced Cardiovascular Systems, Inc.Inventor: Pamela A. Kramer
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Patent number: 7172663Abstract: Provided are palladium-containing powders and a method and apparatus for manufacturing the palladium-containing particles of high quality, of a small size and narrow size distribution. An aerosol is generated from liquid feed and sent to a furnace, where liquid in droplets in the aerosol is vaporized to permit formation of the desired particles, which are then collected in a particle collector. The aerosol generation involves preparation of a high quality aerosol, with a narrow droplet size distribution, with close control over droplet size and with a high droplet loading suitable for commercial applications. Powders may have high resistance to oxidation of palladium. Multi-phase particles are provided including a palladium-containing metallic phase and a second phase that is dielectric. Electronic components are provided manufacturable using the powders.Type: GrantFiled: March 2, 2004Date of Patent: February 6, 2007Assignee: Cabot CorporationInventors: Mark J. Hampden-Smith, Toivo T. Kodas, Quint H. Powell, Daniel J. Skamser, James Caruso, Clive D. Chandler
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Patent number: 7163715Abstract: Thermal spray processing and cold spray processing are utilized to manufacture porous starting materials (such as tube stock, wire and substrate sheets) from biocompatible metals, metal alloys, ceramics and polymers that may be further processed into porous medical devices, such as stents. The spray processes are also used to form porous coatings on consolidated biocompatible medical devices. The porous substrates and coatings may be used as a reservoir to hold a drug or therapeutic agent for elution in the body. The spray-formed porous substrates and coatings may be functionally graded to allow direct control of drug elution without an additional polymer topcoat. The spray processes are also used to apply the drug or agent to the porous substrate or coating when drug or agent is robust enough to withstand the temperatures and velocities of the spray process with minimal degradation.Type: GrantFiled: December 30, 2002Date of Patent: January 16, 2007Assignee: Advanced Cardiovascular Systems, Inc.Inventor: Pamela A. Kramer
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Patent number: 7128945Abstract: A method of producing a material library of surface areas having different properties is described, in which mixtures of substances are applied to a substrate by a combinatory method so that a combinatory system is obtained. At least two suspensions are used to produce the mixtures.Type: GrantFiled: August 8, 2002Date of Patent: October 31, 2006Assignee: Robert Bosch GmbHInventors: Gerd Scheying, Thomas Brinz
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Patent number: 7083850Abstract: A porous, flexible, resilient heat transfer material which comprises network of metal flakes. Such heat transfer materials are preferably produced by first forming a conductive paste comprising a volatile organic solvent and conductive metal flakes. The conductive paste is heated to a temperature below the melting point of the metal flakes, thereby evaporating the solvent and sintering the flakes only at their edges. The edges of the flakes are fused to the edges of adjacent flakes such that open pores are defined between at least some of the adjacent flakes, thereby forming a network of metal flakes. This network structure allows the heat transfer material to have a low storage modulus of less than about 10 GPa, while having good electrical resistance properties.Type: GrantFiled: October 18, 2001Date of Patent: August 1, 2006Assignee: Honeywell International Inc.Inventor: Ignatius J. Rasiah
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Patent number: 7066977Abstract: A method for producing fine or ultra fine powder particles comprising mixing a metal alkoxide with a non-metallic hydride in an organic solvent, agitating the mixed solution, and then burning the mixed solution. The burning process comprises igniting the solution directly or burning the solution in situ. A self-sustaining flame will result. When the precursor solution burns, the metallic compound will be co-fired with the organic solvent. As a result, fine or ultra fine particles of mixed metal will burst from the flame, or thrust through the flame and be synthesized.Type: GrantFiled: July 2, 2003Date of Patent: June 27, 2006Inventor: Fu-Kuo Huang
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Patent number: 7019445Abstract: A process for fabricating a ceramic electroactive transducer of a predetermined shape is disclosed. The process comprises the steps of providing a suitably shaped core having an outer surface, attaching a first conductor to the outer surface of the core, coating an inner conductive electrode on the the outer surface of the core such that the inner conductive electrode is in electrical communication with the first conductor, coating a ceramic layer onto the inner electrode, thereafter sintering the ceramic layer, coating an outer electrode onto the sintered ceramic layer to produce an outer electrode that is not in electrical communication with the first conductor, and then poling the sintered ceramic layer across the inner electrode and the outer electrode to produce the ceramic electrode.Type: GrantFiled: October 10, 2003Date of Patent: March 28, 2006Assignee: The Penn State Research FoundationInventors: Jindong Zhang, Robert E. Newnham
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Patent number: 6998151Abstract: The present invention provides a method to coat an article using a plating process, either electroless or electrolytic, whereby nickel is plated on the article using a solution that includes a suspension of powders or containing one or more of the following elements: Ni, Cr, Al, Zr, Hf, Ti, Ta, Si, Ca, Fe, Y and Ga. Optionally, the coating is then heat treated at a temperature above about 1600° F. for an effective amount of time to allow to homogenize the coating by allowing effective interdiffusion between the species. The level of aluminum may be altered to produce a coating of the predominantly ? phase of the NiAl alloy composition. Optionally, a TBC layer is applied over the predominantly ? phase NiAl alloy composition metallic bond coat.Type: GrantFiled: May 10, 2002Date of Patent: February 14, 2006Assignee: General Electric CompanyInventors: Richard Grylls, Theodore Robert Grossman
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Patent number: 6949300Abstract: The present invention is directed to a process for preparing aluminum and aluminum alloy surfaces in heat exchangers for brazing by depositing thereon a kinetic sprayed brazing composition. The process simultaneously deposits monolith or composite coatings that can include all braze materials and corrosion protection materials used in the brazing of aluminum fins to plates and tubes in a single stage.Type: GrantFiled: April 16, 2003Date of Patent: September 27, 2005Assignee: Delphi Technologies, Inc.Inventors: Bryan A. Gillispie, Zhibo Zhao, John Robert Smith, Thomas Hubert Van Steenkiste, Alaa A. Elmoursi, Yang Luo, Hartley F. Hutchins
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Patent number: 6926964Abstract: Disclosed is a fuel tank for a motor vehicle whose inner face is processed with an inorganic coating agent comprising (A) fine particles carrying silver and/or copper and (B) inorganic fine particles, and the tank inhibits oxidation of the fuel such as gasoline or light oil, and further decreases the cluster of gasoline or light oil to make finer the particle size of atomized fuel, thereby improving ignitionability and combustibility, which makes it possible to decrease imperfect combustion and to decrease substantially the consumption of the fuel.Type: GrantFiled: December 12, 2003Date of Patent: August 9, 2005Assignee: Kabushiki Kaisha NippankenkyushoInventor: Yoshio Ichikawa
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Patent number: 6911231Abstract: A method for preparing a superconducting heat transfer medium having three basic layers, the method having the steps of preparing a first layer mixture, applying the first layer mixture to a surface of a substrate so as to form a first layer, preparing a second layer mixture, applying the second layer mixture to the substrate over the first layer so as to form a second layer on top of the first layer, preparing a third layer powder, and exposing the second layer to the third layer powder so as to form a third layer on top of the second layer, thus forming the three layer superconducting heat transfer medium.Type: GrantFiled: May 3, 2002Date of Patent: June 28, 2005Assignee: New Qu Energy LimitedInventor: Yu Zhi Qu
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Patent number: 6905728Abstract: A new method for repairing turbine engine components is provided. The method utilizes a cold gas-dynamic spray technique to repair degradation on turbine blades, vanes and other components. In the cold gas-dynamic spray process particles at a temperature below their fusing temperature are accelerated and directed to a target surface on the turbine blade. When the particles strike the target surface, the kinetic energy of the particles is converted into plastic deformation of the particle, causing the particle to form a strong bond with the target surface. Post-spray processing is then performed to consolidate and homogenize the applied materials and restore integrity to the material properties in the repaired turbine component. Thus, the cold gas-dynamic spray process and post-spray processing can be employed to effectively repair degraded areas on gas turbine components.Type: GrantFiled: March 22, 2004Date of Patent: June 14, 2005Assignee: Honeywell International, Inc.Inventors: Yiping Hu, Murali Madhava, Federico Renteria
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Patent number: 6902815Abstract: There is provided a coating liquid for forming a colored transparent conductive film using ruthenium in a fine particle form, which has a satisfactory electromagnetic wave shielding effect, which is excellent in transparency, chemical resistance, and abrasion resistance, and which achieves a neutral transmitted color tone. There are provided a substrate with the colored transparent conductive film and a method for its production, and a display device having the substrate as a front panel. A coating liquid for forming a colored transparent conductive film is one characterized by containing noble metal-supporting ruthenium in a fine particle form wherein a noble metal except for ruthenium is supported in a fine particle form on ruthenium. A method for making the noble metal supported in the fine particle form is a method of adding a reducing agent into a dispersing liquid containing ruthenium particles and then adding thereinto a solvent containing a compound of a noble metal.Type: GrantFiled: December 4, 2003Date of Patent: June 7, 2005Assignee: Asahi Glass Company, LimitedInventors: Satoshi Kashiwabara, Satoshi Mototani
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Patent number: 6899914Abstract: A method of applying a marker element (6; 6?; 6?; 25; 25?; 26; 28) to an implant (1; 1?; 1?; 1??; 20; 20?), in particular a stent, intended for implantation in the human or animal body, comprising a main body and an opening (3; 3?; 3?; 3??; 21; 21?) provided in said main body (2; 2?; 2?; 2??; 22; 22?) for receiving the marker element (6; 6?; 6?; 25; 25?; 26; 28), wherein to form at least a part of the marker element (6; 6?; 6?; 25; 25?; 26; 28) a hardenable material or material mix is introduced into the opening and hardened therein.Type: GrantFiled: December 13, 2001Date of Patent: May 31, 2005Assignee: Biotronik Mess-und Therapiegeraete GmbH Ingeniurbuero BerlinInventors: Max Schaldach, Jr., Klaus-Peter Schmitz, Jens Gobrecht, Alexander Rzany, Detlef Behrend, Max Schaldach
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Patent number: 6896933Abstract: A method of maintaining a non-obstructed interior opening in a kinetic spray nozzle is disclosed. The method includes the steps of providing a mixture of particles including first particle population and a second particle population; entraining the mixture of particles into a flow of a gas at a temperature below the melt temperature of the particle populations; and directing the mixture of particles entrained in the flow of gas through a supersonic nozzle to accelerate the first particle population to a velocity sufficient to result in adherence of the first particle population on a substrate positioned opposite the nozzle. The operating conditions of the kinetic spray system are selected such that the second particle population is not accelerated to a velocity sufficient to result in adherence when it impacts the substrate.Type: GrantFiled: April 5, 2002Date of Patent: May 24, 2005Assignee: Delphi Technologies, Inc.Inventors: Thomas Hubert Van Steenkiste, John R. Smith, Daniel William Gorkiewicz, Alaa A. Elmoursi, Bryan A. Gillispie, Nilesh B. Patel
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Patent number: 6872427Abstract: A new kinetic spray process is disclosed that enables the coating to withstand severe bending and stress without delamination. The method includes use of a low pressure kinetic spray supersonic nozzle having a throat located between a converging region and a diverging region. A main gas temperature is raised to from 1000 to 1300 degrees Fahrenheit and the coating particles are directly injected into the diverging region of the nozzle at a point after the throat. The particles are entrained in the flow of the gas and accelerated to a velocity sufficient to result in partial melting of the particles upon impact on a substrate positioned opposite the nozzle and adherence of the particles to the substrate. The coating also has a desirable shinny surface. The method finds special application in coating substrates for use in formation of electrical connections.Type: GrantFiled: February 7, 2003Date of Patent: March 29, 2005Assignee: Delphi Technologies, Inc.Inventors: Thomas Hubert Van Steenkiste, Daniel William Gorkiewicz, George Albert Drew
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Patent number: 6866898Abstract: A method and related apparatus to link and/or pattern self-assembled first objects to a second object. Each of the first object (e.g., a nanoparticle) can be embedded in a mobile binder (i.e., a stabilizer). The invention applies energy to the first object and stabilizer, links this first object to the second object, and provides a controlled linkage of the first object with respect to the second object. Applying this procedure to many such objects results in a larger a real arrangement of these linked objects. An appropriate solvent may be used to remove non-linked objects, yielding a patterned array. Thermal annealing can be applied to control the physical and chemical properties of the array.Type: GrantFiled: January 14, 2003Date of Patent: March 15, 2005Assignee: International Business Machines CorporationInventors: John E. E. Baglin, Hendrik F. Hamann, Shouheng Sun
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Patent number: 6833275Abstract: A composition which contains stabilized conjugates composed of colloidal particles and biomolecules is obtained by adding a detergent to a solution containing biomolecules before or/and during treatment of colloidal particles with this solution.Type: GrantFiled: August 7, 2000Date of Patent: December 21, 2004Assignee: Roche Diagnostics GmbHInventor: Alfons Nichtl