Metal-containing Coating Patents (Class 427/376.6)
  • Patent number: 6713123
    Abstract: A piezoelectric element includes: a ceramic substrate, an electrode and a piezoelectric portion made of a piezoelectric ceramic composition containing a Pb(Mg, Ni)1/3Nb2/3O3—PbZrO3—PbTiO3 ternary system solid solution composition being represented by the following general formula (1) as a main component: Pbx{(Mg1−yNiy)1/3×aNb2/3}bTicZrdO3 (1), wherein 0.95≦x≦1.05; 0.05≦y≦0.20; 0.90≦a≦1.10; b,c, and d are decimals falling in a range surrounded by (b, c, d)=(0.550, 0.425, 0.025), (0.550, 0.325, 0.125), (0.375, 0.325, 0.300), (0.100, 0.425, 0.475), (0.100, 0.475, 0.425) and (0.375, 0.425, 0.200) in the coordinates with coordinate axes of said b, c and d, and b+c+d=1.000. The electrode is electrically connected to the piezoelectric portion, and the piezoelectric portion is solidly attached to the ceramic substrate directly or via the electrode.
    Type: Grant
    Filed: May 2, 2003
    Date of Patent: March 30, 2004
    Assignee: NGK Insulators, Ltd.
    Inventors: Toshikatsu Kashiwaya, Mutsumi Kitagawa
  • Patent number: 6676992
    Abstract: A method for coating an article includes preparing a coating precursor paint including aluminum-containing pigment particles, a temporary organic binder comprising an acrylic, and a solvent for the temporary organic binder. The coating precursor paint is applied to a surface of the article and thereafter heated to a temperature of from about 1200° F. to about 2100° F. in a non-oxidizing environment.
    Type: Grant
    Filed: August 22, 2001
    Date of Patent: January 13, 2004
    Assignee: General Electric Company
    Inventors: Jeffrey Allan Pfaendtner, Michael James Weimer, William Evan McCormack, Joseph David Rigney, Mark Lloyd Miller, John Lewis Lackman
  • Patent number: 6651871
    Abstract: A substrate is coated with a conductive layer, which comprises a conductive layer of bonded ultrafine metal particles formed on the top surface thereof. The ultrafine metal particles have a diameter of 1-20 nm, and the substrate is of a flexible high polymer material. Since the conductive layer is formed by bonded layer of the ultrafine metal particles, an extremely thin layer having high conductivity can be formed. This structure enables the formation of a flexible printed circuit board with high-density interconnects or a transparent conductive film provided with both transparency and conductivity. Conventional vacuum equipments and complicated processes are not necessary for forming the conductive layer on the substrate.
    Type: Grant
    Filed: November 18, 2002
    Date of Patent: November 25, 2003
    Assignee: Ebara Corporation
    Inventor: Naoaki Ogure
  • Patent number: 6645560
    Abstract: An environmentally resistant coating (34) for improving the oxidation resistance of a niobium-based refractory metal intermetallic composite (Nb-based RMIC) at high temperatures, the environmentally resistant coating (34) comprising silicon, titanium, chromium, and niobium. The invention includes a turbine system (10) having turbine components (11) comprising at least one Nb-based RMIC, the environmentally resistant coating (34) disposed on a surface (33) of the Nb-based RMIC, and a thermal barrier coating (42) disposed on an outer surface (40) of the environmentally resistant coating (34). Methods of making a turbine component (11) having the environmentally resistant coating (34) and coating a Nb-based RMIC substrate (32) with the environmentally resistant coating (34) are also disclosed.
    Type: Grant
    Filed: December 10, 2002
    Date of Patent: November 11, 2003
    Assignee: General Electric Company
    Inventors: Ji-Cheng Zhao, Melvin Robert Jackson, Bernard Patrick Bewlay
  • Publication number: 20030198750
    Abstract: A heat-rejection coating is applied to a metallic component of a gas turbine engine, preferably made of a nickel-base superalloy. A component surface is preferably pre-treated, as by polishing the component surface, thereafter pre-oxidizing the component surface, and thereafter applying a ceramic barrier coating onto the component surface. A reflective-coating mixture is air sprayed onto the pre-treated component surface. The reflective-coating mixture includes a metallic pigment, such as platinum, gold, palladium, and alloys thereof, and a reflective-coating-mixture carrier. The component with the reflective-coating mixture sprayed thereon is fired.
    Type: Application
    Filed: April 23, 2002
    Publication date: October 23, 2003
    Inventors: Andrew Jay Skoog, Jane Ann Murphy, John Frederick Ackerman, Paul Vincent Arszman, Bryan Thomas Bojanowski, Timothy Ray Lattire
  • Patent number: 6635339
    Abstract: The disclosed invention relates to the field of ceramics and concerns an open-cell expanded ceramic which may be used in the form of a deep-bed filter, and a process for the production thereof. The primary object is to produce an open-cell expanded ceramic by a simple and economical process. This object is attained by an open-cell expanded ceramic in which the inner cavities, cracks and the porosity of the ceramic members are filled partially or completely by one or a plurality of metal and/or ceramic phases and/or glass phases. The open-cell expanded ceramic is also produced in that during or after sintering the cavities, cracks and the porosity of the ceramic members are partially or completely filled with a melt or a suspension which melt below the melting temperature of the expanded ceramic, have a coefficient of expansion similar to the coefficient of expansion of the expanded ceramic, and a very good wetting capacity, and only react partially or not at all with constituents of the expanded ceramic.
    Type: Grant
    Filed: May 24, 1999
    Date of Patent: October 21, 2003
    Assignee: Frauhofer-Gesellschaft zur Forderung der Angewandten Forschung E V
    Inventors: Joerg Adler, Michael Teichgraeber, Gisela Standke, Helmut Jaunich, Heike Stoever, Reinhard Stoetzel
  • Publication number: 20030180451
    Abstract: A precursor composition for the deposition and formation of an electrical feature such as a conductive feature. The precursor composition advantageously has a low viscosity enabling deposition using direct-write tools. The precursor composition also has a low conversion temperature, enabling the deposition and conversion to an electrical feature on low temperature substrates. A particularly preferred precursor composition includes copper metal for the formation of highly conductive copper features.
    Type: Application
    Filed: October 4, 2002
    Publication date: September 25, 2003
    Inventors: Toivo T. Kodas, Mark J. Hampden-Smith, Karel Vanheusden, Hugh Denham, Aaron D. Stump, Allen B. Schult, Paolina Atanassova, Klaus Kunze
  • Patent number: 6605316
    Abstract: Provided are low-cost, mechanically strong, highly electronically conductive porous substrates and associated structures for solid-state electrochemical devices, techniques for forming these structures, and devices incorporating the structures. The invention provides solid state electrochemical device substrates of novel composition and techniques for forming thin electrode/membrane/electrolyte coatings on the novel or more conventional substrates. In particular, in one embodiment the invention provides techniques for co-firing of device substrate (often an electrode) with an electrolyte or membrane layer to form densified electrolyte/membrane films 5 to 20 microns thick. In another embodiment, densified electrolyte/membrane films 5 to 20 microns thick may be formed on a pre-sintered substrate by a constrained sintering process. In some cases, the substrate may be a porous metal, alloy, or non-nickel cermet incorporating one or more of the transition metals Cr, Fe, Cu and Ag, or alloys thereof.
    Type: Grant
    Filed: July 27, 2000
    Date of Patent: August 12, 2003
    Assignee: The Regents of the University of California
    Inventors: Steven J. Visco, Craig P. Jacobson, Lutgard C. DeJonghe
  • Patent number: 6599564
    Abstract: Distributed Bragg reflectors may be formed in fewer layers by the method, which is capable of producing greater differences in indexes of refraction. Group III-V alternating layers are deposited. The microstructure of alternating layers is controlled to be different. A combination of alternating polycrystalline layers or amorphous and polycrystalline layers results. Alternate ones of the layers oxidize more quickly than the others. A lateral wet oxidation of the alternate ones of the layers produces a structure with large differences in indexes of refraction between adjacent layers. The microstructure between alternating layers may be controlled by controlling Group V overpressure alone or in combination with growth temperature.
    Type: Grant
    Filed: August 9, 2000
    Date of Patent: July 29, 2003
    Assignee: The Board of Trustees of the University of Illinois
    Inventors: Kuang-Chien Hsieh, Keh-Yung Cheng
  • Publication number: 20030124342
    Abstract: An environmentally resistant coating (34) for improving the oxidation resistance of a niobium-based refractory metal intermetallic composite (Nb-based RMIC) at high temperatures, the environmentally resistant coating (34) comprising silicon, titanium, chromium, and niobium. The invention includes a turbine system (10) having turbine components (11) comprising at least one Nb-based RMIC, the environmentally resistant coating (34) disposed on a surface (33) of the Nb-based RMIC, and a thermal barrier coating (42) disposed on an outer surface (40) of the environmentally resistant coating (34). Methods of making a turbine component (11) having the environmentally resistant coating (34) and coating a Nb-based RMIC substrate (32) with the environmentally resistant coating (34) are also disclosed.
    Type: Application
    Filed: December 10, 2002
    Publication date: July 3, 2003
    Inventors: Ji-Cheng Zhao, Melvin Robert Jackson, Bernard Patrick Bewlay
  • Publication number: 20030124259
    Abstract: A precursor composition for the deposition and formation of an electrical feature such as a conductive feature. The precursor composition advantageously has a viscosity of at least about 1000 centipoise and can be deposited by screen printing. The precursor composition also has a low conversion temperature, enabling the deposition and conversion to an electrical feature on low temperature substrates. A particularly preferred precursor composition includes silver and/or copper metal for the formation of highly conductive features.
    Type: Application
    Filed: October 4, 2002
    Publication date: July 3, 2003
    Inventors: Toivo T. Kodas, Mark J. Hampden-Smith, Karel Vanheusden, Hugh Denham, Aaron D. Stump, Allen B. Schult, Paolina Atanassova, Klaus Kunze
  • Patent number: 6585878
    Abstract: A thermal barrier coating for nickel based superalloy articles such as turbine engine vanes and blades that are exposed to high temperature gas is disclosed. The coating includes a columnar grained ceramic layer applied to a platinum modified Ni3Al gamma prime phase bond coat having a high purity alumina scale. The preferred composition of the bond coat is 5 to 16% by weight of aluminum, 5 to 25% by weight of platinum with the balance, at least 50% by weight, nickel. A method for making the bond coat is also disclosed.
    Type: Grant
    Filed: August 7, 2002
    Date of Patent: July 1, 2003
    Assignee: Honeywell International, Inc.
    Inventors: Thomas E. Strangman, Derek Raybould
  • Patent number: 6586052
    Abstract: A method for coating a nickel- or cobalt-based superalloy surface by slurry deposition/heat diffusion. The method includes preparing a slurry of a metal coating powder mixed into an adhesive carrier that will burn off ash-free during a diffusion cycle, depositing the slurry onto the surface of a Ni- or Co-based superalloy material to form a coated surface, and heating the coated surface to a temperature of at least about 1600° F. to diffuse the metal coating powder into the metal substrate.
    Type: Grant
    Filed: September 21, 2001
    Date of Patent: July 1, 2003
    Assignee: Rolls-Royce Corporation
    Inventors: George Edward Creech, Kevin E. Garing
  • Patent number: 6541075
    Abstract: An article includes a substrate and an adhesion layer overlying the substrate. The adhesion layer includes a first phase including particles, and a second phase including braze alloy that bonds the particles to the substrate. The article further includes a ceramic layer overlying the adhesion layer. In one embodiment, the ceramic layer is a thermal barrier coating (TBC), formed of stabilized zirconia (ZrO2).
    Type: Grant
    Filed: February 12, 2001
    Date of Patent: April 1, 2003
    Assignee: General Electric Company
    Inventors: Wayne Charles Hasz, Jeffrey Allen Conner
  • Patent number: 6528123
    Abstract: This invention relates to a method for preparing the surface of a ceramic component that enables direct brazing using a non-active braze alloy. The present invention also relates to a method for directly brazing a ceramic component to a ceramic or metal member using this method of surface preparation, and to articles produced by using this brazing method. The ceramic can be high purity alumina. The method comprises applying a first coating of a silicon-bearing oxide material (e.g. silicon dioxide or mullite (3Al2O3.2SiO2) to the ceramic. Next, a thin coating of active metal (e.g. Ti or V) is applied. Finally, a thicker coating of a non-active metal (e.g. Au or Cu) is applied. The coatings can be applied by physical vapor deposition (PVD). Alternatively, the active and non-active metals can be co-deposited (e.g. by sputtering a target made of mullite).
    Type: Grant
    Filed: June 28, 2000
    Date of Patent: March 4, 2003
    Assignee: Sandia Corporation
    Inventors: Charles H. Cadden, F. Michael Hosking
  • Patent number: 6528112
    Abstract: The present invention relates to a transparent conductive layered structure having a transparent substrate and a transparent conductive layer and transparent coating layer formed in succession on this substrate, used in, for instance, the front panel of CRT, etc., display devices. The main components of said transparent conductive layer are noble metal microparticles with a mean particle diameter of 1 to 100 nm, wherein the microparticles are made from gold and/or platinum and silver and the gold and/or platinum content is within a range exceeding 50 wt % up to 95 wt %, and a binder matrix.
    Type: Grant
    Filed: April 30, 2002
    Date of Patent: March 4, 2003
    Assignee: Sumitomo Metal Mining Co., Ltd.
    Inventors: Kenji Kato, Masaya Yukinobu
  • Patent number: 6514389
    Abstract: A workpiece is processed which includes a multiplicity of recesses formed in the exposed surface. The invention includes depositing a first barrier layer 13 of for example, titanium nitride, a second layer 11 of aluminium alloy and a third relatively thin layer 12 of titanium nitride and then exposing the sandwich of layers to elevated heat and pressure so that the second layer is deformed to fill the recesses 10.
    Type: Grant
    Filed: October 8, 1996
    Date of Patent: February 4, 2003
    Assignee: Trikon Technologies Limited
    Inventors: Paul Rich, David John Thomas
  • Publication number: 20030017270
    Abstract: A thermal barrier coating for nickel based superalloy articles such as turbine engine vanes and blades that are exposed to high temperature gas is disclosed. The coating includes a columnar grained ceramic layer applied to a platinum modified Ni3Al gamma prime phase bond coat having a high purity alumina scale. The preferred composition of the bond coat is 5 to 16% by weight of aluminum, 5 to 25% by weight of platinum with the balance, at least 50% by weight, nickel. A method for making the bond coat is also disclosed.
    Type: Application
    Filed: August 7, 2002
    Publication date: January 23, 2003
    Inventors: Thomas E. Strangman, Derek Raybould
  • Patent number: 6503572
    Abstract: Improved silicon carbide composites made by an infiltration process feature a metal phase in addition to any residual silicon phase. Not only are properties such as mechanical toughness improved, but the infiltrant can be so engineered as to have much diminished amounts of expansion upon solidification, thereby enhancing net-shape-making capabilities. Further, multi-component infiltrant materials may have a lower liquidus temperature than pure silicon, thereby providing the practitioner greater control over the infiltration process. In particular, the infiltration may be conducted at the lower temperatures, where low-cost but effective bedding or barrier materials can terminate the infiltration process once the infiltrant has migrated through the permeable mass up to the boundary between the mass and the bedding material.
    Type: Grant
    Filed: July 21, 2000
    Date of Patent: January 7, 2003
    Assignee: M Cubed Technologies, Inc.
    Inventors: W. Michael Waggoner, Barry R. Rossing, Michael A. Richmond, Michael K. Aghajanian, Allyn L. McCormick
  • Patent number: 6497920
    Abstract: An internal passage of an article such as a gas turbine airfoil is coated with an aluminum-containing coating. To accomplish this coating process, a coating slurry of a mixture of a carrier component of water and a hectorite clay or a bentonite clay, together with a solids component of a source of aluminum, a halide activator, and an oxide dispersant, is prepared. The coating slurry is applied to the internal passage of the gas turbine airfoil and dried. The gas turbine airfoil and the applied coating slurry are heated to form an aluminum-containing coating bonded to the internal passage of the gas turbine airfoil. Excess coating material is removed from the article internal passage.
    Type: Grant
    Filed: September 6, 2000
    Date of Patent: December 24, 2002
    Assignee: General Electric Company
    Inventors: Jeffrey Allan Pfaendtner, Joseph David Rigney, Nripendra Nath Das, Michael James Weimer, John Lewis Lackman
  • Patent number: 6488986
    Abstract: A method for imparting an aluminide coating to an alloy gas turbine engine component, heat treating the component, and quenching the component. The component is exposed to a source of aluminum at an elevated temperature in a coating furnace to deposit an aluminum-based oxidation barrier on the component, heated in the coating furnace to a temperature of at least the solution temperature of the alloy, and quenched by flowing a chilled inert gas around the component in the coating furnace to cool the component from the temperature of at least the solution temperature of the alloy to a temperature at which a gamma′ phase of the alloy is set in the alloy in less than about 10 minutes.
    Type: Grant
    Filed: January 29, 2001
    Date of Patent: December 3, 2002
    Assignee: General Electric Company
    Inventors: Nripendra N. Das, Terri K. Brown, Matthew D. Saylor, Brian H. Pilsner, Carl H. Snyder
  • Patent number: 6488981
    Abstract: A method of manufacturing a touch screen panel, the method including applying a resistive coating to one surface of an insulative substrate, applying an insulative protective coating to the resistive coating, depositing a conductive edge electrode pattern including a plurality of edge electrodes on the protective coating, and firing the panel until the edge electrodes etch through the protective coating and make electrical contact with the resistive coating.
    Type: Grant
    Filed: June 20, 2001
    Date of Patent: December 3, 2002
    Assignee: 3M Innovative Properties Company
    Inventors: Paul J. Richter, Michael J. Kardauskas, Frank J. Bottari
  • Patent number: 6482469
    Abstract: A thermal barrier coating (TBC) system and method for improving the thermal fatigue life of a thermal barrier coating. The invention entails modifying the surface morphology of an aluminide bond coat that adheres the thermal barrier coating to a substrate of a superalloy component. The aluminide bond coat has columnar grains, such that grain boundaries are exposed at the surface of the bond coat and define ridges. The surface of the bond coat is then treated so that a sufficient amount of material is removed from the grain boundary ridges and other surface peaks to flatten the bond coat surface, i.e., the ridges and peaks are replaced with flattened surfaces that are nearly parallel to the diffusion zone of the bond coat. By removing these surface irregularities, it is believed that a more stable bond coat surface is created where the critical alumina-bond coat interface will exist following a thermal treatment, such as TBC deposition.
    Type: Grant
    Filed: April 11, 2000
    Date of Patent: November 19, 2002
    Assignee: General Electric Company
    Inventors: Irene T. Spitsberg, Ramgopal Darolia
  • Publication number: 20020168478
    Abstract: The present invention relates to a transparent conductive layered structure having a transparent substrate and a transparent conductive layer and transparent coating layer formed in succession on this substrate, used in, for instance, the front panel of CRT, etc., display devices. The main components of said transparent conductive layer are noble metal microparticles with a mean particle diameter of 1 to 100 nm, wherein the microparticles are made from gold and/or platinum and silver and the gold and/or platinum content is within a range exceeding 50 wt % up to 95 wt %, and a binder matrix.
    Type: Application
    Filed: April 30, 2002
    Publication date: November 14, 2002
    Applicant: SUMITOMO METAL MINING CO., LTD.
    Inventors: Kenji Kato, Masaya Yukinobu
  • Patent number: 6475558
    Abstract: An over the highway heavy duty vehicle in the form of a selected one of a truck and a tractor is disclosed. The vehicle has a frame rail having a through aperture. A conductive solder ring is bonded to the rail and surrounds the aperture. A fastener extends through the aperture to secure an electrical connector in electrically conductive engagement with the ring. A ground cable is connected to the connector. A process for forming the ring is also disclosed.
    Type: Grant
    Filed: February 26, 2001
    Date of Patent: November 5, 2002
    Assignee: Volvo Trucks North America, Inc.
    Inventor: Frank T. Baginski
  • Patent number: 6457234
    Abstract: A self-aligned (i.e., spatially selective) process for fabricating a corrosion-resistant conductive pad on a substrate, and an associated structure that includes an interconnect to allow a terminal connection to the conductive pad (e.g., a chip-to-package connection). The conductive pad may include a metal such as copper, aluminum, or tungsten. The self-aligned process generates a metallic layer on an initially exposed metal layer, wherein the metallic layer is electrically conductive and corrosion resistant. The process may be accomplished by providing a substrate having a metal layer with an exposed surface, depositing a second metal layer on the exposed surface, annealing the substrate to alloy a portion of the metal layer that includes the exposed surface and a portion of the second metal layer, and removing the unalloyed portion of the second metal layer.
    Type: Grant
    Filed: May 14, 1999
    Date of Patent: October 1, 2002
    Assignee: International Business Machines Corporation
    Inventors: Daniel C. Edelstein, Judith M. Rubino, Carlos J. Sambucetti, Anthony K. Stamper
  • Patent number: 6447924
    Abstract: A gamma titanium aluminide turbine blade (10) has a titanium oxide layer (20) on its outer surface. A protective coating (22) is applied to the aerofoil (12) and the platform (14) of the turbine blade (10) onto the titanium oxide layer (20). The protective coating (22) comprises a silicate glass having a chromium oxide filler. The protective coating (22) preferably comprise a boron titanate silicate glass having a chromium oxide filler. The oxide layer (20) adheres the protective coating (22) to the titanium aluminide turbine blade (10). The protective coating (22) provides oxidation and sulphidation resistance.
    Type: Grant
    Filed: September 24, 1999
    Date of Patent: September 10, 2002
    Assignee: Rolls-Royce plc
    Inventor: David F Bettridge
  • Patent number: 6447910
    Abstract: Disclosed is a powder consisting of composite barium titanate particles having surface deposition of a water-insoluble rare earth compound such as yttrium oxide. The powder is used advantageously as a base material for the preparation of a sintered body such as ceramic capacitors of small thickness or compact size as compared with conventional powder blends of barium titanate particles and yttrium oxide particles in respect of greatly improved uniformity in the distribution of the yttrium element. The composite barium titanate particles with surface deposition of yttrium oxide can be prepared by conducting hydrolysis of urea in an aqueous medium containing a water-soluble yttrium salt dissolved therein in the presence of barium titanate particles to deposit basic yttrium carbonate on the particle surface followed by calcination of the particles to convert the basic yttrium carbonate into yttrium oxide.
    Type: Grant
    Filed: January 28, 2000
    Date of Patent: September 10, 2002
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Kazuhiro Wataya
  • Patent number: 6436479
    Abstract: Disclosed is a method of forming a nickel metal thin film, comprising the steps of coating a substrate with a solution for forming a nickel metal thin film, the solution being formed of an alcohol solution containing nickel ions and a reducible chelate type ligand having a hydrazone unit so as to form a gel film, and subjecting the resultant gel film to a heat treatment under an inert gas atmosphere.
    Type: Grant
    Filed: December 13, 2000
    Date of Patent: August 20, 2002
    Assignee: President of Gifu University
    Inventors: Yasutaka Takahashi, Yutaka Ohya, Takayuki Ban
  • Patent number: 6432570
    Abstract: The invention relates to a fuel electrode for high-temperature solid electrolyte fuel cells and a process for manufacture of the electrode. The fuel electrode of the invention is a porous element composed of a high-melting metal, such as ruthenium, osmium, rhodium or iridium, or an alloy containing the metal. The process for manufacture of the fuel electrode comprises coating an electrode material with a solution or dispersion of the high-melting metal and/or its chloride, sintering the same and finally reducing the product.
    Type: Grant
    Filed: April 25, 2000
    Date of Patent: August 13, 2002
    Assignee: Osaka Gas Company Limited
    Inventors: Masamichi Ippommatsu, Minoru Suzuki, Hirokazu Sasaki, Shoji Otoshi, Hisao Ohnishi
  • Patent number: 6413589
    Abstract: A method of coating a ceramic and bonding ceramic onto a substrate for practical uses over 630° C. includes forming a brazed bonding layer at a contact area between the ceramic and the substrate by a fluidic reaction and causing the bonding layer to wet both the ceramic and substrate with a wetting angle of 0-5° to thereby coat and bond the ceramic onto bond the substrate over the entire contact area with a continuous, essentially 100% dense bonding layer. The bonding layer is so free of bonding defects that the resulting bonded product can withstand repeated thermal shocks by quenching in 0° ice water from a temperature in the range of 630-980° C.
    Type: Grant
    Filed: June 8, 1995
    Date of Patent: July 2, 2002
    Inventor: Chou H. Li
  • Publication number: 20020051848
    Abstract: A method of coating a ceramic onto a substrate, comprising:
    Type: Application
    Filed: June 8, 1995
    Publication date: May 2, 2002
    Inventor: CHOU H. LI
  • Patent number: 6368394
    Abstract: A heat curable bonding composition for providing a coating to a solid substrate comprises water, phosphate ions, borate ions, and aluminum ions. The bonding composition has a pH in the range from about 1.4 to about 2.2, and is substantially free of chromate ions, molybdate ions, and magnesium ions.
    Type: Grant
    Filed: October 18, 1999
    Date of Patent: April 9, 2002
    Assignee: Sermatech International, Inc.
    Inventors: John E. Hughes, Mark F. Mosser, Kevin B. Eddinger, Ronald E. Myers
  • Publication number: 20020018845
    Abstract: A method for manufacturing an electron-emitting device processing an electroconductive film upon which an electron-emission region is formed is characterized in that the formation process of formation of the electron-emission region includes a process of application of metal compound-containing material and film thickness controlling agent to the substrate.
    Type: Application
    Filed: August 24, 2001
    Publication date: February 14, 2002
    Inventors: Yasuo Takahashi, Naoko Miura
  • Patent number: 6342301
    Abstract: The present invention aims at providing a material for a diamond sintered compact tool, which has a high strength and is available as a material for a cutting tool. Accordingly, the present invention is concerned with a diamond sintered compact comprising a WC-Co type cemented carbide substrate having slight undulation and a diamond sintered compact bonded to one surface of the substrate by sintering during a step of sintering at an ultra-high pressure and high temperature, which has a plate thickness is 0.5 mm to 5 mm and an outer diameter is at least 20 mm and whose diamond sintered compact layer has at least 50% of a thickness area within a range of 0.05 mm to 0.4 mm and contains Co diffusing from the cemented carbide substrate.
    Type: Grant
    Filed: July 28, 1999
    Date of Patent: January 29, 2002
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Katsuhito Yoshida, Michinari Asano, Junichi Shiraishi, Tetsuo Nakai
  • Patent number: 6284316
    Abstract: A titanium layer is formed on a substrate with chemical vapor deposition (CVD). First, a seed layer is formed on the substrate by combining a first precursor with a reducing agent by CVD. Then, the titanium layer is formed on the substrate by combining a second precursor with the seed layer by CVD. The titanium layer is used to form contacts to active areas of substrate and for the formation of interlevel vias.
    Type: Grant
    Filed: January 20, 2000
    Date of Patent: September 4, 2001
    Assignee: Micron Technology, Inc.
    Inventors: Gurtej Singh Sandhu, Donald L. Westmoreland
  • Publication number: 20010004477
    Abstract: A solution containing a metal component comprises composite ultrafine metal particles each having a core substantially made of a metal component and a covering layer made of an organic compound chemically bonded to the core. The core has an average diameter ranging from 1 to 10 nm. The composite ultrafine metal particles are uniformly dispersed in a solvent.
    Type: Application
    Filed: December 11, 2000
    Publication date: June 21, 2001
    Inventors: Akira Fukunaga, Hiroshi Nagasawa, Takao Kato
  • Publication number: 20010003631
    Abstract: The method serves for the sealing of porous layers (10) at body surfaces (11), in particular of thermal spray layers of a ceramic coating material. Communicating capillary spaces (12) in the layer (10) have openings at the surface (11). A liquid (2) is used as a sealing medium which consists of a solvent and at least one oxidizable metal which is contained therein.
    Type: Application
    Filed: December 6, 2000
    Publication date: June 14, 2001
    Applicant: Sulzer Innotec AG
    Inventors: Raoul Patrick Villiger, Emad Batawi
  • Patent number: 6242050
    Abstract: A method of providing a roughened bond coat, for example in a thermal barrier coating system, comprises providing an oxidation-resistant plasma-sprayed layer onto a substrate and disposing a slurry overlayer on the oxidation-resistant plasma-sprayed layer. These steps form a roughened bond coat possessing an uneven, undulated, and irregular surface. A roughened bond coat in a thermal barrier coating system reduces de-bonding of the bond coat and a thermal barrier coating layer, which is desirable to maintain the insulation features of the thermal barrier coating system.
    Type: Grant
    Filed: November 24, 1998
    Date of Patent: June 5, 2001
    Assignee: General Electric Company
    Inventors: Ann Melinda Ritter, Melvin Robert Jackson, Curtis Alan Johnson
  • Patent number: 6232004
    Abstract: The present invention provides methods for treating ceramic materials, including oxide ceramic materials such as zirconia, with a treatment agent comprising a metallic material, such as titanium, by contacting a surface of the ceramic material with the treatment agent and heating the assembly to a temperature at which the ceramic material incorporates a portion of the metallic material by diffusion. The treated ceramic material is uniformly darkened and exhibits improved structural and physical properties.
    Type: Grant
    Filed: January 22, 1999
    Date of Patent: May 15, 2001
    Assignee: Pacific Coast Technologies, Inc.
    Inventor: Brian J. Lasater
  • Patent number: 6224657
    Abstract: A heat curable bonding composition of the present invention comprises an aqueous solution containing phosphate ion (PO4−3) and chromium(III) ion (Cr+3, or trivalent chromium) and is substantially free of hexavalent chromium ions. The bonding composition may further contain at least one secondary cationic species. The bonding composition has a pH in the range of about 1 to about 3.5.
    Type: Grant
    Filed: October 13, 1998
    Date of Patent: May 1, 2001
    Assignee: Sermatech International, Inc.
    Inventors: Ronald E. Myers, Mark F. Mosser, Kevin B. Eddinger, John E. Hughes
  • Patent number: 6210791
    Abstract: A coated article suitable for use at elevated temperature is formed of a substrate made from metal or a ceramic, a diffuse reflective barrier coating overlying the substrate, and a low-emissivity top coat covering the diffuse reflective barrier coating. The diffuse reflective barrier coating includes a transmissive medium having a transmissive-medium index of refraction, and a plurality of radiation-scattering centers distributed in the transmissive medium, the radiation-scattering centers having a scattering-center index of refraction different from the transmissive-medium index of refraction. The radiation scattering centers may be voids or second ceramic particles. The diffuse reflective barrier coating has a surface roughness of less than about 150 microinches RMS.
    Type: Grant
    Filed: June 16, 1999
    Date of Patent: April 3, 2001
    Assignee: General Electric Company
    Inventors: Andrew J. Skoog, Jane A. Murphy, William R. Stowell
  • Patent number: 6197437
    Abstract: A composite barrel for use in extrusion or injection molding is disclosed. The composite barrel includes an outer housing having a cylindrical bore that extends throughout the length of the outer housing. A wear-resistant lining is disposed on an interior surface that defines the cylindrical bore. The lining is fabricated from an alloy that includes a base metal and phosphorus and the lining may contain hard abrasion-resistant particulate, such as tungsten carbide. The base metal is nickel or cobalt or a mixture of nickel and cobalt. The alloy is typically applied by centrifugal casting and can be cast in a nitrogen-rich atmosphere without creating undesirable lining porosity. Such linings can be made for a fraction of the cost of comparable linings that must be cast under vacuum or in an atmosphere of argon.
    Type: Grant
    Filed: February 22, 1999
    Date of Patent: March 6, 2001
    Assignee: Wall Colmonoy Corporation
    Inventors: David Martin Bielec, Samuel Conrad DuBois, Subramaniam Rangaswamy
  • Patent number: 6194069
    Abstract: A process for the production of insulator-coated black particles, which comprises the steps of (1-a) dispersing particles of silica or a metal oxide in an alcohol-based solvent consisting mainly of an intermediate alcohol to obtain a dispersion of the above particles, (1-c) forming a titanium oxide coating of TiO2 on the surface of each of the particles whose surfaces have been activated in the above step, to obtain titanium oxide-coated particles, (1-d) calcining the titanium oxide-coated particles obtained in the above step in a reducing and/or nitriding atmosphere and thereby blackening the above titanium oxide coatings to obtain black particles, and (1-e) forming an electrical insulator coating on a surface of each of the black particles obtained in the above step, to obtain insulator-coated black particles; characerized in that the process includes a step of (1-b) adding an alkaline aqueous solution to the dispersion obtained instep (1-a) to activate a surface of each of the particles of a metal oxi
    Type: Grant
    Filed: July 29, 1999
    Date of Patent: February 27, 2001
    Assignee: Ube Nitto Kasei Co., Ltd.
    Inventors: Tatsuhiko Adachi, Kazuhiko Sakai, Norihiro Nakayama, Kenichi Fujino, Hidekazu Takagi