Heating Or Fusing Applied Coating Patents (Class 427/461)
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Patent number: 8420747Abstract: A thermosetting polymer material capable of being used in powder coatings. The thermosetting polymer material includes at least one hydroxyl functional aliphatic polycarbonates that is formulated and crosslinked with isocyanates to yield a thermoset organic coating material. These materials provide improved weatherability as compared to prior art powder coating materials while also being less expensive than prior art materials utilizing fluorinated polymers.Type: GrantFiled: July 17, 2008Date of Patent: April 16, 2013Assignee: Sabic Innovative Plastics IP B.V.Inventors: Jon M Malinoski, Paul D Sybert, Christopher Michael Eastman, Sumeet Jain, Rainer Koeniger, Michael Todd Luttrell, Glen David Merfeld, James Edward Pickett, Jason Joseph Testa
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Patent number: 8420180Abstract: Electrostatic deposition of high performance powdered materials onto gas turbine surfaces. The process also includes post-deposition thermal staging of the deposited powder to provide a durable coating that will satisfy the demands of turbine engine operation. The process envisions application of organic-based powdered materials, glass/ceramic powdered materials and metal-based powdered materials and combinations thereof using electrostatic techniques to components exposed to low temperature operations, such as may be found in the front section of a gas turbine engine or to the exterior portions of an aircraft engine, and metal-containing glass ceramics, glass-ceramic materials, or materials that can be transformed into glass ceramic materials, when applied to components exposed to high temperature operations, such as may be found in the turbine and exhaust sections of a gas turbine engine or the flaps of an aircraft.Type: GrantFiled: December 24, 2008Date of Patent: April 16, 2013Assignee: General Electric CompanyInventors: Matthew B. Buczek, Andrew J. Skoog, Mark Rechtsteiner, Jane Ann Murphy
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Patent number: 8293338Abstract: A method of applying a protective coating over ink printed media in a digital printing engine whereby horizontally discharging ink jet nozzles arranged in a vertical array, discharging a protective coating onto the marked surface of media disposed on a belt in vertical disposition. The coated media is then transported vertically to an adjacent source of ultraviolet radiation for curing the protective coating.Type: GrantFiled: April 15, 2008Date of Patent: October 23, 2012Assignee: Xerox CorporationInventors: Vittorio Castelli, Gregory Joseph Kovacs
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Patent number: 8007692Abstract: It is aimed at providing: a coating liquid for nickel film formation suitable for forming a nickel film combinedly possessing an excellent electroconductivity and an excellent film-forming ability (surface flatness), by a coating method, particularly inkjet printing; a nickel film obtained by using the nickel film formation coating liquid; and a production method of such a nickel film. A coating liquid for nickel film formation comprises: nickel formate; and an amine based solvent having a boiling point within a range between 180° C. inclusive and 300° C. exclusive, as a main solvent, thereby allowing obtainment of a coating liquid for nickel film formation suitable for inkjet printing; and there can be obtained a uniform and flat nickel film having a low resistance and being excellent in film strength (adhesion force), by coating the nickel film formation coating liquid onto a substrate; drying the coated coating liquid; and subsequently calcining the dried coating liquid at a temperature of 200° C.Type: GrantFiled: June 16, 2006Date of Patent: August 30, 2011Assignee: Sumitomo Metal Mining Co., Ltd.Inventors: Yoshihiro Otsuka, Masaya Yukinobu
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Patent number: 7972660Abstract: The present invention pertains to a process for forming a coating on a substrate using a tribo-charging electrostatic fluidized bed process; characterized in that a powder coating is used which has a particle size distribution such that a) d(v,90)?42.5 ?m, and b) i) the percentage of particles <10 ?m in size is ?12% by volume, and/or ii) [d(s,90)÷d(s,10)]2?3.5, [d(s,90)?7]d(s,90) being greater than 7 ?m and d(s,90) and d(s,10) being measured in microns.Type: GrantFiled: July 11, 2006Date of Patent: July 5, 2011Assignee: Akzo Nobel Coatings International B.V.Inventors: John Ring, Michele Falcone, Robert Edward Barker, Andrew George Cordiner
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Patent number: 7951427Abstract: The invention relates to thermosetting powder compositions which give coatings proving remarkable weatherability, excellent mechanical properties and an outstanding flow containing a binder which comprises a mixture of amorphous polyesters (A) containing from 50 to 100 mol % of isophthalic acid and from 70 to 100 mol % of neopentyl glycol, and (B) which comprises from 75 to 100 mol % of at least one straight-chain saturated di-carboxylic aliphatic acid having from 4 to 14 carbon atoms and from 75 to 100 mol % of at least one branched chain aliphatic diol.Type: GrantFiled: May 15, 2006Date of Patent: May 31, 2011Assignee: Cytec Surface Specialties, S.A.Inventors: Luc Moens, Nele Knoops, Daniel Maetens
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Patent number: 7935755Abstract: A method for forming a heat sealable coating on a substrate, wherein the substrate is formed from at least one oriented polymer is shown. The method includes depositing an aqueous polymer dispersion on the substrate, wherein the aqueous polymer dispersion includes (A) at least one thermoplastic resin; (B) at least one dispersing agent; and (C) water; wherein the dispersion has a pH of less than 12, and drying the dispersion to form a first layer.Type: GrantFiled: June 15, 2010Date of Patent: May 3, 2011Assignee: Dow Global Technologies LLCInventors: Brad M. Moncla, Sarah T. Eckersley, Ralph G. Czerepinksi, Charles F. Diehl, Matthew J. Kalinowski, Dale C. Schmidt
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Patent number: 7794799Abstract: A method for manufacturing an array plate for biomolecules includes coating a surface of a substrate with a hydrophobic material to form a hydrophobic layer having initial hydrophobic properties, etching the hydrophobic layer through an etch mask placed thereon to form a hydrophilic binding site, removing the etch mask, and processing the remaining region of the hydrophobic layer to recover the initial hydrophobic properties. A method for manufacturing a biochip using this array plate, includes processing the surface of the hydrophilic binding site of the array plate to increase an affinity of biomolecules to the hydrophilic binding site, and applying a solution containing biomolecules to the surface of the hydrophilic binding site.Type: GrantFiled: May 15, 2003Date of Patent: September 14, 2010Assignee: Samsung Electronics Co., Ltd.Inventors: Woon-bae Kim, Chang-ho Cho, Kae-dong Back, Hwan-young Choi
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Publication number: 20100216917Abstract: A thermosetting polymer material capable of being used in powder coatings. The thermosetting polymer material includes at least one hydroxyl functional aliphatic polycarbonates that is formulated and crosslinked with isocyanates to yield a thermoset organic coating material. These materials provide improved weatherability as compared to prior art powder coating materials while also being less expensive than prior art materials utilizing fluorinated polymers.Type: ApplicationFiled: July 17, 2008Publication date: August 26, 2010Applicant: SABIC INNOVATIVE PLASTICS IP B.V.Inventors: Jon M. Malinoski, Paul D. Sybert, Christopher Michael Eastman, Sumeet Jain, Rainer Koeniger, Michael Todd Luttrell, Glen David Merfeld, James Edward Pickett, Jason Joseph Testa
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Patent number: 7763676Abstract: A method for forming a heat sealable coating on a substrate, wherein the substrate is formed from at least one oriented polymer is shown. The method includes depositing an aqueous polymer dispersion on the substrate, wherein the aqueous polymer dispersion includes (A) at least one thermoplastic resin; (B) at least one dispersing agent; and (C) water; wherein the dispersion has a pH of less than 12, and drying the dispersion to form a first layer.Type: GrantFiled: February 28, 2005Date of Patent: July 27, 2010Assignee: Dow Global Technologies Inc.Inventors: Brad Maurice Moncla, Sarah T. Eckersley, Ralph G. Czerepinski, Charles F. Diehl, Matthew James Kalinowski, Dale C. Schmidt
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Publication number: 20100143605Abstract: An apparatus and related method for forming a three-dimensional polymer based part including a die tool having a specified shape and size and exhibiting an exposed polymer adhering surface corresponding in configuration to a polymeric based part to be created. A volume holding bin supports a three-dimensional article including at least one exposed and pattern defining surface. A volume of a granulated polymer material is deposited into the bin and around the article. A sub-volume of the material adheres to and forms a hardened layer upon the exposed pattern defining surface, a corresponding part created having a specified thickness and matching configuration.Type: ApplicationFiled: February 10, 2010Publication date: June 10, 2010Inventor: Miguel A. Linares
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Patent number: 7674401Abstract: The present invention relates to a metal oxide dispersion, which can form a metal thin film onto a substrate by heat treatment at a low temperature, wherein a metal oxide having a particle diameter of less than 200 nm is dispersed in the dispersion medium. By heat treating the dispersion after applying it onto a substrate, a metal thin film is formed.Type: GrantFiled: December 16, 2002Date of Patent: March 9, 2010Assignee: Asahi Kasei Kabushiki KaishaInventor: Mutsuhiro Maruyama
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Publication number: 20080286481Abstract: The present invention relates to an isophthalic acid rich carboxyl functionalized polyester, containing linear chain aliphatic (poly)ether diols, and to thermosetting powder compositions comprising a mixture of the polyester with a beta-hydroxylkylamide group containing cross-linking agent. The invention also relates to the use of said compositions for the preparation of powdered paints and varnishes for the making of coatings and to coating obtained therewith.Type: ApplicationFiled: June 11, 2008Publication date: November 20, 2008Inventors: Luc Moens, Kris Buysens, Daniel Maetens
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Patent number: 7384671Abstract: An apparatus and process for forming a coating on a substrate, including establishing a fluidised-bed having a fluidising gas and a powder coating composition, immersing the substrate wholly or partly in the fluidised bed, the substrate being either electrically isolated or earthed, providing an electrically conductive electrode, to which a voltage is applied, positioned to influence the extent to which charged particles adhere to a region of the substrate, withdrawing the substrate from the fluidised-bed and forming the adherent particles into a continuous coating over at least part of the substrates. The apparatus is arranged and the process is conducted such that the maximum potential gradient existing in the fluidised bed is below the ionisation potential of the fluidising gas.Type: GrantFiled: December 11, 2003Date of Patent: June 10, 2008Assignee: Akzo Nobel Coatings International B.V.Inventors: Kevin Jeffrey Kittle, Michele Falcone
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Patent number: 7358465Abstract: A ceramic heater for heating a semiconductor wafer under processing and has a layered structure wherein on one surface of a supporting substrate made of carbon or a carbon-based composite material, successively formed layers including an insulating layer, and electroconductive layer as an electric heating element and a dielectric layer. A first step for partly or completely removing the layer or layers having degraded properties by means of a suitable method such as sandblasting and a second step of re-forming the layer or layers having been removed in the first step. The invention allows for a substantial cost decrease as compared with the conventional way by replacing the worn-out ceramic heater with a newly manufactured one.Type: GrantFiled: December 27, 2005Date of Patent: April 15, 2008Assignee: Shin-Etsu Chemical Co., Ltd.Inventor: Hideki Fujii
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Patent number: 7323226Abstract: A process for forming a coating on a substrate, including the steps of effecting tribostatic charging of a body of powder by establishing a fluidised-bed of the body of powder in a fluidising chamber at least a part of which is conductive, applying a voltage to the conductive part of the fluidising chamber, immersing a substrate which is electrically non-conductive or poorly conductive, either electrically isolated or earthed, wholly or partly in the fluidised bed, withdrawing the substrate from the fluidised-bed and forming adherent particles of the powder into a continuous coating over at least part of the substrate.Type: GrantFiled: December 11, 2003Date of Patent: January 29, 2008Assignee: AKZO Nobel Coatings International B.V.Inventors: Kevin Jeffrey Kittle, Michele Falcone
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Patent number: 7238390Abstract: The purpose of the invention is a coating precursor comprising a silicone resin and a mineral filler capable of chemically reacting so as to produce a solid layer on a substrate and a cohesive refractory layer after a calcination operation. The precursor may also include an additive capable of reducing its viscosity. Another purpose of the invention is a method for coating a given surface of a substrate with at least one refractory layer containing silicon in which the substrate is coated with a coating precursor according to the invention so as to form a green layer and a heat treatment is carried out to calcine the said green layer and to form a cohesive refractory layer. The invention is a means of obtaining a protective coating capable of resisting oxidising environments, liquid metal and a solid or molten salt.Type: GrantFiled: October 14, 2002Date of Patent: July 3, 2007Assignees: Aluminium Pechiney, Pechiney RhenaluInventors: Airy-Pierre Lamaze, Christian Barthelemy, Thomas Spadone, Robert Rey-Flandrin
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Patent number: 7211615Abstract: A composition containing from 88 to 99.99% by weight of a polyamide, a compound of a polyamide and mixtures of these, and from 0.01 to 0.25% by weight of a flow aid where the drying loss from the flow aid after 5 days of conditioning at a relative humidity of 95% is less than or equal to 1%, determined by ISO 787/2.Type: GrantFiled: November 5, 2003Date of Patent: May 1, 2007Assignee: Degussa AGInventors: Franz-Erich Baumann, Sylvia Monsheimer, Maik Grebe, Wolfgang Christoph, Dirk Heinrich, Holger Renners, Heinz Scholten, Thomas Schiffer, Joachim Muegge, Johannes Chiovaro
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Patent number: 7153585Abstract: The invention concerns to the use of a powder comprising 99.95 to 95% of at least one polyamide and 0.05 to 5% of at least one silane for coating metals. This powder may be prepared by simple dry blending of the constituents. The silane can also be added to the molten polyamide in a mixing device and the resulting product reduced to powder. The addition of silane makes it possible to significantly improve electrostatic application by preventing a substantial portion of the powder from falling off during the electrostatic discharge which follows application, while providing lasting adhesion between the coating and metal. Advantageously, the silane is chosen from aminopropyltriethoxysilane and aminopropyltrimethoxysilane. The invention also concerns a method of coating an object with a film resulting from melting a thin layer of the powder.Type: GrantFiled: December 13, 2002Date of Patent: December 26, 2006Assignee: Arkema FranceInventors: Marc Audenaert, Denis Huze, Emmanuel Rastelletti
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Patent number: 7144976Abstract: The present invention includes photocurable, liquid polymers incorporating coumarin ester endgroups into their molecular structure, which polymers are crosslinked upon irradiation with ultraviolet light by photochemically allowed [2+2] cycloaddition reactions among the chain ends, and which crosslinked polymers are useful in the preparation of medical devices, tissue engineering scaffolds, drug delivery systems and, in particular, in vivo preparation of implants in an open surgical procedure or laproscopically.Type: GrantFiled: May 8, 2002Date of Patent: December 5, 2006Assignee: Ethicon, Inc.Inventors: Takehisa Matsuda, Manabu Mizutani, Steven Arnold
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Patent number: 7041340Abstract: A process for forming a coating on a conductive substrate, including the steps of: establishing a fluidised-bed of a powder coating composition, thereby effecting tribostatic charging of the powder coating composition, the fluidised-bed including a fluidising chamber at least a part of which is conductive, applying a voltage to the conductive part of the fluidising chamber, immersing the substrate wholly or partly in the fluidised bed, whereby charged particles of the powder coating composition adhere to the substrate, the substrate being either electrically isolated or earthed, withdrawing the substrate from the fluidised-bed and forming the adherent particles into a continuous coating over at least part of the substrate.Type: GrantFiled: June 6, 2002Date of Patent: May 9, 2006Assignee: International Coatings LimitedInventors: Kevin Jeffrey Kittle, Michele Falcone
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Patent number: 6903161Abstract: This invention relates to a low-density polyethylene composition useful for coating polar substrates. This invention particularly relates to a low-density polyethylene composition useful for coating metal foils, wherein the composition comprises an ethylene/(meth)acrylic acid copolymer having a low acid content.Type: GrantFiled: May 15, 2002Date of Patent: June 7, 2005Assignee: E. I. du Pont de Nemours and CompanyInventor: Barry Alan Morris
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Patent number: 6858257Abstract: The invention provides a powder coating composition in which the powder particles are an agglomerate of individual particulate components fused or bonded together into composite particles.Type: GrantFiled: March 9, 2000Date of Patent: February 22, 2005Assignee: International Coatings LimitedInventor: Andrew George Cordiner
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Patent number: 6849303Abstract: The use of electrostatic impregnation to load materials such as binders and flavors onto substrates such as fibers and medical devices is disclosed. Substrates loaded with materials such as binders and flavors, wherein the materials are loaded on the substrates via electrostatic impregnation are also disclosed.Type: GrantFiled: November 4, 2002Date of Patent: February 1, 2005Inventor: Vipul Bhupendra Dave
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Patent number: 6838123Abstract: The invention relates to a method for coating fibers shaped as fiber strands (roving and mats) using a fluidized bed technique, wherein (i) the desired composition of the individual coating constituents is directly applied from the fluidized bed without previous compounding and (ii) the individual coating constituents contained in the fluidized bed are additionally mixed in the mass so that dissociation of individual constituents is substantially avoided. The invention also relates to a device for implementing the method.Type: GrantFiled: July 1, 2002Date of Patent: January 4, 2005Assignee: Neopreg AGInventor: Theo Staheli
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Patent number: 6783808Abstract: A method for coating a golf ball, including the steps of providing a golf ball component; providing a polymeric material; creating a particulate from the polymer material; charging at least one of the component or the particulate; fluidizing the polymer particulate; and coating the golf ball component with a thin layer of the polymer material by placing the golf ball component within the fluidized particulate.Type: GrantFiled: February 19, 2003Date of Patent: August 31, 2004Assignee: Acushnet CompanyInventors: Mitchell E. Lutz, Matthew F. Hogge
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Patent number: 6720079Abstract: The invention concerns a polyester bearing tertiary carboxyl groups, characterised in that it consists of: (a) 8.1 to 35 moles of an aliphatic or cycloaliphatic of a polyol; (b) 9.1 to 36 moles of an aliphatic, cycloaliphatic or aromatic polycarboxylic acid; (c) 1.6 to 2.8 moles of an aliphatic, cycloaliphatic or aromatic compound comprising a tertiary carboxyl group and either a primary or secondary carboxyl group, or a primary or secondary hydroxyl group. Said polyester is prepared in several steps, the first steps consisting in the preparation of a polyester by condensation between (a) an aliphatic or cycloaliphatic polyol, and (b) an aliphatic, cycloaliphatic or aromatic polycarboxylic acid, the final step consisting in condensing said polyester with (c) an aliphatic, cycloaliphatic or aromatic compound comprising a tertiary carboxyl group and either a primary or secondary carboxyl group, or a primary or secondary hydroxyl group.Type: GrantFiled: August 27, 2002Date of Patent: April 13, 2004Assignee: UCB, S.A.Inventors: Luc Moens, Kris Buysens, Daniel Maetens
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Patent number: 6706332Abstract: A method for coating a golf ball comprising the steps of providing a golf ball component; providing a polymer material; creating a polymer particulate; fluidizing the polymer particulate; placing the golf ball component within the fluidized particulate; and fluidized coating the golf ball component with a thin layer of the polymer material.Type: GrantFiled: February 4, 2003Date of Patent: March 16, 2004Assignee: Acushnet CompanyInventors: Mitchell E. Lutz, Matthew F. Hogge
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Patent number: 6596084Abstract: A fluidized bed pyrolytic carbon coating apparatus (1) is provided for coating substrate surfaces with pyrolytic carbon. The preferred coating apparatus (1) includes a fluidized bed reactor (10) having a reactor chamber (22), a gas feed inlet (24), an exhaust gas outlet (26), a source (12) of process feed gas and a gas line (14) through which the process feed gas can pass from the source (12) of process feed gas to the gas feed inlet (24) and into the reactor chamber (22). The gas line (14) includes an actuator (20) having a timing circuit (37) which acts to vary a rate of flow of process feed gas through the gas line (14) into the reactor chamber (22) such that the rate of flow into the reactor chamber (22), cycles regularly and consistently over a period of time so as to create a pulsating gas flow and a pulsation effect upon the fluidized bed within the reactor chamber (22).Type: GrantFiled: May 19, 2000Date of Patent: July 22, 2003Assignee: MedicalCV, Inc.Inventor: Nandkishor G. Patke
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Patent number: 6593006Abstract: A method of fabricating a decorative wood article includes the steps of applying a decorative overlay onto at least one surface of a wood article, applying a radiation curable powder coating onto the outer surface of the overlay, heating the applied radiation curable powder coating at a temperature sufficient to melt and flow the powder coating, and exposing the applied powder coating to radiation energy to cure the powder coating and form a film on the outer surface of the decorative overlay.Type: GrantFiled: September 27, 2001Date of Patent: July 15, 2003Assignee: O'Sullivan Industries, Inc.Inventor: David Russell Worsley
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Patent number: 6528125Abstract: A corrosion resistant tube comprises a metal tube having an outer surface. A zinc layer is electrostatically bonded to the outer surface, wherein the zinc layer is selected from the group consisting of powdered zinc, powdered zinc nickel alloys, powdered zinc cobalt alloys, and powdered zinc aluminum alloys. One or more polymeric layers may be electrostatically bonded to the zinc layer, or to a surface treatment layer, wherein the polymeric layer(s) comprises powdered thermoplastic materials selected from the group consisting of powdered nylons, powdered fluoropolymers, powdered polyesters, and mixtures thereof. Optionally, the polymeric layer(s) may be electrostatically bonded directly to the outer surface.Type: GrantFiled: October 3, 2000Date of Patent: March 4, 2003Assignee: ITT Manufacturing Enterprises, Inc.Inventors: Timothy E. Jackson, Tao Nie, Steve Obbish, John F. Schloemp, II, William Robert Church, Michael W. Boles, Gary O. Klinger, Christopher R. Terry
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Patent number: 6506455Abstract: The present invention relates to as triboelectric fluidized bed method and apparatus for coating an object with powder prior to heating to form a coating. The methods includes arranging a bed of fluidixed powder in a vat where the powder can be charged by a tribocharging device such as a honeycomb comprising prisms or vertical tubes open at both ends.Type: GrantFiled: June 7, 2001Date of Patent: January 14, 2003Assignee: AtofinaInventors: Ariel Bru, Ion Inculet, Arnaud Tedoldi
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Patent number: 6491986Abstract: Transparent or pigmented powder coating materials with crosslinkers comprising hydroxyalkylamides and polyisocyanates containing uretdione groups.Type: GrantFiled: February 26, 2001Date of Patent: December 10, 2002Assignee: Degussa AGInventor: Andreas Wenning
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Patent number: 6465049Abstract: In subjecting a substrate of low electric conductivity to a pretreatment by holding the same within a fluidized bed of diamond particles for the formation of a diamond film on the substrate surface, a treatment method is disclosed which is capable of preventing decrease in the effect of the pretreatment. The pretreatment of the substrate is conducted within a fluidized bed of diamond particles by keeping the electrostatic potential of the substrate in the range from −1.5 to +1.5 kV. It is desirable that the relative humidity of the gas for the fluidization of diamond particles is controlled to be 40% or higher. It is more desirable that ion bombardment onto the substrate surface to effect neutralization of the electrostatic charges. The fluidizing gas is humidified preferably by using a bubbling apparatus or spraying apparatus.Type: GrantFiled: December 21, 2000Date of Patent: October 15, 2002Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Hitoshi Noguchi, Yoshihiro Kubota
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Patent number: 6461742Abstract: The invention concerns a polyester bearing tertiary carboxyl groups, characterised in that it consists of: (a) 8.1 to 35 moles of an aliphatic or cycloaliphatic of a polyol; (b) 9.1 to 36 moles of an aliphatic, cycloaliphatic or aromatic polycarboxylic acid; (c) 1.6 to 2.8 moles of an aliphatic, cycloaliphatic or aromatic compound comprising a tertiary carboxyl group and either a primary or secondary carboxyl group, or a primary or secondary hydroxyl group. Said polyester is prepared in several steps, the first steps consisting in the preparation of a polyester by condensation between (a) an aliphatic or cycloaliphatic polyol, and (b) an aliphatic, cycloaliphatic or aromatic polycarboxylic acid, the final step consisting in condensing said polyester with (c) an aliphatic, cycloaliphatic or aromatic compound comprising a tertiary carboxyl group and either a primary or secondary carboxyl group, or a primary or secondary hydroxyl group.Type: GrantFiled: July 27, 2000Date of Patent: October 8, 2002Assignee: UCB, S.A.Inventors: Luc Moens, Kris Buysens, Daniel Maetens
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Patent number: 6444254Abstract: Functionalized polymer surfaces having reactive moieties thereon are contacted with stamps having ligands adsorbed thereto, the ligands also comprising reactive moieties. The reactive moieties of the functionalized surfaces and the ligands form covalent bonds, thus providing a method of microstamping polymer surfaces directly with ligands such as biological ligands. Using this method, devices such as tissue culture plates with polymer surfaces that are microstamped directly with ligands can be made.Type: GrantFiled: March 3, 2000Date of Patent: September 3, 2002Assignee: Duke UniversityInventors: Ashutosh Chilkoti, Zhongping Yang
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Patent number: 6406738Abstract: A method of coating a substrate which is a core for a pharmaceutical dosage form, which comprises electrostatically applying to a surface of the core a powder material comprising active material, the coating material applied constituting a dosage of active material, wherein the powder material includes composite particles, each composite particle comprising two or more components having different physical and/or chemical properties.Type: GrantFiled: November 10, 1997Date of Patent: June 18, 2002Assignee: Phoqus LimitedInventors: John E. Hogan, Trevor Page, Linda Reeves, John N. Staniforth
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Patent number: 6355309Abstract: A method of forming a thermoplastic layer on an adhesive layer is provided. In the steps of the method, a thermoplastic powder is provided having a melt flow index of at least about 0.008 grams/10 minutes, the powder is applied to at least one surface of the adhesive layer to form a particle layer, and the combination is then subjected to elevated heat and pressure until particle layer is fused into a continuous layer and the continuous layer is bonded to the adhesive layer.Type: GrantFiled: June 13, 2000Date of Patent: March 12, 2002Assignee: 3M Innovative Properties CompanyInventors: Danny L. Fleming, Ernest M. Rinehart
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Patent number: 6294222Abstract: A method of attaching a substantially uniform distribution of particulates to individual exposed surfaces of a matrix of fibrous material. The method includes the following steps: 1) electrically charging a matrix of fibrous material having individual exposed surfaces to create a substantially uniform distribution of charged sites at the exposed surfaces; 2) applying particulates to the charged matrix of fibrous material so that at least some particulates adhere at the charged sites; and 3) attaching particulates adhering to the fibrous material at charged sites by substantially non-transient bonding.Type: GrantFiled: June 10, 1996Date of Patent: September 25, 2001Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Bernard Cohen, Judith Katherine Faass, Lamar Heath Gipson, Lee Kirby Jameson
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Patent number: 6280798Abstract: A process for forming a coating on a conductive substrate, which comprises establishing a fluidized bed of a powder coating composition, in which the mechanism for particle charging is tribostatic charging immersing the substrate wholly or partly within the said fluidized bed, applying a voltage to the substrate for at least part of the period of immersion, whereby particles of the powder coating composition adhere to the substrate, withdrawing the substrate from the fluidized bed and forming the adherent particles into a continuous coating over at least part of the substrate. The process enables the coating of substrate areas which, because of the Faraday cage effect, are inaccessible in conventional electrostatic coating processes, and also enables the formation of thinner coatings than are obtainable by conventional fluidized-bed processes.Type: GrantFiled: July 24, 2000Date of Patent: August 28, 2001Assignee: International Coatings LimitedInventors: John Ring, Kevin J. Kittle, Gianfranco Arpe
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Patent number: 6249957Abstract: In rotors for electric motors, it is usual to fix the commutator on the rotor shaft by a press fit. In the present invention, the rotor shaft, with the rotor core fixed thereon, is electrostatically coated with an epoxy layer on opposite portions of the rotor shaft and in the winding slots, and is then heated to the plasticizing and curing temperature of the epoxy. After that, by a sliding tool, the commutator, whose inner bore has a clearance fit relative to the rotor shaft, is slipped onto the rotor shaft in a terminal position, in the process the still-viscous epoxy is pushed backward and is deposited radially on a connecting end face, forming a bead, and penetrates the annular gap between the inner bore and the rotor shaft. Once the epoxy layer has cooled, the commutator is fixed against rotation and displacement on the rotor shaft. The rotor is suitable for electric motors of various types.Type: GrantFiled: October 21, 1998Date of Patent: June 26, 2001Assignee: Robert Bosch GmbHInventors: Martin Wiesler, Klaus Maldener, Martin Kiefer, Lothar Fauth, Hans Kobschaetzky, Dieter Kern
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Patent number: 6200678Abstract: Concrete strengthening members, particularly prestressing tendons such as strands of steel wire, are provided with a strongly adherent plastic coating which may be substantially impermeable for improved corrosion resistance, and/or which may have embedded therein abrasive or grit-form particles to provide improved bond with the concrete, and particularly to provide controllable bond transfer in prestressing tendons of the pre-tensioned type. The plastic coating preferably is applied electrostatically in powder form, and fusion bonded by heat. The abrasive can be applied by spraying during a viscous state of the heated resin, and can be varied as to size and spacing density so as to control the surface condition and the bonding effect. Fusion and curing heat may come from preheating of the member before application of the resin powder, which preferably is a heat curable, thermosetting epoxy. Coating thickness and grit application are readily variable to meet particular requirements.Type: GrantFiled: June 6, 1995Date of Patent: March 13, 2001Assignee: Florida Wire & Cable, Inc.Inventors: Frederick F. Hunt, Donald J. Gillette
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Patent number: 6121408Abstract: The powder coating for use in a coating method which includes the steps of mixing and applying two or more powder coatings to a substrate, the powder coating comprising a resin not having thermosetting properties at a temperature of 160.degree. C. or less by itself, and being heat-cured at a temperature of 160.degree. C. or less when used in combination with other powder coatings. The powder coating composition comprising two or more powder coatings, wherein each of the powder coatings comprises a resin not having thermosetting properties at a temperature of 160.degree. C. or less by itself, and being heat-cured at a temperature of 160.degree. C. or less to form a coating film when used in combination with other powder coatings.Type: GrantFiled: April 7, 1998Date of Patent: September 19, 2000Assignee: Kao CorporationInventors: Katsutoshi Aoki, Masayuki Maruta, Yukiya Sato, Hisakazu Tajima, Takehiko Tohjo, Yasunori Inagaki, Shingo Tanaka
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Patent number: 6103794Abstract: A description is given of powder coating compositions comprising a) an organic film-forming binder and b) as stabilizer at least one compound of formula I ##STR1## wherein the general symbols are as defined in claim 1. Using powder coating compositions stabilized in this manner reduces the discoloration of the coatings during heat-cures, in particular during gas furnace cures.Type: GrantFiled: August 13, 1998Date of Patent: August 15, 2000Assignee: Ciba Specialty Chemicals CorporationInventor: Hugh Stephen Laver
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Patent number: 6042892Abstract: An apparatus and a method for coating zinc on steel sheets for use on automobiles and electronic apparatuses are disclosed. A fluidized bed forming chamber is provided to fluidize zinc powders in carrying out a zinc coating on a heated steel sheet, so that not only a uniformly coated layer but also a thick coated layer can be obtained. The apparatus for continuously coating zinc on a steel sheet according to the present invention includes a zinc coating chamber for forming a fluidized bed of zinc powders, for passing a heated steel sheet through the fluidized bed of the zinc powders, and for making the zinc powders melt-adhere on the steel sheet during its passing through the fluidized bed. A fluidized bed forming chamber forms a fluidized bed of the zinc powders by making the zinc powders suspended by spouting a gas.Type: GrantFiled: June 19, 1998Date of Patent: March 28, 2000Assignee: Pohang Iron & Steel Co., Ltd.Inventors: Sang Hean Kim, Jin Hwan Chung, Noi Ha Cho
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Patent number: 5994110Abstract: Compounds which possess a complementary structure to a desired molecule, such as a biomolecule, in particular polymeric or oligomeric compounds, which are useful as in vivo or in vitro diagnostic and therapeutic agents are provided. Also, various methods for producing such compounds are provided. These polymeric or oligomeric compounds are useful in particular as antimicrobial agents, receptor, hormone or enzyme agonists and antagonists.Type: GrantFiled: September 2, 1998Date of Patent: November 30, 1999Inventors: Klaus Mosbach, Peter A. G. Cormack, Olof Ramstrom, Karsten Haupt
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Patent number: 5968642Abstract: An article having a water-repellent fluororesin surface and a method for manufacturing the same, wherein the article has a water-repellent fluororesin surface composed of an irregularly porous material which has a maximum IPA diffusion diameter of at least 8 mm and is formed by irregularly stacking fluororesin particles with an average diameter of no more than 40 microns over one another and has a water droplet roll angle tangent of no more than 50/500. The obtained article has a fluororesin surface which exhibits excellent water-repellency, inhibits adhesion of water drops and soil entrained by the water drops and imparts a great bond strength to the substrate.Type: GrantFiled: August 18, 1995Date of Patent: October 19, 1999Assignee: DuPont-Mitsui Fluorochemicals Co., Ltd.Inventor: Takumi Saito
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Patent number: 5895622Abstract: A composite manufacturing system moves a multi-fiber tow through a processing space. A resin particle source provides particles to the space. This source may include an airstream entrained with particles which is discharged into the space through an orifice; the airstream diverging as it enters the space. An electrode is disposed in the space to electrostatically charge the particles and facilitate deposition of the charged particles on the tow. In one embodiment, the electrode includes a corona wire disposed proximate to the tow to provide a generally cylindrical charging region. An electric field useful to direct deposition of the particles may be generated by appropriately shaping a wire electrode and orienting it in a predetermined manner relative to the tow. After the particles are deposited, a fixation unit may be used to at least partially melt the deposited particles. A processing stage may be included which has a pair of surfaces configured to heat and compress the tow therebetween.Type: GrantFiled: April 7, 1997Date of Patent: April 20, 1999Assignee: Purdue Research FoundationInventors: Karthik Ramani, Daniel Edward Woolard, Mark Stephen Duvall
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Patent number: 5891515Abstract: A process for preparing a metal plastic composite comprising prime coating at least a portion of a metal substrate with one or more layers of an adhesion primer powder consisting of a solid thermosetting resin using a conventional powder application technique, heating the thus coated substrate to a temperature sufficient to melt a surface coating powder to be subsequently applied, immersing the thus coated substrate into a fluidized bed of a surface coating powder for a time sufficient to give the thickness of surface coating desired.Type: GrantFiled: June 5, 1995Date of Patent: April 6, 1999Assignee: Elf Atochem S.A.Inventors: Jean-Yves Dutheil, Eric Perraud
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Patent number: RE35879Abstract: The apparatus, system and method utilize sequential sprays of wet, low-temperature steam, and dry, high-temperature steam to clean the exterior of laminated objects as well as to effect volatilization of liquid contaminates trapped between lamina thereof. Water is injected into the conduit through which the low-temperature steam is delivered, so as to produce a desirable concentration of droplets therein. A conveyor moves the laminated objects along a horizontal path through zones in which they are sprayed by the low temperature and high temperature steam, and then through a zone in which they are electrostatically coated with powder.Type: GrantFiled: December 21, 1995Date of Patent: August 25, 1998Assignee: Electrostatic Technology, Inc.Inventors: Daniel Castelli, John Donahue, Donald J. Gillette, Bedrich Hajek